#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/83/2228359.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228359_Fobs loop_ _publ_author_name 'Pojarov\'a, Michaela' 'Fejfarov\'a, Karla' 'Makrl\'ik, Emanuel' _publ_section_title ; Hydronium perchlorate--dibenzo-18-crown-6 (1/1): monoclinic polymorph ; _journal_coeditor_code HB5736 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3341 _journal_page_last o3342 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 100.0011(10) _cell_angle_gamma 90 _cell_length_a 8.65860(10) _cell_length_b 26.7718(3) _cell_length_c 19.1518(2) _exptl_crystal_F_000 2016 _reflns_d_resolution_high 0.8686 _[local]_cod_data_source_file hb5736Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 425.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 82.12 82.20 6.87 o 2 0 0 157424.41 181145.75 612.23 o 3 0 0 193.69 210.94 11.25 o 4 0 0 34386.98 30703.15 49.59 o 5 0 0 532.87 460.22 16.97 o 6 0 0 5168.54 5397.15 32.61 o 7 0 0 57.34 45.39 23.27 < 8 0 0 32.02 40.05 20.03 < 9 0 0 613.80 662.77 28.42 o 1 1 0 9.44 9.35 7.25 < 2 1 0 1639.77 2003.76 10.30 o 3 1 0 394.57 381.83 7.63 o 4 1 0 6687.69 5586.54 16.21 o 5 1 0 6.75 5.53 13.92 < 6 1 0 70.38 31.09 15.45 < 7 1 0 374.34 351.70 18.31 o 8 1 0 76.93 49.97 14.30 o 9 1 0 0.82 5.34 17.74 < 0 2 0 650.51 721.70 3.05 o 1 2 0 945.02 1159.80 14.30 o 2 2 0 2708.98 3280.09 16.78 o 3 2 0 1806.32 1880.36 11.06 o 4 2 0 6966.87 6447.66 17.17 o 5 2 0 459.04 425.32 13.35 o 6 2 0 372.72 360.66 16.02 o 7 2 0 1653.77 1729.12 20.60 o 8 2 0 941.67 1010.84 18.50 o 9 2 0 308.02 247.75 16.02 o 1 3 0 15894.09 21068.28 39.29 o 2 3 0 1256.92 1082.56 9.35 o 3 3 0 69.99 59.70 6.29 o 4 3 0 290.59 315.27 8.77 o 5 3 0 5849.20 5649.86 22.12 o 6 3 0 171.24 158.87 16.78 o 7 3 0 1932.58 2075.28 21.55 o 8 3 0 1008.00 1140.16 21.36 o 9 3 0 785.13 772.63 15.83 o 0 4 0 3328.30 4638.44 7.25 o 1 4 0 2844.69 4100.40 12.78 o 2 4 0 22767.43 24995.12 36.05 o 3 4 0 98.51 119.39 7.44 o 4 4 0 64.93 89.07 7.44 o 5 4 0 652.46 666.78 13.92 o 6 4 0 891.17 878.48 19.45 o 7 4 0 5.36 11.06 19.45 < 8 4 0 2133.90 2225.57 20.79 o 9 4 0 28.97 18.31 13.16 < 1 5 0 57823.57 71483.66 194.54 o 2 5 0 743.51 724.95 7.63 o 3 5 0 1217.84 1172.96 9.73 o 4 5 0 126.39 103.75 8.01 o 5 5 0 69.40 105.28 13.92 o 6 5 0 150.02 146.10 16.59 o 7 5 0 8.61 13.35 22.70 < 8 5 0 333.12 294.48 16.59 o 9 5 0 900.99 750.89 19.07 o 0 6 0 143.72 154.30 4.77 o 1 6 0 2737.66 3203.04 12.59 o 2 6 0 118.64 132.36 6.10 o 3 6 0 5973.42 5817.88 17.36 o 4 6 0 26.67 16.78 9.92 < 5 6 0 1859.78 1724.54 17.74 o 6 6 0 0.97 14.50 32.80 < 7 6 0 536.51 588.39 19.84 o 8 6 0 92.21 51.11 16.02 o 9 6 0 146.81 111.77 13.92 o 1 7 0 12123.79 13406.08 27.08 o 2 7 0 1252.88 1353.77 12.02 o 3 7 0 5005.90 4874.94 16.02 o 4 7 0 407.48 372.11 9.73 o 5 7 0 324.12 211.51 16.40 o 6 7 0 828.27 888.21 20.79 o 7 7 0 3700.51 4020.30 25.75 o 8 7 0 504.94 530.41 17.17 o 9 7 0 2119.94 2035.80 21.74 o 0 8 0 13555.46 15940.82 37.38 o 1 8 0 2299.88 2079.48 12.02 o 2 8 0 1688.63 1916.60 13.54 o 3 8 0 477.65 424.36 8.20 o 4 8 0 2115.02 1881.12 12.97 o 5 8 0 68.67 74.96 15.64 o 6 8 0 680.01 717.89 20.79 o 7 8 0 834.31 886.11 20.03 o 8 8 0 118.91 133.51 16.02 o 9 8 0 100.79 105.09 12.97 o 1 9 0 2731.80 2793.17 10.49 o 2 9 0 2210.74 2157.48 14.11 o 3 9 0 635.75 512.10 11.25 o 4 9 0 9.90 19.64 9.15 < 5 9 0 6446.57 6265.52 24.60 o 6 9 0 726.81 722.85 20.79 o 7 9 0 4.85 28.80 20.03 < 8 9 0 336.33 275.22 17.74 o 9 9 0 33.28 29.37 13.16 < 0 10 0 16191.20 17374.31 45.01 o 1 10 0 4088.53 4718.54 19.45 o 2 10 0 2028.04 1858.62 13.73 o 3 10 0 213.31 169.55 12.78 o 4 10 0 31.54 44.44 11.63 o 5 10 0 157.12 159.83 15.64 o 6 10 0 2797.39 2794.70 23.46 o 7 10 0 23.89 53.78 18.69 < 8 10 0 43.42 45.77 18.12 < 9 10 0 1.56 2.29 14.50 < 1 11 0 1992.81 2004.33 15.45 o 2 11 0 939.43 879.82 8.96 o 3 11 0 274.74 248.52 13.35 o 4 11 0 764.60 688.14 15.83 o 5 11 0 173.64 170.70 19.07 o 6 11 0 77.25 88.12 22.12 o 7 11 0 47.92 74.96 20.22 o 8 11 0 265.28 209.23 20.79 o 9 11 0 21.97 -2.67 25.94 < 0 12 0 422.01 280.75 11.25 o 1 12 0 19.78 29.56 7.44 o 2 12 0 95.82 120.73 6.68 o 3 12 0 647.26 559.59 11.25 o 4 12 0 3116.83 2689.61 20.98 o 5 12 0 1850.88 1918.32 21.74 o 6 12 0 3205.86 3520.79 29.56 o 7 12 0 849.58 962.40 23.65 o 8 12 0 782.10 804.86 25.56 o 9 12 0 812.39 738.30 28.99 o 1 13 0 3534.39 3527.27 25.94 o 2 13 0 2454.55 1874.45 11.63 o 3 13 0 3442.94 3258.35 19.45 o 4 13 0 294.58 288.76 14.69 o 5 13 0 0.24 23.84 23.46 < 6 13 0 242.57 312.41 29.56 o 7 13 0 203.40 264.15 24.03 o 8 13 0 16.81 8.96 30.13 < 0 14 0 8.05 4.01 9.73 < 1 14 0 11.61 26.13 8.58 o 2 14 0 1599.46 1435.59 13.35 o 3 14 0 50.70 43.68 9.73 o 4 14 0 1816.40 1854.80 21.55 o 5 14 0 854.67 950.38 24.22 o 6 14 0 2871.95 3070.30 36.24 o 7 14 0 216.22 228.30 25.18 o 8 14 0 992.48 923.49 23.65 o 1 15 0 6250.19 6217.84 37.38 o 2 15 0 389.49 384.88 10.87 o 3 15 0 761.09 756.04 14.69 o 4 15 0 2.76 5.34 16.78 < 5 15 0 4179.86 4578.93 34.14 o 6 15 0 319.37 341.02 28.04 o 7 15 0 2425.92 2604.74 31.09 o 8 15 0 175.33 131.98 19.45 o 0 16 0 1540.21 1509.97 21.74 o 1 16 0 2706.35 2787.83 28.04 o 2 16 0 1928.11 1788.62 18.12 o 3 16 0 78.17 65.80 11.06 o 4 16 0 1465.14 1551.93 24.99 o 5 16 0 1195.86 1328.78 27.66 o 6 16 0 75.10 107.19 30.13 o 7 16 0 2195.44 2452.16 33.38 o 8 16 0 29.86 42.15 18.50 < 1 17 0 7.75 12.97 11.06 < 2 17 0 0.72 -0.95 12.40 < 3 17 0 93.18 76.10 12.78 o 4 17 0 505.93 551.20 19.64 o 5 17 0 7969.46 8972.48 42.72 o 6 17 0 906.02 944.66 27.66 o 7 17 0 33.83 34.33 22.51 < 8 17 0 21.75 26.89 23.27 < 0 18 0 22.46 16.21 15.26 < 1 18 0 533.78 546.81 12.78 o 2 18 0 249.50 225.82 12.78 o 3 18 0 378.75 352.46 14.30 o 4 18 0 7.53 15.64 17.93 < 5 18 0 1061.15 1099.53 26.13 o 6 18 0 237.81 283.61 29.75 o 7 18 0 2.44 21.74 22.51 < 1 19 0 4903.75 5677.32 34.71 o 2 19 0 1596.51 1740.75 20.60 o 3 19 0 2007.14 2086.92 20.41 o 4 19 0 2459.72 2812.05 30.13 o 5 19 0 4940.75 5642.61 34.14 o 6 19 0 112.90 118.44 27.85 o 7 19 0 238.43 231.92 18.12 o 0 20 0 1356.52 1249.82 23.84 o 1 20 0 618.35 718.65 16.40 o 2 20 0 62.07 62.37 12.97 o 3 20 0 676.30 691.95 16.59 o 4 20 0 159.89 159.26 20.79 o 5 20 0 0.08 -13.35 26.13 < 6 20 0 10.38 6.68 22.51 < 7 20 0 3.72 10.49 19.07 < 1 21 0 1387.87 1538.96 18.12 o 2 21 0 14.86 14.69 21.17 < 3 21 0 3298.52 3587.73 23.27 o 4 21 0 2927.85 3175.00 26.51 o 5 21 0 320.01 372.87 27.66 o 6 21 0 648.69 577.13 31.85 o 7 21 0 113.59 115.01 21.93 o 0 22 0 10587.55 10865.81 58.17 o 1 22 0 67.24 42.72 15.45 < 2 22 0 829.21 930.36 19.64 o 3 22 0 2.42 -6.48 18.12 < 4 22 0 63.31 50.16 22.31 < 5 22 0 557.13 584.19 28.23 o 6 22 0 104.45 177.76 28.04 o 1 23 0 1124.98 1189.74 23.27 o 2 23 0 1486.72 1550.60 21.93 o 3 23 0 1021.88 953.63 17.36 o 4 23 0 52.23 36.81 15.64 < 5 23 0 1383.81 1334.31 41.01 o 6 23 0 722.04 601.93 27.66 o 0 24 0 3010.75 3319.00 38.15 o 1 24 0 16.74 13.16 14.88 < 2 24 0 2385.56 2761.51 25.94 o 3 24 0 168.58 137.32 13.54 o 4 24 0 2563.58 2793.74 37.19 o 5 24 0 333.19 240.89 28.23 o 6 24 0 570.33 611.27 25.18 o 1 25 0 273.22 171.84 15.45 o 2 25 0 59.48 34.52 14.30 < 3 25 0 39.22 29.75 12.21 < 4 25 0 229.88 211.90 23.27 o 5 25 0 13.29 20.41 25.37 < 0 26 0 95.90 18.31 33.00 < 1 26 0 204.26 209.23 14.88 o 2 26 0 7.83 5.15 12.97 < 3 26 0 21.42 11.06 17.93 < 4 26 0 13.19 36.05 19.84 < 5 26 0 1.92 -1.53 18.31 < 1 27 0 5499.72 6050.95 47.49 o 2 27 0 202.37 163.26 12.59 o 3 27 0 228.14 174.32 13.73 o 4 27 0 51.80 8.39 24.22 < 0 28 0 2.95 25.18 27.27 < 1 28 0 17.01 48.25 19.45 < 2 28 0 234.07 206.56 13.35 o 3 28 0 0.61 17.93 15.45 < 1 29 0 241.54 250.23 17.74 o 2 29 0 45.28 60.08 22.12 < 0 30 0 7.73 -1.91 20.98 < 1 30 0 1.46 15.64 19.45 < -9 1 1 470.31 417.12 19.64 o -8 1 1 265.21 339.68 16.02 o -7 1 1 7.53 0.19 20.22 < -6 1 1 116.93 93.26 14.30 o -5 1 1 1279.00 1356.63 12.97 o -4 1 1 1825.94 1540.87 9.92 o -3 1 1 249.64 262.06 6.48 o -2 1 1 9.76 0.38 6.48 < -1 1 1 5911.70 7145.71 9.92 o 1 1 1 483.23 525.83 5.53 o 2 1 1 558.81 632.25 10.30 o 3 1 1 906.11 970.79 10.30 o 4 1 1 1111.98 1027.25 9.35 o 5 1 1 4267.99 3744.89 19.07 o 6 1 1 59.81 38.15 16.21 < 7 1 1 1163.43 1307.80 17.74 o 8 1 1 5.76 11.44 16.78 < 9 1 1 618.88 584.19 22.31 o -9 2 1 40.70 51.88 14.11 o -8 2 1 1377.14 1658.74 18.88 o -7 2 1 714.23 868.56 19.26 o -6 2 1 33.73 41.58 15.64 < -5 2 1 2695.01 2553.62 14.88 o -4 2 1 511.67 437.14 6.87 o -3 2 1 6695.15 6657.08 16.21 o -2 2 1 299.16 315.27 10.68 o -1 2 1 2402.76 3319.76 10.68 o 0 2 1 164.91 137.70 2.48 o 1 2 1 11092.63 13781.43 18.88 o 2 2 1 116.81 109.29 8.77 o 3 2 1 1593.73 2100.84 12.78 o 4 2 1 7561.79 7011.63 18.31 o 5 2 1 1420.88 1280.72 15.07 o 6 2 1 21.56 39.67 19.64 < 7 2 1 8470.20 8986.98 29.75 o 8 2 1 531.33 495.89 18.31 o 9 2 1 43.70 25.56 16.02 < -9 3 1 627.21 676.31 16.21 o -8 3 1 1333.53 1581.88 23.08 o -7 3 1 1867.18 2196.96 21.93 o -6 3 1 1054.64 1099.91 18.12 o -5 3 1 5726.52 5327.91 18.12 o -4 3 1 58.36 25.56 8.20 o -3 3 1 3038.86 3025.48 11.82 o -2 3 1 7.03 -0.95 9.54 < -1 3 1 13443.07 15876.17 33.76 o 0 3 1 3565.99 4809.52 6.87 o 1 3 1 2138.61 2705.25 17.74 o 2 3 1 11588.16 12042.78 29.37 o 3 3 1 43.85 52.64 7.06 o 4 3 1 3884.21 3538.72 14.50 o 5 3 1 5015.47 4868.65 21.36 o 6 3 1 3200.22 3309.27 22.89 o 7 3 1 45.27 83.73 17.36 o 8 3 1 738.80 800.28 19.64 o 9 3 1 0.78 7.06 18.12 < -9 4 1 49.72 51.11 14.11 o -8 4 1 836.25 878.67 19.45 o -7 4 1 470.59 598.50 20.79 o -6 4 1 270.89 212.09 14.11 o -5 4 1 5171.52 5077.30 21.17 o -4 4 1 62.60 23.65 8.58 < -3 4 1 1967.80 2172.74 12.02 o -2 4 1 78918.94 88473.85 263.01 o -1 4 1 616.06 604.98 7.44 o 0 4 1 984.34 1179.83 3.43 o 1 4 1 210.13 180.62 6.87 o 2 4 1 27741.57 30920.96 47.87 o 3 4 1 287.83 275.03 8.01 o 4 4 1 4802.27 4120.81 14.11 o 5 4 1 128.09 110.62 13.16 o 6 4 1 1752.19 1891.42 23.84 o 7 4 1 8.11 38.91 18.69 < 8 4 1 2036.72 2212.03 22.31 o 9 4 1 3.27 24.03 17.74 < -9 5 1 90.72 67.71 13.54 o -8 5 1 3.55 11.63 16.59 < -7 5 1 259.31 266.63 20.22 o -6 5 1 2739.06 2968.64 19.26 o -5 5 1 105.04 92.31 12.40 o -4 5 1 12097.34 9754.46 19.45 o -3 5 1 53.52 29.75 6.48 o -2 5 1 2055.77 2332.38 10.87 o -1 5 1 81.73 146.86 6.10 o 0 5 1 40671.14 55307.10 104.13 o 1 5 1 1544.41 1817.23 9.54 o 2 5 1 7195.29 6852.38 18.12 o 3 5 1 432.64 403.00 8.01 o 4 5 1 2196.13 2019.97 12.21 o 5 5 1 1103.85 1081.60 20.03 o 6 5 1 3487.79 3759.20 28.04 o 7 5 1 488.60 520.30 19.45 o 8 5 1 3579.94 3605.66 22.89 o 9 5 1 9.69 24.22 17.74 < -9 6 1 253.26 206.17 14.11 o -8 6 1 446.84 472.05 17.74 o -7 6 1 649.98 758.90 21.74 o -6 6 1 107.94 94.41 15.45 o -5 6 1 70.02 67.14 12.21 o -4 6 1 3346.23 2932.59 12.59 o -3 6 1 62.18 81.82 6.68 o -2 6 1 194.88 323.66 8.39 o -1 6 1 173.01 204.08 5.91 o 0 6 1 4510.53 4941.69 11.25 o 1 6 1 63.54 63.32 6.68 o 2 6 1 611.75 613.18 10.49 o 3 6 1 4.17 4.01 6.10 < 4 6 1 621.23 522.21 11.25 o 5 6 1 3.91 37.57 17.74 < 6 6 1 1368.04 1651.30 24.79 o 7 6 1 13.07 28.80 22.89 < 8 6 1 9.68 20.98 16.02 < 9 6 1 152.21 123.97 17.93 o -9 7 1 28.17 38.91 12.21 o -8 7 1 120.07 137.13 16.59 o -7 7 1 27.79 129.88 22.12 o -6 7 1 557.65 590.10 19.45 o -5 7 1 0.83 2.67 21.55 < -4 7 1 4405.92 3690.53 15.45 o -3 7 1 20.72 4.96 5.91 < -2 7 1 84.89 57.79 8.20 o -1 7 1 2350.80 2889.68 9.35 o 0 7 1 12614.46 14297.53 19.45 o 1 7 1 68.27 47.87 6.68 o 2 7 1 17039.09 18722.36 35.28 o 3 7 1 3288.82 3255.49 16.02 o 4 7 1 3740.20 3479.78 20.98 o 5 7 1 210.56 223.53 15.64 o 6 7 1 2781.34 3051.22 27.66 o 7 7 1 17.79 13.92 15.83 < 8 7 1 126.57 103.56 15.26 o 9 7 1 350.98 346.55 18.12 o -9 8 1 75.03 62.94 11.82 o -8 8 1 317.66 341.78 16.97 o -7 8 1 602.84 629.78 17.55 o -6 8 1 504.40 536.13 19.84 o -5 8 1 2336.40 2295.38 18.12 o -4 8 1 6986.73 5980.38 20.22 o -3 8 1 499.80 384.12 8.01 o -2 8 1 259.53 316.22 8.77 o -1 8 1 2811.16 4064.17 12.02 o 0 8 1 31875.44 36716.91 52.64 o 1 8 1 5328.76 5740.64 11.25 o 2 8 1 3046.72 3517.93 16.97 o 3 8 1 45.97 40.24 6.10 o 4 8 1 1954.65 1693.83 12.97 o 5 8 1 286.33 297.72 15.07 o 6 8 1 5228.79 5769.63 30.33 o 7 8 1 362.55 339.30 19.07 o 8 8 1 584.61 624.82 18.12 o 9 8 1 180.92 200.07 20.03 o -9 9 1 146.23 144.57 12.40 o -8 9 1 348.79 327.28 16.59 o -7 9 1 17.01 52.07 17.36 < -6 9 1 252.11 229.63 19.26 o -5 9 1 4422.29 4229.14 21.55 o -4 9 1 170.73 175.85 9.73 o -3 9 1 543.05 453.93 8.77 o -2 9 1 92.56 98.22 9.54 o -1 9 1 7585.04 8064.82 14.88 o 0 9 1 1230.08 1454.85 7.63 o 1 9 1 1836.19 2135.93 9.35 o 2 9 1 6459.49 5901.80 21.36 o 3 9 1 24.53 34.33 9.15 o 4 9 1 429.58 383.93 10.68 o 5 9 1 8339.85 8600.95 27.66 o 6 9 1 5116.54 5509.48 30.13 o 7 9 1 678.40 663.53 19.64 o 8 9 1 635.98 634.54 18.12 o 9 9 1 0.53 38.15 17.55 < -9 10 1 1.47 11.25 15.64 < -8 10 1 1258.79 1294.64 18.69 o -7 10 1 399.29 353.60 15.83 o -6 10 1 253.07 242.79 16.40 o -5 10 1 1917.81 1814.94 16.97 o -4 10 1 8.71 12.78 14.11 < -3 10 1 5927.51 5104.95 26.51 o -2 10 1 24.81 10.68 8.58 < -1 10 1 3105.32 3564.66 15.64 o 0 10 1 2968.26 3061.14 11.44 o 1 10 1 14070.53 14458.89 32.23 o 2 10 1 149.57 130.07 7.25 o 3 10 1 905.89 737.92 15.26 o 4 10 1 152.51 138.47 12.78 o 5 10 1 8.64 55.50 15.83 o 6 10 1 51.73 55.88 20.60 < 7 10 1 3238.34 3630.46 25.18 o 8 10 1 117.81 108.52 20.22 o 9 10 1 279.80 160.59 25.75 o -9 11 1 648.00 488.07 17.55 o -8 11 1 851.19 737.34 22.51 o -7 11 1 298.22 246.04 18.12 o -6 11 1 814.85 831.56 22.89 o -5 11 1 3855.46 3940.19 24.03 o -4 11 1 328.46 270.26 15.83 o -3 11 1 9339.08 8832.68 34.90 o -2 11 1 651.90 682.42 10.30 o -1 11 1 3313.62 3117.98 17.93 o 0 11 1 17.37 13.92 8.58 < 1 11 1 14582.40 14141.33 36.43 o 2 11 1 33.45 16.59 5.15 o 3 11 1 235.50 245.65 9.15 o 4 11 1 220.27 204.08 13.92 o 5 11 1 4758.37 4914.61 30.90 o 6 11 1 162.71 216.09 23.46 o 7 11 1 1450.29 1805.98 28.23 o 8 11 1 19.47 40.43 21.55 < 9 11 1 31.45 53.02 22.51 < -8 12 1 75.10 68.85 22.89 o -7 12 1 64.74 65.42 21.93 < -6 12 1 81.65 95.55 24.41 o -5 12 1 2009.66 2083.10 27.46 o -4 12 1 24.30 36.62 15.64 < -3 12 1 2583.69 2309.49 19.26 o -2 12 1 0.40 -3.24 6.68 < -1 12 1 9789.04 10883.36 34.14 o 0 12 1 42.89 42.72 10.68 o 1 12 1 26839.03 27145.74 77.63 o 2 12 1 115.75 81.44 6.29 o 3 12 1 784.91 834.61 11.44 o 4 12 1 9.93 6.68 15.45 < 5 12 1 2506.17 2886.25 32.23 o 6 12 1 481.59 493.79 26.51 o 7 12 1 691.63 770.72 23.27 o 8 12 1 195.54 185.19 19.26 o -8 13 1 3.34 11.06 24.41 < -7 13 1 2038.43 2514.14 31.85 o -6 13 1 198.10 195.87 28.04 o -5 13 1 51.64 68.85 21.36 o -4 13 1 65.09 67.52 16.59 o -3 13 1 12735.53 12491.55 38.34 o -2 13 1 1346.58 1230.18 9.15 o -1 13 1 16.27 26.32 6.10 o 0 13 1 6476.01 7023.84 35.09 o 1 13 1 272.01 251.95 9.92 o 2 13 1 1328.36 1051.66 9.54 o 3 13 1 7912.19 7653.43 27.08 o 4 13 1 307.53 330.91 16.78 o 5 13 1 20.61 32.42 24.99 < 6 13 1 145.95 138.66 29.75 o 7 13 1 5478.44 6428.21 38.15 o 8 13 1 128.52 108.90 21.17 o -8 14 1 22.26 2.67 22.89 < -7 14 1 657.93 669.26 26.70 o -6 14 1 7.06 17.74 36.62 < -5 14 1 5319.34 5992.40 33.00 o -4 14 1 2.85 7.06 17.93 < -3 14 1 33.83 36.62 9.92 o -2 14 1 4.62 -0.95 8.01 < -1 14 1 110.90 90.21 8.58 o 0 14 1 1725.85 2037.14 17.55 o 1 14 1 1087.04 929.21 17.55 o 2 14 1 396.39 342.54 8.96 o 3 14 1 393.57 321.56 9.73 o 4 14 1 1584.53 1601.52 19.26 o 5 14 1 1660.98 1846.79 31.66 o 6 14 1 437.27 499.32 30.71 o 7 14 1 291.19 381.45 23.84 o 8 14 1 428.71 411.78 24.60 o 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