#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:57:28 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181206 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/85/2228541.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228541_Fobs loop_ _publ_author_name 'Zhu, Chengchen' 'Yang, Liguo' 'Li, Dacheng' _publ_section_title ; [1,1'-Bis(diphenylphosphanyl)ferrocene-\k^2^P,P']dichloridocadmium(II) dichloromethane disolvate ; _journal_coeditor_code RZ2517 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1586 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.349 _cell_angle_gamma 90.000 _cell_length_a 9.8114 _cell_length_b 23.5939 _cell_length_c 17.6058 _exptl_crystal_F_000 1816.00 _reflns_d_resolution_high 0.8403 _cod_data_source_file rz2517Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 090915c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 275.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 45389.41 51783.75 1704.52 o 3 0 0 17117.27 18259.39 806.22 o 4 0 0 17707.85 19324.70 616.30 o 5 0 0 523.44 508.92 85.54 o 6 0 0 1471.87 1564.49 102.37 o 7 0 0 18686.31 17610.74 684.29 o 8 0 0 3790.13 4446.41 355.04 o 9 0 0 1112.58 801.33 280.99 o 10 0 0 1118.48 927.52 374.57 o 11 0 0 464.10 402.67 303.32 o 2 1 0 39649.88 43880.32 710.47 o 4 1 0 25241.94 28122.15 716.71 o 5 1 0 25.90 -66.59 44.39 o 6 1 0 16008.30 15878.03 223.00 o 7 1 0 4263.91 4820.06 236.61 o 8 1 0 844.31 678.95 164.44 o 9 1 0 293.70 316.52 337.94 o 10 1 0 158.35 -10.60 167.64 o 11 1 0 218.79 469.56 390.75 o 1 2 0 6946.32 5647.49 1186.04 o 2 2 0 4112.29 4518.22 133.61 o 3 2 0 10365.21 10790.84 404.42 o 4 2 0 9595.81 10666.50 195.65 o 5 2 0 5224.28 5519.74 197.52 o 6 2 0 140.12 176.55 99.72 o 7 2 0 3890.43 3966.87 174.53 o 8 2 0 1249.64 1408.01 203.74 o 9 2 0 292.28 538.87 185.80 o 10 2 0 381.08 183.07 198.82 o 11 2 0 23.30 41.38 178.45 o 1 3 0 4639.82 4760.05 274.89 o 2 3 0 74038.87 76015.30 3248.23 o 3 3 0 12154.75 11616.36 248.54 o 4 3 0 5682.09 5636.63 273.87 o 5 3 0 2223.22 2654.39 187.91 o 6 3 0 118.48 229.59 87.22 o 7 3 0 192.28 199.25 77.18 o 8 3 0 931.51 804.46 188.97 o 9 3 0 131.78 93.22 158.79 o 10 3 0 0.10 186.18 230.96 o 11 3 0 19.94 186.03 246.74 o 1 4 0 24759.20 21350.79 5506.19 o 2 4 0 5061.36 5492.36 296.87 o 3 4 0 1687.96 2070.07 453.85 o 4 4 0 3341.84 3626.46 123.29 o 5 4 0 11409.85 12403.32 297.93 o 6 4 0 4170.09 4232.56 140.94 o 7 4 0 1917.44 1976.18 135.45 o 8 4 0 2.39 -57.32 182.87 o 9 4 0 14.03 -51.54 207.88 o 10 4 0 251.50 101.27 234.15 o 11 4 0 395.94 337.55 259.48 o 1 5 0 0.87 231.27 86.21 o 2 5 0 3213.40 3346.92 592.79 o 3 5 0 32132.10 30098.78 4452.51 o 4 5 0 26478.89 27224.79 632.63 o 5 5 0 5567.39 5268.70 164.08 o 6 5 0 2779.56 2901.40 105.70 o 7 5 0 5529.01 6401.52 193.24 o 8 5 0 4244.43 3159.42 670.68 o 9 5 0 25.89 -37.98 149.95 o 10 5 0 77.44 87.31 195.80 o 11 5 0 204.86 -33.79 192.69 o 1 6 0 9407.56 7295.45 1982.84 o 2 6 0 217.57 203.40 76.83 o 3 6 0 11039.62 11535.21 459.10 o 4 6 0 261.73 254.62 72.81 o 5 6 0 1221.55 1252.58 131.10 o 6 6 0 838.24 925.13 123.25 o 7 6 0 5180.16 5273.95 233.01 o 8 6 0 1705.15 1880.77 137.47 o 9 6 0 97.29 -87.57 216.32 o 10 6 0 1386.11 1560.57 240.74 o 11 6 0 690.86 623.71 222.44 o 2 7 0 6564.30 6830.39 140.13 o 4 7 0 24331.14 24692.09 1319.80 o 5 7 0 312.95 471.49 69.11 o 6 7 0 5769.06 6776.65 218.69 o 7 7 0 236.84 232.72 85.94 o 8 7 0 340.28 315.16 104.39 o 9 7 0 851.67 773.87 164.54 o 10 7 0 16.99 4.63 173.41 o 11 7 0 523.46 670.93 278.20 o 1 8 0 5527.35 5374.51 273.68 o 2 8 0 8134.47 8514.28 574.51 o 3 8 0 21872.36 19742.95 2705.19 o 4 8 0 1754.06 1957.44 87.58 o 5 8 0 16414.26 16852.87 505.63 o 6 8 0 477.99 626.59 122.67 o 7 8 0 2493.94 2291.65 117.87 o 8 8 0 1768.99 1727.09 140.03 o 9 8 0 268.72 353.72 179.91 o 10 8 0 312.77 298.10 177.26 o 11 8 0 149.50 206.67 227.34 o 1 9 0 32653.58 24560.56 5647.77 o 2 9 0 39787.07 39777.51 932.48 o 3 9 0 277.92 746.68 205.40 o 4 9 0 20.69 126.93 150.26 o 6 9 0 907.77 979.05 124.95 o 7 9 0 142.56 -56.49 101.09 o 8 9 0 1480.77 1263.05 128.92 o 9 9 0 3217.74 3190.42 278.32 o 10 9 0 200.89 173.94 210.68 o 11 9 0 112.34 180.34 188.74 o 1 10 0 5848.74 3986.63 1272.26 o 2 10 0 19768.46 19758.66 645.45 o 3 10 0 53.70 63.05 62.92 o 4 10 0 4928.70 4978.66 457.14 o 5 10 0 3279.30 3158.96 156.98 o 6 10 0 2319.86 2406.16 161.90 o 7 10 0 19.47 56.51 126.29 o 8 10 0 100.32 117.80 100.39 o 9 10 0 16.07 18.62 147.45 o 10 10 0 1.52 162.44 189.78 o 1 11 0 3641.15 3193.85 142.24 o 2 11 0 2546.22 2686.47 194.01 o 3 11 0 60.03 12.67 68.11 o 4 11 0 459.74 513.43 78.36 o 5 11 0 932.65 1017.07 129.89 o 6 11 0 547.43 544.27 133.64 o 7 11 0 8.24 -84.90 100.27 o 8 11 0 411.63 489.68 125.48 o 9 11 0 648.12 477.12 117.99 o 10 11 0 99.44 205.99 198.06 o 0 12 0 3747.65 3895.93 210.49 o 2 12 0 421.77 337.72 66.89 o 3 12 0 243.17 152.45 70.51 o 4 12 0 1113.06 1116.55 80.31 o 5 12 0 204.21 454.05 104.35 o 6 12 0 0.47 40.72 100.29 o 7 12 0 955.96 801.09 148.73 o 8 12 0 1133.62 1470.18 141.20 o 9 12 0 167.42 192.42 120.95 o 10 12 0 0.73 -123.49 204.95 o 1 13 0 14159.79 14663.79 386.27 o 2 13 0 7863.54 8140.92 552.66 o 3 13 0 8.31 5.22 63.87 o 4 13 0 2663.43 2909.56 167.41 o 5 13 0 413.82 377.69 104.53 o 6 13 0 14.13 137.85 118.73 o 7 13 0 369.95 404.60 134.58 o 8 13 0 154.67 140.06 86.99 o 9 13 0 466.30 427.47 132.73 o 10 13 0 3.30 -54.45 208.38 o 0 14 0 1942.55 1630.52 291.78 o 2 14 0 6949.12 6803.71 307.13 o 3 14 0 3354.18 3158.28 145.63 o 4 14 0 2143.08 1786.40 105.38 o 5 14 0 6939.51 6853.87 229.97 o 6 14 0 1105.85 1148.77 156.05 o 7 14 0 295.04 95.41 137.65 o 8 14 0 581.85 651.84 123.89 o 9 14 0 3.76 128.84 118.49 o 10 14 0 46.28 -243.11 432.53 o 1 15 0 11206.13 10232.27 723.19 o 2 15 0 4015.40 3895.74 164.73 o 3 15 0 88.29 2.17 71.15 o 4 15 0 332.35 207.06 113.51 o 5 15 0 14.75 -18.82 101.71 o 6 15 0 2646.33 2565.08 183.81 o 7 15 0 521.90 330.23 137.86 o 8 15 0 591.83 621.50 111.47 o 9 15 0 1126.50 1108.79 168.88 o 0 16 0 3867.69 3795.73 219.44 o 1 16 0 512.23 556.58 81.02 o 2 16 0 4961.45 5230.41 166.70 o 3 16 0 1219.15 1171.12 91.19 o 4 16 0 23.74 -75.44 89.33 o 5 16 0 3585.22 3697.54 194.51 o 6 16 0 620.97 722.66 170.61 o 7 16 0 330.54 367.85 150.77 o 8 16 0 5.06 117.52 155.52 o 9 16 0 41.80 73.68 130.15 o 1 17 0 3618.60 3413.04 148.01 o 2 17 0 1671.97 2077.26 123.12 o 3 17 0 122.47 -41.79 84.65 o 4 17 0 872.79 785.10 134.52 o 5 17 0 20.93 -55.46 139.83 o 6 17 0 1077.94 1204.35 191.51 o 7 17 0 249.08 97.67 173.36 o 8 17 0 88.59 133.66 160.06 o 9 17 0 332.40 401.13 158.86 o 0 18 0 30.40 -65.86 111.53 o 1 18 0 8.71 35.19 90.86 o 2 18 0 236.14 166.72 86.41 o 3 18 0 456.57 324.51 144.97 o 4 18 0 9.68 -111.54 138.81 o 5 18 0 0.68 129.76 149.57 o 6 18 0 480.91 647.49 179.17 o 7 18 0 1.48 -102.34 129.50 o 8 18 0 7.51 -122.07 157.68 o 1 19 0 1046.36 761.75 130.49 o 2 19 0 52.28 -0.81 109.01 o 3 19 0 73.21 -146.24 98.25 o 4 19 0 16.67 -82.29 290.02 o 5 19 0 0.29 -71.64 124.98 o 6 19 0 274.22 97.41 140.76 o 7 19 0 113.67 84.67 138.13 o 8 19 0 314.03 54.09 178.53 o 0 20 0 3704.43 3772.58 399.91 o 1 20 0 4.50 25.85 113.75 o 2 20 0 1701.04 1588.29 159.21 o 3 20 0 925.20 980.73 223.79 o 4 20 0 202.52 157.38 178.20 o 5 20 0 2624.36 2509.96 483.81 o 6 20 0 149.13 69.16 168.08 o 7 20 0 44.29 -132.87 151.34 o 8 20 0 30.65 0.44 164.89 o 1 21 0 1536.89 1621.39 188.56 o 2 21 0 1004.84 950.71 139.74 o 3 21 0 318.12 341.61 163.77 o 4 21 0 1388.67 1188.62 224.12 o 5 21 0 304.21 489.49 181.87 o 6 21 0 383.17 314.03 167.84 o 7 21 0 1.88 283.36 191.67 o 0 22 0 2587.87 2663.90 312.10 o 1 22 0 606.06 818.24 130.30 o 2 22 0 3213.82 3346.02 224.31 o 3 22 0 2058.49 2597.80 270.22 o 4 22 0 759.58 975.75 206.23 o 5 22 0 1152.33 1099.79 299.56 o 6 22 0 0.18 -19.01 146.32 o 7 22 0 158.73 181.98 153.77 o 1 23 0 1967.26 2230.23 404.18 o 2 23 0 818.64 888.77 147.16 o 3 23 0 1775.98 2362.19 289.06 o 4 23 0 1143.82 1592.30 258.08 o 5 23 0 185.36 53.51 173.53 o 6 23 0 675.97 677.96 251.22 o 0 24 0 2779.92 2898.23 345.72 o 1 24 0 242.90 294.90 163.06 o 2 24 0 826.81 844.69 145.76 o 3 24 0 634.85 645.25 201.51 o 4 24 0 33.11 313.95 202.76 o 5 24 0 261.99 222.46 241.23 o 6 24 0 16.41 20.88 178.81 o 1 25 0 489.21 720.24 185.11 o 2 25 0 14.24 34.95 181.85 o 3 25 0 485.15 723.28 299.81 o 4 25 0 193.71 52.02 151.70 o 5 25 0 102.66 -99.77 145.61 o 0 26 0 464.48 460.63 195.69 o 1 26 0 123.90 24.93 155.99 o 2 26 0 8.96 -171.86 211.25 o 3 26 0 16.06 165.25 159.51 o 4 26 0 17.59 -278.08 185.50 o 1 27 0 137.37 150.20 126.55 o 2 27 0 0.82 -231.07 207.48 o 3 27 0 0.77 -60.96 159.39 o 0 28 0 319.36 269.95 225.04 o -11 1 1 2.35 -211.64 187.91 o -10 1 1 84.44 -65.98 177.95 o -9 1 1 501.74 544.97 244.11 o -8 1 1 292.70 144.10 149.64 o -7 1 1 915.58 1162.15 108.95 o -6 1 1 105.96 289.83 111.55 o -5 1 1 2898.59 2866.33 84.93 o -4 1 1 13.70 -86.73 57.82 o -2 1 1 2359.56 2157.27 116.50 o -1 1 1 1543.25 1687.86 93.08 o 0 1 1 18974.14 12634.19 4309.27 o 1 1 1 21875.38 22261.75 951.49 o 2 1 1 97.55 56.01 95.58 o 3 1 1 9590.43 10350.75 377.64 o 4 1 1 21.95 120.81 72.79 o 5 1 1 3665.48 3820.95 135.82 o 6 1 1 310.02 313.25 100.42 o 8 1 1 552.38 514.39 152.15 o 9 1 1 0.75 77.49 163.84 o 10 1 1 101.97 -253.40 169.99 o 11 1 1 318.20 154.11 190.46 o -11 2 1 358.19 630.00 240.22 o -10 2 1 487.55 562.39 247.77 o -9 2 1 477.58 438.12 219.37 o -8 2 1 2004.43 1738.52 215.34 o -7 2 1 3946.73 3995.23 224.10 o -6 2 1 13186.41 13705.68 231.24 o -4 2 1 18994.19 19648.45 414.34 o -3 2 1 43828.52 46749.13 562.87 o -2 2 1 25918.12 28893.48 1214.32 o -1 2 1 2147.43 1809.77 93.52 o 0 2 1 2428.64 2307.60 86.80 o 1 2 1 395.21 404.81 56.15 o 3 2 1 12686.37 14114.34 601.28 o 4 2 1 26647.20 29004.61 319.31 o 5 2 1 4976.22 4998.73 103.67 o 6 2 1 275.05 235.76 45.10 o 7 2 1 11872.57 12857.75 236.45 o 8 2 1 3088.65 3140.95 252.33 o 9 2 1 196.16 75.98 149.59 o 10 2 1 47.06 -31.34 234.68 o 11 2 1 2.01 463.68 271.95 o -11 3 1 23.32 -20.19 243.12 o -10 3 1 1416.48 1544.53 284.73 o -9 3 1 1341.62 1204.92 187.47 o -8 3 1 1808.08 1583.54 210.94 o -7 3 1 8681.73 8639.24 235.73 o -6 3 1 1355.90 1468.37 76.58 o -5 3 1 2578.87 2669.20 95.54 o -4 3 1 5796.27 6330.36 385.18 o -3 3 1 232.37 169.03 46.34 o -2 3 1 13609.48 13997.79 456.12 o -1 3 1 37778.81 41785.49 912.14 o 1 3 1 58414.88 43727.51 12147.74 o 2 3 1 22324.09 25259.24 2007.57 o 3 3 1 5573.28 5373.38 232.97 o 4 3 1 27130.22 29782.00 852.51 o 5 3 1 867.61 899.50 164.97 o 6 3 1 29.43 -95.20 75.30 o 7 3 1 2875.50 2950.14 125.62 o 8 3 1 2055.48 1955.88 205.67 o 9 3 1 393.15 288.21 166.26 o 10 3 1 522.84 264.89 189.99 o 11 3 1 2079.24 2389.91 343.48 o -11 4 1 1058.23 1097.59 266.20 o -10 4 1 81.19 199.42 233.28 o -9 4 1 637.51 685.89 186.92 o -8 4 1 4164.46 4040.39 290.20 o -7 4 1 2.53 129.74 111.38 o -6 4 1 13389.82 13075.51 165.08 o -5 4 1 2728.66 2777.94 219.76 o -4 4 1 17365.81 19097.57 436.11 o -3 4 1 12309.26 13832.98 377.35 o -2 4 1 11642.36 12708.14 627.39 o -1 4 1 15499.73 16608.67 762.84 o 0 4 1 8404.35 4587.70 2577.31 o 1 4 1 51535.17 49803.63 1228.03 o 2 4 1 1781.96 1675.93 69.12 o 3 4 1 626.25 1304.50 257.45 o 4 4 1 10165.57 11350.30 333.51 o 5 4 1 502.76 494.03 113.55 o 6 4 1 2668.24 2425.08 137.16 o 7 4 1 1899.55 1768.43 118.63 o 8 4 1 2049.68 1804.24 216.92 o 9 4 1 55.70 -38.27 136.98 o 10 4 1 679.89 500.03 218.07 o 11 4 1 0.14 152.76 188.19 o -11 5 1 1.12 290.07 214.75 o -10 5 1 984.49 1046.14 266.95 o -9 5 1 81.54 98.28 160.06 o -8 5 1 2045.99 2093.93 138.55 o -7 5 1 4002.68 3993.06 161.97 o -6 5 1 831.66 925.85 92.97 o -5 5 1 20901.21 21623.31 864.12 o -4 5 1 6833.38 6628.32 211.10 o -3 5 1 25380.01 26745.39 547.43 o -2 5 1 11580.21 12410.73 754.18 o -1 5 1 107.61 137.56 47.01 o 0 5 1 3396.92 3257.88 90.13 o 1 5 1 70568.68 67451.26 1767.45 o 2 5 1 1193.58 1319.69 175.42 o 3 5 1 6519.14 5870.81 999.64 o 4 5 1 2098.98 2492.04 295.55 o 5 5 1 450.24 582.51 114.98 o 6 5 1 54.63 -60.94 100.60 o 8 5 1 938.61 430.62 177.59 o 9 5 1 838.90 514.39 159.35 o 10 5 1 257.18 425.12 203.27 o 11 5 1 995.87 906.69 253.72 o -11 6 1 462.34 520.72 273.87 o -10 6 1 29.45 -29.41 180.77 o -9 6 1 881.60 951.20 179.99 o -8 6 1 3455.82 3540.82 170.58 o -7 6 1 839.25 858.58 147.02 o -6 6 1 1659.49 1638.42 175.56 o -5 6 1 6103.21 6369.83 191.66 o -4 6 1 378.54 411.48 56.85 o -3 6 1 1264.26 1395.25 158.74 o -2 6 1 4823.26 4795.71 327.08 o -1 6 1 3072.90 2899.82 69.36 o 0 6 1 5355.57 2871.66 1838.79 o 1 6 1 9794.80 7018.25 1905.38 o 2 6 1 28573.63 29622.29 1215.47 o 3 6 1 156.55 67.53 40.75 o 4 6 1 5890.97 6294.35 202.82 o 5 6 1 0.07 43.71 82.24 o 6 6 1 1505.12 1347.82 133.50 o 7 6 1 17.16 82.92 109.11 o 8 6 1 340.97 106.26 108.38 o 9 6 1 156.09 80.14 218.11 o 10 6 1 1149.58 1215.69 213.11 o 11 6 1 85.79 41.11 246.08 o -11 7 1 111.27 113.47 215.17 o -10 7 1 28.13 18.06 180.38 o -9 7 1 116.72 145.55 177.53 o -8 7 1 1418.67 1383.03 150.28 o -7 7 1 127.74 39.96 90.93 o -6 7 1 6264.37 6625.17 190.92 o -5 7 1 1792.60 1943.99 109.41 o -4 7 1 3077.76 3174.69 116.52 o -3 7 1 1204.14 1381.06 77.63 o -2 7 1 9668.12 9296.80 303.00 o -1 7 1 237.96 12.27 158.56 o 0 7 1 8703.77 7004.23 2373.35 o 1 7 1 9124.84 8829.01 205.79 o 2 7 1 2072.22 2123.12 119.32 o 3 7 1 2099.29 2134.99 122.25 o 4 7 1 10463.32 10649.07 221.76 o 5 7 1 3695.09 3868.88 231.87 o 6 7 1 4045.46 3958.36 195.83 o 7 7 1 615.06 566.44 149.83 o 8 7 1 135.23 79.71 93.80 o 9 7 1 52.35 33.25 139.37 o 10 7 1 186.96 197.76 169.51 o 11 7 1 66.80 -25.23 243.60 o -11 8 1 0.04 20.00 215.31 o -10 8 1 34.29 63.68 192.16 o -9 8 1 1.27 19.95 139.17 o -8 8 1 265.21 219.70 106.39 o -7 8 1 2.02 -15.85 106.27 o -6 8 1 165.39 221.36 72.44 o -5 8 1 4495.55 4512.03 183.51 o -4 8 1 1614.12 1780.18 90.66 o -3 8 1 16066.96 16796.25 510.68 o -1 8 1 3703.60 4316.07 268.15 o 0 8 1 221.36 194.14 59.42 o 1 8 1 1134.59 868.19 183.74 o 2 8 1 215.84 457.11 124.43 o 3 8 1 3139.14 2898.84 122.29 o 4 8 1 12720.27 11838.13 242.37 o 5 8 1 384.98 345.58 118.54 o 6 8 1 2894.93 2723.38 167.01 o 7 8 1 3576.38 3792.85 216.32 o 8 8 1 407.70 334.34 93.33 o 9 8 1 660.86 439.09 182.10 o 10 8 1 265.58 211.44 176.03 o 11 8 1 169.16 32.77 166.81 o -11 9 1 71.43 244.16 225.93 o -10 9 1 65.64 227.55 203.16 o -9 9 1 707.30 1011.61 205.84 o -8 9 1 124.01 277.16 110.23 o -7 9 1 669.66 749.33 116.74 o -6 9 1 1870.28 1724.63 151.48 o -5 9 1 392.60 523.56 126.00 o -4 9 1 12168.43 12419.70 335.32 o -3 9 1 378.02 736.56 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