#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/83/2228311.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228311_Fobs loop_ _publ_author_name 'Chen, Ji-Fang' 'Liu, Ying' 'Wang, Jing-Yang' 'Liu, Deng-Ke' _publ_section_title ; 2-Chloroethyl 2-(2-chlorophenyl)-2-(4,5,6,7-tetrahydrothieno[3,2-c]pyridin-5-yl)acetate ; _journal_coeditor_code FK2029 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3213 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.509 _cell_angle_gamma 90.000 _cell_length_a 9.6890 _cell_length_b 11.2670 _cell_length_c 15.5670 _exptl_crystal_F_000 768.00 _reflns_d_resolution_high 0.8080 _[local]_cod_data_source_file fk2029Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _c100329b' _shelx_refln_list_code 4 _shelx_f_calc_maximum 301.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3370.61 3469.10 107.88 o 4 0 0 4711.75 5401.24 235.44 o 6 0 0 1587.14 1635.01 42.12 o 8 0 0 607.32 624.91 26.23 o 10 0 0 308.80 326.57 19.45 o 1 1 0 2756.52 2709.76 47.18 o 2 1 0 1530.81 1515.62 36.90 o 3 1 0 2193.37 2130.88 31.72 o 4 1 0 6743.38 7359.11 146.55 o 5 1 0 23.26 42.28 7.66 o 6 1 0 477.23 414.93 19.43 o 7 1 0 6.39 8.34 2.02 o 8 1 0 5314.09 5548.53 137.30 o 9 1 0 505.94 537.84 20.11 o 10 1 0 522.56 530.62 14.69 o 11 1 0 23.33 21.79 3.43 o 0 2 0 292.46 292.60 8.31 o 1 2 0 1224.73 1265.46 38.31 o 2 2 0 99.04 77.07 5.20 o 3 2 0 884.16 853.98 16.44 o 4 2 0 1222.47 1114.38 25.07 o 5 2 0 858.87 748.28 30.48 o 6 2 0 1486.97 1368.53 38.11 o 7 2 0 209.21 208.40 9.83 o 8 2 0 3116.36 3205.45 70.01 o 9 2 0 7.69 5.61 2.50 o 10 2 0 12.32 11.35 3.14 o 11 2 0 54.09 56.39 7.25 o 1 3 0 9871.23 9971.18 727.03 o 2 3 0 1896.15 2035.68 60.03 o 3 3 0 0.46 5.38 1.78 o 4 3 0 57.32 49.32 5.75 o 5 3 0 515.25 526.79 27.13 o 6 3 0 2481.12 2231.99 48.62 o 7 3 0 937.99 952.54 22.67 o 8 3 0 239.94 206.68 20.50 o 9 3 0 135.06 148.59 9.82 o 10 3 0 1246.85 1240.48 54.87 o 11 3 0 71.69 57.53 5.02 o 0 4 0 597.32 652.05 31.13 o 1 4 0 1229.31 1153.45 26.08 o 2 4 0 5633.92 6188.80 81.42 o 3 4 0 2956.95 2991.21 77.97 o 4 4 0 4879.10 5453.77 110.98 o 5 4 0 335.26 324.51 13.86 o 6 4 0 71.97 62.83 4.66 o 7 4 0 7896.91 8001.48 486.01 o 8 4 0 138.29 136.89 14.44 o 9 4 0 196.50 168.73 10.94 o 10 4 0 280.99 307.33 14.69 o 11 4 0 39.61 37.33 6.88 o 1 5 0 12.55 43.84 6.15 o 2 5 0 56.19 110.91 11.83 o 3 5 0 1115.94 1093.43 36.68 o 4 5 0 1613.51 1487.83 33.54 o 5 5 0 199.63 196.93 6.25 o 6 5 0 532.70 517.82 12.53 o 7 5 0 708.30 627.90 16.39 o 8 5 0 12.13 26.57 4.53 o 9 5 0 43.41 47.90 9.42 o 10 5 0 7.94 6.04 4.53 o 0 6 0 50.48 111.42 14.55 o 1 6 0 3179.99 3328.66 129.80 o 2 6 0 2.80 7.19 2.83 o 3 6 0 87.98 74.85 6.59 o 4 6 0 544.64 534.90 10.47 o 5 6 0 3.32 5.00 1.57 o 6 6 0 37.96 25.83 3.39 o 7 6 0 108.22 97.78 8.91 o 8 6 0 441.78 446.41 12.76 o 9 6 0 48.49 44.26 5.47 o 10 6 0 16.31 8.14 9.99 o 1 7 0 603.02 545.20 17.49 o 2 7 0 718.95 690.04 14.87 o 3 7 0 2765.98 2660.91 53.30 o 4 7 0 425.87 440.00 11.08 o 5 7 0 195.70 200.33 9.11 o 6 7 0 480.81 454.97 13.73 o 7 7 0 1.80 2.99 1.26 o 8 7 0 34.05 34.04 4.93 o 9 7 0 783.18 735.12 22.97 o 10 7 0 223.73 231.17 19.60 o 0 8 0 198.14 188.89 13.66 o 1 8 0 187.19 186.78 7.32 o 2 8 0 375.84 346.92 10.46 o 3 8 0 133.43 120.94 7.44 o 4 8 0 1253.40 1298.35 27.57 o 5 8 0 1583.75 1562.57 34.78 o 6 8 0 19.77 22.95 4.50 o 7 8 0 232.77 244.59 13.06 o 8 8 0 4.75 6.91 2.23 o 9 8 0 11.02 3.10 1.71 o 1 9 0 64.42 58.51 5.28 o 2 9 0 47.82 42.35 4.64 o 3 9 0 63.58 61.36 6.94 o 4 9 0 1218.91 1172.12 32.38 o 5 9 0 87.25 93.58 5.65 o 6 9 0 356.44 384.38 11.82 o 7 9 0 1.22 1.98 1.19 o 8 9 0 2.74 3.10 1.69 o 0 10 0 640.13 597.11 24.92 o 1 10 0 562.88 549.58 15.04 o 2 10 0 25.79 21.79 4.66 o 3 10 0 78.48 90.31 6.07 o 4 10 0 212.07 232.02 12.41 o 5 10 0 598.71 595.84 14.64 o 6 10 0 0.45 1.38 1.01 o 7 10 0 12.27 10.72 5.43 o 8 10 0 17.47 13.13 3.73 o 1 11 0 7.09 4.26 2.08 o 2 11 0 10.74 14.29 3.10 o 3 11 0 2.17 1.86 1.68 o 4 11 0 483.95 521.25 12.79 o 5 11 0 5.15 6.98 3.07 o 6 11 0 41.86 45.33 5.98 o 7 11 0 57.86 67.01 11.85 o 0 12 0 507.71 613.12 30.04 o 1 12 0 37.85 38.33 4.32 o 2 12 0 160.39 161.29 13.42 o 3 12 0 176.70 191.38 9.50 o 4 12 0 30.93 26.50 2.96 o 5 12 0 0.25 1.37 0.79 o 1 13 0 36.06 38.04 6.20 o 2 13 0 122.00 133.21 13.12 o 3 13 0 3.63 5.34 3.06 o 4 13 0 25.67 21.71 4.86 o -11 0 1 60.33 49.72 7.54 o -9 0 1 2716.54 3070.98 157.13 o -7 0 1 547.15 584.17 19.73 o -5 0 1 353.61 361.08 28.32 o -3 0 1 8327.64 7575.78 645.42 o -1 0 1 1714.65 1595.74 47.16 o 1 0 1 2127.46 1778.64 85.44 o 3 0 1 5806.11 6631.01 122.67 o 5 0 1 0.74 4.58 10.71 o 7 0 1 1469.77 1498.96 44.56 o 9 0 1 200.91 225.74 24.78 o 11 0 1 1.09 1.35 1.20 o -11 1 1 766.46 627.80 41.83 o -10 1 1 1490.69 1445.60 94.59 o -9 1 1 0.42 7.36 2.52 o -8 1 1 3.03 4.80 2.02 o -7 1 1 1473.24 1449.97 26.11 o -6 1 1 0.41 1.77 1.09 o -5 1 1 3.69 11.88 3.79 o -4 1 1 3959.94 4267.40 66.76 o -3 1 1 2.27 8.15 1.97 o -2 1 1 107.21 118.03 6.51 o -1 1 1 139.00 127.58 6.05 o 0 1 1 10.37 15.37 1.91 o 1 1 1 4329.07 4326.07 116.76 o 2 1 1 1.45 8.17 3.51 o 3 1 1 33.91 24.73 3.19 o 4 1 1 720.06 764.13 30.83 o 5 1 1 3267.69 3510.17 65.80 o 6 1 1 6107.33 6552.91 152.27 o 7 1 1 2652.98 2605.41 56.37 o 8 1 1 11.49 10.32 3.86 o 9 1 1 266.69 274.13 19.42 o 10 1 1 540.30 538.21 13.00 o 11 1 1 1527.00 1420.97 103.45 o -11 2 1 1.93 2.06 1.68 o -10 2 1 254.46 269.23 19.75 o -9 2 1 292.19 278.48 11.97 o -8 2 1 2460.10 2391.49 48.17 o -7 2 1 201.47 213.64 7.79 o -6 2 1 451.66 460.72 10.34 o -5 2 1 7161.11 8326.08 187.03 o -4 2 1 48.55 36.80 5.07 o -3 2 1 1696.88 1588.91 30.19 o -2 2 1 1943.28 2017.84 44.41 o -1 2 1 19005.14 19544.46 1429.21 o 0 2 1 59.27 68.97 3.24 o 1 2 1 18678.71 18244.84 1312.45 o 2 2 1 10897.80 10914.60 739.67 o 3 2 1 619.04 615.90 11.96 o 4 2 1 2173.05 2345.95 50.81 o 5 2 1 2339.51 2446.56 67.86 o 6 2 1 1039.84 1018.82 20.43 o 7 2 1 0.01 3.75 1.53 o 8 2 1 303.43 333.21 21.77 o 9 2 1 823.19 903.74 36.69 o 10 2 1 115.09 114.60 9.69 o 11 2 1 193.96 183.34 11.40 o -11 3 1 1.24 3.50 2.00 o -10 3 1 11.71 9.36 3.36 o -9 3 1 591.37 647.23 16.98 o -8 3 1 106.31 131.35 13.32 o -7 3 1 55.20 46.72 4.32 o -6 3 1 14.18 17.01 2.35 o -5 3 1 4743.60 4900.06 143.85 o -4 3 1 160.50 190.54 11.12 o -3 3 1 598.70 595.75 22.77 o -2 3 1 4255.95 4399.02 98.92 o -1 3 1 11724.35 12486.74 839.61 o 0 3 1 3024.23 3100.76 57.34 o 1 3 1 288.12 256.60 6.66 o 2 3 1 194.28 175.20 9.63 o 3 3 1 7257.73 7518.46 204.55 o 4 3 1 3119.05 3065.66 72.04 o 5 3 1 544.31 564.88 20.25 o 6 3 1 321.86 326.20 9.02 o 7 3 1 745.36 728.56 21.42 o 8 3 1 70.21 75.93 14.91 o 9 3 1 61.61 61.45 9.93 o 10 3 1 915.99 873.44 38.18 o 11 3 1 8.80 8.72 4.24 o -11 4 1 537.52 505.69 19.14 o -10 4 1 500.57 487.21 24.97 o -9 4 1 111.59 114.08 8.34 o -8 4 1 538.46 512.79 12.48 o -7 4 1 312.24 286.21 12.43 o -6 4 1 1340.59 1317.10 24.13 o -5 4 1 7.18 9.26 1.84 o -4 4 1 1567.72 1506.23 43.29 o -3 4 1 3988.60 4719.56 96.38 o -2 4 1 735.73 687.43 22.38 o -1 4 1 620.09 537.10 19.79 o 0 4 1 2655.52 2649.98 53.80 o 1 4 1 2560.20 2785.18 95.63 o 2 4 1 397.77 330.91 12.71 o 3 4 1 194.69 172.81 8.95 o 4 4 1 803.22 849.46 32.82 o 5 4 1 600.51 542.00 12.21 o 6 4 1 3408.45 3326.33 55.09 o 7 4 1 270.05 266.51 12.68 o 8 4 1 59.04 58.42 9.65 o 9 4 1 899.98 960.84 22.97 o 10 4 1 33.03 27.33 13.07 o 11 4 1 7.06 2.03 2.55 o -10 5 1 134.50 153.23 14.91 o -9 5 1 340.27 355.05 12.27 o -8 5 1 115.25 101.62 6.61 o -7 5 1 533.08 490.74 12.78 o -6 5 1 184.01 166.14 8.32 o -5 5 1 822.40 794.66 17.88 o -4 5 1 1.71 8.62 2.60 o -3 5 1 8830.83 10119.88 324.52 o -2 5 1 3449.33 3351.48 104.69 o -1 5 1 6494.14 7113.80 155.73 o 0 5 1 408.74 455.10 18.65 o 1 5 1 129.39 112.71 8.97 o 2 5 1 4842.00 5068.81 102.25 o 3 5 1 5960.65 6285.27 228.52 o 4 5 1 902.76 824.89 15.99 o 5 5 1 83.66 65.87 5.03 o 6 5 1 626.65 644.45 17.35 o 7 5 1 47.38 51.82 7.51 o 8 5 1 964.74 1007.40 32.83 o 9 5 1 529.95 530.66 13.85 o 10 5 1 12.26 9.96 7.77 o -10 6 1 377.97 336.09 19.41 o -9 6 1 376.75 348.65 15.23 o -8 6 1 172.99 161.44 8.78 o -7 6 1 104.65 97.56 9.66 o -6 6 1 478.17 462.93 11.15 o -5 6 1 407.90 391.02 10.54 o -4 6 1 224.54 191.58 9.73 o -3 6 1 34.49 30.78 3.78 o -2 6 1 935.11 884.79 27.90 o -1 6 1 1589.11 1619.57 45.46 o 0 6 1 46.22 49.60 6.87 o 1 6 1 3910.22 4373.78 100.12 o 2 6 1 173.15 142.19 10.96 o 3 6 1 998.07 973.70 18.39 o 4 6 1 9.29 7.72 1.45 o 5 6 1 455.28 420.82 10.19 o 6 6 1 199.25 172.07 10.78 o 7 6 1 3395.98 3797.79 75.59 o 8 6 1 14.00 27.77 5.36 o 9 6 1 147.63 138.60 11.14 o 10 6 1 154.60 151.24 10.93 o -10 7 1 197.92 211.43 12.58 o -9 7 1 255.25 221.58 8.08 o -8 7 1 187.69 178.23 8.97 o -7 7 1 1219.44 1342.53 26.35 o -6 7 1 198.21 190.25 17.24 o -5 7 1 456.47 438.02 13.77 o -4 7 1 169.98 165.24 6.69 o -3 7 1 2550.53 2338.07 53.63 o -2 7 1 64.84 61.54 5.31 o -1 7 1 2538.54 2592.84 55.07 o 0 7 1 385.50 339.72 17.26 o 1 7 1 5.38 13.95 2.45 o 2 7 1 31.66 31.18 3.92 o 3 7 1 1630.65 1488.37 26.84 o 4 7 1 214.57 212.24 9.06 o 5 7 1 1718.97 1581.11 37.15 o 6 7 1 2497.88 2398.26 73.77 o 7 7 1 180.96 169.45 9.74 o 8 7 1 2.92 3.24 1.30 o 9 7 1 217.11 206.45 12.04 o 10 7 1 844.54 757.19 31.57 o -9 8 1 1346.41 1265.23 59.38 o -8 8 1 201.17 225.16 12.92 o -7 8 1 991.96 1017.00 36.01 o -6 8 1 265.63 275.14 11.14 o -5 8 1 657.41 712.39 16.96 o -4 8 1 8.28 6.04 1.79 o -3 8 1 5.93 10.88 2.31 o -2 8 1 25.08 24.39 3.04 o -1 8 1 1575.62 1452.68 28.30 o 0 8 1 45.06 56.49 5.26 o 1 8 1 3.53 7.98 2.03 o 2 8 1 10.08 13.98 2.65 o 3 8 1 60.17 55.23 5.21 o 4 8 1 82.70 84.00 6.37 o 5 8 1 193.79 179.21 17.19 o 6 8 1 10.56 9.15 2.72 o 7 8 1 413.35 416.25 10.67 o 8 8 1 107.64 107.15 6.63 o 9 8 1 1168.27 1080.60 37.42 o -8 9 1 296.77 321.00 14.05 o -7 9 1 12.47 15.67 4.26 o -6 9 1 0.06 2.45 1.36 o -5 9 1 3445.56 3615.35 97.95 o -4 9 1 1066.44 1028.27 29.39 o -3 9 1 58.99 50.44 6.80 o -2 9 1 0.96 3.81 1.55 o -1 9 1 812.96 779.06 22.41 o 0 9 1 6.83 10.23 3.06 o 1 9 1 3955.75 3678.26 118.83 o 2 9 1 32.56 30.76 4.78 o 3 9 1 622.63 576.30 14.98 o 4 9 1 417.25 430.11 12.51 o 5 9 1 8.90 10.33 2.88 o 6 9 1 275.99 274.71 16.88 o 7 9 1 19.97 22.99 4.43 o 8 9 1 6.81 4.00 2.22 o -7 10 1 171.12 166.74 11.05 o -6 10 1 364.78 346.64 13.20 o -5 10 1 49.71 49.46 4.99 o -4 10 1 194.93 196.22 14.47 o -3 10 1 0.69 3.33 2.21 o -2 10 1 183.43 165.89 16.81 o -1 10 1 177.71 172.69 19.57 o 0 10 1 1047.15 1000.35 25.19 o 1 10 1 3.82 5.80 2.24 o 2 10 1 267.10 280.72 21.30 o 3 10 1 611.55 612.50 18.02 o 4 10 1 91.11 92.98 6.37 o 5 10 1 271.63 270.68 8.51 o 6 10 1 34.10 40.35 4.40 o 7 10 1 464.07 479.96 23.23 o -7 11 1 611.86 634.91 34.90 o -6 11 1 1.82 1.49 1.30 o -5 11 1 526.25 553.98 14.07 o -4 11 1 1582.05 1574.55 43.39 o -3 11 1 318.28 310.36 17.31 o -2 11 1 111.76 116.08 9.33 o -1 11 1 1122.61 1164.96 38.00 o 0 11 1 707.98 696.05 25.43 o 1 11 1 142.93 137.32 9.99 o 2 11 1 105.77 115.93 8.15 o 3 11 1 769.97 779.31 15.90 o 4 11 1 15.33 15.44 4.04 o 5 11 1 22.55 18.49 4.03 o 6 11 1 317.65 324.57 18.09 o 7 11 1 66.60 68.94 11.24 o -5 12 1 66.39 67.96 5.31 o -4 12 1 303.95 295.36 13.08 o -3 12 1 50.04 52.69 5.01 o -2 12 1 596.03 576.87 31.40 o -1 12 1 278.68 281.98 22.02 o 0 12 1 64.58 65.91 6.89 o 1 12 1 448.38 413.48 23.36 o 2 12 1 52.90 54.04 3.93 o 3 12 1 357.24 352.84 16.73 o 4 12 1 32.20 30.65 4.50 o 5 12 1 73.31 73.75 7.35 o -4 13 1 83.95 79.58 12.53 o -3 13 1 58.26 55.79 4.55 o -2 13 1 236.91 236.00 28.17 o -1 13 1 22.83 24.26 4.47 o 0 13 1 4.49 3.84 2.37 o 1 13 1 43.42 44.68 6.79 o 2 13 1 1065.42 1090.49 29.23 o 3 13 1 16.40 19.15 5.03 o 4 13 1 9.32 4.32 12.08 o -10 0 2 696.20 672.18 22.03 o -8 0 2 3823.67 3765.47 94.01 o -6 0 2 2483.39 2499.05 202.53 o -4 0 2 1484.06 1363.90 61.17 o -2 0 2 431.43 404.02 11.42 o 0 0 2 734.59 600.23 14.19 o 2 0 2 7653.70 8805.40 912.57 o 4 0 2 2643.98 3171.38 79.65 o 6 0 2 1004.36 946.85 26.75 o 8 0 2 1955.78 1946.21 159.35 o 10 0 2 20.04 27.95 6.32 o -11 1 2 236.47 212.27 16.41 o -10 1 2 119.99 135.52 10.51 o -9 1 2 1171.75 1294.41 37.50 o -8 1 2 580.44 557.94 16.67 o -7 1 2 842.08 806.78 18.97 o -6 1 2 925.12 893.63 20.10 o -5 1 2 110.13 77.46 9.17 o -4 1 2 0.23 4.38 2.14 o -3 1 2 3467.06 3491.87 80.81 o -2 1 2 855.43 836.53 28.67 o -1 1 2 99.17 100.86 4.82 o 0 1 2 68.53 79.70 3.96 o 1 1 2 9.67 10.40 1.69 o 2 1 2 84.38 74.83 4.99 o 3 1 2 171.46 169.69 12.59 o 4 1 2 1548.09 1693.76 48.32 o 5 1 2 2957.82 3138.51 116.37 o 6 1 2 3.27 6.99 2.34 o 7 1 2 353.89 357.48 15.87 o 8 1 2 6.38 3.90 2.18 o 9 1 2 760.85 799.09 27.44 o 10 1 2 562.81 571.90 23.26 o 11 1 2 27.68 15.39 6.61 o -11 2 2 364.22 326.58 32.98 o -10 2 2 154.92 147.44 9.95 o -9 2 2 5.86 10.53 3.88 o -8 2 2 109.85 106.83 13.23 o -7 2 2 138.77 125.59 6.56 o -6 2 2 3280.97 3272.98 59.30 o -5 2 2 1805.74 2084.13 63.56 o -4 2 2 3218.55 3608.61 119.91 o -3 2 2 594.98 650.59 23.04 o -2 2 2 7649.48 7003.53 580.72 o -1 2 2 5064.01 5247.94 136.33 o 0 2 2 2409.11 2480.39 34.93 o 1 2 2 19493.75 19368.65 1303.19 o 2 2 2 749.60 684.73 28.70 o 3 2 2 439.59 450.64 20.74 o 4 2 2 21.03 15.24 4.59 o 5 2 2 34.32 46.24 8.81 o 6 2 2 63.65 57.03 5.07 o 7 2 2 480.91 470.27 16.48 o 8 2 2 234.99 218.50 27.08 o 9 2 2 48.57 39.45 10.00 o 10 2 2 171.02 180.03 12.34 o 11 2 2 998.07 934.82 30.78 o -11 3 2 354.30 325.26 18.66 o -10 3 2 953.77 1010.34 23.66 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2496.05 78.38 o 3 4 2 3625.39 3909.55 203.31 o 4 4 2 31.57 37.33 6.24 o 5 4 2 618.43 616.20 14.65 o 6 4 2 1163.03 1108.07 24.85 o 7 4 2 7.21 7.06 2.20 o 8 4 2 624.13 672.70 20.64 o 9 4 2 3128.79 3599.01 67.45 o 10 4 2 132.40 138.19 10.97 o -11 5 2 584.67 504.01 16.43 o -10 5 2 503.52 516.82 15.69 o -9 5 2 420.69 433.07 17.49 o -8 5 2 16.53 15.79 3.27 o -7 5 2 1221.34 1214.59 29.27 o -6 5 2 3902.58 3778.92 68.59 o -5 5 2 3259.93 3102.33 59.14 o -4 5 2 23.92 17.42 2.83 o -3 5 2 330.43 372.93 17.39 o -2 5 2 610.61 665.32 26.84 o -1 5 2 1825.58 1920.58 39.14 o 0 5 2 674.28 563.16 21.86 o 1 5 2 128.62 164.78 10.27 o 2 5 2 271.20 264.34 13.61 o 3 5 2 728.32 676.06 27.31 o 4 5 2 2525.04 2405.71 36.64 o 5 5 2 1960.25 1961.43 33.81 o 6 5 2 1626.82 1605.56 41.35 o 7 5 2 109.14 93.49 10.55 o 8 5 2 0.05 2.73 1.29 o 9 5 2 15.29 19.96 5.14 o 10 5 2 451.87 485.64 32.49 o -10 6 2 1263.55 1245.86 25.67 o -9 6 2 202.66 205.10 11.13 o -8 6 2 537.87 602.24 21.04 o -7 6 2 89.91 82.30 10.18 o -6 6 2 69.61 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