#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/85/2228549.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228549_Fobs loop_ _publ_author_name 'Wu, Dayu' 'Zhao, Yan' 'Ye, Hui' 'Wu, Genhua' _publ_section_title ; Bis[4-chloro-N'-(2-pyridylmethylidene)benzohydrazidato]cobalt(III) nitrate sesquihydrate ; _journal_coeditor_code SI2290 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1568 _journal_page_last m1569 _journal_volume 66 _journal_year 2010 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yac' _symmetry_space_group_name_H-M 'P 1 2/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.196 _cell_angle_gamma 90.000 _cell_length_a 14.1978 _cell_length_b 10.8758 _cell_length_c 18.5534 _exptl_crystal_F_000 1356.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file si2290Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tt in P2/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 489.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1964.68 1354.17 55.35 o 4 0 0 239873.55 244314.23 3477.84 o 6 0 0 982.28 1767.16 87.41 o 8 0 0 39815.91 40024.49 722.07 o 10 0 0 835.66 594.93 59.09 o 12 0 0 8207.76 7657.51 268.54 o 14 0 0 18.01 32.41 31.92 o 1 1 0 18124.91 15954.08 778.69 o 2 1 0 625.29 643.30 31.67 o 3 1 0 27661.68 25557.18 491.15 o 4 1 0 59686.19 62129.32 762.71 o 5 1 0 1626.47 2019.16 39.11 o 6 1 0 1.76 4.42 7.83 o 7 1 0 18240.35 17833.94 238.36 o 8 1 0 16523.36 16416.80 224.71 o 9 1 0 2689.31 2720.68 72.66 o 10 1 0 406.32 468.85 25.08 o 11 1 0 1363.67 1462.88 43.64 o 12 1 0 1399.26 1499.68 65.20 o 13 1 0 759.83 872.57 58.86 o 14 1 0 482.93 421.67 47.25 o 15 1 0 919.17 884.92 68.07 o 16 1 0 238.21 287.94 89.01 o 0 2 0 2076.46 1461.89 45.38 o 1 2 0 5622.62 7242.73 131.44 o 2 2 0 281.53 205.03 14.47 o 3 2 0 8931.17 10110.00 134.00 o 4 2 0 3459.56 3463.49 55.81 o 5 2 0 3126.96 3361.49 56.86 o 6 2 0 2103.91 1686.95 75.43 o 7 2 0 1047.08 1035.20 55.38 o 8 2 0 939.28 830.87 33.69 o 9 2 0 37.53 37.40 13.50 o 10 2 0 1.01 23.81 11.88 o 11 2 0 836.64 733.27 43.40 o 12 2 0 12.97 10.39 13.63 o 13 2 0 0.28 0.00 13.70 o 14 2 0 11.70 37.42 19.51 o 15 2 0 105.33 54.53 28.83 o 16 2 0 11.65 31.10 29.69 o 0 3 0 3664.73 3186.19 89.01 o 1 3 0 2620.42 2432.81 41.06 o 2 3 0 148.15 156.92 15.01 o 3 3 0 4186.15 3787.72 58.82 o 4 3 0 200.51 162.67 11.40 o 5 3 0 2660.81 2684.79 49.56 o 6 3 0 57.21 53.80 10.33 o 7 3 0 2405.45 2137.35 68.63 o 8 3 0 949.58 938.70 36.62 o 9 3 0 810.83 768.83 36.89 o 10 3 0 309.24 273.10 21.61 o 11 3 0 90.49 87.18 17.77 o 12 3 0 642.74 516.14 30.50 o 13 3 0 161.49 281.94 25.74 o 14 3 0 64.88 55.74 21.54 o 15 3 0 108.08 136.89 51.61 o 16 3 0 10.15 56.85 46.63 o 0 4 0 21367.37 23732.39 422.11 o 1 4 0 10063.39 10746.88 142.89 o 2 4 0 933.85 856.65 23.17 o 3 4 0 5004.01 4801.06 86.59 o 4 4 0 4961.50 5034.62 92.53 o 5 4 0 449.43 385.21 17.59 o 6 4 0 709.51 773.45 26.49 o 7 4 0 2196.04 2039.81 46.15 o 8 4 0 2359.76 2666.97 57.25 o 9 4 0 350.47 423.58 24.44 o 10 4 0 22.16 24.84 13.98 o 11 4 0 508.37 561.77 31.04 o 12 4 0 47.25 56.40 30.67 o 13 4 0 50.58 95.93 28.86 o 14 4 0 23.40 73.00 29.92 o 15 4 0 0.32 0.00 27.29 o 16 4 0 353.83 346.58 77.05 o 0 5 0 7887.52 7316.91 219.42 o 1 5 0 5686.72 5415.52 80.96 o 2 5 0 229.15 198.07 11.60 o 3 5 0 220.16 251.86 15.40 o 4 5 0 8103.17 8205.89 152.29 o 5 5 0 82.97 65.63 9.86 o 6 5 0 38.76 36.55 10.24 o 7 5 0 1166.09 1069.82 37.03 o 8 5 0 6750.65 6535.32 157.88 o 9 5 0 1307.03 1263.83 49.99 o 10 5 0 40.90 22.61 17.57 o 11 5 0 458.80 421.78 44.92 o 12 5 0 1343.65 1420.75 75.71 o 13 5 0 219.18 232.75 39.58 o 14 5 0 37.44 7.82 26.03 o 15 5 0 123.76 74.00 32.78 o 0 6 0 2.78 22.15 13.96 o 1 6 0 2436.29 2947.85 52.72 o 2 6 0 75.51 61.87 9.68 o 3 6 0 1576.22 1631.34 46.34 o 4 6 0 228.29 216.29 49.74 o 5 6 0 3791.23 4180.91 113.27 o 6 6 0 22.14 12.62 13.56 o 7 6 0 1731.98 1869.61 58.58 o 8 6 0 4494.61 4512.54 215.69 o 9 6 0 282.22 288.98 29.37 o 10 6 0 1.03 0.00 27.05 o 11 6 0 295.99 385.98 47.32 o 12 6 0 499.06 525.32 53.96 o 13 6 0 316.77 444.54 53.28 o 14 6 0 73.00 93.81 37.01 o 0 7 0 7132.63 6673.88 201.97 o 1 7 0 2226.69 2049.56 54.70 o 2 7 0 5.04 5.60 9.17 o 3 7 0 89.01 102.46 16.57 o 4 7 0 2791.64 2709.07 60.45 o 5 7 0 1084.36 1226.44 104.65 o 6 7 0 99.12 87.92 18.85 o 7 7 0 900.35 1017.84 64.83 o 8 7 0 1123.55 1215.30 54.36 o 9 7 0 8.56 20.10 23.07 o 10 7 0 20.17 0.00 21.15 o 11 7 0 167.48 214.55 39.97 o 12 7 0 330.67 465.08 54.76 o 13 7 0 23.11 0.00 29.42 o 14 7 0 59.92 107.07 38.87 o 0 8 0 306.06 349.83 47.37 o 1 8 0 1624.16 1692.59 66.40 o 2 8 0 189.66 189.57 19.95 o 3 8 0 1831.62 1849.95 55.05 o 4 8 0 5.32 19.22 13.00 o 5 8 0 638.01 590.30 32.89 o 6 8 0 48.41 39.78 15.07 o 7 8 0 1820.42 1771.47 61.79 o 8 8 0 415.95 457.38 46.72 o 9 8 0 789.60 667.89 55.15 o 10 8 0 47.77 67.66 61.84 o 11 8 0 298.18 432.49 52.45 o 12 8 0 14.82 38.91 31.81 o 13 8 0 162.61 113.94 39.56 o 0 9 0 1703.45 1507.02 93.25 o 1 9 0 43.18 21.19 25.43 o 2 9 0 123.56 178.28 42.39 o 3 9 0 363.11 281.04 42.66 o 4 9 0 308.05 334.44 32.02 o 5 9 0 1.32 0.00 13.31 o 6 9 0 8.01 5.82 13.56 o 7 9 0 32.54 19.95 17.48 o 8 9 0 385.89 473.30 53.14 o 9 9 0 8.29 42.48 21.02 o 10 9 0 9.55 0.00 31.79 o 11 9 0 38.55 68.71 33.54 o 12 9 0 342.31 337.34 53.95 o 0 10 0 1.71 0.00 27.68 o 1 10 0 39.20 87.46 26.94 o 2 10 0 52.86 25.52 30.17 o 3 10 0 275.95 319.72 33.53 o 4 10 0 1569.01 1361.16 81.57 o 5 10 0 25.71 7.33 21.25 o 6 10 0 37.85 55.66 26.60 o 7 10 0 133.59 118.69 38.90 o 8 10 0 57.91 36.15 26.45 o 9 10 0 156.86 202.80 32.91 o 10 10 0 31.42 32.76 24.89 o 0 11 0 699.73 798.89 82.78 o 1 11 0 1.90 12.27 22.48 o 2 11 0 1.30 0.36 22.04 o 3 11 0 62.11 62.82 22.94 o 4 11 0 1584.06 1793.81 89.65 o 5 11 0 20.14 29.22 27.62 o 6 11 0 5.62 2.54 23.62 o 7 11 0 6.58 0.00 23.68 o 8 11 0 401.31 470.71 57.97 o 0 12 0 28.96 64.83 41.39 o 1 12 0 268.21 240.62 94.38 o 2 12 0 3.08 14.27 22.70 o 3 12 0 430.98 440.89 55.10 o 4 12 0 15.47 18.31 29.31 o 5 12 0 247.54 260.69 142.00 o 6 12 0 1.20 18.05 34.16 o -15 0 1 672.09 674.72 83.78 o -13 0 1 1224.67 1170.66 90.51 o -11 0 1 2709.55 2700.61 131.90 o -9 0 1 3081.07 2968.15 127.66 o -7 0 1 11323.90 12974.88 255.02 o -5 0 1 547.72 563.77 26.98 o -3 0 1 5.73 140.89 50.62 o -1 0 1 9055.37 8349.93 210.69 o 1 0 1 19004.79 23833.99 582.21 o 3 0 1 2938.69 2641.18 79.54 o 5 0 1 33647.08 33054.45 479.94 o 7 0 1 17494.96 17125.32 264.29 o 9 0 1 19921.68 18592.60 359.27 o 11 0 1 1412.79 1487.07 93.50 o 13 0 1 3801.38 3773.28 172.29 o 15 0 1 87.28 240.61 58.84 o -16 1 1 65.72 48.85 77.17 o -15 1 1 11.49 1.75 25.38 o -14 1 1 665.68 634.84 54.29 o -13 1 1 4.64 0.00 20.51 o -12 1 1 711.05 788.87 41.82 o -11 1 1 472.33 405.31 30.54 o -10 1 1 3027.57 3283.14 80.29 o -9 1 1 1244.87 1264.25 43.69 o -8 1 1 2081.29 1933.01 67.30 o -7 1 1 486.37 387.17 37.21 o -6 1 1 17112.10 16274.11 216.14 o -5 1 1 10720.25 10859.15 147.52 o -4 1 1 5769.49 4890.57 72.15 o -3 1 1 102.09 109.88 10.21 o -2 1 1 31264.05 30410.82 890.90 o -1 1 1 158.19 276.53 11.55 o 0 1 1 7401.09 5142.89 94.59 o 1 1 1 1422.83 817.08 49.49 o 2 1 1 22372.00 22412.97 391.12 o 3 1 1 3893.61 4496.32 75.72 o 4 1 1 297.23 321.60 31.42 o 5 1 1 656.54 800.29 22.54 o 6 1 1 22478.50 25068.27 323.00 o 7 1 1 455.56 498.48 21.66 o 8 1 1 971.01 1056.37 37.15 o 9 1 1 96.62 108.87 14.35 o 10 1 1 2592.62 2680.49 59.36 o 11 1 1 730.57 701.86 32.68 o 12 1 1 671.32 636.18 89.36 o 13 1 1 203.35 180.32 33.30 o 14 1 1 1174.88 1021.40 66.20 o 15 1 1 390.94 367.73 80.04 o 16 1 1 218.16 149.30 38.07 o -16 2 1 0.06 25.28 27.24 o -15 2 1 432.90 504.27 94.62 o -14 2 1 160.66 219.38 31.67 o -13 2 1 13.63 13.69 17.42 o -12 2 1 95.32 116.26 23.07 o -11 2 1 99.27 90.51 16.34 o -10 2 1 715.81 707.67 30.51 o -9 2 1 1240.03 1203.71 36.18 o -8 2 1 441.65 394.76 20.93 o -7 2 1 6842.16 7944.79 203.12 o -6 2 1 4503.73 4839.71 94.47 o -5 2 1 1373.51 1413.45 35.09 o -4 2 1 1026.84 999.00 24.28 o -3 2 1 6720.00 8085.45 155.31 o -2 2 1 12119.87 13161.05 195.45 o -1 2 1 6599.64 7172.34 114.14 o 0 2 1 25.61 3.28 4.11 o 1 2 1 28011.31 29991.46 735.31 o 2 2 1 10004.20 10967.76 162.92 o 3 2 1 9481.15 10486.40 138.96 o 4 2 1 3752.23 3935.16 61.92 o 5 2 1 6226.18 5642.90 85.37 o 6 2 1 4132.09 4235.09 70.56 o 7 2 1 320.92 491.07 21.58 o 8 2 1 1077.73 1236.37 54.42 o 9 2 1 1693.53 1544.77 49.38 o 10 2 1 2692.66 2897.00 62.98 o 11 2 1 19.98 21.86 17.60 o 12 2 1 45.94 64.76 16.54 o 13 2 1 287.36 338.87 27.06 o 14 2 1 335.00 333.01 42.58 o 15 2 1 118.68 193.82 38.57 o 16 2 1 38.71 44.30 34.41 o -16 3 1 7.67 0.00 40.64 o -15 3 1 42.75 89.06 31.73 o -14 3 1 168.66 170.06 28.85 o -13 3 1 68.30 72.00 22.29 o -12 3 1 37.38 50.32 19.42 o -11 3 1 2307.82 2792.19 64.90 o -10 3 1 322.46 311.96 22.69 o -9 3 1 43.47 45.44 12.75 o -8 3 1 582.50 590.82 25.23 o -7 3 1 18.81 22.88 11.68 o -6 3 1 4897.99 4892.13 96.49 o -5 3 1 410.99 445.84 18.19 o -4 3 1 13.37 0.00 7.85 o -3 3 1 1278.35 1519.30 57.04 o -2 3 1 516.75 583.89 15.11 o -1 3 1 358.72 296.43 12.27 o 0 3 1 49.56 108.66 7.95 o 1 3 1 3.09 25.48 11.84 o 2 3 1 832.27 916.04 57.72 o 3 3 1 2176.92 2353.81 48.33 o 4 3 1 301.79 307.94 18.10 o 5 3 1 1523.28 1305.27 34.09 o 6 3 1 3648.15 3916.40 67.68 o 7 3 1 1222.33 1157.66 38.51 o 8 3 1 137.81 98.22 15.99 o 9 3 1 2042.24 2125.78 52.66 o 10 3 1 404.66 377.38 24.26 o 11 3 1 90.72 118.77 31.35 o 12 3 1 6.73 3.48 13.45 o 13 3 1 197.67 225.39 24.11 o 14 3 1 121.16 138.13 51.86 o 15 3 1 14.01 0.00 36.90 o 16 3 1 2.12 77.05 48.12 o -16 4 1 19.88 0.00 27.06 o -15 4 1 337.17 332.85 46.84 o -14 4 1 200.33 110.29 33.82 o -13 4 1 136.60 186.32 36.50 o -12 4 1 33.20 9.34 17.07 o -11 4 1 1530.85 1466.73 55.53 o -10 4 1 333.33 387.84 25.30 o -9 4 1 235.23 192.15 18.93 o -8 4 1 0.31 14.54 10.07 o -7 4 1 3527.47 3804.25 88.57 o -6 4 1 319.23 351.58 21.73 o -5 4 1 402.21 500.46 28.04 o -4 4 1 1.23 3.06 6.95 o -3 4 1 3067.23 2972.09 50.57 o -2 4 1 4335.45 4589.95 63.16 o -1 4 1 2767.59 2523.94 45.28 o 0 4 1 2428.67 2153.28 37.70 o 1 4 1 4025.51 4917.35 86.95 o 2 4 1 326.98 359.24 12.56 o 3 4 1 4387.31 4156.98 72.46 o 4 4 1 756.18 615.30 27.29 o 5 4 1 745.00 610.94 21.33 o 6 4 1 218.46 354.62 18.53 o 7 4 1 1283.98 1107.69 59.74 o 8 4 1 400.86 415.02 27.36 o 9 4 1 3011.90 3181.30 66.74 o 10 4 1 376.63 431.89 38.43 o 11 4 1 19.88 37.00 18.03 o 12 4 1 1.13 0.00 17.50 o 13 4 1 292.32 351.53 70.69 o 14 4 1 157.28 178.82 38.73 o 15 4 1 1.07 17.95 42.64 o -15 5 1 184.23 244.89 44.92 o -14 5 1 593.67 621.39 59.24 o -13 5 1 18.17 59.72 29.51 o -12 5 1 21.94 62.56 28.44 o -11 5 1 476.61 495.34 47.97 o -10 5 1 1406.74 1543.39 72.64 o -9 5 1 262.75 316.15 34.85 o -8 5 1 494.30 490.60 26.63 o -7 5 1 2246.41 2231.07 49.62 o -6 5 1 1645.14 1458.57 37.86 o -5 5 1 1909.95 1763.56 51.97 o -4 5 1 2177.44 2175.90 50.51 o -3 5 1 3295.65 3154.01 50.32 o -2 5 1 14447.45 15726.08 206.89 o -1 5 1 529.33 500.42 28.04 o 0 5 1 6991.66 6880.49 98.77 o 1 5 1 12588.36 12209.71 163.58 o 2 5 1 7026.18 7076.30 114.38 o 3 5 1 4.64 0.00 9.94 o 4 5 1 4376.13 4674.89 93.75 o 5 5 1 3464.72 3596.72 63.53 o 6 5 1 737.86 757.68 43.27 o 7 5 1 550.40 571.61 73.80 o 8 5 1 1276.72 1286.44 48.19 o 9 5 1 352.60 506.34 34.37 o 10 5 1 422.49 403.87 33.29 o 11 5 1 633.48 698.44 41.50 o 12 5 1 548.82 605.28 54.62 o 13 5 1 493.58 570.01 55.44 o 14 5 1 252.79 254.48 44.15 o 15 5 1 153.80 154.34 58.84 o -14 6 1 369.87 405.27 55.78 o -13 6 1 2.29 5.27 25.81 o -12 6 1 78.06 119.59 35.08 o -11 6 1 4.15 5.22 21.95 o -10 6 1 893.64 903.68 96.12 o -9 6 1 396.61 335.99 39.71 o -8 6 1 1453.33 1521.40 53.40 o -7 6 1 564.64 596.78 44.52 o -6 6 1 6884.82 7156.11 135.24 o -5 6 1 687.03 757.13 54.57 o -4 6 1 2454.38 2459.02 63.24 o -3 6 1 2793.74 2523.05 44.84 o -2 6 1 4382.70 4169.55 74.21 o -1 6 1 2878.46 2913.61 52.36 o 0 6 1 5152.79 6002.47 90.65 o 1 6 1 9356.87 9588.23 134.81 o 2 6 1 4812.80 4810.23 94.26 o 3 6 1 19.61 30.17 13.78 o 4 6 1 3715.83 4139.92 88.95 o 5 6 1 225.46 194.57 58.47 o 6 6 1 4316.03 4321.33 147.28 o 7 6 1 2.08 16.91 15.05 o 8 6 1 1994.98 2043.02 75.91 o 9 6 1 142.94 171.15 26.35 o 10 6 1 657.14 690.08 42.28 o 11 6 1 21.03 13.96 65.70 o 12 6 1 215.15 213.23 40.25 o 13 6 1 106.03 132.70 38.15 o 14 6 1 354.28 404.35 53.75 o -14 7 1 34.64 0.00 27.62 o -13 7 1 338.74 336.78 62.34 o -12 7 1 38.36 47.52 61.09 o -11 7 1 625.83 666.78 87.27 o -10 7 1 138.54 203.64 37.59 o -9 7 1 94.40 94.43 28.11 o -8 7 1 58.09 77.49 50.49 o -7 7 1 4757.70 4871.77 107.58 o -6 7 1 119.64 117.84 17.22 o -5 7 1 521.88 512.49 32.33 o -4 7 1 108.11 121.48 17.92 o -3 7 1 1295.82 1502.79 48.37 o -2 7 1 165.90 134.04 22.94 o -1 7 1 1391.84 1404.40 33.75 o 0 7 1 86.20 50.34 12.64 o 1 7 1 1864.10 1622.01 46.67 o 2 7 1 38.59 58.05 14.82 o 3 7 1 1497.76 1600.65 53.45 o 4 7 1 64.66 49.87 12.96 o 5 7 1 3044.70 2827.11 90.95 o 6 7 1 179.50 160.96 23.96 o 7 7 1 1671.76 1667.34 73.09 o 8 7 1 342.18 341.45 32.46 o 9 7 1 599.45 646.49 41.52 o 10 7 1 33.13 32.16 26.01 o 11 7 1 41.46 42.71 34.66 o 12 7 1 12.76 1.82 26.65 o 13 7 1 283.54 296.34 47.24 o 14 7 1 34.28 73.82 36.48 o -13 8 1 0.16 12.86 32.73 o -12 8 1 25.68 50.81 31.62 o -11 8 1 0.38 0.00 26.69 o -10 8 1 723.20 695.90 73.06 o -9 8 1 17.73 0.00 22.54 o -8 8 1 5.90 6.92 16.21 o -7 8 1 1158.88 1274.61 53.75 o -6 8 1 973.14 1046.47 40.10 o -5 8 1 0.07 0.00 12.32 o -4 8 1 8.70 8.40 11.04 o -3 8 1 509.93 482.00 32.75 o -2 8 1 3000.01 2744.48 87.82 o -1 8 1 477.52 458.37 37.12 o 0 8 1 37.29 32.46 16.07 o 1 8 1 108.53 116.23 16.62 o 2 8 1 2653.74 2624.26 67.27 o 3 8 1 75.09 78.20 17.08 o 4 8 1 114.85 133.02 17.73 o 5 8 1 167.51 168.30 19.94 o 6 8 1 898.53 1049.20 95.44 o 7 8 1 402.33 407.38 33.92 o 8 8 1 79.81 166.93 32.92 o 9 8 1 2.11 11.80 23.00 o 10 8 1 286.87 291.34 45.88 o 11 8 1 72.18 112.60 34.04 o 12 8 1 58.74 72.60 47.75 o 13 8 1 0.87 41.74 32.50 o -12 9 1 0.10 40.14 33.32 o -11 9 1 55.68 46.92 22.87 o -10 9 1 2.97 0.00 17.95 o -9 9 1 104.12 95.73 23.99 o -8 9 1 82.69 105.47 24.93 o -7 9 1 116.04 119.54 24.57 o -6 9 1 0.21 0.00 15.98 o -5 9 1 192.82 171.36 35.54 o -4 9 1 185.20 195.05 25.70 o -3 9 1 2117.08 2149.17 69.04 o -2 9 1 148.90 168.68 28.78 o -1 9 1 410.84 488.96 61.59 o 0 9 1 76.56 43.39 28.42 o 1 9 1 2349.48 2164.93 99.36 o 2 9 1 45.04 3.74 26.93 o 3 9 1 0.98 13.46 28.18 o 4 9 1 5.50 8.34 13.37 o 5 9 1 706.57 790.98 37.55 o 6 9 1 58.77 62.96 18.28 o 7 9 1 1.05 0.00 15.00 o 8 9 1 6.87 0.00 22.04 o 9 9 1 425.67 530.32 54.31 o 10 9 1 60.48 31.54 27.69 o 11 9 1 53.11 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