#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/82/2228262.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228262_Fobs loop_ _publ_author_name 'Wang, Haixia' _publ_section_title ; 2-(5,6-Dibromo-7-methyl-3H-imidazo[4,5-b]pyridin-2-yl)phenol ; _journal_coeditor_code CV2784 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3132 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.1805 _cell_length_b 8.4941 _cell_length_c 22.6920 _exptl_crystal_F_000 1488.00 _reflns_d_resolution_high 0.8408 _[local]_cod_data_source_file cv2784Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' test in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 554.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 28514.17 32194.40 995.73 o 4 0 0 125443.60 132485.30 4078.67 o 6 0 0 81.97 64.70 18.59 o 8 0 0 7855.64 9126.67 213.18 o 10 0 0 1673.09 1891.01 100.11 o 12 0 0 138.48 259.48 62.61 o 14 0 0 38.83 71.31 83.70 o 2 1 0 16498.89 24431.56 434.49 o 4 1 0 27375.31 24926.46 443.13 o 6 1 0 15206.70 15022.56 272.73 o 8 1 0 37839.73 37320.46 666.75 o 10 1 0 0.43 28.81 27.50 o 12 1 0 2035.54 2439.06 76.24 o 14 1 0 807.55 607.19 66.45 o 2 2 0 242.58 401.29 67.30 o 4 2 0 85888.61 78762.30 1387.67 o 6 2 0 5426.05 5366.18 117.39 o 8 2 0 3158.28 2777.92 67.94 o 10 2 0 4342.78 3814.51 90.57 o 12 2 0 386.51 540.33 63.59 o 14 2 0 130.41 59.99 47.51 o 2 3 0 3355.65 2952.21 62.84 o 4 3 0 10390.71 10611.97 220.14 o 6 3 0 5931.61 6201.32 123.27 o 8 3 0 4948.25 4586.29 142.90 o 10 3 0 3569.69 3547.28 90.21 o 12 3 0 1557.83 1305.98 59.50 o 14 3 0 29.93 56.70 61.29 o 0 4 0 12364.36 12196.82 388.72 o 2 4 0 2857.30 3015.40 67.58 o 4 4 0 13489.11 13563.42 260.54 o 6 4 0 1323.24 1133.40 42.02 o 8 4 0 1491.71 1597.79 55.27 o 10 4 0 869.88 640.28 45.54 o 12 4 0 93.78 63.80 42.41 o 14 4 0 699.56 796.73 63.50 o 2 5 0 4009.65 4241.99 92.74 o 4 5 0 267.03 271.74 23.61 o 6 5 0 7246.26 6854.90 251.78 o 8 5 0 31.47 79.83 34.02 o 10 5 0 3252.45 3198.80 96.75 o 12 5 0 11.27 -71.74 47.83 o 0 6 0 375.72 509.92 51.90 o 2 6 0 7257.67 6998.12 146.29 o 4 6 0 335.95 419.15 43.24 o 6 6 0 518.91 496.92 42.14 o 8 6 0 215.00 216.84 90.06 o 10 6 0 742.50 866.50 63.46 o 12 6 0 127.69 0.05 56.98 o 2 7 0 2454.01 2466.54 80.66 o 4 7 0 83.59 99.29 32.40 o 6 7 0 4800.38 5062.15 139.20 o 8 7 0 345.83 473.19 89.23 o 10 7 0 587.20 787.44 75.67 o 0 8 0 1162.86 1140.78 125.05 o 2 8 0 1149.72 1288.12 66.41 o 4 8 0 755.29 893.05 60.44 o 6 8 0 136.26 131.93 50.13 o 8 8 0 1743.23 1671.76 85.11 o 2 9 0 0.56 25.43 41.40 o 4 9 0 73.04 95.83 44.61 o 6 9 0 175.12 202.34 58.44 o 2 10 0 527.90 578.55 102.79 o 1 1 1 7999.51 13108.09 203.80 o 2 1 1 10414.92 11662.90 218.29 o 3 1 1 4788.29 4141.53 506.53 o 4 1 1 1365.01 1521.12 25.07 o 5 1 1 4760.36 4529.96 62.46 o 6 1 1 2291.27 2842.43 43.35 o 7 1 1 71.12 164.68 13.68 o 8 1 1 25.06 40.53 19.94 o 9 1 1 13.84 43.41 17.51 o 10 1 1 803.67 918.94 29.49 o 11 1 1 148.22 135.13 24.14 o 12 1 1 299.80 333.34 29.79 o 13 1 1 22.62 8.50 30.47 o 14 1 1 1.38 0.58 39.85 o 15 1 1 2.48 8.10 42.49 o 0 2 1 5100.66 5172.94 118.47 o 1 2 1 1993.24 1383.09 23.41 o 2 2 1 5021.94 5282.84 70.62 o 3 2 1 4665.33 6480.82 85.81 o 4 2 1 1252.50 1546.41 29.50 o 5 2 1 1265.21 1156.96 50.06 o 6 2 1 3212.25 3464.08 52.12 o 7 2 1 7851.13 7191.21 98.88 o 8 2 1 237.95 302.71 19.66 o 9 2 1 6534.92 6265.12 90.61 o 10 2 1 1037.24 1042.44 31.95 o 11 2 1 121.90 149.67 24.04 o 12 2 1 358.80 361.39 31.59 o 13 2 1 1168.61 1117.73 42.26 o 14 2 1 105.46 61.27 33.70 o 15 2 1 110.60 165.18 42.04 o 1 3 1 29007.73 28385.40 405.57 o 2 3 1 157.14 109.77 8.48 o 3 3 1 4206.52 3676.61 50.43 o 4 3 1 396.41 360.01 13.53 o 5 3 1 29409.88 27918.93 387.26 o 6 3 1 1784.64 1746.73 34.54 o 7 3 1 408.78 405.86 19.75 o 8 3 1 383.48 374.57 21.17 o 9 3 1 6915.78 6648.77 97.58 o 10 3 1 786.96 763.05 30.92 o 11 3 1 150.53 182.65 25.71 o 12 3 1 5.98 26.41 28.32 o 13 3 1 69.57 171.47 33.16 o 14 3 1 99.67 20.90 36.00 o 0 4 1 22.59 39.67 13.89 o 1 4 1 4802.86 5489.21 122.97 o 2 4 1 957.28 971.15 23.75 o 3 4 1 17644.92 17048.85 197.20 o 4 4 1 117.26 98.17 11.19 o 5 4 1 622.31 709.64 20.83 o 6 4 1 1245.38 1179.41 32.76 o 7 4 1 4317.52 4044.89 70.27 o 8 4 1 5.65 33.66 19.66 o 9 4 1 1733.09 1636.69 43.06 o 10 4 1 240.53 237.43 27.84 o 11 4 1 2080.69 2004.98 51.63 o 12 4 1 23.04 11.52 31.42 o 13 4 1 1654.69 1792.02 54.85 o 14 4 1 0.75 31.62 37.41 o 1 5 1 15195.39 15093.42 221.94 o 2 5 1 46.40 67.06 14.04 o 3 5 1 3128.05 3267.35 46.46 o 4 5 1 317.70 364.81 16.15 o 5 5 1 15782.64 14736.22 194.82 o 6 5 1 736.44 765.12 27.62 o 7 5 1 34.49 21.22 33.39 o 8 5 1 285.52 340.88 27.61 o 9 5 1 3913.91 3771.67 73.35 o 10 5 1 671.37 716.18 35.45 o 11 5 1 26.87 7.48 31.73 o 12 5 1 35.27 72.99 36.81 o 13 5 1 413.59 469.82 44.16 o 0 6 1 470.63 453.99 37.40 o 1 6 1 3661.29 3304.91 55.46 o 2 6 1 42.76 36.43 15.37 o 3 6 1 4744.94 4943.34 66.50 o 4 6 1 167.14 237.79 30.60 o 5 6 1 690.59 766.86 30.05 o 6 6 1 581.55 587.00 28.39 o 7 6 1 652.01 714.66 31.89 o 8 6 1 1.33 17.26 28.07 o 9 6 1 812.86 809.53 38.26 o 10 6 1 649.17 573.76 37.45 o 11 6 1 112.05 195.48 40.04 o 12 6 1 4.05 10.33 47.49 o 1 7 1 1017.90 1045.24 29.70 o 2 7 1 19.94 0.34 17.22 o 3 7 1 27.34 37.90 21.35 o 4 7 1 128.30 144.41 25.21 o 5 7 1 3774.25 3833.24 80.32 o 6 7 1 33.60 62.78 25.89 o 7 7 1 11.60 14.94 31.35 o 8 7 1 320.51 259.98 35.73 o 9 7 1 1457.84 1449.03 56.15 o 10 7 1 7.49 13.09 37.41 o 11 7 1 40.03 -60.34 40.23 o 0 8 1 246.95 206.87 33.07 o 1 8 1 3822.10 3903.84 66.60 o 2 8 1 22.39 6.98 22.92 o 3 8 1 896.98 970.29 48.55 o 4 8 1 24.29 -2.33 29.24 o 5 8 1 801.28 830.16 42.48 o 6 8 1 8.67 -5.35 33.88 o 7 8 1 65.91 102.60 36.59 o 8 8 1 40.29 39.31 44.94 o 9 8 1 54.40 52.35 40.65 o 1 9 1 18.32 8.42 29.26 o 2 9 1 0.74 -19.07 32.91 o 3 9 1 536.92 526.15 43.72 o 4 9 1 65.20 66.43 34.54 o 5 9 1 447.66 421.08 39.00 o 6 9 1 130.90 122.48 37.53 o 7 9 1 521.69 562.39 43.20 o 1 10 1 632.77 703.55 60.05 o 2 10 1 3.95 -29.58 49.08 o 0 0 2 48609.75 35551.55 1104.54 o 1 0 2 8740.82 7210.82 225.33 o 2 0 2 974.47 512.32 165.56 o 3 0 2 200.82 276.89 11.80 o 4 0 2 61757.36 67655.93 951.41 o 5 0 2 5357.97 6249.86 93.71 o 6 0 2 984.26 1389.34 36.05 o 7 0 2 693.55 679.40 41.42 o 8 0 2 6220.80 6173.92 152.46 o 9 0 2 2635.33 2485.89 73.02 o 10 0 2 7654.42 7346.02 149.03 o 11 0 2 2724.65 2787.22 78.78 o 12 0 2 442.90 396.82 53.27 o 13 0 2 14.46 -27.79 51.14 o 14 0 2 1011.05 893.13 75.50 o 15 0 2 227.98 246.25 66.97 o 1 1 2 6401.90 8284.51 130.69 o 2 1 2 113.98 12.06 10.21 o 3 1 2 14835.59 14648.03 268.66 o 4 1 2 61458.58 59847.98 816.59 o 5 1 2 7185.30 6837.04 85.76 o 6 1 2 35.22 37.29 9.19 o 7 1 2 2025.34 1996.47 33.44 o 8 1 2 23530.46 21129.41 271.22 o 9 1 2 310.07 377.52 21.52 o 10 1 2 276.74 292.81 22.75 o 11 1 2 687.93 665.83 29.85 o 12 1 2 7476.06 7559.21 123.81 o 13 1 2 30.58 0.26 32.09 o 14 1 2 141.42 96.35 35.82 o 15 1 2 20.48 1.49 46.54 o 0 2 2 39184.63 44735.84 837.16 o 1 2 2 11935.70 11883.88 146.40 o 2 2 2 3260.62 2906.88 39.15 o 3 2 2 107.84 1.75 7.56 o 4 2 2 40205.34 38332.77 526.15 o 5 2 2 4632.26 4089.65 64.11 o 6 2 2 1699.57 1898.00 50.67 o 7 2 2 242.63 189.57 12.96 o 8 2 2 2991.61 2896.19 49.76 o 9 2 2 87.88 45.24 17.83 o 10 2 2 1201.00 1035.83 32.18 o 11 2 2 127.33 77.44 24.54 o 12 2 2 36.12 86.37 27.10 o 13 2 2 238.48 246.26 31.98 o 14 2 2 982.77 1004.05 53.55 o 15 2 2 175.50 276.88 51.29 o 1 3 2 3944.59 3758.35 53.87 o 2 3 2 312.45 209.29 14.48 o 3 3 2 1809.48 1942.08 30.91 o 4 3 2 10288.76 9794.33 122.68 o 5 3 2 138.42 211.91 13.58 o 6 3 2 2683.38 2715.78 41.78 o 7 3 2 2974.35 2801.40 52.51 o 8 3 2 8695.87 8213.92 114.65 o 9 3 2 190.22 232.55 22.53 o 10 3 2 344.87 391.34 26.49 o 11 3 2 266.27 147.55 26.35 o 12 3 2 1929.42 1789.81 49.64 o 13 3 2 376.83 262.16 35.01 o 14 3 2 82.63 90.27 35.26 o 0 4 2 12893.82 13329.54 257.21 o 1 4 2 710.29 842.13 23.97 o 2 4 2 14872.79 15147.85 200.42 o 3 4 2 282.93 208.70 14.16 o 4 4 2 5755.46 5512.75 69.99 o 5 4 2 3582.35 3495.68 52.72 o 6 4 2 86.40 103.43 17.31 o 7 4 2 63.90 86.18 18.94 o 8 4 2 368.18 386.90 24.43 o 9 4 2 317.00 366.11 27.33 o 10 4 2 48.18 35.74 33.58 o 11 4 2 332.89 371.18 31.41 o 12 4 2 315.22 248.72 34.09 o 13 4 2 37.49 63.29 41.08 o 14 4 2 597.41 650.25 45.78 o 1 5 2 878.58 935.86 25.91 o 2 5 2 127.83 156.53 14.58 o 3 5 2 1193.94 1390.23 30.67 o 4 5 2 43.39 39.50 12.90 o 5 5 2 860.46 878.24 26.93 o 6 5 2 3277.27 3037.49 73.28 o 7 5 2 70.63 85.48 21.53 o 8 5 2 84.95 71.52 23.79 o 9 5 2 234.27 280.17 31.01 o 10 5 2 851.18 852.14 38.98 o 11 5 2 396.60 403.70 37.22 o 12 5 2 3.12 -7.03 34.99 o 13 5 2 6.02 71.07 40.44 o 0 6 2 501.64 633.18 46.86 o 1 6 2 13.77 -5.43 16.00 o 2 6 2 10712.67 10573.28 137.75 o 3 6 2 392.00 460.72 19.00 o 4 6 2 68.98 82.56 19.46 o 5 6 2 5.15 4.28 20.46 o 6 6 2 2462.46 2489.72 55.40 o 7 6 2 367.63 420.62 30.45 o 8 6 2 46.07 75.69 27.50 o 9 6 2 144.86 143.52 31.60 o 10 6 2 0.80 5.36 30.94 o 11 6 2 417.30 416.18 39.64 o 12 6 2 93.03 171.96 43.11 o 1 7 2 200.50 197.39 20.31 o 2 7 2 282.94 283.26 21.63 o 3 7 2 1882.05 1829.19 40.92 o 4 7 2 80.04 45.92 25.21 o 5 7 2 116.54 107.49 26.27 o 6 7 2 1318.29 1381.06 48.28 o 7 7 2 3.13 -7.40 29.06 o 8 7 2 3.19 33.05 30.16 o 9 7 2 35.37 -24.49 41.33 o 10 7 2 1089.95 1102.71 50.49 o 11 7 2 63.30 47.14 40.38 o 0 8 2 525.93 482.40 53.14 o 1 8 2 46.36 45.23 25.12 o 2 8 2 2335.55 2425.04 50.39 o 3 8 2 80.88 107.49 27.07 o 4 8 2 438.28 526.37 37.94 o 5 8 2 42.10 35.83 30.11 o 6 8 2 930.56 916.02 41.52 o 7 8 2 200.91 196.74 34.87 o 8 8 2 39.03 -31.20 34.78 o 9 8 2 23.06 -8.93 36.16 o 1 9 2 190.06 214.89 39.42 o 2 9 2 93.69 129.70 53.22 o 3 9 2 116.80 115.14 39.67 o 4 9 2 3.70 21.03 38.11 o 5 9 2 64.17 34.65 39.76 o 6 9 2 50.96 34.45 41.57 o 7 9 2 119.84 40.29 38.09 o 0 10 2 380.51 247.43 98.10 o 1 10 2 0.14 -1.27 48.55 o 1 1 3 5743.71 7795.81 117.91 o 2 1 3 58.39 631.89 17.83 o 3 1 3 827.91 482.11 10.57 o 4 1 3 22.90 49.04 6.72 o 5 1 3 8549.56 6757.04 84.74 o 6 1 3 498.65 654.37 17.34 o 7 1 3 352.94 569.92 17.68 o 8 1 3 600.11 655.67 20.86 o 9 1 3 1451.85 1526.92 37.14 o 10 1 3 1231.33 1285.84 36.64 o 11 1 3 0.41 -10.77 24.26 o 12 1 3 46.45 102.50 34.58 o 13 1 3 130.70 96.77 32.91 o 14 1 3 102.57 237.72 37.58 o 15 1 3 3.12 -14.35 44.73 o 0 2 3 66444.87 64477.73 1204.14 o 1 2 3 71453.63 74317.99 981.35 o 2 2 3 4710.17 4337.58 56.96 o 3 2 3 10989.02 12558.47 165.46 o 4 2 3 1763.01 2543.77 36.91 o 5 2 3 197.31 194.18 12.30 o 6 2 3 2677.24 2940.55 46.47 o 7 2 3 2381.81 2211.42 36.43 o 8 2 3 724.34 768.50 24.28 o 9 2 3 945.48 1039.98 49.57 o 10 2 3 90.39 96.08 22.06 o 11 2 3 1973.74 1815.81 52.18 o 12 2 3 51.16 82.87 26.75 o 13 2 3 261.42 217.06 33.04 o 14 2 3 167.44 180.94 38.30 o 15 2 3 137.33 123.96 43.36 o 1 3 3 28749.00 30217.51 368.10 o 2 3 3 4639.22 4409.15 59.06 o 3 3 3 5507.85 5933.77 76.72 o 4 3 3 2988.29 2874.99 44.07 o 5 3 3 12509.32 12703.71 157.24 o 6 3 3 755.05 720.80 32.14 o 7 3 3 321.30 294.51 19.07 o 8 3 3 2539.92 2448.04 72.16 o 9 3 3 1633.32 1674.28 41.24 o 10 3 3 630.86 527.73 27.41 o 11 3 3 71.94 30.00 25.12 o 12 3 3 674.56 716.34 36.64 o 13 3 3 8.17 29.24 31.83 o 14 3 3 295.17 255.98 38.15 o 0 4 3 896.25 755.50 29.69 o 1 4 3 3022.77 3212.53 46.15 o 2 4 3 17267.80 17078.87 212.26 o 3 4 3 9865.87 9441.83 118.80 o 4 4 3 8703.30 8453.61 108.47 o 5 4 3 409.22 469.89 22.29 o 6 4 3 6605.21 6408.76 96.93 o 7 4 3 3063.29 2961.14 93.42 o 8 4 3 1284.26 1240.27 35.32 o 9 4 3 2548.00 2420.50 51.19 o 10 4 3 311.97 393.01 29.52 o 11 4 3 209.54 269.58 29.27 o 12 4 3 265.19 204.10 35.47 o 13 4 3 915.06 1029.92 49.36 o 14 4 3 77.58 54.11 39.76 o 1 5 3 5028.31 4657.12 66.11 o 2 5 3 1612.35 1647.98 32.00 o 3 5 3 944.00 892.32 23.17 o 4 5 3 71.11 117.75 16.40 o 5 5 3 8754.96 8194.86 114.60 o 6 5 3 1714.07 1637.85 57.07 o 7 5 3 75.03 48.03 21.31 o 8 5 3 7.73 72.49 25.12 o 9 5 3 5553.60 5318.77 93.59 o 10 5 3 526.48 586.75 36.39 o 11 5 3 130.44 131.12 34.30 o 12 5 3 1003.30 910.61 50.35 o 13 5 3 259.37 300.80 36.93 o 0 6 3 359.92 287.98 27.80 o 1 6 3 6801.64 6768.25 92.04 o 2 6 3 5102.91 4942.11 71.37 o 3 6 3 5176.37 5542.08 73.64 o 4 6 3 2302.28 2333.01 44.46 o 5 6 3 701.63 687.24 30.68 o 6 6 3 776.89 755.19 32.12 o 7 6 3 2250.81 2356.41 55.40 o 8 6 3 1132.66 1109.84 49.68 o 9 6 3 21.25 -0.97 30.74 o 10 6 3 4.62 -6.31 31.19 o 11 6 3 18.60 35.02 33.88 o 12 6 3 45.77 89.56 37.54 o 1 7 3 1509.30 1559.30 40.22 o 2 7 3 118.35 172.80 22.71 o 3 7 3 253.30 242.86 22.68 o 4 7 3 144.07 86.69 24.12 o 5 7 3 3415.40 3433.46 64.87 o 6 7 3 248.96 294.87 28.69 o 7 7 3 693.47 805.18 35.33 o 8 7 3 562.25 594.22 35.06 o 9 7 3 2268.37 2227.31 58.01 o 10 7 3 128.43 90.15 37.12 o 11 7 3 26.56 79.61 38.83 o 0 8 3 29.16 93.86 45.20 o 1 8 3 1647.71 1642.80 51.03 o 2 8 3 452.03 488.89 31.41 o 3 8 3 440.97 475.72 47.24 o 4 8 3 11.79 10.63 27.57 o 5 8 3 683.17 729.55 35.74 o 6 8 3 51.31 41.04 32.21 o 7 8 3 38.96 45.05 33.18 o 8 8 3 162.95 135.41 36.83 o 9 8 3 171.01 100.95 37.65 o 1 9 3 92.66 109.96 39.00 o 2 9 3 21.04 -18.28 38.11 o 3 9 3 917.70 950.50 59.08 o 4 9 3 133.85 189.94 49.92 o 5 9 3 740.59 772.62 89.38 o 6 9 3 36.48 21.95 44.85 o 0 10 3 354.51 419.18 100.44 o 1 10 3 655.26 582.48 63.59 o 0 0 4 89900.13 81693.84 2509.74 o 1 0 4 66.17 250.70 12.70 o 2 0 4 1687.63 1755.16 82.21 o 3 0 4 663.35 135.42 13.84 o 4 0 4 62584.74 61853.70 900.44 o 5 0 4 1218.15 864.76 22.16 o 6 0 4 3255.51 3515.80 59.16 o 7 0 4 20281.88 20217.56 300.98 o 8 0 4 1415.19 1311.90 90.22 o 9 0 4 10628.23 10317.40 197.55 o 10 0 4 3008.83 2906.08 77.23 o 11 0 4 554.08 529.93 40.75 o 12 0 4 748.10 922.99 63.86 o 13 0 4 2245.75 2160.74 97.06 o 14 0 4 45.19 23.87 60.77 o 15 0 4 526.67 643.01 73.36 o 1 1 4 48375.54 57154.40 776.42 o 2 1 4 6652.79 8099.88 89.64 o 3 1 4 27156.69 28041.91 285.36 o 4 1 4 17689.96 18016.05 184.19 o 5 1 4 3175.38 2807.19 40.73 o 6 1 4 16623.65 17365.00 198.88 o 7 1 4 11434.63 11375.69 125.99 o 8 1 4 15270.67 14845.81 186.98 o 9 1 4 105.88 179.15 16.07 o 10 1 4 2644.26 2589.55 54.62 o 11 1 4 1739.94 1816.14 52.24 o 12 1 4 1297.32 1476.74 47.72 o 13 1 4 10.02 -15.88 32.31 o 14 1 4 12.58 49.79 34.74 o 15 1 4 54.47 126.25 43.56 o 0 2 4 307357.00 302580.47 8627.91 o 1 2 4 4551.63 3907.00 50.03 o 2 2 4 18675.23 20614.37 240.07 o 3 2 4 42.05 21.35 7.27 o 4 2 4 42607.06 44655.79 502.64 o 5 2 4 6564.79 6403.32 78.13 o 6 2 4 2260.93 2016.48 31.78 o 7 2 4 1248.79 1088.91 32.27 o 8 2 4 2189.79 2562.47 47.08 o 9 2 4 2079.25 1982.99 43.07 o 10 2 4 445.22 383.88 23.97 o 11 2 4 2010.96 1821.72 46.13 o 12 2 4 33.45 10.73 27.18 o 13 2 4 362.32 401.95 37.59 o 14 2 4 225.64 275.13 42.14 o 15 2 4 335.70 364.27 44.76 o 1 3 4 804.57 505.99 21.11 o 2 3 4 13830.19 14168.20 176.01 o 3 3 4 3774.10 3889.46 50.67 o 4 3 4 4693.95 4642.07 60.85 o 5 3 4 1290.79 1372.27 28.36 o 6 3 4 10804.91 10308.14 130.48 o 7 3 4 2676.26 2306.45 43.30 o 8 3 4 6438.31 6080.66 89.26 o 9 3 4 1016.40 1104.00 52.29 o 10 3 4 2185.55 2150.45 53.34 o 11 3 4 874.09 929.38 32.61 o 12 3 4 220.15 221.94 31.97 o 13 3 4 1.86 -47.43 33.72 o 14 3 4 33.58 84.96 37.79 o 0 4 4 13175.29 13775.32 265.24 o 1 4 4 894.89 865.85 20.15 o 2 4 4 5512.44 5293.58 71.36 o 3 4 4 140.08 127.08 13.32 o 4 4 4 7157.09 6576.29 82.67 o 5 4 4 1525.28 1574.65 30.75 o 6 4 4 120.19 134.37 17.27 o 7 4 4 919.12 984.87 30.78 o 8 4 4 32.15 88.04 25.48 o 9 4 4 50.42 68.92 23.61 o 10 4 4 1397.48 1224.41 42.11 o 11 4 4 24.52 3.45 26.26 o 12 4 4 369.34 425.62 33.30 o 13 4 4 47.64 23.37 35.96 o 14 4 4 110.61 69.80 41.80 o 1 5 4 1421.58 1345.02 27.76 o 2 5 4 2485.21 2743.32 40.96 o 3 5 4 402.51 484.94 26.07 o 4 5 4 1713.78 1812.77 33.51 o 5 5 4 272.54 280.21 17.78 o 6 5 4 5986.97 5734.23 88.39 o 7 5 4 56.94 52.84 21.95 o 8 5 4 42.06 60.61 28.32 o 9 5 4 62.04 62.74 26.03 o 10 5 4 1072.45 1184.54 45.67 o 11 5 4 136.53 150.86 32.31 o 12 5 4 3.83 4.68 33.07 o 13 5 4 197.98 179.48 37.78 o 0 6 4 176.64 221.34 26.72 o 1 6 4 380.19 394.67 18.89 o 2 6 4 1970.57 1905.52 46.32 o 3 6 4 1353.83 1367.25 34.14 o 4 6 4 202.99 222.18 19.91 o 5 6 4 856.92 922.39 30.62 o 6 6 4 470.45 522.67 27.80 o 7 6 4 277.16 257.36 26.41 o 8 6 4 351.74 373.96 30.05 o 9 6 4 531.94 574.02 37.91 o 10 6 4 113.75 76.83 30.89 o 11 6 4 283.50 325.00 35.87 o 12 6 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