#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/83/2228391.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228391_Fobs loop_ _publ_author_name 'Li, He-Ping' 'Ng, Seik Weng' _publ_section_title ; Ammonium 4-(4-carboxyphenoxy)benzoate ; _journal_coeditor_code HG2754 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3345 _journal_volume 66 _journal_year 2010 _space_group_IT_number 52 _symmetry_space_group_name_Hall '-P 2a 2bc' _symmetry_space_group_name_H-M 'P n n a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1916 _cell_length_b 28.5483 _cell_length_c 7.1123 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file hg2754Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pnna' _shelx_refln_list_code 4 _shelx_f_calc_maximum 224.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5738.87 5032.54 69.08 o 4 0 0 43.40 30.96 1.07 o 6 0 0 10.22 6.79 0.75 o 2 1 0 1813.03 1762.62 23.71 o 4 1 0 1524.82 1711.15 18.41 o 6 1 0 9.29 9.62 0.68 o 2 2 0 2313.04 2081.23 29.28 o 4 2 0 7.41 5.91 1.11 o 6 2 0 125.99 117.27 1.94 o 8 2 0 4.30 2.07 0.86 o 2 3 0 95.41 102.94 1.26 o 4 3 0 656.39 651.16 9.58 o 6 3 0 110.66 106.33 1.82 o 8 3 0 48.18 54.35 2.22 o 0 4 0 95.74 123.89 2.90 o 2 4 0 365.38 348.43 3.58 o 4 4 0 48.66 44.80 1.39 o 6 4 0 10.02 8.37 0.82 o 2 5 0 5.80 2.58 0.21 o 4 5 0 349.23 284.48 3.27 o 6 5 0 119.76 105.05 2.68 o 0 6 0 540.64 465.60 5.44 o 2 6 0 1265.72 1297.86 12.60 o 4 6 0 232.71 228.57 3.02 o 6 6 0 3.82 3.58 0.68 o 2 7 0 109.77 110.97 1.36 o 4 7 0 96.09 90.22 1.39 o 6 7 0 89.46 77.77 2.29 o 0 8 0 2293.48 2466.74 22.86 o 2 8 0 218.33 169.66 2.07 o 4 8 0 13.25 12.68 0.79 o 6 8 0 15.79 16.20 1.18 o 2 9 0 16.16 15.02 0.41 o 4 9 0 6.44 4.53 0.34 o 6 9 0 35.47 43.41 1.79 o 0 10 0 2449.92 2521.13 22.54 o 2 10 0 314.49 288.82 4.54 o 4 10 0 714.06 733.22 10.91 o 6 10 0 259.31 254.36 5.01 o 2 11 0 9079.68 9643.10 92.68 o 4 11 0 813.61 738.15 10.98 o 6 11 0 210.24 215.21 4.51 o 0 12 0 2120.49 2184.38 19.33 o 2 12 0 1386.38 1619.60 15.56 o 4 12 0 1.34 2.43 0.54 o 6 12 0 1225.26 1166.52 17.31 o 2 13 0 215.83 251.60 2.64 o 4 13 0 750.83 725.46 10.91 o 6 13 0 172.21 179.13 4.04 o 0 14 0 62.51 52.88 0.86 o 2 14 0 5.17 9.07 0.70 o 4 14 0 2880.59 2848.41 38.79 o 6 14 0 325.24 295.69 5.72 o 2 15 0 7.03 5.76 0.37 o 4 15 0 610.27 579.79 9.05 o 6 15 0 112.09 108.76 3.04 o 0 16 0 2742.77 2871.76 25.65 o 2 16 0 101.72 105.77 1.28 o 4 16 0 93.58 82.94 1.57 o 6 16 0 49.22 53.77 2.07 o 2 17 0 430.63 422.12 3.82 o 4 17 0 57.82 57.06 1.28 o 6 17 0 0.95 1.14 0.72 o 0 18 0 426.96 324.61 5.29 o 2 18 0 26.06 32.36 0.87 o 4 18 0 28.50 27.11 1.23 o 6 18 0 56.01 59.57 2.22 o 2 19 0 972.72 896.92 9.10 o 4 19 0 7.08 7.89 0.89 o 6 19 0 8.37 10.15 1.11 o 0 20 0 196.12 204.01 3.83 o 2 20 0 205.13 187.71 3.45 o 4 20 0 0.82 0.67 0.48 o 6 20 0 5.83 6.36 1.00 o 2 21 0 482.31 472.60 5.24 o 4 21 0 0.06 0.74 0.45 o 6 21 0 24.14 31.43 1.79 o 0 22 0 2472.34 2399.26 32.64 o 2 22 0 12.66 6.51 0.86 o 4 22 0 42.40 42.03 1.22 o 6 22 0 0.74 0.32 0.72 o 2 23 0 178.89 186.41 2.60 o 4 23 0 312.95 276.35 3.70 o 6 23 0 32.41 40.80 2.00 o 0 24 0 2269.70 2100.14 28.93 o 2 24 0 63.52 74.74 3.00 o 4 24 0 13.56 15.26 0.86 o 6 24 0 325.73 355.65 7.01 o 2 25 0 600.56 502.90 5.67 o 4 25 0 25.93 26.43 2.31 o 0 26 0 21.14 21.99 1.32 o 2 26 0 1394.39 1264.67 18.27 o 4 26 0 137.92 122.87 2.25 o 2 27 0 929.32 977.17 14.59 o 4 27 0 26.68 27.14 1.12 o 0 28 0 68.62 73.26 2.36 o 2 28 0 56.93 75.16 2.47 o 4 28 0 2.43 1.61 0.57 o 2 29 0 110.85 100.76 2.86 o 4 29 0 42.26 42.97 1.35 o 0 30 0 217.65 206.91 4.51 o 2 30 0 4.13 7.69 1.18 o 4 30 0 35.21 35.36 1.89 o 2 31 0 140.47 144.48 3.65 o 4 31 0 27.87 24.17 1.68 o 0 32 0 106.70 106.37 3.07 o 2 32 0 0.16 2.65 1.00 o 4 32 0 23.87 29.46 1.93 o 2 33 0 3.90 5.33 1.14 o 0 34 0 77.75 93.39 3.00 o 2 34 0 59.65 52.88 2.29 o 2 35 0 64.62 70.04 2.72 o 1 0 1 12072.51 10480.71 200.49 o 3 0 1 1929.38 2078.75 19.97 o 5 0 1 119.41 127.74 1.95 o 7 0 1 1.21 3.22 0.75 o 0 1 1 70.35 82.13 1.32 o 1 1 1 13876.99 11740.11 169.71 o 2 1 1 60.55 50.17 1.31 o 3 1 1 466.11 518.59 3.79 o 4 1 1 7.24 4.62 0.26 o 5 1 1 61.62 61.01 0.87 o 6 1 1 109.14 102.81 1.49 o 7 1 1 246.86 217.32 3.52 o 1 2 1 1859.85 2127.90 18.06 o 2 2 1 23.89 26.53 0.49 o 3 2 1 2272.63 2425.55 18.85 o 4 2 1 9.97 11.42 0.36 o 5 2 1 120.08 107.82 1.23 o 6 2 1 0.54 1.19 0.34 o 7 2 1 11.18 9.22 1.00 o 0 3 1 24.03 24.10 0.54 o 1 3 1 882.23 982.46 9.04 o 2 3 1 1294.05 1394.83 21.01 o 3 3 1 117.00 182.83 2.26 o 4 3 1 42.25 48.06 0.82 o 5 3 1 71.87 87.46 1.26 o 6 3 1 22.70 23.19 0.72 o 7 3 1 5.66 3.65 0.79 o 1 4 1 2978.75 2853.54 30.96 o 2 4 1 3596.39 3858.06 34.30 o 3 4 1 497.11 558.31 5.80 o 4 4 1 25.58 27.01 0.77 o 5 4 1 1.87 4.56 0.55 o 6 4 1 33.40 27.38 0.96 o 7 4 1 96.08 90.78 2.65 o 0 5 1 65.40 63.32 1.48 o 1 5 1 545.78 642.94 4.51 o 2 5 1 27.61 30.29 0.53 o 3 5 1 337.41 370.91 3.28 o 4 5 1 139.64 129.58 1.92 o 5 5 1 145.14 148.32 2.24 o 6 5 1 5.87 6.57 1.39 o 7 5 1 0.45 0.46 0.61 o 1 6 1 1683.06 1549.39 9.73 o 2 6 1 925.45 1047.26 9.23 o 3 6 1 5.34 0.20 0.16 o 4 6 1 47.44 42.46 0.85 o 5 6 1 58.22 61.71 1.04 o 6 6 1 1.41 1.34 0.44 o 7 6 1 37.37 32.75 1.61 o 0 7 1 1518.40 1491.29 25.65 o 1 7 1 156.57 155.92 1.04 o 2 7 1 387.94 418.97 3.33 o 3 7 1 138.20 144.27 1.43 o 4 7 1 141.40 130.87 1.53 o 5 7 1 73.34 71.24 1.13 o 6 7 1 3.31 2.05 0.46 o 7 7 1 4.99 5.08 0.89 o 1 8 1 5788.04 5523.32 31.59 o 2 8 1 450.90 533.41 3.80 o 3 8 1 0.74 1.10 0.17 o 4 8 1 188.80 209.84 2.17 o 5 8 1 391.21 395.42 4.72 o 6 8 1 15.13 16.79 1.04 o 7 8 1 29.85 31.96 1.68 o 0 9 1 131.18 110.85 1.03 o 1 9 1 598.12 668.01 3.55 o 2 9 1 349.22 346.18 2.76 o 3 9 1 306.72 325.68 2.76 o 4 9 1 18.00 23.76 0.58 o 5 9 1 165.82 155.34 2.50 o 6 9 1 61.91 63.24 2.27 o 7 9 1 3.63 3.11 0.82 o 1 10 1 1427.84 1328.49 6.91 o 2 10 1 0.72 6.99 0.23 o 3 10 1 312.34 343.88 2.89 o 4 10 1 144.47 150.74 3.15 o 5 10 1 510.37 502.20 8.30 o 6 10 1 42.28 41.21 1.26 o 7 10 1 40.59 38.11 1.86 o 0 11 1 0.92 0.30 0.16 o 1 11 1 4271.19 4658.06 24.94 o 2 11 1 2.28 1.05 0.22 o 3 11 1 33.15 35.37 0.51 o 4 11 1 56.10 48.89 1.15 o 5 11 1 617.23 660.99 7.29 o 6 11 1 47.76 45.63 2.20 o 7 11 1 0.21 0.86 0.72 o 1 12 1 4755.41 5034.30 26.31 o 2 12 1 841.98 840.30 5.57 o 3 12 1 167.11 232.25 2.31 o 4 12 1 1.29 1.82 0.38 o 5 12 1 1789.47 1812.36 23.33 o 6 12 1 2.05 1.06 0.58 o 7 12 1 5.10 6.69 1.04 o 0 13 1 1823.87 2034.61 14.12 o 1 13 1 12.52 8.02 0.48 o 2 13 1 77.13 90.83 0.79 o 3 13 1 840.29 915.22 7.54 o 4 13 1 44.50 40.98 0.86 o 5 13 1 935.57 885.04 22.95 o 6 13 1 17.98 15.81 1.00 o 7 13 1 0.00 0.68 0.79 o 1 14 1 373.26 435.13 2.61 o 2 14 1 127.90 109.06 1.07 o 3 14 1 15.15 18.33 0.92 o 4 14 1 10.95 15.34 1.47 o 5 14 1 71.60 74.35 1.63 o 6 14 1 107.43 109.75 2.17 o 7 14 1 243.44 252.28 5.43 o 0 15 1 1855.02 1938.40 13.29 o 1 15 1 552.78 660.28 3.46 o 2 15 1 112.02 112.94 1.11 o 3 15 1 1143.13 1144.00 9.32 o 4 15 1 318.46 322.17 3.19 o 5 15 1 0.39 0.29 0.50 o 6 15 1 4.47 5.37 0.66 o 7 15 1 3.84 5.83 1.07 o 1 16 1 132.34 136.31 0.92 o 2 16 1 76.08 60.19 0.89 o 3 16 1 21.65 23.49 0.56 o 4 16 1 103.03 84.67 1.30 o 5 16 1 33.55 29.35 1.04 o 6 16 1 14.47 12.91 0.86 o 7 16 1 0.98 1.54 0.89 o 0 17 1 1.48 3.99 0.27 o 1 17 1 15.65 17.55 0.40 o 2 17 1 17.29 16.85 0.54 o 3 17 1 17.65 21.16 0.55 o 4 17 1 48.45 46.67 0.96 o 5 17 1 5.68 6.71 0.59 o 6 17 1 2.26 2.75 0.58 o 7 17 1 13.70 18.95 1.57 o 1 18 1 0.15 0.00 0.17 o 2 18 1 80.65 68.15 1.06 o 3 18 1 245.77 249.43 2.25 o 4 18 1 23.65 21.76 0.59 o 5 18 1 1.62 1.46 0.48 o 6 18 1 3.96 4.29 0.89 o 0 19 1 574.22 544.64 4.10 o 1 19 1 168.75 222.17 2.04 o 2 19 1 5.52 5.69 0.35 o 3 19 1 71.03 85.68 1.11 o 4 19 1 4.07 4.92 0.38 o 5 19 1 4.72 5.05 0.49 o 6 19 1 5.77 4.36 0.89 o 1 20 1 10.51 10.97 0.53 o 2 20 1 2.02 1.17 0.29 o 3 20 1 44.08 39.89 0.87 o 4 20 1 69.96 61.73 1.00 o 5 20 1 6.39 5.64 0.62 o 6 20 1 3.02 3.33 0.62 o 0 21 1 11.15 9.45 0.52 o 1 21 1 54.13 57.65 0.80 o 2 21 1 8.04 8.28 0.48 o 3 21 1 23.53 32.96 0.82 o 4 21 1 1.65 2.06 0.42 o 5 21 1 48.10 47.12 1.35 o 6 21 1 0.05 -0.53 0.50 o 1 22 1 691.89 661.08 4.70 o 2 22 1 63.06 60.03 1.15 o 3 22 1 395.07 348.69 3.47 o 4 22 1 100.97 89.21 1.44 o 5 22 1 109.11 111.52 2.16 o 6 22 1 5.28 3.79 0.70 o 0 23 1 1400.27 1345.35 13.45 o 1 23 1 1754.09 1738.20 13.95 o 2 23 1 19.36 21.24 0.68 o 3 23 1 160.88 164.67 2.05 o 4 23 1 14.09 15.34 0.71 o 5 23 1 4.92 6.54 0.79 o 6 23 1 0.00 -0.43 0.57 o 1 24 1 131.29 147.82 3.26 o 2 24 1 0.50 1.73 0.38 o 3 24 1 175.80 142.08 2.23 o 4 24 1 8.85 5.18 0.52 o 5 24 1 301.92 298.59 4.15 o 6 24 1 0.01 -0.91 0.61 o 0 25 1 63.99 59.78 2.04 o 1 25 1 851.87 852.96 9.02 o 2 25 1 62.60 61.87 1.29 o 3 25 1 39.05 32.72 1.03 o 4 25 1 40.12 39.02 1.01 o 5 25 1 6.16 12.15 0.88 o 1 26 1 1273.67 1211.27 17.60 o 2 26 1 65.54 68.04 1.59 o 3 26 1 4.77 6.67 0.55 o 4 26 1 10.38 8.41 0.75 o 5 26 1 71.04 89.47 2.03 o 0 27 1 11.18 11.49 1.25 o 1 27 1 3.00 14.84 1.32 o 2 27 1 27.64 25.81 1.41 o 3 27 1 55.53 43.51 1.03 o 4 27 1 53.33 53.05 1.49 o 5 27 1 16.05 12.02 0.93 o 1 28 1 30.61 30.24 0.94 o 2 28 1 35.42 36.72 1.52 o 3 28 1 4.25 4.99 0.72 o 4 28 1 41.71 47.25 1.41 o 5 28 1 76.01 86.60 2.06 o 0 29 1 78.90 70.11 2.43 o 1 29 1 36.83 31.75 1.69 o 2 29 1 44.35 44.63 1.38 o 3 29 1 104.15 98.30 2.06 o 4 29 1 17.86 20.64 1.07 o 1 30 1 15.57 19.20 0.81 o 2 30 1 2.19 4.85 0.74 o 3 30 1 1.46 2.32 0.65 o 4 30 1 3.31 1.00 1.07 o 0 31 1 14.00 13.62 1.29 o 1 31 1 40.74 38.20 1.07 o 2 31 1 17.93 17.86 1.01 o 3 31 1 74.03 83.82 1.97 o 4 31 1 1.81 1.75 1.14 o 1 32 1 4.43 7.07 0.80 o 2 32 1 0.01 0.52 0.63 o 3 32 1 0.06 0.53 0.68 o 0 33 1 39.52 36.18 1.89 o 1 33 1 2.08 3.79 0.72 o 2 33 1 3.31 5.24 1.20 o 3 33 1 1.25 0.33 0.69 o 1 34 1 1.77 3.83 0.72 o 2 34 1 70.69 81.69 2.00 o 3 34 1 106.47 102.25 2.93 o 0 35 1 42.76 38.61 2.11 o 1 35 1 86.53 93.36 2.14 o 2 35 1 1.90 5.68 0.86 o 1 36 1 237.03 280.42 6.01 o 0 0 2 50473.63 35753.82 516.69 o 2 0 2 899.10 906.66 17.39 o 4 0 2 96.43 112.36 2.09 o 6 0 2 24.07 20.17 1.25 o 1 1 2 672.43 733.65 6.52 o 2 1 2 157.98 161.43 1.49 o 3 1 2 838.45 812.37 6.78 o 4 1 2 362.54 424.82 3.90 o 5 1 2 175.36 184.08 2.59 o 6 1 2 0.41 0.05 0.39 o 7 1 2 39.83 32.21 1.14 o 0 2 2 158.22 180.02 2.82 o 1 2 2 6151.93 6192.29 71.27 o 2 2 2 2048.23 2054.09 15.67 o 3 2 2 92.74 58.84 1.49 o 4 2 2 132.24 138.41 1.62 o 5 2 2 61.89 75.37 1.47 o 6 2 2 128.73 114.17 2.43 o 7 2 2 0.21 0.68 0.68 o 1 3 2 11342.02 10909.56 345.51 o 2 3 2 1367.42 1531.58 11.55 o 3 3 2 226.87 186.04 1.90 o 4 3 2 56.42 68.15 1.01 o 5 3 2 0.18 0.15 0.32 o 6 3 2 111.53 100.84 1.87 o 7 3 2 3.95 6.36 0.97 o 0 4 2 69.89 47.70 1.36 o 1 4 2 1751.03 1855.86 15.32 o 2 4 2 15.74 25.58 0.53 o 3 4 2 846.40 884.04 7.38 o 4 4 2 0.36 0.25 0.21 o 5 4 2 13.45 14.87 0.68 o 6 4 2 8.11 8.48 0.62 o 7 4 2 0.65 0.79 0.64 o 1 5 2 16.04 19.56 0.36 o 2 5 2 60.43 50.44 0.93 o 3 5 2 110.08 123.99 1.73 o 4 5 2 3.51 3.94 0.38 o 5 5 2 115.89 99.72 2.54 o 6 5 2 20.84 16.95 1.18 o 7 5 2 0.00 -0.82 0.61 o 0 6 2 47.82 52.20 0.80 o 1 6 2 133.23 127.23 1.18 o 2 6 2 17.01 23.07 0.62 o 3 6 2 721.36 678.34 7.16 o 4 6 2 21.14 19.92 1.07 o 5 6 2 159.77 165.97 3.54 o 6 6 2 2.85 2.11 0.68 o 7 6 2 17.85 25.78 1.54 o 1 7 2 239.36 256.26 2.10 o 2 7 2 19.29 20.84 0.46 o 3 7 2 61.98 73.10 0.80 o 4 7 2 16.83 13.33 0.57 o 5 7 2 33.41 37.26 1.54 o 6 7 2 0.49 0.79 0.61 o 7 7 2 0.81 1.97 0.79 o 0 8 2 178.14 167.67 2.97 o 1 8 2 1575.81 1641.32 16.76 o 3 8 2 1655.34 1515.85 10.49 o 4 8 2 369.55 355.99 6.08 o 5 8 2 35.93 27.17 1.39 o 6 8 2 11.39 10.58 1.04 o 7 8 2 4.94 6.76 1.00 o 1 9 2 893.78 1008.98 6.85 o 2 9 2 42.81 30.48 0.53 o 3 9 2 44.95 50.26 0.64 o 4 9 2 2.17 3.26 0.39 o 5 9 2 42.23 38.08 1.61 o 6 9 2 0.02 -0.04 0.61 o 7 9 2 298.46 295.65 5.97 o 0 10 2 57.27 61.59 1.97 o 1 10 2 2.46 5.92 0.23 o 2 10 2 117.67 118.71 0.98 o 3 10 2 68.74 86.83 1.07 o 4 10 2 214.07 234.45 2.94 o 5 10 2 219.37 200.26 4.18 o 6 10 2 108.85 103.87 2.93 o 7 10 2 0.61 2.57 0.82 o 1 11 2 247.23 266.05 1.63 o 2 11 2 1535.76 1918.86 11.81 o 3 11 2 2.71 3.72 0.26 o 4 11 2 388.88 378.53 6.40 o 5 11 2 363.38 369.77 6.54 o 6 11 2 86.43 90.74 2.75 o 7 11 2 6.58 5.79 1.00 o 0 12 2 253.85 312.97 3.09 o 1 12 2 512.12 620.42 3.49 o 2 12 2 934.58 1056.13 6.62 o 3 12 2 46.84 66.68 0.95 o 4 12 2 11.04 6.94 0.79 o 5 12 2 0.01 -0.79 0.61 o 6 12 2 448.62 453.22 7.97 o 7 12 2 32.47 27.57 1.68 o 1 13 2 841.44 847.37 4.51 o 2 13 2 467.34 450.80 3.13 o 3 13 2 32.05 28.76 1.20 o 4 13 2 180.80 160.39 3.47 o 5 13 2 0.19 -0.21 0.61 o 6 13 2 129.79 136.30 3.50 o 7 13 2 41.47 44.12 2.11 o 0 14 2 78.36 69.07 1.02 o 1 14 2 300.91 311.25 1.83 o 2 14 2 27.77 18.19 0.42 o 3 14 2 297.17 285.62 3.35 o 4 14 2 1725.36 1737.63 24.42 o 5 14 2 40.76 42.33 1.75 o 6 14 2 81.04 83.56 2.72 o 7 14 2 0.54 -0.97 0.64 o 1 15 2 582.23 545.58 3.02 o 2 15 2 15.66 8.97 0.37 o 3 15 2 206.44 216.79 2.73 o 4 15 2 173.98 159.46 3.50 o 5 15 2 8.26 8.58 0.97 o 6 15 2 24.75 30.11 1.64 o 7 15 2 134.85 143.02 3.86 o 0 16 2 1325.58 1429.11 12.52 o 1 16 2 492.74 513.07 2.98 o 2 16 2 145.27 125.43 1.31 o 3 16 2 913.44 944.82 10.42 o 4 16 2 8.54 7.26 0.86 o 5 16 2 0.43 -0.07 0.61 o 6 16 2 21.85 23.63 1.54 o 7 16 2 22.37 21.85 1.61 o 1 17 2 134.41 119.20 1.07 o 2 17 2 179.75 169.49 1.63 o 3 17 2 889.51 826.10 6.98 o 4 17 2 14.46 17.41 1.14 o 5 17 2 39.40 42.51 1.79 o 6 17 2 3.98 5.90 1.00 o 0 18 2 1.18 1.09 0.22 o 1 18 2 212.76 202.72 1.75 o 2 18 2 40.98 38.74 0.71 o 3 18 2 233.50 240.36 2.53 o 4 18 2 5.60 6.47 0.79 o 5 18 2 42.80 41.44 1.79 o 6 18 2 0.18 -0.21 0.64 o 1 19 2 204.80 180.28 1.63 o 2 19 2 13.30 14.17 0.50 o 3 19 2 4.63 2.88 0.40 o 4 19 2 1.44 1.04 0.45 o 5 19 2 21.82 24.63 1.43 o 6 19 2 20.97 26.78 1.68 o 0 20 2 14.10 16.02 1.14 o 1 20 2 37.13 35.55 0.77 o 2 20 2 2.88 1.18 0.28 o 3 20 2 19.45 14.33 0.65 o 4 20 2 6.86 4.94 0.60 o 5 20 2 81.25 81.98 2.61 o 6 20 2 0.93 1.14 0.75 o 1 21 2 243.75 248.81 2.10 o 2 21 2 33.23 30.46 0.68 o 3 21 2 38.81 34.12 0.93 o 4 21 2 1.98 0.89 0.49 o 5 21 2 3.86 3.52 0.62 o 6 21 2 1.54 3.05 0.64 o 0 22 2 1594.60 1585.39 22.24 o 1 22 2 183.04 173.47 2.05 o 2 22 2 14.26 11.62 1.57 o 3 22 2 42.60 37.95 1.12 o 4 22 2 27.04 24.86 1.01 o 5 22 2 41.27 39.29 1.31 o 6 22 2 14.23 17.55 1.09 o 1 23 2 617.00 614.59 5.52 o 2 23 2 1.23 2.84 0.39 o 3 23 2 136.75 121.74 2.43 o 4 23 2 137.65 121.14 3.54 o 5 23 2 0.02 0.34 0.93 o 6 23 2 4.33 5.59 0.78 o 0 24 2 1335.98 1356.13 19.41 o 1 24 2 64.50 62.50 2.30 o 2 24 2 111.01 112.13 1.95 o 3 24 2 44.05 38.99 1.32 o 4 24 2 20.05 21.76 1.01 o 5 24 2 6.49 8.93 0.84 o 1 25 2 23.88 27.43 0.87 o 2 25 2 276.17 244.74 2.69 o 3 25 2 120.28 117.45 2.13 o 4 25 2 16.11 13.83 0.90 o 5 25 2 42.82 46.81 1.48 o 0 26 2 12.39 11.26 1.14 o 1 26 2 7.04 6.33 0.57 o 2 26 2 506.85 453.96 5.42 o 3 26 2 57.63 63.09 1.54 o 4 26 2 3.30 1.93 0.55 o 5 26 2 0.88 0.39 0.59 o 1 27 2 374.47 353.38 3.68 o 2 27 2 273.04 273.65 3.74 o 3 27 2 157.68 150.69 2.53 o 4 27 2 18.85 17.96 0.99 o 5 27 2 65.51 75.96 3.61 o 0 28 2 155.61 147.27 3.58 o 1 28 2 69.80 62.23 1.59 o 2 28 2 31.59 33.00 1.21 o 3 28 2 27.77 25.42 1.64 o 4 28 2 2.78 3.48 0.65 o 1 29 2 38.87 31.05 1.24 o 2 29 2 0.05 0.20 0.58 o 3 29 2 58.11 55.17 2.32 o 4 29 2 5.61 4.53 0.70 o 0 30 2 7.73 7.65 1.11 o 1 30 2 13.61 14.48 0.95 o 2 30 2 13.29 15.21 0.99 o 3 30 2 108.10 107.05 3.29 o 4 30 2 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16.50 o 3 3 3 251.25 290.82 3.09 o 4 3 3 39.10 62.89 1.15 o 5 3 3 41.72 32.97 1.01 o 6 3 3 49.31 51.11 1.68 o 7 3 3 1.25 1.54 0.75 o 1 4 3 2523.64 2558.80 17.59 o 2 4 3 3654.95 3969.83 32.69 o 3 4 3 17.28 14.79 0.71 o 4 4 3 58.13 57.22 2.48 o 5 4 3 65.02 51.08 1.36 o 6 4 3 38.43 35.81 1.14 o 7 4 3 0.14 1.79 0.75 o 0 5 3 128.18 130.60 1.68 o 1 5 3 464.14 435.78 3.03 o 2 5 3 48.58 47.64 1.07 o 3 5 3 7.42 10.73 0.49 o 4 5 3 293.97 267.73 3.36 o 5 5 3 114.00 120.86 2.03 o 6 5 3 6.98 5.66 0.66 o 7 5 3 1.66 2.04 0.82 o 1 6 3 204.92 208.07 1.61 o 2 6 3 640.72 763.33 5.51 o 3 6 3 864.99 845.07 9.71 o 4 6 3 165.91 128.21 1.99 o 5 6 3 125.59 127.64 2.09 o 6 6 3 0.04 0.00 0.61 o 7 6 3 0.46 1.04 0.72 o 0 7 3 1110.17 1178.18 11.45 o 1 7 3 96.32 128.71 1.12 o 2 7 3 667.63 703.36 4.52 o 3 7 3 505.25 564.99 7.21 o 4 7 3 157.30 151.24 3.29 o 5 7 3 2.89 1.86 0.64 o 6 7 3 19.09 18.56 1.36 o 7 7 3 13.07 14.66 1.32 o 1 8 3 71.34 54.91 0.64 o 2 8 3 344.05 384.42 2.94 o 3 8 3 499.77 497.92 7.83 o 4 8 3 352.86 384.57 6.54 o 5 8 3 233.65 225.15 4.58 o 6 8 3 59.35 61.00 2.25 o 7 8 3 124.42 133.51 3.65 o 1 9 3 0.54 1.77 0.17 o 2 9 3 324.95 282.86 2.42 o 3 9 3 422.79 390.33 6.40 o 4 9 3 305.83 335.98 5.90 o 5 9 3 72.95 72.37 2.29 o 6 9 3 125.98 132.90 3.47 o 7 9 3 0.01 1.89 0.89 o 1 10 3 325.59 408.13 3.32 o 2 10 3 43.07 66.37 0.85 o 3 10 3 356.76 352.99 3.22 o 4 10 3 231.65 244.29 3.12 o 5 10 3 227.40 223.93 4.65 o 6 10 3 171.15 170.23 4.04 o 7 10 3 7.79 12.26 1.32 o 0 11 3 320.03 375.67 4.06 o 1 11 3 18.78 28.74 0.55 o 2 11 3 16.77 13.72 0.38 o 3 11 3 115.75 147.75 1.62 o 4 11 3 98.60 91.60 2.47 o 5 11 3 260.57 255.47 5.11 o 6 11 3 59.33 61.86 2.32 o 7 11 3 21.32 21.35 1.64 o 1 12 3 81.07 84.87 0.90 o 2 12 3 576.35 557.83 4.07 o 3 12 3 21.79 30.10 0.81 o 4 12 3 4.15 2.93 0.75 o 5 12 3 102.39 111.16 3.00 o 6 12 3 1.77 1.47 0.79 o 7 12 3 6.09 8.44 1.18 o 0 13 3 2044.41 2139.28 20.43 o 1 13 3 346.75 391.12 2.68 o 2 13 3 108.64 106.19 1.08 o 3 13 3 111.45 99.10 2.74 o 4 13 3 176.31 176.48 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470.03 3.65 o 3 6 4 61.45 73.44 1.42 o 4 6 4 1.20 3.54 0.50 o 5 6 4 53.51 41.73 1.21 o 6 6 4 5.12 3.11 0.82 o 7 6 4 15.96 30.28 1.82 o 1 7 4 7.26 10.90 0.35 o 2 7 4 23.61 19.78 0.58 o 3 7 4 59.94 51.81 1.31 o 4 7 4 220.80 216.24 2.99 o 5 7 4 0.01 0.07 0.39 o 6 7 4 74.92 80.23 2.65 o 7 7 4 0.01 0.50 0.79 o 0 8 4 1565.85 1576.82 21.74 o 1 8 4 283.74 307.69 2.46 o 2 8 4 131.17 145.36 1.65 o 3 8 4 419.12 419.60 3.86 o 4 8 4 1322.47 1325.47 14.43 o 5 8 4 12.42 10.76 1.11 o 6 8 4 17.47 19.13 1.43 o 7 8 4 1.06 0.82 0.82 o 1 9 4 113.34 147.27 1.39 o 2 9 4 77.67 56.54 0.88 o 3 9 4 85.18 77.75 1.16 o 4 9 4 2.63 5.04 0.86 o 5 9 4 38.23 37.15 1.72 o 6 9 4 88.84 100.11 3.07 o 0 10 4 1372.13 1489.57 11.83 o 1 10 4 26.50 26.18 0.52 o 2 10 4 21.36 21.95 0.50 o 3 10 4 69.58 69.26 1.32 o 4 10 4 52.08 55.63 2.00 o 5 10 4 18.64 18.16 1.39 o 6 10 4 2.93 2.50 0.89 o 1 11 4 64.54 62.97 0.82 o 2 11 4 69.32 47.61 0.82 o 3 11 4 18.22 17.32 0.70 o 4 11 4 11.06 12.91 1.14 o 5 11 4 228.88 213.45 4.61 o 6 11 4 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