#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:56:55 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181205 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/84/2228489.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228489_Fobs loop_ _publ_author_name 'He, Guangwen' 'Aitipamula, Srinivasulu' 'Chow, Pui Shan' 'Tan, Reginald B. H.' _publ_section_title ; 2-Aminopyridinium 1-phenylcyclopropane-1-carboxylate ; _journal_coeditor_code NG5075 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3339 _journal_page_last o3340 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.563 _cell_angle_beta 87.716 _cell_angle_gamma 72.788 _cell_length_a 8.6147 _cell_length_b 9.0555 _cell_length_c 9.2346 _exptl_crystal_F_000 272.00 _reflns_d_resolution_high 0.7500 _cod_data_source_file ng5075Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelxs in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 75.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 59.86 56.39 0.43 o 3 0 0 21.76 20.77 0.38 o 4 0 0 9.22 6.54 0.19 o 5 0 0 335.30 391.62 4.55 o 6 0 0 15.90 18.88 0.61 o 7 0 0 123.19 123.48 5.08 o 8 0 0 0.44 0.59 0.27 o 9 0 0 0.42 1.18 0.38 o 10 0 0 57.53 62.34 2.37 o -10 1 0 6.08 3.09 0.36 o -9 1 0 0.62 0.66 0.22 o -8 1 0 36.04 35.30 0.89 o -7 1 0 210.20 238.19 3.39 o -6 1 0 15.34 15.49 0.85 o -5 1 0 476.75 507.09 3.36 o -4 1 0 3.92 5.91 0.27 o -3 1 0 390.34 389.43 2.36 o -2 1 0 1728.85 1726.66 3.91 o -1 1 0 91.14 92.51 0.29 o 0 1 0 723.33 491.05 2.29 o 1 1 0 525.33 477.16 1.28 o 2 1 0 1601.66 1526.66 6.16 o 3 1 0 32.61 35.05 0.38 o 4 1 0 83.31 79.75 1.06 o 5 1 0 0.60 0.56 0.08 o 6 1 0 146.21 140.58 2.18 o 7 1 0 90.79 91.89 5.01 o 8 1 0 153.52 156.44 2.95 o 9 1 0 45.48 46.61 1.14 o 10 1 0 4.12 4.40 0.54 o 11 1 0 2.64 1.58 0.38 o -10 2 0 5.24 4.56 0.35 o -9 2 0 29.14 32.27 1.21 o -8 2 0 3.45 3.25 0.55 o -7 2 0 27.09 25.66 0.90 o -6 2 0 30.05 29.95 0.61 o -5 2 0 10.99 10.04 0.76 o -4 2 0 128.50 145.96 1.97 o -3 2 0 71.32 76.29 0.62 o -2 2 0 421.66 425.10 2.53 o -1 2 0 98.66 81.80 0.58 o 0 2 0 1084.70 1052.59 3.66 o 1 2 0 26.15 25.99 0.18 o 2 2 0 31.74 31.99 0.33 o 3 2 0 711.48 683.31 1.33 o 4 2 0 358.16 375.97 3.33 o 5 2 0 761.43 861.55 10.61 o 6 2 0 61.92 50.46 4.15 o 7 2 0 122.51 114.49 1.58 o 8 2 0 23.13 22.45 0.56 o 9 2 0 55.92 57.13 3.41 o 10 2 0 0.00 0.76 0.49 o 11 2 0 32.80 32.95 1.26 o -9 3 0 3.09 1.77 0.25 o -8 3 0 3.08 2.33 0.28 o -7 3 0 51.79 49.37 1.60 o -6 3 0 65.58 61.64 1.98 o -5 3 0 6.12 4.47 0.30 o -4 3 0 42.03 46.67 1.28 o -3 3 0 631.97 682.04 7.87 o -2 3 0 9.35 8.36 0.32 o -1 3 0 40.74 36.52 0.28 o 0 3 0 1772.13 1793.29 4.88 o 1 3 0 52.10 42.54 0.41 o 2 3 0 42.48 41.32 0.35 o 3 3 0 313.63 320.91 3.22 o 4 3 0 274.72 305.98 3.75 o 5 3 0 329.73 367.30 3.13 o 6 3 0 127.50 140.61 3.55 o 7 3 0 33.61 32.40 1.72 o 8 3 0 20.34 16.89 0.48 o 9 3 0 15.81 14.17 0.81 o 10 3 0 2.56 0.55 0.38 o 11 3 0 1.68 2.03 0.35 o -9 4 0 57.97 68.00 2.93 o -8 4 0 8.15 6.31 0.76 o -7 4 0 7.97 6.72 0.38 o -6 4 0 4.07 1.78 0.31 o -5 4 0 4.36 4.83 0.33 o -4 4 0 134.18 142.24 1.71 o -3 4 0 129.60 117.36 1.69 o -2 4 0 370.85 393.05 1.56 o -1 4 0 110.03 110.40 0.68 o 0 4 0 11.45 8.67 0.31 o 1 4 0 254.02 235.20 1.14 o 2 4 0 0.02 0.80 0.12 o 3 4 0 529.91 579.06 1.95 o 4 4 0 64.67 66.52 0.99 o 5 4 0 186.99 198.38 2.01 o 6 4 0 144.95 133.50 1.70 o 7 4 0 12.41 7.83 0.45 o 8 4 0 71.07 56.33 0.96 o 9 4 0 7.14 6.32 0.58 o 10 4 0 43.26 50.09 0.99 o 11 4 0 40.83 45.06 2.07 o -8 5 0 12.23 13.95 0.67 o -7 5 0 25.14 20.31 0.78 o -6 5 0 8.39 6.74 0.49 o -5 5 0 2.32 1.72 0.19 o -4 5 0 16.51 16.55 0.37 o -3 5 0 10.11 9.86 0.66 o -2 5 0 11.03 9.43 0.31 o -1 5 0 133.64 130.42 1.30 o 0 5 0 304.33 321.81 1.54 o 1 5 0 608.98 637.97 9.60 o 2 5 0 17.67 18.96 0.40 o 3 5 0 8.35 5.07 0.24 o 4 5 0 60.46 46.55 0.96 o 5 5 0 40.77 35.15 1.75 o 6 5 0 38.53 36.69 1.05 o 7 5 0 12.98 13.01 0.62 o 8 5 0 0.44 1.14 0.35 o 9 5 0 28.04 27.93 1.03 o 10 5 0 0.70 1.21 0.25 o 11 5 0 0.60 0.93 0.23 o -7 6 0 1.35 1.06 0.27 o -6 6 0 0.00 0.43 0.19 o -5 6 0 0.02 0.60 0.44 o -4 6 0 1.38 1.02 0.21 o -3 6 0 1.42 1.20 0.16 o -2 6 0 65.08 62.40 0.81 o -1 6 0 98.49 100.56 1.43 o 0 6 0 96.09 95.23 1.46 o 1 6 0 162.42 182.78 2.85 o 2 6 0 0.12 0.36 0.23 o 3 6 0 18.99 17.21 0.95 o 4 6 0 0.01 0.87 0.31 o 5 6 0 84.96 87.02 1.67 o 6 6 0 88.72 89.10 1.07 o 7 6 0 61.74 57.79 3.46 o 8 6 0 54.83 55.72 2.29 o 9 6 0 20.19 20.01 0.82 o 10 6 0 2.80 1.95 0.32 o 11 6 0 4.03 4.33 0.47 o -6 7 0 9.26 12.50 1.09 o -5 7 0 1.01 1.42 0.49 o -4 7 0 124.14 141.54 2.95 o -3 7 0 33.05 32.42 1.19 o -2 7 0 2.40 1.24 0.16 o -1 7 0 0.84 0.70 0.17 o 0 7 0 12.24 12.53 0.58 o 1 7 0 13.33 13.50 0.56 o 2 7 0 1.71 1.00 0.39 o 3 7 0 27.54 26.38 0.62 o 4 7 0 94.39 100.72 1.25 o 5 7 0 275.08 278.71 2.68 o 6 7 0 169.59 169.12 1.74 o 7 7 0 7.48 8.22 0.82 o 8 7 0 5.63 2.95 0.38 o 9 7 0 17.75 19.78 0.97 o 10 7 0 0.24 0.35 0.18 o -5 8 0 3.50 3.93 0.55 o -4 8 0 15.21 14.19 0.87 o -3 8 0 112.94 127.89 2.84 o -2 8 0 38.67 40.50 1.53 o -1 8 0 5.06 5.13 0.74 o 0 8 0 26.55 22.56 0.81 o 1 8 0 20.05 19.31 0.59 o 2 8 0 3.85 2.75 0.43 o 3 8 0 4.63 4.28 0.43 o 4 8 0 526.89 570.39 4.23 o 5 8 0 0.93 1.05 0.18 o 6 8 0 8.35 9.23 0.70 o 7 8 0 1.69 1.64 0.25 o 8 8 0 26.95 27.82 1.77 o 9 8 0 10.44 11.41 1.13 o 10 8 0 40.14 58.21 4.47 o -4 9 0 5.66 5.19 0.82 o -3 9 0 0.57 1.15 0.49 o -2 9 0 1.45 1.86 0.55 o -1 9 0 65.32 66.54 1.86 o 0 9 0 35.59 36.38 0.98 o 1 9 0 10.09 8.84 0.71 o 2 9 0 2.20 1.31 0.32 o 3 9 0 25.14 24.59 0.95 o 4 9 0 225.16 248.38 2.62 o 5 9 0 196.04 211.84 4.41 o 6 9 0 8.23 6.71 0.41 o 7 9 0 0.54 0.86 0.16 o 8 9 0 5.04 7.12 0.87 o 9 9 0 0.56 1.66 0.49 o -2 10 0 2.13 2.35 0.49 o -1 10 0 0.01 1.31 0.60 o 0 10 0 0.14 0.16 0.33 o 1 10 0 76.49 76.04 2.13 o 2 10 0 22.99 21.79 1.06 o 3 10 0 14.11 12.35 0.81 o 4 10 0 0.06 0.30 0.12 o 5 10 0 0.42 0.41 0.21 o 6 10 0 2.36 1.60 0.24 o 7 10 0 0.01 0.17 0.14 o 8 10 0 12.73 11.28 0.80 o 0 11 0 0.04 0.60 0.33 o 1 11 0 7.06 6.66 0.76 o 2 11 0 0.03 0.66 0.38 o 3 11 0 5.93 6.00 0.71 o 4 11 0 64.59 67.14 2.10 o 5 11 0 3.36 1.95 0.43 o 6 11 0 2.28 2.16 0.27 o -6 -11 1 7.91 4.36 0.45 o -5 -11 1 3.79 2.24 0.25 o -4 -11 1 4.34 3.37 0.29 o -3 -11 1 25.04 20.41 2.29 o -2 -11 1 1.97 1.80 0.44 o -1 -11 1 6.68 4.64 0.76 o -8 -10 1 45.79 59.01 3.66 o -7 -10 1 0.03 0.71 0.17 o -6 -10 1 4.92 4.74 0.61 o -5 -10 1 43.67 45.20 1.42 o -4 -10 1 33.82 33.40 1.05 o -3 -10 1 78.88 87.04 3.11 o -2 -10 1 5.19 4.04 0.54 o -1 -10 1 0.30 0.38 0.38 o 0 -10 1 2.49 1.26 0.49 o 1 -10 1 1.31 1.86 0.49 o 2 -10 1 46.35 52.67 3.33 o -9 -9 1 0.47 0.94 0.49 o -8 -9 1 3.26 2.96 0.46 o -7 -9 1 1.04 1.61 0.32 o -6 -9 1 0.02 0.23 0.18 o -5 -9 1 35.43 39.36 1.12 o -4 -9 1 0.08 0.44 0.17 o -3 -9 1 143.59 152.91 1.97 o -2 -9 1 50.06 50.56 0.94 o -1 -9 1 6.82 5.61 0.27 o 0 -9 1 17.99 17.47 0.56 o 1 -9 1 5.34 4.48 0.66 o 2 -9 1 12.24 10.70 1.04 o 3 -9 1 0.53 0.22 0.55 o 4 -9 1 0.46 1.09 0.55 o -10 -8 1 3.51 4.54 0.58 o -9 -8 1 0.27 0.84 0.25 o -8 -8 1 0.71 0.14 0.14 o -7 -8 1 5.12 4.83 1.00 o -6 -8 1 65.05 69.78 1.85 o -5 -8 1 464.99 518.20 8.41 o -4 -8 1 82.63 83.78 1.63 o -3 -8 1 4.29 4.31 0.37 o -2 -8 1 26.48 30.26 0.70 o -1 -8 1 13.06 11.00 0.49 o 0 -8 1 25.77 27.07 1.09 o 1 -8 1 12.76 13.37 0.98 o 2 -8 1 8.31 10.10 0.87 o 3 -8 1 1.06 1.75 0.60 o 4 -8 1 6.82 8.84 0.98 o 5 -8 1 5.36 4.59 0.71 o -10 -7 1 12.31 11.40 0.71 o -9 -7 1 0.56 0.61 0.14 o -8 -7 1 9.99 9.69 0.97 o -7 -7 1 4.38 4.64 0.52 o -6 -7 1 3.13 2.55 0.35 o -5 -7 1 192.56 200.69 2.03 o -4 -7 1 139.14 144.34 2.21 o -3 -7 1 3.90 3.17 0.27 o -2 -7 1 0.12 0.55 0.20 o -1 -7 1 80.81 77.57 1.29 o 0 -7 1 6.13 3.71 0.31 o 1 -7 1 2.97 1.95 0.22 o 2 -7 1 187.38 207.00 3.53 o 3 -7 1 4.47 3.03 0.34 o 4 -7 1 0.46 0.87 0.44 o 5 -7 1 0.99 0.76 0.38 o 6 -7 1 0.02 0.82 0.55 o -11 -6 1 1.92 2.17 0.40 o -10 -6 1 5.79 6.62 0.75 o -9 -6 1 0.58 0.90 0.21 o -8 -6 1 57.32 53.74 1.13 o -7 -6 1 8.69 8.25 0.39 o -6 -6 1 10.78 9.24 0.52 o -5 -6 1 232.19 222.91 2.33 o -4 -6 1 12.33 11.74 2.81 o -3 -6 1 197.12 187.26 2.20 o -2 -6 1 56.02 59.31 1.45 o -1 -6 1 0.51 0.66 0.22 o 0 -6 1 178.58 193.01 3.77 o 1 -6 1 2.20 2.17 0.18 o 2 -6 1 4.96 4.78 0.25 o 3 -6 1 78.59 76.16 0.86 o 4 -6 1 3.20 2.17 0.20 o 5 -6 1 24.37 23.15 1.07 o 6 -6 1 0.17 0.34 0.16 o 7 -6 1 0.23 0.93 0.55 o -11 -5 1 3.74 4.17 0.34 o -10 -5 1 14.19 11.38 0.66 o -9 -5 1 21.77 19.07 0.65 o -8 -5 1 24.64 18.09 1.31 o -7 -5 1 133.94 99.36 1.39 o -6 -5 1 0.89 0.93 0.33 o -5 -5 1 50.09 49.40 2.36 o -4 -5 1 2.02 0.86 0.17 o -3 -5 1 33.56 39.34 1.05 o -2 -5 1 128.61 150.61 1.49 o -1 -5 1 35.34 34.85 1.02 o 0 -5 1 110.85 99.01 3.88 o 1 -5 1 298.25 305.40 3.44 o 2 -5 1 91.15 96.21 1.22 o 3 -5 1 518.48 578.78 5.41 o 4 -5 1 101.80 112.34 1.24 o 5 -5 1 29.21 27.03 1.86 o 6 -5 1 7.00 5.71 0.36 o 7 -5 1 0.27 0.19 0.41 o 8 -5 1 3.28 2.47 1.20 o -11 -4 1 0.01 0.58 0.21 o -10 -4 1 3.01 3.46 0.40 o -9 -4 1 30.46 22.28 0.68 o -8 -4 1 3.68 2.54 0.33 o -7 -4 1 2.25 1.02 0.18 o -6 -4 1 6.71 6.30 0.36 o -5 -4 1 111.37 128.13 2.22 o -4 -4 1 642.94 692.75 6.23 o -3 -4 1 78.88 88.85 1.21 o -2 -4 1 11.80 10.93 0.32 o -1 -4 1 61.11 71.28 1.26 o 0 -4 1 44.46 44.75 0.75 o 1 -4 1 1004.97 1079.06 7.49 o 2 -4 1 18.00 16.53 0.39 o 3 -4 1 6.15 5.04 0.28 o 4 -4 1 11.12 10.75 0.37 o 5 -4 1 4.89 4.74 0.31 o 6 -4 1 15.74 12.14 0.62 o 7 -4 1 15.33 10.38 0.97 o 8 -4 1 4.78 3.09 0.27 o -11 -3 1 14.34 14.45 1.23 o -10 -3 1 28.06 29.63 0.92 o -9 -3 1 6.74 4.35 0.31 o -8 -3 1 2.69 1.72 0.21 o -7 -3 1 87.75 72.03 1.87 o -6 -3 1 111.31 119.98 3.11 o -5 -3 1 3.12 4.66 0.37 o -4 -3 1 1206.85 1368.20 4.69 o -3 -3 1 225.38 242.11 2.33 o -2 -3 1 148.39 145.63 1.09 o -1 -3 1 86.22 80.04 0.87 o 0 -3 1 423.07 443.40 2.28 o 1 -3 1 122.15 109.57 0.81 o 2 -3 1 19.91 17.39 0.47 o 3 -3 1 250.52 272.53 2.45 o 4 -3 1 47.69 48.99 1.06 o 5 -3 1 0.19 0.31 0.25 o 6 -3 1 1.80 2.80 0.23 o 7 -3 1 84.05 80.12 2.33 o 8 -3 1 10.86 9.21 0.90 o 9 -3 1 0.28 0.87 0.21 o -11 -2 1 11.65 12.06 0.67 o -10 -2 1 3.11 1.98 0.38 o -9 -2 1 58.73 59.16 1.06 o -8 -2 1 0.08 0.89 0.21 o -7 -2 1 103.69 106.31 1.36 o -5 -2 1 179.72 199.29 2.80 o -4 -2 1 163.09 179.03 1.50 o -3 -2 1 276.10 261.31 1.53 o -2 -2 1 0.49 0.36 0.06 o -1 -2 1 1444.59 1383.28 5.81 o 0 -2 1 3.57 2.85 0.15 o 1 -2 1 5736.49 5546.83 22.24 o 2 -2 1 778.54 810.28 7.50 o 3 -2 1 261.90 293.24 3.69 o 4 -2 1 42.94 40.55 1.34 o 5 -2 1 6.96 4.92 0.52 o 6 -2 1 207.49 235.66 3.03 o 7 -2 1 3.09 3.73 0.32 o 8 -2 1 1.59 2.18 0.28 o 9 -2 1 15.05 14.89 0.54 o 10 -2 1 0.07 0.71 0.22 o -11 -1 1 2.72 2.00 0.44 o -10 -1 1 4.13 3.92 0.60 o -9 -1 1 73.97 73.41 1.48 o -8 -1 1 28.13 29.01 0.76 o -7 -1 1 64.57 52.58 2.82 o -6 -1 1 0.36 0.52 0.12 o -5 -1 1 12.13 15.50 0.42 o -4 -1 1 1061.06 1159.85 6.19 o -3 -1 1 62.64 66.96 0.35 o -2 -1 1 878.92 835.68 2.63 o -1 -1 1 905.96 831.56 3.52 o 0 -1 1 1746.67 1662.77 7.87 o 2 -1 1 86.02 83.11 0.69 o 3 -1 1 423.42 454.63 3.32 o 4 -1 1 161.43 177.57 1.95 o 5 -1 1 43.76 41.76 0.77 o 6 -1 1 156.30 155.20 3.11 o 7 -1 1 33.05 29.94 0.95 o 8 -1 1 2.73 2.40 0.27 o 9 -1 1 61.87 71.63 1.17 o 10 -1 1 23.11 26.70 0.96 o -10 0 1 6.94 5.35 0.46 o -9 0 1 113.61 128.08 2.51 o -8 0 1 1.79 2.14 0.32 o -7 0 1 411.84 444.03 5.19 o -6 0 1 372.29 385.09 4.32 o -5 0 1 58.98 49.70 0.83 o -3 0 1 78.53 79.13 0.60 o -2 0 1 14.48 16.62 0.15 o -1 0 1 957.20 904.12 2.57 o 0 0 1 3.62 2.01 0.11 o 1 0 1 137.27 120.28 0.43 o 2 0 1 686.39 661.97 1.23 o 3 0 1 3.31 2.32 0.14 o 4 0 1 3.02 2.02 0.12 o 5 0 1 23.51 26.13 0.51 o 6 0 1 22.79 24.24 1.42 o 7 0 1 29.68 27.64 0.85 o 8 0 1 3.56 2.74 0.37 o 9 0 1 0.66 0.90 0.33 o 10 0 1 77.52 86.43 1.71 o -10 1 1 3.79 3.76 0.39 o -9 1 1 2.51 2.69 0.36 o -8 1 1 4.98 5.71 0.91 o -7 1 1 36.67 36.19 0.99 o -6 1 1 26.78 23.68 0.94 o -5 1 1 4.92 5.06 0.23 o -4 1 1 134.92 141.84 2.08 o -3 1 1 218.75 226.41 0.99 o -2 1 1 181.09 165.53 0.72 o -1 1 1 3411.90 3253.01 9.37 o 0 1 1 59.76 73.30 0.30 o 1 1 1 382.07 366.81 1.32 o 2 1 1 36.62 38.81 0.32 o 3 1 1 21.46 22.87 0.37 o 4 1 1 62.33 63.22 0.81 o 5 1 1 0.36 0.20 0.13 o 6 1 1 434.08 471.27 10.84 o 7 1 1 242.90 245.16 6.73 o 8 1 1 74.25 75.34 2.07 o 9 1 1 9.59 9.94 0.55 o 10 1 1 0.68 1.06 0.35 o 11 1 1 1.71 2.08 0.27 o -10 2 1 0.78 0.93 1.06 o -9 2 1 24.80 28.84 1.83 o -8 2 1 46.22 48.15 1.09 o -7 2 1 19.56 18.61 0.87 o -6 2 1 18.16 16.56 0.72 o -5 2 1 69.33 78.98 2.07 o -4 2 1 21.92 15.15 0.32 o -3 2 1 42.19 48.17 0.43 o -2 2 1 454.06 429.41 2.02 o -1 2 1 380.92 370.80 1.20 o 0 2 1 2642.73 2466.96 22.11 o 1 2 1 48.05 47.91 0.19 o 2 2 1 309.11 280.24 0.90 o 3 2 1 0.33 0.24 0.08 o 4 2 1 636.75 699.68 4.29 o 5 2 1 44.27 32.96 0.67 o 6 2 1 407.64 432.70 9.55 o 7 2 1 46.65 36.23 1.62 o 8 2 1 147.96 151.52 1.46 o 9 2 1 0.07 0.37 0.68 o 10 2 1 23.39 24.62 1.28 o 11 2 1 0.38 0.43 0.27 o -9 3 1 11.12 12.50 0.69 o -8 3 1 96.41 114.52 1.89 o -7 3 1 16.39 15.63 0.60 o -6 3 1 33.37 29.20 0.69 o -5 3 1 11.67 10.15 0.66 o -4 3 1 21.37 19.78 0.83 o -3 3 1 730.77 789.22 5.86 o -2 3 1 9.28 9.55 0.27 o -1 3 1 276.52 290.94 1.45 o 0 3 1 167.84 189.62 0.65 o 1 3 1 859.61 864.39 2.59 o 2 3 1 131.57 121.85 0.56 o 3 3 1 26.14 22.39 0.39 o 4 3 1 345.31 383.97 2.39 o 5 3 1 22.18 19.31 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