#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/84/2228494.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228494_Fobs loop_ _publ_author_name 'Guzei, Ilia A.' 'Spencer, Lara C.' 'Yankey, Margaret' 'Darkwa, James' _publ_section_title ; Bis(2-hydroxyethanaminium) tetrachloridopalladate(II) ; _journal_coeditor_code NK2068 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1551 _journal_page_last m1552 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.445 _cell_angle_gamma 90.000 _cell_length_a 8.9401 _cell_length_b 8.1621 _cell_length_c 8.5921 _exptl_crystal_F_000 368.00 _reflns_d_resolution_high 0.6992 _[local]_cod_data_source_file nk2068Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'DARKWA130 IN P21/C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 143.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1872.77 1922.69 24.78 o 3 0 0 15635.35 15957.06 210.02 o 4 0 0 18892.86 19745.49 263.71 o 5 0 0 5654.25 5624.34 54.64 o 6 0 0 1.96 10.22 1.49 o 7 0 0 3556.50 3549.68 40.38 o 8 0 0 3478.79 3475.65 40.41 o 11 0 0 875.46 891.94 31.46 o 12 0 0 545.88 622.50 25.97 o 1 1 0 11.39 16.54 1.50 o 3 1 0 6470.86 6699.19 58.60 o 4 1 0 176.34 166.08 2.81 o 5 1 0 662.66 611.00 6.74 o 6 1 0 967.40 979.31 11.90 o 7 1 0 1010.22 993.14 13.31 o 8 1 0 374.56 371.33 6.10 o 9 1 0 46.19 42.35 2.82 o 10 1 0 304.91 291.02 5.93 o 11 1 0 47.70 45.81 2.88 o 12 1 0 0.41 0.99 2.05 o 1 2 0 2390.37 2352.55 18.95 o 3 2 0 3423.77 3451.29 26.25 o 4 2 0 9402.60 9411.76 72.81 o 5 2 0 1243.26 1252.31 12.96 o 6 2 0 423.27 430.26 6.66 o 7 2 0 2664.46 2692.33 39.49 o 8 2 0 6330.59 6277.03 59.85 o 9 2 0 877.30 870.77 12.71 o 10 2 0 760.19 727.35 11.73 o 11 2 0 2791.42 2757.86 31.62 o 12 2 0 1869.35 1904.29 21.91 o 1 3 0 2251.39 2309.26 17.30 o 2 3 0 55.41 63.46 1.64 o 3 3 0 939.02 1011.76 8.76 o 4 3 0 180.03 177.39 3.07 o 5 3 0 2366.25 2423.57 18.62 o 6 3 0 36.72 38.23 2.37 o 7 3 0 48.27 47.96 3.07 o 8 3 0 320.09 327.02 7.24 o 9 3 0 225.84 242.67 10.22 o 10 3 0 0.42 -1.42 1.85 o 11 3 0 135.98 142.18 6.58 o 12 3 0 104.63 97.82 6.20 o 0 4 0 7452.15 7316.95 74.18 o 1 4 0 4003.31 4004.39 28.94 o 2 4 0 1154.25 1151.83 10.76 o 3 4 0 3070.31 3060.63 25.51 o 4 4 0 6169.50 6276.01 43.42 o 5 4 0 1715.05 1727.94 14.63 o 6 4 0 670.74 692.36 10.63 o 7 4 0 2126.31 2123.80 24.71 o 8 4 0 2279.40 2243.66 28.60 o 9 4 0 827.21 808.29 13.90 o 10 4 0 483.74 464.37 15.03 o 11 4 0 999.67 987.15 16.66 o 1 5 0 1249.35 1251.00 9.68 o 2 5 0 4.43 4.10 0.90 o 3 5 0 409.08 415.73 5.85 o 4 5 0 185.59 174.22 4.29 o 5 5 0 1863.35 1907.17 16.87 o 6 5 0 17.57 17.62 2.00 o 7 5 0 55.35 67.43 3.81 o 8 5 0 371.79 384.76 10.98 o 9 5 0 277.06 274.02 8.16 o 10 5 0 1.17 5.43 2.52 o 11 5 0 99.85 112.92 7.00 o 0 6 0 7166.85 7058.05 67.73 o 1 6 0 4346.28 4370.01 31.39 o 2 6 0 3986.85 4049.79 34.33 o 3 6 0 2991.85 2965.68 28.43 o 4 6 0 4276.98 4279.00 37.55 o 5 6 0 2150.41 2132.28 19.92 o 6 6 0 782.63 793.97 11.86 o 7 6 0 1549.83 1571.42 20.57 o 8 6 0 495.50 507.50 16.36 o 9 6 0 676.20 666.96 14.99 o 10 6 0 198.21 192.04 8.35 o 1 7 0 196.47 192.76 3.54 o 2 7 0 91.96 99.68 2.95 o 3 7 0 1941.61 1951.62 20.93 o 4 7 0 41.56 40.45 2.82 o 5 7 0 64.95 60.96 3.65 o 6 7 0 528.35 513.50 10.80 o 7 7 0 1083.49 1121.77 19.21 o 8 7 0 78.58 76.71 6.13 o 9 7 0 5.33 11.97 3.94 o 0 8 0 56.29 61.10 6.84 o 1 8 0 577.07 599.46 12.23 o 2 8 0 88.43 94.46 3.34 o 3 8 0 342.08 358.67 9.49 o 4 8 0 927.62 916.44 28.11 o 5 8 0 523.55 526.16 10.55 o 6 8 0 1050.75 1090.53 26.71 o 7 8 0 743.23 746.16 22.83 o 8 8 0 1360.43 1361.17 30.29 o 9 8 0 1235.90 1280.60 40.38 o 1 9 0 756.05 766.26 10.18 o 2 9 0 0.67 1.49 1.20 o 3 9 0 7.31 11.47 1.66 o 4 9 0 189.28 200.86 6.32 o 5 9 0 946.18 957.80 16.62 o 6 9 0 107.41 109.94 7.06 o 7 9 0 0.41 2.09 2.71 o 0 10 0 1964.29 1938.29 34.34 o 1 10 0 1476.62 1487.75 18.62 o 2 10 0 1704.46 1727.69 21.00 o 3 10 0 1147.36 1162.98 18.16 o 4 10 0 1043.65 1024.83 15.95 o 5 10 0 1097.07 1087.72 17.80 o 6 10 0 540.29 557.31 14.46 o 1 11 0 238.63 236.31 6.43 o 2 11 0 31.14 24.79 2.83 o 3 11 0 273.98 294.42 9.83 o 4 11 0 0.03 1.24 1.81 o -12 1 1 1461.27 1443.65 18.46 o -11 1 1 1633.09 1603.44 19.05 o -10 1 1 577.85 557.53 8.20 o -9 1 1 793.01 784.00 11.19 o -8 1 1 4704.62 4629.65 42.27 o -7 1 1 4560.28 4613.93 41.49 o -6 1 1 1699.05 1715.14 16.33 o -5 1 1 3942.22 3948.18 34.48 o -4 1 1 14095.65 13982.15 112.48 o -3 1 1 5827.73 6010.25 46.52 o -2 1 1 7141.56 7060.20 60.79 o 1 1 1 7950.44 8039.45 92.09 o 2 1 1 1472.97 1342.77 12.63 o 3 1 1 9729.51 9745.65 78.98 o 4 1 1 4433.96 4362.37 33.79 o 5 1 1 109.77 113.04 2.65 o 6 1 1 1428.96 1451.62 12.91 o 7 1 1 2812.92 2798.81 22.58 o 8 1 1 1224.79 1217.24 12.74 o 9 1 1 71.63 67.06 3.34 o 10 1 1 491.97 458.52 7.88 o 11 1 1 1900.80 1902.02 28.80 o 12 1 1 614.47 575.64 16.84 o -12 2 1 28.00 23.40 2.80 o -11 2 1 404.62 399.29 8.39 o -10 2 1 135.39 148.04 5.67 o -9 2 1 72.15 71.37 3.89 o -8 2 1 121.98 116.68 4.55 o -7 2 1 223.62 218.90 5.19 o -6 2 1 10.15 12.26 1.61 o -5 2 1 39.35 29.42 1.87 o -4 2 1 2.20 -0.77 0.77 o -3 2 1 654.50 688.92 6.43 o -2 2 1 290.21 275.48 3.26 o 0 2 1 10.25 4.99 0.85 o 1 2 1 2047.78 2091.08 17.26 o 2 2 1 3746.98 3918.17 26.80 o 3 2 1 4.44 -0.04 0.69 o 4 2 1 803.32 813.62 7.13 o 5 2 1 10.76 12.31 1.45 o 6 2 1 365.15 349.94 6.52 o 7 2 1 14.18 13.74 2.01 o 8 2 1 241.92 257.18 5.26 o 9 2 1 6.69 8.85 1.75 o 10 2 1 7.14 6.18 2.09 o 11 2 1 120.11 118.53 5.10 o -12 3 1 1745.03 1739.88 23.36 o -11 3 1 1464.78 1402.51 19.91 o -10 3 1 139.24 136.16 5.74 o -9 3 1 148.03 141.94 5.66 o -8 3 1 1175.36 1164.90 19.25 o -7 3 1 1782.82 1754.08 19.46 o -6 3 1 100.52 97.01 3.52 o -5 3 1 451.21 462.28 6.30 o -4 3 1 2227.10 2187.25 16.86 o -3 3 1 1454.57 1449.22 11.66 o -2 3 1 260.66 267.55 3.35 o -1 3 1 1104.63 1019.36 8.49 o 0 3 1 11592.29 11487.81 108.39 o 1 3 1 1899.16 1838.10 16.89 o 2 3 1 4275.11 4347.90 28.73 o 3 3 1 7403.06 7301.16 51.16 o 4 3 1 9070.30 9059.71 60.57 o 5 3 1 3795.37 3885.98 29.53 o 6 3 1 2761.40 2783.06 29.52 o 7 3 1 8018.07 7981.64 74.08 o 8 3 1 3600.80 3571.18 40.69 o 9 3 1 1504.04 1471.93 20.02 o 10 3 1 1210.61 1219.94 22.65 o 11 3 1 2781.18 2754.97 32.66 o -11 4 1 121.62 119.13 6.15 o -10 4 1 16.40 16.71 2.88 o -9 4 1 1373.94 1324.21 18.78 o -8 4 1 130.69 144.81 5.54 o -7 4 1 0.53 2.41 1.42 o -6 4 1 79.04 74.18 3.31 o -5 4 1 0.12 0.93 0.90 o -4 4 1 40.69 46.18 1.95 o -3 4 1 2505.59 2533.73 19.10 o -2 4 1 132.80 115.05 2.35 o -1 4 1 363.23 397.06 4.23 o 0 4 1 2531.75 2572.73 20.15 o 1 4 1 2599.46 2528.36 20.05 o 2 4 1 741.26 738.98 6.84 o 3 4 1 294.98 308.28 4.57 o 4 4 1 1873.44 1895.47 15.85 o 5 4 1 167.58 163.56 3.71 o 6 4 1 9.17 7.56 1.65 o 7 4 1 113.20 104.89 4.92 o 8 4 1 168.78 167.18 6.30 o 9 4 1 11.55 14.81 2.66 o 10 4 1 821.75 794.21 14.36 o 11 4 1 41.60 38.97 4.25 o -11 5 1 1845.91 1873.36 25.51 o -10 5 1 452.67 444.38 11.87 o -9 5 1 703.74 690.10 12.68 o -8 5 1 4693.82 4651.09 48.50 o -7 5 1 3535.74 3512.75 34.33 o -6 5 1 3451.70 3468.67 30.13 o -5 5 1 2434.87 2441.93 19.64 o -4 5 1 8803.02 8873.06 60.40 o -3 5 1 7985.00 8038.40 54.61 o -2 5 1 2010.76 2003.46 17.35 o -1 5 1 5826.07 5773.24 41.40 o 0 5 1 5956.29 5845.31 43.19 o 1 5 1 3623.65 3651.16 25.80 o 2 5 1 427.50 434.75 4.63 o 3 5 1 2223.02 2209.31 18.09 o 4 5 1 1584.86 1577.59 14.61 o 5 5 1 292.21 304.99 5.25 o 6 5 1 58.26 64.47 3.59 o 7 5 1 471.44 476.95 10.12 o 8 5 1 954.46 947.68 16.34 o 9 5 1 4.45 5.65 2.46 o 10 5 1 211.20 207.71 9.12 o -10 6 1 359.31 340.41 10.34 o -9 6 1 13.59 10.85 2.93 o -8 6 1 10.55 14.14 2.78 o -7 6 1 701.36 694.81 12.55 o -6 6 1 159.37 163.77 4.78 o -5 6 1 598.21 596.60 7.66 o -4 6 1 37.51 35.59 2.78 o -3 6 1 84.37 87.61 2.74 o -2 6 1 39.51 37.63 1.93 o -1 6 1 2492.58 2533.74 18.92 o 0 6 1 148.49 138.89 2.69 o 1 6 1 47.16 48.01 1.77 o 2 6 1 1000.70 984.54 10.14 o 3 6 1 1022.18 1001.98 12.43 o 4 6 1 38.04 34.05 2.42 o 5 6 1 170.18 161.38 4.99 o 6 6 1 468.59 480.82 10.48 o 7 6 1 158.58 134.73 5.63 o 8 6 1 331.48 341.55 9.44 o 9 6 1 152.82 147.03 7.43 o 10 6 1 31.37 30.03 5.09 o -10 7 1 319.55 315.03 12.48 o -9 7 1 391.59 396.74 16.00 o -8 7 1 976.41 975.80 20.05 o -7 7 1 983.35 995.14 17.46 o -6 7 1 612.65 619.35 11.87 o -5 7 1 535.37 551.64 9.75 o -4 7 1 1090.11 1135.66 15.30 o -3 7 1 1796.80 1822.81 19.60 o -2 7 1 778.50 790.20 9.24 o -1 7 1 1202.62 1200.98 11.62 o 0 7 1 2496.15 2478.97 22.22 o 1 7 1 1365.66 1348.63 12.99 o 2 7 1 1959.21 1948.26 16.32 o 3 7 1 1765.79 1766.66 17.30 o 4 7 1 2007.45 2037.44 22.07 o 5 7 1 1918.24 1926.48 22.84 o 6 7 1 1042.86 1040.33 17.54 o 7 7 1 1842.51 1789.25 45.74 o 8 7 1 1373.19 1429.97 25.64 o 9 7 1 619.21 620.24 16.59 o -9 8 1 147.69 148.20 9.80 o -8 8 1 200.12 213.12 10.52 o -7 8 1 371.46 375.57 12.05 o -6 8 1 127.51 134.16 7.26 o -5 8 1 655.47 650.24 11.29 o -4 8 1 31.17 27.64 2.80 o -3 8 1 465.18 477.62 10.14 o -2 8 1 0.53 1.38 1.28 o -1 8 1 609.12 602.65 7.76 o 0 8 1 2.57 3.53 1.12 o 1 8 1 531.06 520.68 7.28 o 2 8 1 53.31 52.55 2.20 o 3 8 1 618.17 614.31 8.90 o 4 8 1 91.53 88.13 6.11 o 5 8 1 303.99 287.09 7.26 o 6 8 1 210.91 216.43 8.24 o 7 8 1 158.44 147.71 8.33 o 8 8 1 128.75 134.02 9.04 o -8 9 1 224.16 252.64 14.56 o -7 9 1 416.84 450.78 12.78 o -6 9 1 598.81 598.68 14.40 o -5 9 1 555.24 557.05 11.28 o -4 9 1 192.77 193.92 6.29 o -3 9 1 707.96 701.86 13.04 o -2 9 1 1164.64 1159.88 15.13 o -1 9 1 673.86 688.70 9.32 o 0 9 1 730.29 732.42 10.09 o 1 9 1 876.27 891.88 10.83 o 2 9 1 2167.56 2115.47 22.13 o 3 9 1 1062.56 1055.51 13.39 o 4 9 1 752.01 738.75 12.55 o 5 9 1 1526.31 1558.01 22.12 o 6 9 1 1441.93 1470.13 25.41 o 7 9 1 1149.55 1122.72 24.64 o -6 10 1 29.78 31.72 4.41 o -5 10 1 211.19 218.75 8.11 o -4 10 1 1.70 2.70 2.21 o -3 10 1 690.93 700.12 11.30 o -2 10 1 28.22 29.92 2.70 o -1 10 1 5.98 2.88 1.91 o 0 10 1 121.00 122.22 6.06 o 1 10 1 809.18 845.82 12.26 o 2 10 1 147.31 145.72 6.69 o 3 10 1 66.08 60.99 3.40 o 4 10 1 521.37 522.07 10.78 o 5 10 1 182.59 177.86 7.18 o 6 10 1 20.18 21.01 4.71 o -4 11 1 847.33 860.38 23.45 o -3 11 1 1188.41 1211.09 21.49 o -2 11 1 2318.61 2334.04 27.07 o -1 11 1 1316.36 1312.38 21.06 o 0 11 1 146.53 159.89 6.31 o 1 11 1 1118.96 1115.48 15.72 o 2 11 1 897.60 897.48 13.85 o 3 11 1 339.38 340.97 9.21 o -12 0 2 3508.77 3585.35 58.62 o -11 0 2 3023.81 2951.04 42.04 o -10 0 2 1113.74 1058.73 23.82 o -9 0 2 3229.85 3060.72 40.84 o -8 0 2 6844.35 6964.85 82.46 o -7 0 2 5890.08 5991.96 57.80 o -6 0 2 718.32 724.59 9.66 o -5 0 2 5647.00 5725.76 62.46 o -4 0 2 9830.56 10238.74 97.41 o -3 0 2 4623.09 4392.44 61.04 o -1 0 2 4093.49 4298.93 43.56 o 2 0 2 15.80 19.70 1.72 o 3 0 2 383.90 364.07 7.76 o 4 0 2 6189.18 6373.13 67.18 o 5 0 2 119.03 118.97 4.35 o 6 0 2 69.15 56.84 3.54 o 7 0 2 4275.94 4304.42 49.23 o 8 0 2 2327.40 2298.43 29.76 o 9 0 2 575.56 574.70 13.35 o 10 0 2 639.45 612.12 12.32 o 11 0 2 2549.89 2450.14 43.15 o -12 1 2 24.37 26.62 4.32 o -11 1 2 0.95 0.42 1.96 o -10 1 2 68.53 63.94 3.45 o -9 1 2 280.89 271.10 5.88 o -8 1 2 150.55 152.09 4.63 o -7 1 2 250.81 245.15 5.08 o -6 1 2 496.95 485.46 6.58 o -5 1 2 1489.18 1472.85 13.82 o -4 1 2 2466.19 2533.59 21.20 o -3 1 2 250.45 248.89 3.77 o -2 1 2 2775.94 3006.55 24.09 o -1 1 2 787.64 821.96 7.83 o 0 1 2 3220.18 3235.24 24.17 o 1 1 2 242.78 247.42 2.75 o 2 1 2 2.22 0.78 0.55 o 3 1 2 300.15 320.15 3.48 o 4 1 2 1310.92 1274.81 11.22 o 5 1 2 164.02 176.96 3.24 o 6 1 2 846.82 846.27 9.47 o 7 1 2 177.23 183.73 4.19 o 8 1 2 513.73 513.97 7.43 o 9 1 2 686.65 706.86 9.28 o 10 1 2 96.01 89.49 4.30 o 11 1 2 121.50 129.47 5.15 o -12 2 2 719.05 681.33 16.66 o -11 2 2 693.31 667.67 11.10 o -10 2 2 1.39 1.98 1.67 o -9 2 2 430.08 403.17 7.88 o -8 2 2 2548.28 2566.66 26.24 o -7 2 2 684.57 733.63 12.64 o -6 2 2 511.58 492.20 6.58 o -5 2 2 1741.08 1756.71 15.59 o -4 2 2 12202.09 12485.38 90.30 o -3 2 2 3439.44 3423.42 26.39 o -1 2 2 20493.15 19880.09 261.57 o 0 2 2 19603.12 19278.08 306.47 o 1 2 2 8482.51 8502.04 63.54 o 2 2 2 1825.95 1771.53 13.01 o 3 2 2 13381.61 13290.46 83.57 o 4 2 2 12048.67 11911.42 72.12 o 5 2 2 2151.52 2133.71 16.24 o 6 2 2 1106.87 1133.73 11.06 o 7 2 2 4150.23 4131.25 32.03 o 8 2 2 3263.31 3268.28 31.61 o 9 2 2 90.70 88.53 4.41 o 10 2 2 386.99 372.17 7.80 o 11 2 2 920.44 894.50 15.10 o -12 3 2 60.02 52.16 4.96 o -11 3 2 25.02 22.12 2.86 o -10 3 2 60.32 58.55 3.87 o -9 3 2 38.06 38.63 3.14 o -8 3 2 92.95 90.87 4.25 o -7 3 2 857.04 863.55 11.05 o -6 3 2 128.33 131.56 3.80 o -5 3 2 164.53 177.86 3.90 o -4 3 2 328.65 326.78 4.23 o -3 3 2 591.25 586.15 5.88 o -2 3 2 938.56 1000.84 8.44 o -1 3 2 504.23 499.84 5.01 o 0 3 2 3.61 -0.41 0.81 o 1 3 2 1919.31 2010.27 16.18 o 2 3 2 169.21 146.75 2.38 o 3 3 2 756.89 781.68 8.43 o 4 3 2 35.80 40.92 1.59 o 5 3 2 77.82 84.98 2.11 o 6 3 2 269.80 265.04 4.98 o 7 3 2 329.95 332.72 8.40 o 8 3 2 21.27 15.90 2.12 o 9 3 2 30.91 31.54 2.77 o 10 3 2 189.03 192.43 6.07 o 11 3 2 149.57 140.64 6.22 o -11 4 2 681.28 638.06 15.11 o -10 4 2 380.93 375.40 8.55 o -9 4 2 1259.33 1218.01 16.41 o -8 4 2 2756.44 2767.07 28.66 o -7 4 2 1078.65 1145.28 14.07 o -6 4 2 608.12 599.07 8.50 o -5 4 2 4037.40 4047.45 29.67 o -4 4 2 5421.66 5484.69 38.46 o -3 4 2 1460.11 1457.20 12.16 o -2 4 2 1261.53 1237.89 10.37 o -1 4 2 7171.02 7249.48 49.35 o 0 4 2 7516.41 7581.29 55.18 o 1 4 2 1325.68 1299.20 11.58 o 2 4 2 1109.92 1067.60 8.67 o 3 4 2 6391.87 6362.43 39.91 o 4 4 2 4129.04 4081.08 29.54 o 5 4 2 647.51 659.72 8.22 o 6 4 2 1040.98 1083.40 17.78 o 7 4 2 2740.38 2668.53 29.94 o 8 4 2 1833.18 1808.26 25.92 o 9 4 2 298.07 294.24 8.86 o 10 4 2 554.91 558.17 12.82 o 11 4 2 1356.75 1361.75 22.24 o -11 5 2 109.18 103.33 6.62 o -10 5 2 19.84 22.43 3.16 o -9 5 2 75.54 85.49 4.92 o -8 5 2 8.93 6.82 1.95 o -7 5 2 1022.91 1011.43 12.84 o -6 5 2 62.06 61.71 3.11 o -5 5 2 263.69 265.66 4.44 o -4 5 2 576.92 570.36 6.65 o -3 5 2 922.94 906.75 8.74 o -2 5 2 73.76 86.77 2.33 o -1 5 2 379.67 377.17 4.32 o 0 5 2 365.42 350.09 4.30 o 1 5 2 943.32 965.46 9.58 o 2 5 2 317.23 315.95 4.18 o 3 5 2 566.99 564.48 6.07 o 4 5 2 108.48 105.23 3.90 o 5 5 2 117.58 131.34 3.96 o 6 5 2 657.30 643.53 10.33 o 7 5 2 308.93 309.97 8.31 o 8 5 2 9.55 10.86 2.77 o 9 5 2 1.98 6.06 2.44 o 10 5 2 328.07 330.21 10.23 o -10 6 2 1462.91 1528.74 39.30 o -9 6 2 1987.54 1997.87 25.34 o -8 6 2 2433.39 2474.69 26.88 o -7 6 2 1790.15 1837.77 20.93 o -6 6 2 712.78 733.68 9.88 o -5 6 2 4376.44 4455.39 33.18 o -4 6 2 1949.70 1966.24 16.62 o -3 6 2 698.13 709.12 8.70 o -2 6 2 945.95 955.51 10.80 o -1 6 2 1328.25 1345.86 11.21 o 0 6 2 2066.28 2044.92 17.70 o 1 6 2 49.41 42.79 2.00 o 2 6 2 341.08 339.16 5.25 o 3 6 2 1382.07 1359.48 12.15 o 4 6 2 943.62 939.66 10.71 o 5 6 2 115.51 116.66 4.67 o 6 6 2 564.79 604.40 11.77 o 7 6 2 1352.24 1309.41 25.75 o 8 6 2 837.40 797.19 23.25 o 9 6 2 688.05 655.82 17.04 o -10 7 2 5.02 1.57 3.57 o -9 7 2 640.30 633.67 22.07 o -8 7 2 4.20 5.34 2.72 o -7 7 2 1.05 0.50 2.34 o -6 7 2 550.16 557.48 12.05 o -5 7 2 1579.57 1583.71 21.02 o -4 7 2 307.25 307.33 8.35 o -3 7 2 73.63 70.97 3.08 o -2 7 2 1908.88 1876.79 18.58 o -1 7 2 1060.80 1044.90 10.56 o 0 7 2 2.32 2.98 0.99 o 1 7 2 168.52 176.02 3.95 o 2 7 2 331.62 336.06 5.26 o 3 7 2 216.89 206.62 4.40 o 4 7 2 1219.74 1186.45 13.21 o 5 7 2 390.90 415.66 8.53 o 6 7 2 0.69 1.20 2.18 o 7 7 2 27.29 26.80 4.33 o 8 7 2 1156.92 1188.96 23.84 o 9 7 2 319.85 337.42 14.54 o -9 8 2 132.50 140.77 9.32 o -8 8 2 280.88 287.36 10.74 o -7 8 2 130.91 135.20 10.51 o -6 8 2 628.97 606.03 15.18 o -5 8 2 839.73 847.11 13.39 o -4 8 2 1502.36 1551.19 19.82 o -3 8 2 1207.17 1214.71 16.43 o -2 8 2 2391.33 2379.31 23.61 o -1 8 2 3176.00 3187.33 28.05 o 0 8 2 2908.38 2933.15 26.38 o 1 8 2 4063.34 4012.60 34.46 o 2 8 2 2061.21 2073.20 19.01 o 3 8 2 4196.31 4130.98 35.95 o 4 8 2 2531.86 2500.32 31.48 o 5 8 2 1862.55 1859.62 25.31 o 6 8 2 1667.22 1674.96 25.12 o 7 8 2 750.40 766.85 15.91 o 8 8 2 1132.06 1149.64 25.18 o -8 9 2 78.93 87.21 7.36 o -7 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