#------------------------------------------------------------------------------ #$Date: 2011-02-15 17:23:33 +0200 (Tue, 15 Feb 2011) $ #$Revision: 11387 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2228371.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228371_Fobs loop_ _publ_author_name 'Shah, Rina D.' 'Jotani, Mukesh M.' 'Tiekink, Edward R. T.' _publ_section_title ; 12-(4-Chlorophenyl)-7-methyl-10-phenyl-3,4,5,6,8,10-hexaazatricyclo[7.3.0.0^2,6^]dodeca-1(9),2,4,7,11-pentaene ; _journal_coeditor_code HB5751 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3305 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.9459 _cell_length_b 9.7010 _cell_length_c 24.0382 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file hb5751Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' r7 in space group P212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 259.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 67412.22 65548.52 926.48 o 4 0 0 2265.31 2391.64 84.27 o 6 0 0 3904.69 3555.71 128.43 o 8 0 0 986.09 918.17 69.77 o 1 1 0 1393.15 1314.51 13.83 o 2 1 0 605.33 558.88 7.99 o 3 1 0 971.16 957.98 21.00 o 4 1 0 1865.80 1940.52 51.64 o 5 1 0 15.85 9.83 8.18 o 6 1 0 1539.61 1531.13 53.40 o 7 1 0 2.49 -0.92 9.37 o 8 1 0 98.78 89.35 20.09 o 0 2 0 25138.62 24119.28 342.56 o 1 2 0 7328.94 7083.79 90.78 o 2 2 0 5102.87 4933.79 54.39 o 3 2 0 1354.36 1339.76 19.33 o 4 2 0 41.95 44.24 7.98 o 5 2 0 567.72 558.75 23.15 o 6 2 0 390.18 412.29 29.04 o 7 2 0 32.52 24.09 11.67 o 8 2 0 90.27 53.67 24.01 o 1 3 0 5468.12 5120.45 68.94 o 2 3 0 696.24 658.59 13.36 o 3 3 0 1722.61 1643.21 25.86 o 4 3 0 68.09 89.05 8.74 o 5 3 0 471.85 483.29 26.99 o 6 3 0 195.84 187.56 27.47 o 7 3 0 345.26 412.10 46.56 o 0 4 0 2094.26 2201.29 52.05 o 1 4 0 2772.68 2936.40 53.18 o 2 4 0 1.19 -0.28 2.48 o 3 4 0 2.10 7.44 3.39 o 4 4 0 442.48 469.14 16.10 o 5 4 0 125.38 133.23 17.45 o 6 4 0 4.96 0.91 7.71 o 7 4 0 11.80 -5.72 11.44 o 1 5 0 168.11 152.08 15.45 o 2 5 0 1568.30 1525.29 142.51 o 3 5 0 0.80 -0.94 3.60 o 4 5 0 59.92 71.80 7.29 o 5 5 0 312.84 284.30 23.67 o 6 5 0 74.49 62.18 14.44 o 7 5 0 161.94 174.33 24.64 o 0 6 0 31.43 28.67 12.90 o 1 6 0 4478.95 4712.66 84.71 o 2 6 0 5.80 0.55 5.11 o 3 6 0 1.47 3.94 4.38 o 4 6 0 41.51 41.11 15.66 o 5 6 0 373.59 363.00 15.71 o 6 6 0 37.54 31.75 19.72 o 7 6 0 83.03 42.38 21.78 o 1 7 0 433.37 423.10 29.70 o 2 7 0 2.49 6.42 7.00 o 3 7 0 635.54 627.27 22.52 o 4 7 0 2.67 0.28 6.02 o 5 7 0 16.76 16.07 7.83 o 6 7 0 3.26 15.06 11.33 o 0 8 0 179.19 154.04 27.60 o 1 8 0 9.79 8.50 10.16 o 2 8 0 247.88 245.24 22.97 o 3 8 0 16.96 20.24 10.98 o 4 8 0 21.82 33.81 19.52 o 5 8 0 3.69 5.62 9.54 o 1 9 0 35.31 23.44 12.55 o 2 9 0 962.59 979.04 54.54 o 3 9 0 89.74 102.28 18.49 o 4 9 0 761.83 734.98 38.18 o 5 9 0 36.37 44.06 14.45 o 0 10 0 54.05 46.82 24.54 o 1 10 0 51.71 68.83 18.10 o 2 10 0 3.24 0.00 15.83 o 3 10 0 14.25 22.08 14.35 o 4 10 0 39.26 36.04 15.36 o 1 11 0 3.94 2.89 14.72 o 2 11 0 13.74 2.59 21.28 o 1 0 1 122.25 100.72 4.81 o 2 0 1 48678.07 48537.47 713.72 o 3 0 1 275.52 250.60 8.78 o 4 0 1 19272.59 19435.39 341.06 o 5 0 1 1445.71 1352.32 84.37 o 6 0 1 2630.09 2770.81 77.11 o 7 0 1 87.89 46.12 14.72 o 8 0 1 7.38 -0.20 11.89 o 0 1 1 4677.49 2250.08 34.99 o 1 1 1 1609.62 1657.66 12.26 o 2 1 1 12518.26 12424.57 83.65 o 3 1 1 2017.14 1960.34 20.33 o 4 1 1 1376.49 1293.64 48.28 o 5 1 1 18.31 26.10 6.88 o 6 1 1 459.16 491.28 23.77 o 7 1 1 146.24 150.12 15.13 o 8 1 1 544.00 541.52 28.87 o 0 2 1 263.21 253.25 6.46 o 1 2 1 1162.23 1049.34 11.77 o 2 2 1 2091.40 2025.84 17.16 o 3 2 1 198.18 198.33 4.40 o 4 2 1 2704.38 2640.86 37.87 o 5 2 1 67.98 59.17 6.91 o 6 2 1 658.88 655.41 23.86 o 7 2 1 50.30 27.91 10.38 o 8 2 1 57.22 72.52 18.32 o 0 3 1 12.04 15.93 3.77 o 1 3 1 14.26 10.71 2.43 o 2 3 1 266.91 251.49 5.90 o 3 3 1 232.13 233.23 8.11 o 4 3 1 277.64 262.69 9.41 o 5 3 1 77.04 68.84 9.25 o 6 3 1 32.97 22.58 7.63 o 7 3 1 136.90 120.44 20.55 o 0 4 1 57.11 50.94 8.40 o 1 4 1 3530.29 3584.77 44.11 o 2 4 1 107.46 110.27 4.26 o 3 4 1 422.91 409.20 9.70 o 4 4 1 90.18 92.54 5.05 o 5 4 1 1022.58 1000.45 28.65 o 6 4 1 93.42 92.54 11.24 o 7 4 1 32.43 28.57 9.91 o 0 5 1 148.72 192.38 14.84 o 1 5 1 1110.26 1240.98 21.68 o 2 5 1 186.27 194.72 14.81 o 3 5 1 646.60 618.28 11.20 o 4 5 1 188.90 183.03 7.28 o 5 5 1 12.73 3.32 5.66 o 6 5 1 9.34 14.65 6.79 o 7 5 1 169.76 196.56 17.80 o 0 6 1 625.82 612.76 27.63 o 1 6 1 512.35 551.43 16.23 o 2 6 1 107.32 95.82 7.45 o 3 6 1 692.55 720.10 13.26 o 4 6 1 380.38 371.63 11.57 o 5 6 1 195.39 215.87 8.91 o 6 6 1 106.30 110.29 15.23 o 7 6 1 10.77 -1.11 7.63 o 0 7 1 0.23 -3.36 7.01 o 1 7 1 350.06 372.53 17.20 o 2 7 1 112.99 88.42 9.11 o 3 7 1 61.39 52.90 5.61 o 4 7 1 12.08 14.17 4.63 o 5 7 1 14.96 12.51 4.84 o 6 7 1 145.75 143.98 15.44 o 0 8 1 116.27 87.39 22.41 o 1 8 1 145.69 166.75 13.74 o 2 8 1 373.72 382.99 22.28 o 3 8 1 76.29 89.62 14.25 o 4 8 1 538.63 553.54 20.09 o 5 8 1 129.06 115.07 13.10 o 0 9 1 699.55 669.45 37.71 o 1 9 1 140.40 131.65 16.89 o 2 9 1 372.50 344.00 20.47 o 3 9 1 8.59 13.88 7.18 o 4 9 1 16.33 8.50 7.08 o 5 9 1 88.65 104.60 13.37 o 0 10 1 7.70 15.29 14.51 o 1 10 1 19.81 15.34 9.77 o 2 10 1 20.40 21.44 14.14 o 3 10 1 12.74 12.35 7.81 o 4 10 1 90.46 76.58 11.44 o 0 11 1 12.32 9.49 15.03 o 1 11 1 46.87 51.77 13.30 o 2 11 1 163.56 177.08 46.76 o 1 0 2 52.15 58.10 2.25 o 2 0 2 11011.54 11569.95 111.59 o 3 0 2 589.11 592.15 17.23 o 4 0 2 1705.89 1804.64 47.07 o 5 0 2 117.79 115.20 15.24 o 6 0 2 551.62 538.12 31.45 o 7 0 2 551.06 515.22 69.00 o 8 0 2 1221.28 1272.41 119.19 o 0 1 2 189.35 154.60 3.90 o 1 1 2 2015.32 1963.38 15.42 o 2 1 2 7584.01 7592.94 52.49 o 3 1 2 1426.45 1482.13 15.85 o 4 1 2 1293.26 1372.87 30.65 o 5 1 2 203.42 190.43 13.06 o 6 1 2 503.49 523.84 22.08 o 7 1 2 74.58 76.88 16.02 o 8 1 2 57.22 53.44 12.14 o 0 2 2 2360.87 2357.80 30.55 o 1 2 2 5268.06 5264.50 41.60 o 2 2 2 1078.32 1091.27 10.63 o 3 2 2 403.98 441.02 6.91 o 4 2 2 76.32 72.87 6.07 o 5 2 2 148.60 124.72 11.36 o 6 2 2 90.57 94.47 16.07 o 7 2 2 58.46 48.86 17.02 o 8 2 2 84.52 102.58 17.27 o 0 3 2 813.94 801.98 14.93 o 1 3 2 2990.19 2972.34 28.84 o 2 3 2 1249.60 1243.13 15.32 o 3 3 2 983.19 989.83 11.31 o 4 3 2 109.41 115.33 6.79 o 5 3 2 101.33 88.76 14.76 o 6 3 2 19.00 15.92 8.93 o 7 3 2 70.61 59.35 27.10 o 0 4 2 2600.38 2519.23 38.04 o 1 4 2 28.26 23.51 3.53 o 2 4 2 557.39 540.33 9.25 o 3 4 2 596.57 594.13 12.10 o 4 4 2 217.36 254.56 7.52 o 5 4 2 397.56 357.22 17.95 o 6 4 2 16.47 10.13 6.84 o 7 4 2 10.40 5.71 8.06 o 0 5 2 296.83 314.09 18.30 o 1 5 2 763.41 799.30 16.64 o 2 5 2 1387.98 1319.12 26.96 o 3 5 2 1414.25 1464.05 19.97 o 4 5 2 25.67 26.41 3.79 o 5 5 2 221.13 231.71 15.35 o 6 5 2 100.42 82.92 11.37 o 7 5 2 5.01 5.36 8.40 o 0 6 2 665.73 673.84 29.09 o 1 6 2 25.40 30.32 5.34 o 2 6 2 108.07 102.71 7.49 o 3 6 2 139.40 157.63 7.63 o 4 6 2 165.43 169.39 8.84 o 5 6 2 42.36 32.31 5.79 o 6 6 2 1.00 3.11 6.54 o 7 6 2 91.05 82.57 13.26 o 0 7 2 337.13 383.73 71.43 o 1 7 2 212.17 214.44 13.75 o 2 7 2 124.13 143.13 9.51 o 3 7 2 13.91 15.01 4.23 o 4 7 2 4.07 4.69 4.21 o 5 7 2 47.26 47.51 6.75 o 6 7 2 33.79 38.77 9.64 o 0 8 2 1697.20 1795.67 58.74 o 1 8 2 142.45 157.23 13.67 o 2 8 2 550.83 511.62 21.66 o 3 8 2 102.60 118.29 10.89 o 4 8 2 7.55 10.45 5.80 o 5 8 2 67.75 65.00 10.60 o 0 9 2 0.64 4.69 11.05 o 1 9 2 156.79 155.03 15.05 o 2 9 2 13.98 2.74 8.04 o 3 9 2 141.45 146.85 12.76 o 4 9 2 91.42 81.83 10.28 o 5 9 2 37.73 49.69 10.54 o 0 10 2 57.80 34.49 16.58 o 1 10 2 28.91 37.74 11.76 o 2 10 2 58.00 36.85 15.01 o 3 10 2 1.39 -7.75 6.33 o 4 10 2 71.30 54.21 9.53 o 0 11 2 2.44 19.80 22.21 o 1 11 2 69.99 53.07 13.62 o 2 11 2 13.06 19.62 15.63 o 1 0 3 1850.90 1769.35 20.76 o 2 0 3 338.14 382.55 9.27 o 3 0 3 47.25 48.03 4.83 o 4 0 3 1566.65 1750.02 38.39 o 5 0 3 131.75 157.02 14.06 o 6 0 3 248.58 294.32 58.93 o 7 0 3 64.57 54.96 22.21 o 8 0 3 3.05 27.60 15.07 o 0 1 3 7195.92 7160.28 90.89 o 1 1 3 9804.40 9915.92 83.29 o 2 1 3 946.40 923.86 8.68 o 3 1 3 155.51 147.72 4.19 o 4 1 3 112.71 129.58 8.75 o 5 1 3 454.83 470.39 14.46 o 6 1 3 47.73 33.63 8.37 o 7 1 3 109.43 146.77 15.03 o 8 1 3 37.51 16.91 12.72 o 0 2 3 142.48 142.11 5.28 o 1 2 3 1123.66 1104.21 12.40 o 2 2 3 1156.45 1170.78 11.37 o 3 2 3 69.46 82.41 3.05 o 4 2 3 552.92 540.93 12.53 o 5 2 3 137.67 126.04 9.30 o 6 2 3 136.44 128.60 14.77 o 7 2 3 7.88 4.63 8.13 o 8 2 3 3.06 2.37 11.26 o 0 3 3 80.92 84.56 5.13 o 1 3 3 1162.27 1134.07 14.92 o 2 3 3 50.67 46.45 2.65 o 3 3 3 649.36 654.23 8.83 o 4 3 3 10.90 15.15 3.02 o 5 3 3 3.72 -1.80 4.30 o 6 3 3 54.94 53.67 9.21 o 7 3 3 16.87 -4.39 8.29 o 0 4 3 319.84 389.77 14.51 o 1 4 3 141.75 163.06 5.95 o 2 4 3 624.55 663.73 12.98 o 3 4 3 1062.42 1091.51 13.61 o 4 4 3 11.42 7.17 2.50 o 5 4 3 274.26 277.41 16.27 o 6 4 3 48.85 30.12 7.81 o 7 4 3 13.69 -4.26 11.77 o 0 5 3 610.87 607.27 22.07 o 1 5 3 906.21 1040.71 21.00 o 2 5 3 172.97 160.58 6.92 o 3 5 3 315.26 309.95 8.69 o 4 5 3 31.84 25.01 3.83 o 5 5 3 30.02 27.29 7.37 o 6 5 3 86.07 88.26 12.32 o 7 5 3 120.76 126.57 15.40 o 0 6 3 110.04 89.52 12.56 o 1 6 3 36.86 31.17 5.95 o 2 6 3 128.90 140.92 7.90 o 3 6 3 344.07 326.15 11.25 o 4 6 3 331.75 308.32 12.57 o 5 6 3 156.94 158.91 8.37 o 6 6 3 2.24 4.71 6.23 o 7 6 3 6.26 5.71 7.87 o 0 7 3 66.11 49.65 11.75 o 1 7 3 113.88 120.58 11.45 o 2 7 3 330.74 307.09 12.85 o 3 7 3 180.84 170.65 14.46 o 4 7 3 52.56 50.79 6.25 o 5 7 3 54.40 63.47 9.66 o 6 7 3 24.71 19.33 7.77 o 0 8 3 19.14 5.48 28.67 o 1 8 3 137.50 115.05 16.37 o 2 8 3 51.02 51.36 10.91 o 3 8 3 299.59 293.95 16.81 o 4 8 3 145.67 158.29 12.89 o 5 8 3 46.59 37.30 8.95 o 0 9 3 133.80 123.63 19.77 o 1 9 3 418.31 427.79 22.20 o 2 9 3 18.94 21.90 9.38 o 3 9 3 377.17 405.36 23.84 o 4 9 3 76.16 78.54 10.15 o 5 9 3 112.38 99.41 16.59 o 0 10 3 252.02 250.91 28.97 o 1 10 3 30.16 27.41 10.77 o 2 10 3 75.19 93.67 19.54 o 3 10 3 44.45 50.55 10.57 o 4 10 3 39.24 48.06 9.37 o 0 11 3 69.30 57.37 19.94 o 1 11 3 30.94 37.67 13.85 o 2 11 3 114.51 109.71 22.68 o 0 0 4 1785.32 1796.44 52.21 o 1 0 4 171.69 169.29 4.41 o 2 0 4 642.95 644.19 11.34 o 3 0 4 1274.81 1391.09 22.64 o 4 0 4 130.08 130.78 17.06 o 5 0 4 281.15 279.34 18.89 o 6 0 4 39.90 70.70 30.16 o 7 0 4 1.84 -3.26 9.05 o 8 0 4 4.02 7.66 16.63 o 0 1 4 49.83 38.05 3.63 o 1 1 4 2291.96 2290.38 20.56 o 2 1 4 885.76 912.50 9.34 o 3 1 4 30.87 42.50 3.13 o 4 1 4 297.03 310.29 9.87 o 5 1 4 119.67 132.27 8.78 o 6 1 4 29.29 35.61 8.11 o 7 1 4 90.65 95.48 14.99 o 8 1 4 8.89 3.31 19.79 o 0 2 4 50.18 46.81 5.87 o 1 2 4 3006.13 2727.97 24.70 o 2 2 4 467.75 462.88 6.94 o 3 2 4 64.54 68.47 2.61 o 4 2 4 11.90 10.48 3.39 o 5 2 4 165.27 176.82 9.91 o 6 2 4 9.13 5.34 6.16 o 7 2 4 35.16 20.72 9.55 o 8 2 4 16.23 -4.84 8.62 o 0 3 4 48.03 32.91 4.07 o 1 3 4 429.06 401.97 8.53 o 2 3 4 110.37 107.25 3.87 o 3 3 4 387.81 366.81 6.85 o 4 3 4 226.36 223.26 6.33 o 5 3 4 5.63 6.03 3.94 o 6 3 4 49.71 45.39 8.79 o 7 3 4 0.61 -4.77 7.05 o 0 4 4 1435.00 1361.21 23.63 o 1 4 4 472.06 480.68 9.82 o 2 4 4 1169.49 1231.39 19.00 o 3 4 4 184.94 187.57 5.65 o 4 4 4 194.47 209.99 6.46 o 5 4 4 53.35 52.98 8.42 o 6 4 4 32.66 40.33 14.26 o 7 4 4 20.68 4.77 8.30 o 0 5 4 11.01 2.91 4.58 o 1 5 4 139.32 155.45 6.74 o 2 5 4 375.04 330.63 9.01 o 3 5 4 193.09 198.99 7.24 o 4 5 4 63.62 60.54 4.68 o 5 5 4 72.13 69.26 9.44 o 6 5 4 134.88 111.09 12.95 o 7 5 4 73.26 56.85 13.50 o 0 6 4 99.85 93.31 19.35 o 1 6 4 920.74 873.52 17.84 o 2 6 4 248.26 234.31 9.01 o 3 6 4 210.65 203.89 8.13 o 4 6 4 81.46 68.43 6.23 o 5 6 4 52.56 71.57 9.96 o 6 6 4 6.20 11.37 7.88 o 0 7 4 253.95 261.21 21.54 o 1 7 4 283.47 280.26 15.47 o 2 7 4 377.23 372.04 12.78 o 3 7 4 76.30 68.80 6.47 o 4 7 4 302.80 305.59 14.98 o 5 7 4 121.67 126.64 9.00 o 6 7 4 6.38 5.05 7.03 o 0 8 4 13.68 6.23 10.24 o 1 8 4 968.26 926.18 28.87 o 2 8 4 49.22 35.29 9.03 o 3 8 4 602.24 616.34 22.81 o 4 8 4 71.48 71.76 9.52 o 5 8 4 296.22 288.13 16.52 o 0 9 4 190.42 163.17 22.06 o 1 9 4 27.38 30.19 9.30 o 2 9 4 136.72 119.27 14.13 o 3 9 4 164.20 156.11 14.48 o 4 9 4 1.20 1.51 5.65 o 5 9 4 45.42 42.23 8.97 o 0 10 4 654.12 649.65 40.98 o 1 10 4 316.27 350.80 22.61 o 2 10 4 122.57 102.64 20.93 o 3 10 4 31.27 12.89 8.52 o 0 11 4 2.72 1.46 15.61 o 1 11 4 62.09 70.81 14.96 o 2 11 4 6.10 -5.83 30.79 o 1 0 5 593.13 593.83 9.57 o 2 0 5 255.05 235.52 7.01 o 3 0 5 1308.31 1437.56 22.48 o 4 0 5 78.41 75.63 8.83 o 5 0 5 276.76 264.97 17.25 o 6 0 5 8.45 6.28 8.42 o 7 0 5 10.62 16.40 16.33 o 8 0 5 2.14 16.68 15.26 o 0 1 5 815.60 841.90 22.03 o 1 1 5 1836.63 1745.06 17.39 o 2 1 5 87.81 85.07 4.10 o 3 1 5 1123.88 1140.79 13.41 o 4 1 5 424.91 441.05 13.24 o 5 1 5 36.55 43.62 6.60 o 6 1 5 139.31 182.98 12.93 o 7 1 5 8.01 9.13 8.57 o 8 1 5 0.07 12.13 10.50 o 0 2 5 2566.35 2478.77 42.79 o 1 2 5 868.40 892.35 10.68 o 2 2 5 182.38 199.54 5.39 o 3 2 5 131.08 131.95 3.69 o 4 2 5 479.87 447.89 12.49 o 5 2 5 25.26 27.90 5.53 o 6 2 5 44.04 39.46 6.56 o 7 2 5 8.94 21.89 9.57 o 8 2 5 3.99 4.42 10.25 o 0 3 5 223.26 247.57 9.21 o 1 3 5 2085.10 1999.16 21.30 o 2 3 5 774.47 722.38 10.19 o 3 3 5 1058.84 1033.48 11.10 o 4 3 5 22.74 28.73 4.21 o 5 3 5 158.05 160.43 13.61 o 6 3 5 235.09 226.83 16.66 o 7 3 5 22.42 25.48 8.79 o 0 4 5 1926.26 2061.65 41.40 o 1 4 5 68.88 63.13 4.72 o 2 4 5 441.38 469.62 10.02 o 3 4 5 789.12 754.29 12.10 o 4 4 5 70.30 71.93 4.23 o 5 4 5 179.03 185.33 11.70 o 6 4 5 144.10 127.53 15.21 o 7 4 5 8.34 10.95 10.15 o 0 5 5 361.92 393.77 21.99 o 1 5 5 121.80 128.91 6.42 o 2 5 5 711.44 716.06 13.79 o 3 5 5 63.80 61.76 4.86 o 4 5 5 31.51 36.82 3.58 o 5 5 5 144.21 119.77 11.00 o 6 5 5 77.08 68.46 10.69 o 7 5 5 22.52 21.27 10.19 o 0 6 5 3098.50 2990.64 59.89 o 1 6 5 181.81 192.19 9.64 o 2 6 5 92.11 90.05 6.12 o 3 6 5 7.60 5.33 3.49 o 4 6 5 846.34 833.78 16.83 o 5 6 5 97.99 96.79 6.56 o 6 6 5 218.15 212.65 20.17 o 0 7 5 11.66 8.41 6.92 o 1 7 5 342.90 378.57 30.68 o 2 7 5 544.03 524.45 14.84 o 3 7 5 70.89 81.61 8.17 o 4 7 5 97.05 100.55 9.78 o 5 7 5 197.48 190.57 9.81 o 6 7 5 59.12 57.56 10.92 o 0 8 5 613.03 685.76 35.13 o 1 8 5 1156.73 1159.17 37.55 o 2 8 5 548.16 573.76 22.63 o 3 8 5 372.08 399.76 19.10 o 4 8 5 227.87 218.90 14.37 o 5 8 5 457.39 471.27 20.26 o 0 9 5 86.90 103.73 18.69 o 1 9 5 173.76 169.37 16.19 o 2 9 5 188.74 206.25 16.89 o 3 9 5 288.34 296.13 18.20 o 4 9 5 38.48 45.76 8.58 o 0 10 5 14.70 13.09 13.91 o 1 10 5 8.49 -2.56 8.67 o 2 10 5 112.04 95.90 32.92 o 3 10 5 11.16 8.36 7.76 o 0 11 5 7.45 20.55 17.34 o 1 11 5 43.27 56.23 14.08 o 2 11 5 97.29 81.02 28.30 o 0 0 6 1238.67 1213.01 41.24 o 1 0 6 389.88 357.10 8.17 o 2 0 6 718.45 722.45 14.71 o 3 0 6 326.08 368.07 8.46 o 4 0 6 10.53 5.27 5.36 o 5 0 6 35.50 47.68 11.43 o 6 0 6 16.91 13.05 7.85 o 7 0 6 0.31 11.12 9.93 o 8 0 6 32.64 38.24 21.42 o 0 1 6 4302.02 4193.92 66.52 o 1 1 6 453.39 445.73 7.16 o 2 1 6 796.58 780.45 8.89 o 3 1 6 583.78 573.19 8.05 o 4 1 6 69.99 79.78 5.61 o 5 1 6 11.81 4.60 4.34 o 6 1 6 130.40 130.43 13.81 o 7 1 6 74.67 97.14 14.63 o 8 1 6 28.91 38.08 22.49 o 0 2 6 627.02 608.06 16.20 o 1 2 6 5598.13 5511.98 48.58 o 2 2 6 131.98 125.72 4.10 o 3 2 6 620.26 680.53 9.96 o 4 2 6 40.91 44.39 3.54 o 5 2 6 516.46 508.55 15.10 o 6 2 6 38.47 35.81 6.51 o 7 2 6 21.24 17.81 9.35 o 0 3 6 1610.21 1825.77 31.33 o 1 3 6 385.73 379.69 7.41 o 2 3 6 638.87 715.78 12.26 o 3 3 6 183.22 163.80 4.47 o 4 3 6 19.13 18.66 2.37 o 5 3 6 8.90 12.61 4.68 o 6 3 6 90.26 78.19 7.98 o 7 3 6 46.01 49.64 10.40 o 0 4 6 1936.30 1922.10 48.43 o 1 4 6 133.39 139.31 5.48 o 2 4 6 495.24 478.99 10.27 o 3 4 6 345.89 354.26 7.58 o 4 4 6 880.45 869.94 11.74 o 5 4 6 60.39 73.67 8.70 o 6 4 6 326.58 295.00 18.83 o 7 4 6 14.69 8.54 8.62 o 0 5 6 686.79 712.62 22.45 o 1 5 6 520.71 591.82 13.24 o 2 5 6 1819.68 1806.70 22.39 o 3 5 6 17.33 15.67 2.96 o 4 5 6 612.01 620.76 11.02 o 5 5 6 19.39 21.26 5.45 o 6 5 6 36.31 40.19 8.91 o 7 5 6 16.56 19.19 10.44 o 0 6 6 150.24 120.40 11.72 o 1 6 6 513.47 491.53 12.97 o 2 6 6 174.45 170.01 7.00 o 3 6 6 14.98 16.71 3.98 o 4 6 6 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3082.04 3075.35 54.82 o 2 0 11 543.26 602.37 14.24 o 3 0 11 179.13 174.39 7.90 o 4 0 11 490.68 488.83 13.97 o 5 0 11 784.09 834.03 36.19 o 6 0 11 24.92 14.41 10.76 o 7 0 11 28.73 17.49 13.22 o 0 1 11 1373.16 1551.62 35.74 o 1 1 11 838.78 886.06 14.03 o 2 1 11 412.63 446.86 8.82 o 3 1 11 617.25 644.36 11.08 o 4 1 11 48.43 49.25 4.13 o 5 1 11 215.67 223.64 13.36 o 6 1 11 229.54 265.46 17.26 o 7 1 11 96.15 92.30 12.56 o 0 2 11 5709.57 5605.24 113.74 o 1 2 11 164.54 171.81 6.53 o 2 2 11 601.13 608.79 11.07 o 3 2 11 185.65 185.85 6.00 o 4 2 11 499.80 509.15 10.86 o 5 2 11 8.06 15.84 5.31 o 6 2 11 259.09 282.76 16.07 o 7 2 11 87.10 93.91 14.10 o 0 3 11 65.83 64.74 10.02 o 1 3 11 406.81 485.40 13.73 o 2 3 11 466.49 443.04 9.42 o 3 3 11 449.42 446.28 8.77 o 4 3 11 24.44 24.90 3.61 o 5 3 11 134.93 124.69 7.89 o 6 3 11 208.56 229.16 13.28 o 7 3 11 22.61 29.42 8.83 o 0 4 11 0.22 0.78 5.97 o 1 4 11 7.25 5.33 3.00 o 2 4 11 199.60 212.96 7.46 o 3 4 11 336.62 340.90 10.42 o 4 4 11 195.44 199.43 7.02 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15.81 o 2 2 21 197.94 201.84 10.25 o 3 2 21 133.05 126.47 9.09 o 4 2 21 100.09 99.92 8.96 o 5 2 21 2.83 11.42 5.75 o 0 3 21 504.84 493.67 31.60 o 1 3 21 283.45 250.00 13.75 o 2 3 21 162.37 176.12 15.56 o 3 3 21 213.03 205.41 20.05 o 4 3 21 18.14 9.86 5.80 o 5 3 21 201.72 221.35 12.46 o 0 4 21 1.53 0.51 9.44 o 1 4 21 72.32 81.87 10.27 o 2 4 21 2.29 0.03 5.41 o 3 4 21 1.37 11.02 6.41 o 4 4 21 1.03 2.62 5.21 o 0 5 21 36.23 46.89 13.87 o 1 5 21 37.45 44.18 10.02 o 2 5 21 34.21 32.14 7.90 o 3 5 21 71.20 71.05 10.34 o 4 5 21 6.50 9.71 5.98 o 0 6 21 62.34 44.88 15.82 o 1 6 21 11.82 5.57 10.17 o 2 6 21 16.06 -3.06 10.52 o 3 6 21 1.35 9.19 11.76 o 0 7 21 35.10 21.40 14.69 o 1 7 21 20.63 24.43 10.26 o 2 7 21 104.34 105.76 14.50 o 0 0 22 178.91 195.27 18.26 o 1 0 22 61.13 70.63 11.39 o 2 0 22 0.10 0.36 4.81 o 3 0 22 0.15 -0.32 5.56 o 4 0 22 48.52 44.29 10.35 o 5 0 22 130.72 126.68 15.40 o 0 1 22 141.65 136.22 11.76 o 1 1 22 93.36 107.14 11.40 o 2 1 22 30.85 25.03 5.24 o 3 1 22 132.86 129.88 9.23 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19.83 8.78 o 1 2 23 214.31 214.90 11.84 o 2 2 23 27.47 29.91 7.16 o 3 2 23 29.84 27.03 6.24 o 4 2 23 78.21 94.95 9.16 o 0 3 23 22.04 32.31 10.67 o 1 3 23 57.05 54.44 7.56 o 2 3 23 89.74 86.57 9.14 o 3 3 23 80.08 79.83 8.45 o 4 3 23 49.60 43.45 8.33 o 0 4 23 1.83 -3.10 8.08 o 1 4 23 125.87 125.25 12.61 o 2 4 23 20.99 31.69 7.57 o 3 4 23 32.25 36.17 7.96 o 0 5 23 28.32 29.14 12.74 o 1 5 23 65.40 61.76 10.69 o 2 5 23 37.59 47.49 9.66 o 3 5 23 100.56 111.54 13.34 o 0 6 23 62.77 75.91 31.79 o 1 6 23 44.18 41.15 13.04 o 2 6 23 28.80 28.78 10.79 o 0 0 24 260.86 273.09 37.05 o 1 0 24 208.97 198.55 18.98 o 2 0 24 15.77 21.61 8.13 o 3 0 24 294.92 287.20 31.56 o 4 0 24 139.04 132.78 16.25 o 0 1 24 0.13 9.13 6.83 o 1 1 24 39.53 43.87 7.05 o 2 1 24 138.64 123.48 8.09 o 3 1 24 27.79 25.83 6.17 o 4 1 24 66.40 68.33 8.02 o 0 2 24 157.06 120.93 15.26 o 1 2 24 21.87 22.96 6.13 o 2 2 24 277.10 281.72 13.92 o 3 2 24 102.89 89.47 9.53 o 4 2 24 35.24 24.80 7.44 o 0 3 24 111.91 112.15 15.79 o 1 3 24 94.67 102.28 9.65 o 2 3 24 30.52 40.57 7.56 o 3 3 24 174.29 178.43 11.90 o 0 4 24 35.46 49.05 12.70 o 1 4 24 138.55 147.75 11.75 o 2 4 24 17.23 21.66 12.08 o 3 4 24 13.48 9.25 8.23 o 0 5 24 123.22 126.27 17.26 o 1 5 24 76.59 66.48 12.09 o 2 5 24 88.01 86.07 11.75 o 0 6 24 8.47 25.03 14.59 o 1 6 24 231.81 306.92 20.02 o 1 0 25 410.95 415.31 25.81 o 2 0 25 0.24 6.77 7.35 o 3 0 25 4.68 11.27 8.91 o 4 0 25 2.54 6.36 12.94 o 0 1 25 9.72 8.76 8.92 o 1 1 25 60.60 53.83 10.42 o 2 1 25 181.90 188.51 12.11 o 3 1 25 31.19 21.38 7.54 o 0 2 25 521.63 504.73 22.39 o 1 2 25 28.89 28.55 7.63 o 2 2 25 47.49 41.43 7.48 o 3 2 25 95.92 95.65 10.07 o 0 3 25 17.62 10.24 10.43 o 1 3 25 78.31 71.93 16.62 o 2 3 25 70.45 69.62 9.60 o 3 3 25 2.58 7.20 5.80 o 0 4 25 100.40 92.21 15.72 o 1 4 25 237.17 220.64 15.85 o 2 4 25 52.63 58.62 10.63 o 0 5 25 5.29 4.82 12.08 o 1 5 25 97.58 112.82 13.56 o 0 0 26 135.00 85.07 24.81 o 1 0 26 1.86 9.33 9.58 o 2 0 26 5.45 -8.80 6.72 o 3 0 26 0.13 -3.14 7.96 o 0 1 26 1.28 8.00 9.30 o 1 1 26 63.52 75.27 10.82 o 2 1 26 36.11 36.42 7.98 o 3 1 26 17.28 17.08 7.46 o 0 2 26 0.00 -6.74 12.93 o 1 2 26 148.88 147.73 13.05 o 2 2 26 11.88 22.95 8.43 o 3 2 26 10.54 8.49 7.17 o 0 3 26 46.92 46.79 13.42 o 1 3 26 26.85 24.52 8.15 o 2 3 26 9.47 0.80 8.48 o 0 4 26 33.98 42.19 12.51 o 1 4 26 0.38 -1.11 6.43 o 1 0 27 35.38 56.70 13.81 o 2 0 27 18.40 19.46 12.88 o 0 1 27 4.90 -5.28 9.47 o 1 1 27 103.76 110.48 11.97 o 2 1 27 62.90 70.24 10.30 o 0 2 27 148.87 157.09 19.42 o 1 2 27 8.81 10.46 7.47 o 2 2 27 6.54 5.57 7.83 o 0 3 27 170.67 188.12 21.02 o 1 3 27 7.07 15.46 7.86 o 0 0 28 170.62 160.95 25.08 o 1 0 28 8.56 17.81 13.64 o 0 1 28 61.06 59.80 16.59 o 1 1 28 48.00 50.42 9.15 o 0 2 28 0.24 -7.54 9.81 o