#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/85/2228516.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228516_Fobs loop_ _publ_author_name 'Batrice, Rami J.' 'Nesterov, Vladimir N.' 'Smucker, Bradley W.' _publ_section_title ; Chlorido(4,4',4''-tri-tert-butyl-2,2':6',2''-terpyridine)platinum(II) tetrafluoridoborate ; _journal_coeditor_code PV2335 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1702 _journal_page_last m1703 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.239 _cell_angle_gamma 90.000 _cell_length_a 12.5921 _cell_length_b 16.4998 _cell_length_c 13.3262 _exptl_crystal_F_000 1416.00 _reflns_d_resolution_high 0.7781 _[local]_cod_data_source_file pv2335Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21n in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 374.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6985.42 6434.24 123.53 o 4 0 0 26245.65 27451.73 485.61 o 6 0 0 1543.44 1474.00 90.42 o 8 0 0 23246.51 23437.34 513.39 o 10 0 0 18716.16 18343.66 376.19 o 12 0 0 9045.47 9279.45 285.44 o 14 0 0 7416.01 7880.93 315.36 o 1 1 0 84589.52 87706.55 1673.49 o 2 1 0 12044.95 12127.78 143.01 o 3 1 0 73035.93 77625.38 1075.57 o 4 1 0 21174.38 21382.01 265.54 o 5 1 0 37389.50 37303.76 462.52 o 6 1 0 2697.87 2890.63 85.43 o 7 1 0 206.24 307.84 70.84 o 8 1 0 3127.05 3091.26 73.94 o 9 1 0 24159.78 24312.13 331.02 o 10 1 0 2785.25 2700.70 74.13 o 11 1 0 157.03 133.51 34.48 o 12 1 0 1079.86 1189.90 87.11 o 13 1 0 18482.24 19021.38 252.02 o 14 1 0 677.64 615.59 75.76 o 15 1 0 791.90 978.54 112.84 o 0 2 0 9534.94 10777.31 196.25 o 1 2 0 22050.58 24298.62 253.71 o 2 2 0 13254.73 15149.72 167.78 o 3 2 0 96899.95 103105.64 1993.83 o 4 2 0 139877.52 145531.48 1601.42 o 5 2 0 552.53 562.15 24.19 o 6 2 0 1005.42 985.77 48.24 o 7 2 0 24071.09 23877.38 568.71 o 8 2 0 6325.86 6195.58 129.57 o 9 2 0 218.52 214.38 35.11 o 10 2 0 5413.66 5359.38 103.61 o 11 2 0 12852.33 13240.29 196.59 o 12 2 0 3863.67 3882.58 126.71 o 13 2 0 16.65 -43.21 43.21 o 14 2 0 8094.12 8685.80 178.98 o 15 2 0 3816.23 4113.29 222.69 o 16 2 0 1588.24 1449.75 203.26 o 1 3 0 14364.93 15056.53 179.09 o 2 3 0 54224.96 57677.06 598.45 o 3 3 0 25767.41 27096.48 290.52 o 4 3 0 59396.42 61714.09 645.40 o 5 3 0 2166.20 2177.26 41.69 o 6 3 0 56867.71 58701.43 923.87 o 7 3 0 9053.02 9127.10 212.15 o 8 3 0 3261.70 3109.60 68.98 o 9 3 0 6753.75 6868.31 116.78 o 10 3 0 6979.79 7300.04 141.04 o 11 3 0 898.24 869.92 71.63 o 12 3 0 7821.50 7984.17 142.19 o 13 3 0 3697.77 3729.81 96.21 o 14 3 0 3259.21 3243.18 125.78 o 15 3 0 437.36 397.56 170.38 o 16 3 0 8740.52 9315.73 416.99 o 0 4 0 420.65 450.72 21.71 o 1 4 0 451.22 521.54 15.41 o 2 4 0 2403.48 2312.59 35.59 o 3 4 0 35099.45 35547.07 378.51 o 4 4 0 703.78 613.86 22.27 o 5 4 0 12294.96 12998.50 154.66 o 6 4 0 2692.88 2939.57 53.31 o 7 4 0 75806.71 78840.94 985.11 o 8 4 0 920.20 1017.42 45.01 o 9 4 0 2909.49 2958.10 70.84 o 10 4 0 15.86 0.12 24.28 o 11 4 0 18954.15 19632.47 288.94 o 12 4 0 4.07 -28.88 36.87 o 13 4 0 383.15 385.02 49.14 o 14 4 0 1463.81 1437.57 132.49 o 15 4 0 11716.75 13187.38 383.98 o 1 5 0 515.75 561.83 17.97 o 2 5 0 32265.01 32011.22 342.18 o 3 5 0 802.66 866.39 26.22 o 4 5 0 936.38 782.55 23.84 o 5 5 0 6528.27 6679.37 90.08 o 6 5 0 48867.71 49996.86 537.89 o 7 5 0 644.19 667.97 32.32 o 8 5 0 19634.30 20223.02 242.46 o 9 5 0 1414.41 1384.36 65.67 o 10 5 0 24350.17 24692.05 319.43 o 11 5 0 92.81 104.15 39.95 o 12 5 0 6603.23 6840.20 135.91 o 13 5 0 500.92 551.96 77.35 o 14 5 0 1362.76 1373.52 213.73 o 15 5 0 99.07 80.67 104.91 o 0 6 0 21863.33 22914.23 454.97 o 1 6 0 2018.46 1896.34 34.36 o 2 6 0 1195.54 1335.37 28.31 o 3 6 0 29133.36 29991.23 358.94 o 4 6 0 8846.30 8436.49 106.60 o 5 6 0 2134.43 2204.49 43.24 o 6 6 0 3927.66 3987.46 65.78 o 7 6 0 38256.30 39053.26 430.37 o 8 6 0 5322.99 5393.36 87.91 o 9 6 0 1552.12 1659.66 52.30 o 10 6 0 2453.75 2661.55 74.07 o 11 6 0 25250.05 26242.07 342.67 o 12 6 0 3867.56 4083.27 263.84 o 13 6 0 612.65 727.74 83.26 o 14 6 0 4819.16 4917.78 217.27 o 15 6 0 3225.29 3175.72 189.80 o 1 7 0 18234.75 17860.18 225.12 o 2 7 0 26077.03 25924.93 283.92 o 3 7 0 15550.90 16458.17 188.69 o 4 7 0 4656.22 4593.89 68.34 o 5 7 0 3946.81 3682.35 65.54 o 6 7 0 15130.33 14575.82 177.69 o 7 7 0 973.96 1008.95 37.06 o 8 7 0 2698.29 2783.34 60.94 o 9 7 0 31714.91 32801.12 475.68 o 10 7 0 13468.98 13451.03 228.54 o 11 7 0 81.59 137.71 56.83 o 12 7 0 3637.02 3615.46 146.56 o 13 7 0 13077.28 13412.62 249.80 o 14 7 0 535.68 443.23 113.77 o 15 7 0 1229.43 1069.76 140.01 o 0 8 0 37794.66 38158.23 581.32 o 1 8 0 2176.35 2494.01 45.78 o 2 8 0 275.97 255.95 19.72 o 3 8 0 3774.08 3694.04 59.15 o 4 8 0 42682.16 43326.16 467.96 o 5 8 0 79.67 122.86 20.43 o 6 8 0 5571.30 5552.65 84.78 o 7 8 0 8105.60 7878.72 122.44 o 8 8 0 18575.16 18775.04 291.68 o 9 8 0 224.18 163.66 51.42 o 10 8 0 20764.85 21701.51 387.35 o 11 8 0 650.08 662.62 64.42 o 12 8 0 4290.47 4405.38 127.65 o 13 8 0 182.49 139.56 61.61 o 14 8 0 11286.57 11174.86 352.88 o 1 9 0 32644.90 32050.60 353.45 o 2 9 0 1345.50 1308.66 34.80 o 3 9 0 17138.20 16946.51 198.67 o 4 9 0 2127.96 2048.52 53.69 o 5 9 0 33960.57 33836.78 377.12 o 6 9 0 21.12 14.92 25.50 o 7 9 0 3030.54 3053.68 74.47 o 8 9 0 943.12 927.41 89.31 o 9 9 0 30787.62 31557.13 450.95 o 10 9 0 206.17 137.53 48.47 o 11 9 0 1321.24 1376.65 82.07 o 12 9 0 2179.29 2152.67 106.78 o 13 9 0 15551.09 16596.33 294.71 o 14 9 0 4.48 8.57 117.32 o 0 10 0 54011.28 52831.96 803.56 o 1 10 0 603.31 643.07 30.45 o 2 10 0 1642.10 1666.61 41.02 o 3 10 0 3964.11 4215.77 69.15 o 4 10 0 28732.80 28618.57 359.80 o 5 10 0 3314.20 3561.47 77.58 o 6 10 0 2962.69 3098.72 74.75 o 7 10 0 7190.94 7346.88 143.44 o 8 10 0 7204.54 7242.29 147.31 o 9 10 0 8.46 1.39 42.62 o 10 10 0 5772.98 5998.75 142.08 o 11 10 0 5230.78 5266.95 136.96 o 12 10 0 2804.35 2857.14 109.94 o 13 10 0 2133.93 2014.63 107.89 o 14 10 0 10827.08 10869.51 359.14 o 1 11 0 8780.17 8715.50 119.42 o 2 11 0 26172.01 26366.02 300.66 o 3 11 0 4667.76 4379.99 73.22 o 4 11 0 1377.97 1396.06 53.36 o 5 11 0 23146.68 23395.26 310.94 o 6 11 0 20353.36 20495.40 312.31 o 7 11 0 127.83 122.50 41.98 o 8 11 0 8746.74 8596.79 168.14 o 9 11 0 1572.89 1511.19 82.19 o 10 11 0 3335.68 3412.42 109.43 o 11 11 0 552.66 577.90 69.36 o 12 11 0 5008.31 5314.52 147.62 o 13 11 0 8856.38 9448.16 208.89 o 0 12 0 10547.55 9893.32 191.02 o 1 12 0 15302.50 15430.09 212.57 o 2 12 0 206.13 292.70 28.02 o 3 12 0 18504.83 18528.64 254.18 o 4 12 0 1945.10 1917.87 62.01 o 5 12 0 1917.96 2046.66 65.75 o 6 12 0 40.46 55.28 39.06 o 7 12 0 17605.31 17312.49 276.43 o 8 12 0 180.65 118.92 48.37 o 9 12 0 38.04 57.82 47.00 o 10 12 0 2540.59 2609.92 100.57 o 11 12 0 11612.88 11837.12 228.59 o 12 12 0 160.63 203.41 63.20 o 13 12 0 199.59 282.83 72.47 o 1 13 0 237.34 285.75 40.49 o 2 13 0 34609.57 34441.20 436.50 o 3 13 0 210.24 225.94 36.88 o 4 13 0 6208.76 5902.93 113.88 o 5 13 0 3097.83 2823.43 88.06 o 6 13 0 8266.45 8454.14 168.05 o 7 13 0 1.25 -17.59 42.34 o 8 13 0 4742.93 4943.71 172.15 o 9 13 0 2.34 40.09 49.74 o 10 13 0 7575.88 7669.80 172.77 o 11 13 0 364.18 400.80 70.23 o 12 13 0 6145.72 6402.03 168.74 o 0 14 0 8847.86 9475.13 253.16 o 1 14 0 14117.66 14207.07 210.29 o 2 14 0 2420.54 2222.40 70.20 o 3 14 0 12982.15 12840.91 197.11 o 4 14 0 1655.54 1718.11 72.78 o 5 14 0 442.12 419.34 53.59 o 6 14 0 336.97 295.29 51.99 o 7 14 0 16509.19 15956.09 269.36 o 8 14 0 1980.94 1852.69 92.66 o 9 14 0 4.98 -39.21 52.41 o 10 14 0 870.37 883.04 79.35 o 11 14 0 10612.91 10951.62 247.22 o 12 14 0 374.92 291.62 74.08 o 1 15 0 6439.96 6433.30 142.01 o 2 15 0 6340.45 6433.83 124.79 o 3 15 0 807.84 767.42 54.51 o 4 15 0 436.66 458.78 55.42 o 5 15 0 9371.88 9184.10 179.09 o 6 15 0 10044.89 9912.54 192.79 o 7 15 0 773.92 785.92 70.70 o 8 15 0 4780.00 4448.89 129.31 o 9 15 0 5863.82 5967.81 152.84 o 10 15 0 2937.16 2810.03 117.11 o 11 15 0 180.66 100.47 67.14 o 0 16 0 17208.01 17529.96 672.56 o 1 16 0 143.69 214.83 49.25 o 2 16 0 153.44 96.73 47.25 o 3 16 0 4035.59 3758.63 106.82 o 4 16 0 17769.48 17562.32 286.17 o 5 16 0 1112.03 1201.78 77.55 o 6 16 0 3714.25 3867.20 118.56 o 7 16 0 4074.94 4075.27 125.74 o 8 16 0 6541.49 6533.53 162.23 o 9 16 0 53.54 90.70 61.63 o 10 16 0 1446.90 1316.51 95.99 o 1 17 0 8945.42 8738.77 191.79 o 2 17 0 185.80 174.69 51.10 o 3 17 0 3393.34 3195.39 173.67 o 4 17 0 14.92 -35.65 47.74 o 5 17 0 15958.40 15411.92 267.75 o 6 17 0 82.40 32.15 53.67 o 7 17 0 1785.06 1749.64 96.55 o 8 17 0 119.81 35.74 61.24 o 9 17 0 12465.09 13035.17 255.35 o 0 18 0 10122.82 10387.19 298.62 o 1 18 0 565.51 471.45 62.27 o 2 18 0 556.85 603.03 76.31 o 3 18 0 584.98 672.17 77.57 o 4 18 0 15470.14 15259.94 314.27 o 5 18 0 955.43 900.89 90.74 o 6 18 0 1738.00 1840.75 99.29 o 7 18 0 337.75 224.43 66.08 o 8 18 0 12079.81 12425.81 247.88 o 1 19 0 6600.32 6593.71 239.13 o 2 19 0 7076.63 6832.22 189.51 o 3 19 0 2553.71 2262.81 119.66 o 4 19 0 74.08 93.86 67.92 o 5 19 0 6375.51 6507.40 191.23 o 6 19 0 2802.34 2533.62 168.46 o 7 19 0 464.46 290.14 83.06 o 0 20 0 4616.35 4776.69 267.53 o 1 20 0 5301.29 5731.86 173.25 o 2 20 0 206.93 223.29 77.92 o 3 20 0 5085.58 4872.34 301.91 o 4 20 0 3422.17 3266.24 137.47 o 5 20 0 1291.38 1183.04 163.65 o 1 21 0 157.07 76.47 88.13 o 2 21 0 11350.78 11809.18 345.11 o -15 0 1 30.47 -41.38 127.79 o -13 0 1 29319.82 30344.69 728.82 o -11 0 1 1604.13 1626.22 83.33 o -9 0 1 21151.07 21057.60 600.03 o -7 0 1 1247.08 1352.45 78.24 o -5 0 1 42068.38 40286.76 2181.93 o -3 0 1 63898.50 63852.96 1251.62 o 1 0 1 67119.62 68528.54 1292.07 o 3 0 1 1383.77 1635.01 42.61 o 5 0 1 28852.85 27607.14 492.36 o 7 0 1 5345.40 5792.19 143.62 o 9 0 1 12447.36 13289.96 358.70 o 11 0 1 269.16 164.16 48.46 o 13 0 1 10108.47 10061.62 1117.95 o 15 0 1 3093.53 3434.55 215.22 o -16 1 1 5183.36 5457.20 303.40 o -15 1 1 374.35 462.99 77.47 o -14 1 1 9963.58 10235.79 224.86 o -13 1 1 268.74 197.48 52.38 o -12 1 1 11393.46 11846.78 173.08 o -11 1 1 859.91 983.68 51.61 o -10 1 1 14229.80 14116.80 189.16 o -9 1 1 1374.58 1385.57 49.50 o -8 1 1 17729.11 18018.15 236.52 o -7 1 1 3045.74 2834.29 62.51 o -6 1 1 1255.45 1151.56 57.59 o -5 1 1 4725.99 4381.29 72.78 o -4 1 1 49302.63 50801.89 574.19 o -3 1 1 32089.65 34167.65 649.25 o -2 1 1 17338.18 16666.81 285.39 o -1 1 1 767.57 788.43 17.06 o 0 1 1 90111.28 86842.73 1829.52 o 1 1 1 62.76 102.88 6.93 o 2 1 1 10180.52 11267.71 164.43 o 3 1 1 8254.96 8977.76 124.08 o 4 1 1 40783.01 40400.30 457.23 o 5 1 1 1734.87 1906.62 41.81 o 6 1 1 12219.45 12453.47 162.82 o 7 1 1 3219.07 3268.67 70.70 o 8 1 1 13712.94 13515.19 207.00 o 9 1 1 63.11 9.29 21.77 o 10 1 1 9746.00 9900.14 164.15 o 11 1 1 753.61 752.55 49.54 o 12 1 1 1395.49 1326.41 79.77 o 13 1 1 123.91 113.87 52.80 o 14 1 1 12237.77 12818.70 275.22 o 15 1 1 2069.52 2056.84 113.77 o 16 1 1 630.86 626.21 97.23 o -16 2 1 4355.42 4701.96 288.45 o -15 2 1 292.53 287.86 163.32 o -14 2 1 1400.26 1569.48 91.89 o -13 2 1 11840.86 12410.97 357.02 o -12 2 1 2423.57 2437.53 75.96 o -11 2 1 163.62 171.93 35.18 o -10 2 1 9011.09 8885.97 223.81 o -9 2 1 28300.31 28432.03 355.41 o -8 2 1 5629.49 5892.71 101.56 o -7 2 1 877.94 992.45 66.06 o -6 2 1 14442.87 14732.14 191.02 o -5 2 1 22463.22 22118.64 265.95 o -4 2 1 4290.37 4212.50 65.00 o -3 2 1 35732.32 37712.71 477.59 o -2 2 1 17978.03 17926.32 243.70 o -1 2 1 33065.28 34295.77 395.53 o 0 2 1 471.01 390.08 17.94 o 1 2 1 18967.09 20125.71 225.25 o 2 2 1 72410.49 75990.37 830.11 o 3 2 1 90297.36 98185.26 1207.12 o 4 2 1 15227.68 16081.44 191.82 o 5 2 1 22850.86 24497.66 287.70 o 6 2 1 1534.80 1492.62 43.45 o 7 2 1 147.59 170.97 22.51 o 8 2 1 4636.31 4452.31 89.17 o 9 2 1 12135.27 12166.96 186.28 o 10 2 1 6745.96 6915.72 128.50 o 11 2 1 897.22 788.99 50.89 o 12 2 1 2710.28 2982.20 83.69 o 13 2 1 6911.74 6985.81 179.56 o 14 2 1 779.58 620.88 76.79 o 15 2 1 2663.17 2715.33 122.73 o 16 2 1 2366.84 2294.52 166.65 o -16 3 1 421.63 390.09 159.92 o -15 3 1 9550.76 9390.58 280.01 o -14 3 1 4439.60 4913.73 138.15 o -13 3 1 182.16 201.37 48.46 o -12 3 1 6560.58 6857.40 166.11 o -11 3 1 10894.86 10971.61 261.45 o -10 3 1 5913.42 5872.19 119.86 o -9 3 1 6218.53 6175.90 108.99 o -8 3 1 7016.20 7152.90 142.75 o -7 3 1 55344.75 57366.66 659.73 o -6 3 1 5690.29 5459.74 93.56 o -5 3 1 3102.13 2968.60 87.77 o -4 3 1 10236.15 10691.08 165.40 o -3 3 1 29308.76 29493.68 315.15 o -2 3 1 18151.03 19718.60 211.92 o -1 3 1 72737.62 78634.12 898.50 o 0 3 1 25822.03 27100.41 302.64 o 1 3 1 21519.20 21841.01 281.85 o 2 3 1 10181.25 10901.56 129.59 o 3 3 1 78852.71 81974.34 901.55 o 4 3 1 35219.96 35301.25 399.95 o 5 3 1 583.38 728.54 48.45 o 6 3 1 1247.48 1321.98 66.73 o 7 3 1 22688.00 22560.58 276.96 o 8 3 1 2615.15 2622.00 102.93 o 9 3 1 65.72 57.98 25.14 o 10 3 1 6204.30 6199.61 224.94 o 11 3 1 18062.50 18999.09 495.61 o 12 3 1 775.64 746.18 53.56 o 13 3 1 1124.59 1064.82 83.04 o 14 3 1 2217.77 2322.67 112.47 o 15 3 1 7245.85 7200.45 196.07 o -15 4 1 0.81 -42.97 71.24 o -14 4 1 4521.44 4609.33 171.06 o -13 4 1 1486.52 1601.38 74.06 o -12 4 1 6178.76 6734.54 131.16 o -11 4 1 62.64 34.04 44.65 o -10 4 1 29702.39 30706.54 385.54 o -9 4 1 601.87 610.79 40.87 o -8 4 1 8189.52 8129.30 126.74 o -7 4 1 2227.26 2275.92 55.83 o -6 4 1 47803.03 46369.11 571.26 o -5 4 1 3251.49 3733.27 63.38 o -4 4 1 11774.56 12207.35 143.31 o -3 4 1 947.84 1090.18 25.64 o -2 4 1 50251.82 51957.85 602.92 o -1 4 1 893.33 859.44 18.48 o 0 4 1 487.15 508.56 21.00 o 1 4 1 9321.40 9965.09 127.08 o 2 4 1 75385.58 80607.18 835.29 o 3 4 1 493.93 546.80 20.07 o 4 4 1 3436.52 3042.33 63.37 o 5 4 1 281.97 452.02 40.44 o 6 4 1 59751.64 61453.41 1354.29 o 7 4 1 11094.49 11794.14 165.26 o 8 4 1 32626.75 33818.20 741.18 o 9 4 1 574.90 544.67 36.36 o 10 4 1 6756.75 6691.05 119.21 o 11 4 1 2155.24 2175.74 72.09 o 12 4 1 15302.50 15775.00 229.70 o 13 4 1 280.55 292.95 61.94 o 14 4 1 3176.89 3326.31 128.08 o 15 4 1 907.13 846.46 118.50 o -15 5 1 5740.81 6101.58 193.39 o -14 5 1 925.99 828.61 77.88 o -13 5 1 306.44 398.35 68.61 o -12 5 1 1879.92 2044.17 92.08 o -11 5 1 26386.32 27515.54 389.96 o -10 5 1 19.11 -42.28 42.28 o -9 5 1 3708.84 3746.81 91.00 o -8 5 1 1490.96 1412.76 54.11 o -7 5 1 39960.52 40331.26 731.45 o -6 5 1 6.26 16.56 17.38 o -5 5 1 30526.49 31550.62 345.95 o -4 5 1 3338.95 3650.20 54.85 o -3 5 1 64573.10 64055.51 669.77 o -2 5 1 149.78 115.13 16.02 o -1 5 1 31739.74 32953.77 350.65 o 0 5 1 3935.58 4124.14 63.61 o 1 5 1 23102.39 23350.11 253.04 o 2 5 1 2072.19 2018.24 35.26 o 3 5 1 32944.79 33748.73 362.26 o 4 5 1 3446.90 3434.03 54.51 o 5 5 1 13881.14 14751.51 174.45 o 6 5 1 12786.41 13228.95 162.08 o 7 5 1 52895.67 53767.94 579.74 o 8 5 1 146.30 168.62 26.09 o 9 5 1 248.73 288.14 31.00 o 10 5 1 3214.34 3135.70 88.23 o 11 5 1 23378.01 24198.95 318.15 o 12 5 1 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