#------------------------------------------------------------------------------ #$Date: 2011-02-15 17:23:33 +0200 (Tue, 15 Feb 2011) $ #$Revision: 11387 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2228341.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228341_Fobs loop_ _publ_author_name 'Vitze, Hannes' 'Lerner, Hans-Wolfram' 'Bolte, Michael' _publ_section_title ; \m~2~-Acetone-diacetone[\m~3~-tris(trifluoromethyl)methanolato]bis[\m~2~-tris(trifluoromethyl)methanolato]trilithium ; _journal_coeditor_code HB5716 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1527 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.246 _cell_angle_gamma 90.000 _cell_length_a 20.6939 _cell_length_b 11.5940 _cell_length_c 15.2211 _exptl_crystal_F_000 1776.00 _reflns_d_resolution_high 0.8182 _[local]_cod_data_source_file hb5716Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa744 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 188.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 18955.53 22763.66 525.66 o 5 0 0 3888.86 3109.27 92.79 o 6 0 0 9082.24 9393.66 189.38 o 7 0 0 11908.19 11289.86 129.26 o 8 0 0 2559.79 1544.62 67.18 o 9 0 0 13402.60 12175.68 169.23 o 10 0 0 646.17 859.37 59.91 o 11 0 0 1563.92 1455.70 70.10 o 12 0 0 1010.84 889.97 79.17 o 13 0 0 698.07 658.49 48.46 o 14 0 0 619.50 544.44 36.27 o 15 0 0 1015.28 957.99 40.64 o 16 0 0 1403.72 1654.67 71.29 o 17 0 0 119.98 75.99 36.79 o 18 0 0 21.88 18.84 35.19 o 19 0 0 10.44 15.08 41.76 o 20 0 0 548.66 450.05 35.84 o 21 0 0 101.72 93.92 32.76 o 22 0 0 142.71 172.16 58.92 o 23 0 0 4.76 32.19 29.96 o 24 0 0 0.50 4.69 53.25 o 3 1 0 2687.58 2692.92 85.76 o 4 1 0 1571.91 1887.98 60.90 o 5 1 0 875.10 1055.40 50.51 o 6 1 0 3831.32 3127.69 58.96 o 7 1 0 1020.74 756.22 40.68 o 8 1 0 3050.72 2654.25 49.01 o 9 1 0 5313.13 4425.79 55.03 o 10 1 0 3595.93 3099.17 67.96 o 11 1 0 4825.04 4792.85 99.66 o 12 1 0 1268.88 1699.31 38.32 o 13 1 0 2464.78 2143.69 40.85 o 14 1 0 421.59 461.69 31.16 o 15 1 0 387.73 408.37 31.51 o 16 1 0 291.71 205.74 26.22 o 17 1 0 543.26 651.58 30.27 o 18 1 0 177.87 86.21 26.47 o 19 1 0 6.45 27.91 23.74 o 20 1 0 188.75 232.63 27.13 o 21 1 0 105.03 121.58 29.47 o 22 1 0 36.49 80.68 22.92 o 23 1 0 2.03 0.47 25.58 o 24 1 0 0.05 25.21 28.98 o 0 2 0 9522.75 9041.62 246.70 o 1 2 0 8992.46 8470.38 189.63 o 2 2 0 3348.88 4207.20 104.34 o 3 2 0 7285.78 6621.76 162.65 o 4 2 0 1934.05 2377.26 57.57 o 5 2 0 10582.92 9216.32 88.97 o 6 2 0 152.30 122.08 49.96 o 7 2 0 5.04 2.45 36.19 o 8 2 0 3977.89 3401.75 53.87 o 9 2 0 524.84 491.56 41.65 o 10 2 0 211.15 212.95 44.52 o 11 2 0 408.28 581.45 34.90 o 12 2 0 342.47 337.85 33.11 o 13 2 0 0.78 18.93 35.60 o 14 2 0 9.16 35.05 28.67 o 15 2 0 28.18 69.10 31.15 o 16 2 0 5.56 21.41 36.50 o 17 2 0 0.00 -5.85 29.29 o 18 2 0 323.58 285.22 27.13 o 19 2 0 67.92 58.96 28.03 o 20 2 0 5.32 22.57 26.32 o 21 2 0 11.01 55.57 26.31 o 22 2 0 5.36 17.24 27.15 o 23 2 0 4.89 44.25 22.67 o 24 2 0 16.63 49.83 24.64 o 1 3 0 6066.78 6561.79 118.56 o 2 3 0 965.63 775.80 57.28 o 3 3 0 5235.23 5533.97 162.78 o 4 3 0 139.52 145.30 55.73 o 5 3 0 14241.81 11941.10 197.31 o 6 3 0 332.73 663.12 43.06 o 7 3 0 24.11 97.94 38.99 o 8 3 0 5461.40 4497.49 91.22 o 9 3 0 3589.13 3042.44 99.21 o 10 3 0 311.60 311.63 34.81 o 11 3 0 323.41 355.00 36.13 o 12 3 0 800.80 874.49 41.02 o 13 3 0 136.83 -6.91 32.18 o 14 3 0 49.12 63.04 47.25 o 15 3 0 265.91 181.62 36.17 o 16 3 0 0.30 14.25 29.71 o 17 3 0 270.55 354.69 35.72 o 18 3 0 2.60 46.44 29.39 o 19 3 0 262.80 259.50 26.91 o 20 3 0 58.52 90.06 26.84 o 21 3 0 134.24 103.55 29.97 o 22 3 0 68.46 72.97 25.84 o 23 3 0 18.99 -0.03 29.62 o 24 3 0 1.25 53.34 66.44 o 0 4 0 8821.18 9110.19 132.63 o 1 4 0 230.26 280.66 53.25 o 2 4 0 1025.04 925.03 48.67 o 3 4 0 46.58 83.14 50.87 o 4 4 0 2727.15 3098.04 62.27 o 5 4 0 9492.75 9599.73 432.66 o 6 4 0 4464.40 4392.49 64.80 o 7 4 0 26.35 56.97 48.71 o 8 4 0 4234.18 5315.74 109.77 o 9 4 0 196.45 121.20 37.94 o 10 4 0 305.57 437.40 37.30 o 11 4 0 291.68 378.11 33.85 o 12 4 0 59.02 97.85 33.76 o 13 4 0 176.78 174.92 33.42 o 14 4 0 10.53 14.95 31.95 o 15 4 0 29.87 -1.09 34.50 o 16 4 0 217.78 288.26 35.55 o 17 4 0 0.00 8.95 26.82 o 18 4 0 242.09 162.87 33.16 o 19 4 0 138.64 170.17 30.60 o 20 4 0 15.43 5.45 23.28 o 21 4 0 0.08 8.72 25.94 o 22 4 0 17.34 91.70 27.16 o 23 4 0 32.46 44.58 25.31 o 1 5 0 69.59 92.10 50.33 o 2 5 0 609.89 620.83 49.12 o 3 5 0 10.07 67.15 49.47 o 4 5 0 8614.83 7458.82 201.91 o 5 5 0 5135.03 6371.25 136.43 o 6 5 0 2752.45 2363.86 49.79 o 7 5 0 176.46 267.82 40.49 o 8 5 0 2148.64 2409.00 98.36 o 9 5 0 5.55 39.89 40.71 o 10 5 0 239.20 172.35 37.16 o 11 5 0 89.03 44.31 35.19 o 12 5 0 37.19 44.41 32.89 o 13 5 0 1667.60 1504.85 42.85 o 14 5 0 1184.60 1350.99 33.93 o 15 5 0 20.35 46.75 30.41 o 16 5 0 31.18 67.32 27.79 o 17 5 0 739.68 730.57 30.75 o 18 5 0 0.30 27.57 26.28 o 19 5 0 74.07 45.91 29.62 o 20 5 0 156.76 123.38 25.91 o 21 5 0 2.62 -8.62 26.84 o 22 5 0 4.33 6.57 24.57 o 23 5 0 3.01 -0.29 72.75 o 0 6 0 1388.59 1681.84 76.30 o 1 6 0 295.25 372.68 46.87 o 2 6 0 1843.86 2178.05 56.86 o 3 6 0 1395.01 1531.29 53.24 o 4 6 0 5260.06 5681.58 82.54 o 5 6 0 267.03 339.54 38.22 o 6 6 0 123.26 126.30 32.04 o 7 6 0 402.40 378.38 45.80 o 8 6 0 1099.66 1412.11 54.63 o 9 6 0 0.90 23.07 40.47 o 10 6 0 226.21 199.81 31.59 o 11 6 0 704.13 509.05 38.30 o 12 6 0 22.62 25.18 33.54 o 13 6 0 1316.71 1129.51 53.39 o 14 6 0 5.79 -8.27 35.98 o 15 6 0 53.11 35.02 26.05 o 16 6 0 469.82 453.07 47.53 o 17 6 0 1.88 34.62 32.29 o 18 6 0 18.02 37.76 31.62 o 19 6 0 93.72 141.81 34.63 o 20 6 0 9.89 -19.09 22.61 o 21 6 0 31.56 34.66 25.98 o 22 6 0 30.75 35.61 21.47 o 1 7 0 545.18 391.17 37.42 o 2 7 0 1165.39 1262.42 41.75 o 3 7 0 23.25 131.32 38.37 o 4 7 0 1046.75 893.10 40.16 o 5 7 0 25.28 3.22 40.42 o 6 7 0 46.26 91.94 38.23 o 7 7 0 567.93 520.32 40.53 o 8 7 0 59.25 89.17 32.66 o 9 7 0 2.93 75.30 35.24 o 10 7 0 569.65 719.34 39.25 o 11 7 0 417.80 327.31 37.92 o 12 7 0 4.31 10.97 34.67 o 13 7 0 7.15 106.19 39.23 o 14 7 0 677.61 772.81 37.21 o 15 7 0 73.70 87.05 36.21 o 16 7 0 35.63 101.16 34.70 o 17 7 0 0.00 -7.19 33.92 o 18 7 0 30.09 112.71 34.60 o 19 7 0 14.46 41.58 30.39 o 20 7 0 26.84 82.60 35.49 o 21 7 0 10.82 31.88 27.53 o 0 8 0 9.92 -11.10 51.51 o 1 8 0 26.29 -24.63 36.31 o 2 8 0 38.34 32.67 37.90 o 3 8 0 7.74 36.45 36.32 o 4 8 0 718.12 713.71 40.69 o 5 8 0 112.32 128.02 31.23 o 6 8 0 27.03 31.12 34.11 o 7 8 0 122.08 178.08 36.43 o 8 8 0 59.01 81.67 42.00 o 9 8 0 17.17 51.80 39.36 o 10 8 0 16.52 12.99 42.81 o 11 8 0 125.35 84.34 33.05 o 12 8 0 248.76 215.49 45.93 o 13 8 0 64.66 144.04 40.55 o 14 8 0 0.09 -12.39 33.36 o 15 8 0 151.40 81.28 38.00 o 16 8 0 6.31 26.75 32.45 o 17 8 0 0.35 1.04 36.33 o 18 8 0 67.42 48.31 31.77 o 19 8 0 20.25 0.56 28.23 o 20 8 0 70.56 54.28 37.93 o 1 9 0 139.64 80.17 36.22 o 2 9 0 184.63 149.56 38.37 o 3 9 0 2.41 15.79 36.18 o 4 9 0 100.97 93.83 33.54 o 5 9 0 209.64 246.23 42.27 o 6 9 0 303.48 219.51 35.45 o 7 9 0 330.14 364.86 36.71 o 8 9 0 311.08 262.21 40.92 o 9 9 0 47.46 17.91 39.07 o 10 9 0 17.26 51.94 38.71 o 11 9 0 5.69 43.96 44.67 o 12 9 0 2.20 47.79 36.14 o 13 9 0 21.76 -1.24 45.25 o 14 9 0 65.10 64.36 38.13 o 15 9 0 0.05 2.64 35.15 o 16 9 0 167.21 86.75 30.44 o 17 9 0 28.14 50.48 36.44 o 18 9 0 32.38 1.79 62.08 o 0 10 0 2513.22 2676.78 67.57 o 1 10 0 166.56 235.73 36.46 o 2 10 0 21.03 -5.85 34.76 o 3 10 0 0.32 14.30 33.00 o 4 10 0 339.70 403.53 38.99 o 5 10 0 32.80 36.22 36.15 o 6 10 0 20.64 42.59 35.94 o 7 10 0 18.06 54.54 36.43 o 8 10 0 3.76 64.77 43.17 o 9 10 0 463.12 446.45 36.32 o 10 10 0 24.60 104.35 44.33 o 11 10 0 245.91 253.41 47.99 o 12 10 0 1.59 18.20 39.15 o 13 10 0 0.19 -31.58 40.47 o 14 10 0 16.73 41.04 34.68 o 15 10 0 103.89 199.61 37.75 o 16 10 0 18.40 66.88 72.45 o 17 10 0 0.51 65.13 37.12 o 1 11 0 25.46 21.11 32.93 o 2 11 0 45.24 37.05 33.60 o 3 11 0 0.55 24.41 33.28 o 4 11 0 65.11 45.02 29.48 o 5 11 0 15.23 53.68 34.56 o 6 11 0 17.22 52.43 33.05 o 7 11 0 1.50 23.87 32.21 o 8 11 0 166.79 149.09 43.48 o 9 11 0 467.12 448.54 47.01 o 10 11 0 76.20 127.71 48.79 o 11 11 0 1.11 66.68 50.91 o 12 11 0 10.87 10.90 43.77 o 13 11 0 36.82 72.17 42.02 o 14 11 0 50.94 30.74 35.57 o 15 11 0 23.99 -48.40 48.40 o 0 12 0 379.00 462.74 73.20 o 1 12 0 70.20 73.35 35.01 o 2 12 0 19.04 27.03 34.32 o 3 12 0 202.94 278.50 37.33 o 4 12 0 60.32 105.97 35.86 o 5 12 0 275.73 259.25 34.53 o 6 12 0 98.33 83.48 35.14 o 7 12 0 129.06 118.41 37.49 o 8 12 0 6.11 0.11 29.10 o 9 12 0 6.62 52.25 37.60 o 10 12 0 0.74 56.37 38.65 o 11 12 0 14.50 14.76 34.35 o 12 12 0 3.38 11.05 34.94 o 1 13 0 0.15 0.01 33.66 o 2 13 0 49.23 67.62 33.11 o 3 13 0 81.47 49.98 36.67 o 4 13 0 53.64 93.73 32.96 o 5 13 0 0.57 11.72 33.39 o 6 13 0 25.15 39.68 33.82 o 7 13 0 0.50 30.13 34.29 o 8 13 0 44.17 53.58 37.67 o 9 13 0 0.69 81.47 47.03 o 0 14 0 5.92 50.33 48.52 o 1 14 0 9.52 56.59 34.70 o 2 14 0 0.84 33.99 52.66 o -24 1 1 9.69 49.58 25.04 o -23 1 1 0.41 -5.05 31.91 o -22 1 1 35.20 46.32 28.75 o -21 1 1 2.39 -3.14 27.18 o -20 1 1 791.61 837.65 32.37 o -19 1 1 18.61 31.64 30.21 o -18 1 1 54.75 58.22 29.51 o -17 1 1 84.88 63.90 33.25 o -16 1 1 1.80 36.55 32.67 o -15 1 1 1128.30 1266.04 51.53 o -14 1 1 382.42 364.95 40.30 o -13 1 1 567.16 526.11 40.24 o -12 1 1 819.96 963.82 45.23 o -11 1 1 170.04 115.73 46.93 o -10 1 1 4297.35 4707.41 166.28 o -9 1 1 276.17 188.30 53.36 o -8 1 1 10926.12 12268.51 379.05 o -7 1 1 212.03 222.14 57.00 o -6 1 1 4509.29 4789.15 79.50 o -5 1 1 5978.24 5302.82 239.51 o -4 1 1 18466.67 18021.65 1355.55 o -3 1 1 8704.34 7680.17 176.32 o 3 1 1 3747.28 4262.53 72.03 o 4 1 1 15541.85 16012.88 102.05 o 5 1 1 4961.60 4510.35 63.88 o 6 1 1 2519.29 2139.21 51.82 o 7 1 1 44.77 113.56 38.47 o 8 1 1 1100.98 1417.70 42.39 o 9 1 1 1150.19 1365.87 40.74 o 10 1 1 465.54 424.44 33.49 o 11 1 1 201.17 235.89 26.29 o 12 1 1 354.49 351.61 27.71 o 13 1 1 1463.94 1558.29 40.40 o 14 1 1 32.28 45.18 23.74 o 15 1 1 106.60 177.40 27.78 o 16 1 1 1.99 -5.18 25.94 o 17 1 1 67.36 49.38 24.07 o 18 1 1 2.39 -3.97 23.13 o 19 1 1 92.12 101.14 23.07 o 20 1 1 4.05 -4.39 22.91 o 21 1 1 28.23 84.04 26.19 o 22 1 1 21.06 69.57 25.43 o 23 1 1 8.79 12.31 21.76 o 24 1 1 19.78 12.35 26.25 o -24 2 1 21.51 66.12 53.90 o -23 2 1 52.77 45.64 24.14 o -22 2 1 253.47 127.72 26.21 o -21 2 1 85.99 50.98 24.78 o -20 2 1 162.07 115.32 45.86 o -19 2 1 1.62 17.77 33.59 o -18 2 1 11.54 5.73 29.59 o -17 2 1 445.90 499.74 37.65 o -16 2 1 316.96 229.08 32.93 o -15 2 1 0.00 68.87 31.90 o -14 2 1 113.19 54.16 32.26 o -13 2 1 2.68 36.66 36.02 o -12 2 1 114.16 122.54 38.68 o -11 2 1 411.45 388.63 37.79 o -10 2 1 880.66 756.06 43.52 o -9 2 1 22.60 39.04 37.49 o -8 2 1 2225.64 2658.59 59.56 o -7 2 1 11.33 91.55 44.20 o -6 2 1 4414.89 4134.32 185.43 o -5 2 1 816.54 850.15 55.30 o -4 2 1 992.19 831.86 59.84 o -3 2 1 97.00 54.51 57.31 o -2 2 1 26339.08 27188.76 507.67 o -1 2 1 822.67 668.97 61.88 o 0 2 1 2361.45 1858.97 70.89 o 1 2 1 19524.18 19175.07 170.78 o 2 2 1 2739.03 2642.33 136.46 o 3 2 1 18485.82 18930.48 337.75 o 4 2 1 16982.61 14692.64 309.98 o 5 2 1 5.77 20.05 35.05 o 6 2 1 5136.81 4766.34 61.03 o 7 2 1 29.00 137.23 38.18 o 8 2 1 697.64 1009.27 45.68 o 9 2 1 641.61 863.29 39.18 o 10 2 1 2937.05 2948.41 46.61 o 11 2 1 612.78 557.74 34.50 o 12 2 1 140.94 90.87 27.71 o 13 2 1 0.72 40.18 29.23 o 14 2 1 301.25 491.14 26.09 o 15 2 1 94.44 98.97 23.98 o 16 2 1 329.98 298.97 29.12 o 17 2 1 63.09 68.88 28.72 o 18 2 1 92.19 139.77 29.16 o 19 2 1 119.95 140.87 30.04 o 20 2 1 201.98 103.55 25.87 o 21 2 1 130.66 142.19 23.05 o 22 2 1 4.40 37.72 25.59 o 23 2 1 7.82 29.23 26.25 o -24 3 1 0.93 -3.54 25.01 o -23 3 1 5.31 -20.34 26.86 o -22 3 1 5.72 29.61 26.83 o -21 3 1 105.73 181.70 33.90 o -20 3 1 64.72 79.58 33.03 o -19 3 1 92.01 187.45 31.10 o -18 3 1 402.94 332.19 35.73 o -17 3 1 315.30 335.78 32.01 o -16 3 1 415.87 330.89 33.31 o -15 3 1 301.54 321.92 36.12 o -14 3 1 5.29 63.16 35.77 o -13 3 1 21.80 -6.70 31.84 o -12 3 1 154.93 96.15 34.44 o -11 3 1 1415.14 1392.04 42.28 o -10 3 1 193.09 145.95 38.77 o -9 3 1 5208.33 5846.19 99.21 o -8 3 1 255.34 111.28 37.35 o -7 3 1 470.42 847.05 45.84 o -6 3 1 8.20 1.37 47.27 o -5 3 1 6357.98 7992.70 162.48 o -4 3 1 334.88 499.83 54.37 o -3 3 1 1094.96 580.09 48.47 o -2 3 1 1871.97 2401.78 71.05 o -1 3 1 3372.89 3451.29 76.32 o 0 3 1 14555.01 16508.72 132.95 o 1 3 1 6571.96 6223.13 95.28 o 2 3 1 20588.87 21505.50 547.68 o 3 3 1 562.12 504.52 62.93 o 4 3 1 571.45 433.82 47.46 o 5 3 1 492.65 318.72 45.28 o 6 3 1 945.93 1032.68 40.94 o 7 3 1 487.80 522.18 41.42 o 8 3 1 5441.81 6265.72 196.78 o 9 3 1 935.55 1165.69 44.77 o 10 3 1 683.47 640.34 42.68 o 11 3 1 422.09 318.99 39.53 o 12 3 1 447.84 587.47 35.85 o 13 3 1 5.80 4.97 31.36 o 14 3 1 808.00 1127.77 56.82 o 15 3 1 81.43 26.26 35.76 o 16 3 1 657.25 711.84 35.65 o 17 3 1 1.61 1.16 26.04 o 18 3 1 0.55 48.08 25.71 o 19 3 1 11.55 24.53 26.29 o 20 3 1 26.90 63.93 27.54 o 21 3 1 64.65 36.78 24.97 o 22 3 1 0.09 -5.96 33.31 o 23 3 1 44.79 52.08 29.57 o -23 4 1 74.01 32.56 29.27 o -22 4 1 29.31 93.74 29.19 o -21 4 1 80.47 92.66 33.51 o -20 4 1 112.06 44.45 33.46 o -19 4 1 3.23 17.79 28.84 o -18 4 1 57.70 39.32 32.54 o -17 4 1 160.43 94.98 31.82 o -16 4 1 261.36 314.99 29.96 o -15 4 1 1204.44 1098.49 36.40 o -14 4 1 181.87 279.98 36.56 o -13 4 1 254.89 182.86 28.30 o -12 4 1 2318.42 2109.55 42.77 o -11 4 1 3831.42 3874.32 47.76 o -10 4 1 576.36 680.75 34.90 o -9 4 1 6596.53 6197.79 167.30 o -8 4 1 341.07 320.18 41.57 o -7 4 1 43.33 75.62 46.11 o -6 4 1 181.63 209.46 48.06 o -5 4 1 538.10 369.50 43.53 o -4 4 1 8489.21 8444.64 233.96 o -3 4 1 11776.45 10703.25 260.74 o -2 4 1 139.45 174.69 51.47 o -1 4 1 9862.69 8966.50 222.54 o 0 4 1 1387.19 1276.89 59.17 o 1 4 1 3188.85 2986.85 71.29 o 2 4 1 15730.56 16372.12 605.83 o 3 4 1 459.46 241.45 47.81 o 4 4 1 1771.96 1868.01 78.15 o 5 4 1 31.04 19.18 42.28 o 6 4 1 259.48 187.62 41.34 o 7 4 1 366.01 533.75 41.37 o 8 4 1 1972.15 1971.38 50.43 o 9 4 1 598.40 479.21 36.19 o 10 4 1 1708.82 1815.71 47.77 o 11 4 1 3.32 -35.41 35.41 o 12 4 1 77.35 85.61 33.88 o 13 4 1 327.90 287.30 33.39 o 14 4 1 1.22 19.81 32.37 o 15 4 1 31.10 42.80 29.03 o 16 4 1 11.93 69.28 31.42 o 17 4 1 0.61 62.36 39.66 o 18 4 1 102.40 179.93 27.87 o 19 4 1 456.40 508.21 29.23 o 20 4 1 38.87 11.34 27.60 o 21 4 1 0.79 13.70 25.93 o 22 4 1 10.81 -31.92 31.92 o 23 4 1 0.12 8.49 29.05 o -23 5 1 4.96 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