#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:56:16 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181204 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/83/2228362.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228362_Fobs loop_ _publ_author_name 'Wu, Hua' 'Shang, Meng-Xiang' 'ShangGuan, Shao-Ping' _publ_section_title ; Poly[[aquatris(\m~3~-hexamethylenetetramine-\k^3^N,N',N'')tris(p-toluenesulfonato-\kO)trisilver(I)] trihydrate] ; _journal_coeditor_code HB5739 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1665 _journal_page_last m1666 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.657 _cell_angle_gamma 90.000 _cell_length_a 17.3181 _cell_length_b 10.7028 _cell_length_c 26.9110 _exptl_crystal_F_000 2704.00 _reflns_d_resolution_high 0.7265 _cod_data_source_file hb5739Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' exp_5329 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 522.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1425.87 1113.40 162.59 o 6 0 0 106901.60 91371.39 6310.81 o 8 0 0 11656.10 10574.05 73.16 o 10 0 0 4174.34 4406.43 55.01 o 12 0 0 39956.66 40795.99 283.47 o 14 0 0 2436.50 2771.07 50.29 o 16 0 0 9055.31 9414.21 257.45 o 18 0 0 2419.86 2747.34 170.14 o 20 0 0 426.04 412.42 138.92 o 22 0 0 1.19 -64.67 130.77 o 3 1 0 233598.28 188559.95 7979.36 o 4 1 0 17001.72 17834.21 136.92 o 5 1 0 1012.52 1125.95 26.93 o 6 1 0 20048.70 19620.54 248.99 o 7 1 0 14854.30 14852.93 130.36 o 8 1 0 26231.32 25574.77 107.82 o 9 1 0 42170.89 40535.39 347.57 o 10 1 0 1308.24 1536.60 35.50 o 11 1 0 1153.23 1326.15 35.10 o 12 1 0 92.08 92.07 28.74 o 13 1 0 5819.94 5831.55 55.68 o 14 1 0 862.68 1095.36 35.36 o 15 1 0 6447.55 6069.22 56.16 o 16 1 0 1196.83 1264.15 37.67 o 17 1 0 792.91 846.08 53.77 o 18 1 0 8.69 -1.72 86.09 o 19 1 0 639.75 797.21 98.79 o 20 1 0 2175.27 2696.34 131.79 o 21 1 0 515.79 472.12 98.33 o 22 1 0 172.84 230.47 95.02 o 2 2 0 7360.73 8022.90 71.24 o 3 2 0 4706.43 4144.95 73.82 o 4 2 0 517.34 457.54 29.11 o 5 2 0 13489.81 13814.69 149.47 o 6 2 0 80072.84 80495.66 708.47 o 7 2 0 7.56 49.41 24.25 o 8 2 0 16904.12 19270.34 88.46 o 9 2 0 428.58 335.89 35.99 o 10 2 0 6002.79 5990.05 62.62 o 11 2 0 17012.88 17631.43 103.48 o 12 2 0 11383.28 11665.13 119.75 o 13 2 0 3692.42 3967.09 56.17 o 14 2 0 223.81 267.30 38.76 o 15 2 0 64.59 104.08 35.42 o 16 2 0 927.06 735.21 37.24 o 17 2 0 9133.54 9532.31 183.04 o 18 2 0 807.63 982.83 102.59 o 19 2 0 395.01 430.56 94.22 o 20 2 0 161.46 200.09 94.03 o 21 2 0 9.99 -17.87 93.44 o 22 2 0 366.00 356.25 98.38 o 2 3 0 92.22 181.57 35.59 o 3 3 0 319.43 494.87 46.05 o 4 3 0 5603.97 4930.99 76.43 o 5 3 0 153.03 124.18 42.41 o 6 3 0 91.68 216.25 41.36 o 7 3 0 275.94 367.69 34.08 o 8 3 0 7045.08 7021.59 62.67 o 9 3 0 15039.13 15652.37 104.92 o 10 3 0 1062.02 1054.42 38.86 o 11 3 0 314.68 305.81 42.86 o 12 3 0 1021.98 877.10 54.15 o 13 3 0 1695.84 1710.70 62.05 o 14 3 0 10512.46 10882.49 115.14 o 15 3 0 400.60 542.91 49.44 o 16 3 0 28.82 65.05 65.37 o 17 3 0 5.42 43.69 73.92 o 18 3 0 240.00 147.95 63.92 o 19 3 0 2.01 9.90 90.20 o 20 3 0 6605.46 6991.46 178.19 o 21 3 0 1047.15 1086.29 110.12 o 22 3 0 85.64 109.26 135.40 o 1 4 0 186.32 157.88 54.07 o 2 4 0 2352.82 2729.91 103.86 o 3 4 0 2619.08 3151.65 72.28 o 4 4 0 234.51 274.15 47.06 o 5 4 0 19596.08 19270.28 158.24 o 6 4 0 12040.46 12405.41 111.80 o 7 4 0 7818.06 8074.38 96.20 o 8 4 0 530.07 871.07 53.93 o 9 4 0 1344.57 1368.38 61.20 o 10 4 0 3306.24 3614.07 70.75 o 11 4 0 28778.14 28873.08 160.63 o 12 4 0 453.79 582.61 55.22 o 13 4 0 167.14 201.76 54.87 o 14 4 0 891.91 876.39 63.00 o 15 4 0 1115.39 1129.23 63.59 o 16 4 0 2134.95 2083.44 101.24 o 17 4 0 15129.64 15737.02 206.04 o 18 4 0 790.43 778.86 88.73 o 19 4 0 1.20 9.14 127.06 o 20 4 0 133.85 87.76 95.34 o 21 4 0 342.29 284.89 99.75 o 22 4 0 265.95 297.10 148.96 o 1 5 0 617.08 687.78 86.78 o 2 5 0 1353.21 1013.75 61.25 o 3 5 0 43411.82 44026.15 247.33 o 4 5 0 190.24 172.94 53.82 o 5 5 0 7964.66 7019.05 127.61 o 6 5 0 0.20 23.46 49.02 o 7 5 0 6204.67 5716.36 112.05 o 8 5 0 6605.80 7248.70 103.22 o 9 5 0 30987.57 31063.63 258.11 o 10 5 0 185.34 176.59 55.57 o 11 5 0 896.94 873.97 62.77 o 12 5 0 1808.31 1973.84 73.10 o 13 5 0 2591.65 2776.32 80.55 o 14 5 0 20433.05 19498.68 281.81 o 15 5 0 146.57 255.00 85.09 o 16 5 0 4.54 -8.02 79.90 o 17 5 0 71.90 113.65 82.58 o 18 5 0 128.77 110.56 78.60 o 19 5 0 164.79 134.27 131.20 o 20 5 0 4791.89 5159.08 238.53 o 21 5 0 67.70 46.27 136.65 o 22 5 0 550.62 359.30 151.45 o 0 6 0 17448.43 16732.46 241.71 o 1 6 0 4020.33 3631.40 135.53 o 2 6 0 78.30 41.03 53.02 o 3 6 0 5600.17 5727.00 194.73 o 4 6 0 3884.95 4152.80 103.43 o 5 6 0 5407.14 5273.62 111.56 o 6 6 0 73369.98 72083.96 363.30 o 7 6 0 313.24 357.43 76.78 o 8 6 0 2019.13 2103.91 93.92 o 9 6 0 557.83 710.10 114.05 o 10 6 0 7527.43 7050.86 195.03 o 11 6 0 2484.38 2730.51 151.14 o 12 6 0 8720.43 9374.68 184.29 o 13 6 0 83.25 14.51 60.42 o 14 6 0 3964.84 3744.57 96.57 o 15 6 0 1098.21 1191.68 100.53 o 16 6 0 1086.09 1065.79 100.64 o 17 6 0 209.17 294.66 93.09 o 18 6 0 3367.46 3215.10 130.80 o 19 6 0 309.24 410.80 153.46 o 20 6 0 189.56 159.96 141.11 o 21 6 0 527.50 563.83 158.38 o 1 7 0 832.19 1050.06 83.12 o 2 7 0 4105.48 4497.06 113.25 o 3 7 0 69665.11 67990.39 1400.44 o 4 7 0 5308.31 5035.71 115.12 o 5 7 0 756.44 701.19 71.67 o 6 7 0 260.92 231.27 98.15 o 7 7 0 325.73 252.04 116.26 o 8 7 0 4672.35 4492.72 180.03 o 9 7 0 7390.91 6591.01 204.39 o 10 7 0 1324.30 1166.51 137.80 o 11 7 0 1432.08 1678.46 145.10 o 12 7 0 1.90 -80.61 113.90 o 13 7 0 5188.81 4959.31 128.72 o 14 7 0 698.88 1151.41 143.23 o 15 7 0 6922.25 7039.98 226.46 o 16 7 0 510.16 355.20 121.52 o 17 7 0 459.88 473.04 123.24 o 0 8 0 48045.82 48497.17 461.45 o 1 8 0 3052.26 3244.55 110.65 o 2 8 0 319.91 179.24 80.46 o 3 8 0 3898.57 4273.78 122.48 o 4 8 0 1410.52 1125.24 131.44 o 5 8 0 73.99 166.15 110.83 o 6 8 0 12173.56 13368.69 273.06 o 7 8 0 9740.89 9723.64 246.26 o 8 8 0 778.88 704.13 135.85 o 9 8 0 539.11 553.45 126.59 o 10 8 0 376.56 331.97 136.65 o 11 8 0 661.79 897.49 150.96 o 12 8 0 11348.33 11149.88 274.56 o 13 8 0 2911.97 2952.49 178.06 o 14 8 0 30.42 57.28 128.12 o 15 8 0 192.38 188.45 76.83 o 16 8 0 805.69 743.49 146.14 o 17 8 0 1179.33 1465.05 155.62 o 1 9 0 72.56 7.70 82.18 o 2 9 0 1607.95 1556.14 109.67 o 3 9 0 12336.95 13412.97 202.23 o 4 9 0 2876.89 2731.35 117.02 o 5 9 0 312.95 332.79 90.99 o 6 9 0 2465.16 2522.95 112.84 o 7 9 0 262.86 276.39 96.14 o 8 9 0 3527.30 3837.04 135.48 o 9 9 0 17707.98 18498.73 301.38 o 10 9 0 4352.41 4167.02 135.91 o 11 9 0 205.59 130.82 86.08 o 12 9 0 350.53 320.57 87.72 o 13 9 0 24.67 98.59 85.92 o 14 9 0 3376.57 3477.81 122.41 o 15 9 0 4633.24 4197.76 212.13 o 16 9 0 190.65 136.69 135.78 o 17 9 0 291.22 372.25 140.59 o 0 10 0 102.23 954.89 184.70 o 1 10 0 2.29 1.62 106.00 o 2 10 0 39.46 -25.07 92.08 o 3 10 0 64.44 65.15 93.65 o 4 10 0 197.54 88.99 99.20 o 5 10 0 2916.10 2765.00 127.74 o 6 10 0 1212.61 1348.86 119.43 o 7 10 0 48.88 22.93 95.96 o 8 10 0 41.79 74.64 91.01 o 9 10 0 25.56 -5.17 90.70 o 10 10 0 208.77 233.83 98.51 o 11 10 0 7102.24 6998.12 168.71 o 12 10 0 465.17 575.00 102.27 o 13 10 0 87.12 142.02 91.30 o 14 10 0 45.73 90.31 86.11 o 15 10 0 11.66 101.93 145.34 o 16 10 0 582.80 616.86 156.58 o 17 10 0 3997.75 3684.36 218.57 o 1 11 0 147.45 122.76 103.67 o 2 11 0 1224.74 1449.39 124.33 o 3 11 0 899.50 1513.77 133.70 o 4 11 0 1.84 30.44 101.03 o 5 11 0 440.60 413.58 109.02 o 6 11 0 15.49 -1.41 95.16 o 7 11 0 815.07 769.35 105.38 o 8 11 0 5173.45 5048.04 159.85 o 9 11 0 1034.16 1146.90 123.82 o 10 11 0 2.73 68.02 98.71 o 11 11 0 133.78 118.77 94.68 o 12 11 0 2.06 26.91 94.78 o 13 11 0 997.44 952.55 110.78 o 14 11 0 3870.84 3690.57 227.94 o 15 11 0 0.19 34.37 165.44 o 0 12 0 6527.75 7215.71 279.29 o 1 12 0 858.68 997.93 127.10 o 2 12 0 3.99 -58.13 101.40 o 3 12 0 0.74 17.65 95.93 o 4 12 0 860.55 724.75 120.08 o 5 12 0 848.53 807.48 112.29 o 6 12 0 2805.98 2842.24 147.92 o 7 12 0 401.11 364.55 111.11 o 8 12 0 686.72 586.07 112.51 o 9 12 0 105.50 117.94 100.88 o 10 12 0 1768.79 1708.86 128.34 o 11 12 0 470.39 440.93 106.63 o 12 12 0 876.26 868.42 155.53 o 1 13 0 245.73 139.07 110.67 o 2 13 0 2551.60 2204.05 257.70 o 3 13 0 8959.70 8444.78 212.00 o 4 13 0 2884.89 2568.10 148.07 o 5 13 0 254.24 168.23 115.44 o 6 13 0 141.42 141.83 150.82 o 7 13 0 2432.65 2213.66 191.14 o 8 13 0 368.15 342.07 159.54 o 9 13 0 4041.09 3597.94 218.71 o 10 13 0 1188.40 1027.47 169.54 o 11 13 0 245.05 148.33 140.79 o -23 0 1 1937.86 1730.50 180.89 o -21 0 1 0.22 35.14 131.27 o -19 0 1 336.31 380.93 128.11 o -17 0 1 22349.78 22836.09 373.09 o -15 0 1 752.63 628.33 121.06 o -13 0 1 4651.80 5256.19 54.41 o -11 0 1 2080.40 2151.11 49.76 o -9 0 1 2495.67 2963.23 63.89 o -7 0 1 5209.11 4256.80 134.87 o -5 0 1 2222.89 2374.71 28.09 o 3 0 1 684.76 1227.32 38.66 o 5 0 1 37612.82 36935.25 334.75 o 7 0 1 312.65 325.47 29.86 o 9 0 1 3570.68 3810.05 56.09 o 11 0 1 34664.32 35613.02 154.25 o 13 0 1 9220.50 9600.54 87.74 o 15 0 1 1176.96 1198.50 44.46 o 17 0 1 39358.04 39874.11 458.11 o 19 0 1 642.20 616.35 129.91 o 21 0 1 335.24 247.47 132.84 o -23 1 1 55.81 -45.31 141.17 o -22 1 1 347.73 322.58 99.53 o -21 1 1 59.55 122.38 96.86 o -20 1 1 6946.90 6879.31 176.42 o -19 1 1 744.38 889.78 104.79 o -18 1 1 75.00 64.80 87.71 o -17 1 1 4.42 50.63 35.04 o -16 1 1 590.28 556.60 47.83 o -15 1 1 138.35 186.42 23.55 o -14 1 1 6174.08 6356.12 59.09 o -13 1 1 1159.43 1215.01 30.09 o -12 1 1 752.38 685.34 28.44 o -11 1 1 7377.22 7898.70 108.92 o -10 1 1 176.08 186.37 21.44 o -9 1 1 14628.74 14834.53 145.00 o -8 1 1 15973.98 17269.87 90.29 o -7 1 1 5216.16 4967.41 40.91 o -6 1 1 5196.81 5515.97 68.27 o -5 1 1 137.87 177.04 26.52 o -4 1 1 2.48 40.05 19.30 o -3 1 1 26379.60 24940.35 173.25 o 3 1 1 20838.27 21551.17 97.14 o 4 1 1 3343.31 3691.03 58.92 o 5 1 1 1167.66 1226.09 25.87 o 6 1 1 1798.21 1841.78 47.93 o 7 1 1 824.97 671.47 28.92 o 8 1 1 37602.09 35098.51 121.79 o 9 1 1 5573.64 6777.35 72.65 o 10 1 1 3532.91 3796.47 49.80 o 11 1 1 749.67 705.83 35.23 o 12 1 1 34.56 37.22 29.78 o 13 1 1 2161.25 2359.99 50.67 o 14 1 1 30098.05 30356.38 173.17 o 15 1 1 479.28 467.54 46.35 o 16 1 1 0.01 10.49 28.06 o 17 1 1 573.58 414.60 56.55 o 18 1 1 55.81 56.93 85.03 o 19 1 1 544.98 640.23 92.22 o 20 1 1 9221.50 9832.00 192.45 o 21 1 1 11.15 93.44 89.80 o 22 1 1 420.24 360.79 135.01 o -23 2 1 3216.65 3336.11 210.18 o -22 2 1 1166.13 1113.80 115.66 o -21 2 1 315.21 228.98 98.08 o -20 2 1 600.10 613.62 102.99 o -19 2 1 33.40 -17.30 91.62 o -18 2 1 3204.12 3492.52 136.14 o -17 2 1 1203.57 1265.22 85.15 o -16 2 1 7836.46 7798.44 134.28 o -15 2 1 67.21 117.18 26.57 o -14 2 1 1751.27 1850.18 44.26 o -13 2 1 1361.25 1327.09 42.38 o -12 2 1 37242.14 37178.77 272.59 o -11 2 1 5075.71 5596.04 69.61 o -10 2 1 4903.22 4395.17 63.33 o -9 2 1 14104.02 14524.10 133.93 o -8 2 1 27590.51 28403.64 101.55 o -7 2 1 3512.91 2844.74 42.73 o -6 2 1 132909.59 124119.70 1376.45 o -5 2 1 617.87 547.82 41.22 o -4 2 1 125.36 161.85 31.87 o -3 2 1 55146.93 52718.15 1169.93 o -2 2 1 1758.85 1659.45 59.91 o -1 2 1 1326.01 1336.19 48.83 o 0 2 1 273185.13 234973.52 1857.73 o 1 2 1 2586.54 2870.91 65.18 o 2 2 1 1242.70 1396.21 40.36 o 3 2 1 5187.43 5362.97 227.61 o 4 2 1 7237.28 7524.78 55.23 o 5 2 1 68712.50 64202.51 379.01 o 6 2 1 68783.92 65906.48 350.52 o 7 2 1 6689.20 6881.96 55.77 o 8 2 1 10491.28 10690.76 70.95 o 9 2 1 102.58 109.36 28.54 o 10 2 1 3407.11 3473.96 53.85 o 11 2 1 27015.64 26707.76 128.75 o 12 2 1 9215.68 9606.86 83.60 o 13 2 1 1672.63 1856.32 48.85 o 14 2 1 2919.10 2955.64 55.65 o 15 2 1 703.78 599.84 39.03 o 16 2 1 507.34 464.38 40.34 o 17 2 1 5821.81 5782.44 145.46 o 18 2 1 400.38 345.51 59.66 o 19 2 1 95.31 110.13 86.06 o 20 2 1 88.97 103.64 88.96 o 21 2 1 173.86 213.67 91.29 o 22 2 1 127.74 147.85 132.62 o -23 3 1 382.74 344.40 151.88 o -22 3 1 107.83 74.47 100.37 o -21 3 1 1817.72 1744.04 124.74 o -20 3 1 2.86 196.07 105.77 o -19 3 1 3960.65 4007.13 148.36 o -18 3 1 43.93 -4.86 135.21 o -17 3 1 3347.82 3158.14 106.36 o -16 3 1 66.13 51.67 27.97 o -15 3 1 9956.60 9623.05 186.11 o -14 3 1 971.27 941.99 50.12 o -13 3 1 8151.13 7997.09 167.79 o -12 3 1 422.57 378.90 48.41 o -11 3 1 4804.41 4949.41 70.18 o -10 3 1 1045.32 1060.98 44.36 o -9 3 1 82765.05 78108.59 260.30 o -8 3 1 2238.29 2386.88 59.66 o -7 3 1 18386.36 16921.43 203.39 o -6 3 1 3285.86 3546.54 61.54 o -5 3 1 2892.60 2480.40 62.50 o -4 3 1 781.59 894.22 52.71 o -3 3 1 163935.19 149285.92 1408.34 o -2 3 1 2694.76 3527.87 85.34 o 0 3 1 16080.31 16065.86 156.72 o 1 3 1 2831.07 3295.18 89.62 o 2 3 1 681.68 1129.59 70.44 o 3 3 1 71402.88 68876.58 456.55 o 4 3 1 263.12 370.89 34.28 o 5 3 1 7685.28 6876.97 63.32 o 6 3 1 4267.49 4766.54 85.70 o 7 3 1 1698.60 1933.60 44.42 o 8 3 1 139.66 271.74 31.48 o 9 3 1 27687.85 24654.80 201.40 o 10 3 1 73.76 111.10 33.23 o 11 3 1 3569.05 3858.93 65.74 o 12 3 1 152.29 144.47 40.19 o 13 3 1 1719.55 1573.72 52.17 o 14 3 1 202.91 428.67 57.73 o 15 3 1 6576.23 6480.11 94.51 o 16 3 1 41.06 40.40 70.85 o 17 3 1 807.33 954.91 87.84 o 18 3 1 49.14 -29.85 63.56 o 19 3 1 0.77 -21.14 88.98 o 20 3 1 259.89 482.08 101.74 o 21 3 1 125.71 89.27 89.94 o 22 3 1 5.86 42.04 133.27 o -22 4 1 1657.93 1697.58 178.13 o -21 4 1 1.76 -32.37 98.31 o -20 4 1 184.39 215.21 100.19 o -19 4 1 4.08 -22.77 135.48 o -18 4 1 4616.77 4931.16 215.50 o -17 4 1 1050.62 1281.14 94.57 o -16 4 1 3762.84 3511.65 114.36 o -15 4 1 234.14 185.66 48.37 o -14 4 1 2464.15 2578.21 72.94 o -13 4 1 676.95 630.95 56.20 o -12 4 1 26033.43 26734.66 176.44 o -11 4 1 1831.08 2153.69 59.95 o -10 4 1 6731.31 6900.69 187.03 o -9 4 1 3422.17 3771.67 79.88 o -8 4 1 49.18 58.75 41.10 o -7 4 1 2495.05 2799.63 89.84 o -6 4 1 140643.97 132342.11 828.75 o -5 4 1 1047.74 1419.95 90.68 o -4 4 1 2818.10 2674.73 69.16 o -3 4 1 941.29 1286.16 55.17 o -2 4 1 987.02 1244.83 69.86 o 0 4 1 60722.63 61400.99 346.54 o 1 4 1 21151.22 20874.32 213.52 o 2 4 1 658.44 699.39 72.85 o 3 4 1 1022.81 1222.68 56.30 o 4 4 1 340.42 389.05 44.20 o 5 4 1 109.04 59.56 50.90 o 6 4 1 42419.60 42515.78 260.12 o 7 4 1 2749.73 2684.81 65.00 o 8 4 1 422.04 509.19 79.69 o 9 4 1 2003.11 2630.07 58.56 o 10 4 1 5947.77 5603.82 78.46 o 11 4 1 16823.54 18177.74 169.41 o 12 4 1 17787.70 17174.85 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