#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/85/2228587.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228587_Fobs loop_ _publ_author_name 'Tsaryk, Natalia V.' 'Dudko, Anatolij V.' 'Kozachkova, Alexandra N.' 'Bon, Vladimir V.' 'Pekhnyo, Vasily I.' _publ_section_title ; trans-Bis[(1-ammoniopentane-1,1-diyl)diphosphonato-\k^2^O,O']diaquacopper(II) ; _journal_coeditor_code WM2420 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1533 _journal_page_last m1534 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.315 _cell_angle_beta 86.666 _cell_angle_gamma 88.398 _cell_length_a 5.5629 _cell_length_b 10.0236 _cell_length_c 10.5237 _exptl_crystal_F_000 307.00 _reflns_d_resolution_high 0.7920 _[local]_cod_data_source_file wm2420Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 94 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 101.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7245.20 7754.73 166.65 o 2 0 0 26.10 10.06 0.98 o 3 0 0 6.85 20.11 1.35 o 4 0 0 217.46 213.48 4.18 o 5 0 0 339.53 344.61 7.20 o 6 0 0 279.88 299.99 9.01 o 7 0 0 140.63 158.86 9.79 o -6 1 0 159.53 162.06 5.13 o -5 1 0 1783.07 1779.70 22.80 o -4 1 0 1048.91 1013.55 29.59 o -3 1 0 535.00 519.97 25.81 o -2 1 0 5905.84 6007.78 164.04 o -1 1 0 10306.05 10194.20 227.50 o 0 1 0 5336.48 5373.35 80.86 o 1 1 0 6.77 5.53 0.42 o 2 1 0 1958.80 2036.26 26.72 o 3 1 0 290.55 300.44 6.86 o 4 1 0 30.95 33.82 2.06 o 5 1 0 487.09 467.59 14.18 o 6 1 0 823.77 847.89 18.09 o -6 2 0 178.35 193.92 7.07 o -5 2 0 1013.89 1031.24 39.60 o -4 2 0 972.31 979.49 18.69 o -3 2 0 2531.45 2755.68 44.56 o -2 2 0 1717.53 1872.98 25.04 o -1 2 0 118.54 146.37 3.16 o 0 2 0 208.19 206.59 2.76 o 1 2 0 8092.21 8004.46 126.22 o 2 2 0 943.01 975.02 17.92 o 3 2 0 938.13 902.40 11.27 o 4 2 0 1424.38 1417.47 17.43 o 5 2 0 776.45 777.53 19.69 o 6 2 0 374.30 370.54 10.33 o -6 3 0 69.08 71.31 6.90 o -5 3 0 424.38 466.58 15.80 o -4 3 0 533.91 579.98 12.50 o -3 3 0 150.22 147.33 4.72 o -2 3 0 4.82 3.25 1.28 o -1 3 0 1470.20 1348.76 16.73 o 0 3 0 4730.77 4954.64 48.67 o 1 3 0 10365.07 10480.40 134.84 o 2 3 0 1968.87 2019.64 56.91 o 3 3 0 1496.46 1538.93 18.19 o 4 3 0 1.67 1.22 1.30 o 5 3 0 71.56 62.91 3.83 o 6 3 0 38.91 46.48 4.23 o -6 4 0 4.64 1.67 2.89 o -5 4 0 55.78 49.28 5.23 o -4 4 0 1530.85 1511.92 27.44 o -3 4 0 1763.66 1639.16 28.58 o -2 4 0 836.78 765.95 10.62 o -1 4 0 377.46 317.37 4.39 o 0 4 0 30.80 25.24 1.01 o 1 4 0 4849.08 5091.63 56.27 o 2 4 0 1223.36 1236.80 40.16 o 3 4 0 92.02 108.35 3.30 o 4 4 0 235.66 219.12 6.60 o 5 4 0 88.59 82.24 6.95 o 6 4 0 0.87 0.12 2.20 o -6 5 0 65.08 84.90 5.70 o -5 5 0 160.13 153.82 6.84 o -4 5 0 1545.00 1504.03 22.56 o -3 5 0 409.55 405.22 7.90 o -2 5 0 176.66 171.28 4.13 o -1 5 0 197.31 165.69 2.93 o 0 5 0 8.63 10.86 0.93 o 1 5 0 302.57 304.47 4.55 o 2 5 0 81.16 74.39 2.58 o 3 5 0 125.64 121.68 3.72 o 4 5 0 124.65 126.04 5.15 o 5 5 0 88.64 87.62 4.75 o 6 5 0 61.88 51.00 4.37 o -6 6 0 326.57 355.11 15.69 o -5 6 0 1.26 3.05 1.81 o -4 6 0 64.79 66.68 3.65 o -3 6 0 105.76 98.98 3.72 o -2 6 0 105.41 92.06 2.87 o -1 6 0 289.59 273.46 6.28 o 0 6 0 347.61 353.29 5.83 o 1 6 0 448.86 442.98 7.89 o 2 6 0 842.69 842.44 13.19 o 3 6 0 38.42 47.76 12.40 o 4 6 0 86.97 94.63 4.63 o 5 6 0 0.77 2.25 2.34 o 6 6 0 57.45 50.82 9.62 o -5 7 0 428.54 432.14 9.95 o -4 7 0 21.56 26.20 2.74 o -3 7 0 564.00 538.74 9.25 o -2 7 0 449.12 433.28 7.62 o -1 7 0 303.17 288.95 5.54 o 0 7 0 182.62 177.12 4.00 o 1 7 0 3.37 2.37 1.42 o 2 7 0 214.51 225.24 5.39 o 3 7 0 1.99 3.10 1.82 o 4 7 0 2.04 1.79 1.96 o 5 7 0 394.94 392.69 11.25 o -5 8 0 1.75 0.96 1.95 o -4 8 0 40.36 34.72 3.13 o -3 8 0 549.99 540.23 10.66 o -2 8 0 260.49 242.72 6.12 o -1 8 0 116.24 106.84 2.78 o 0 8 0 125.07 125.45 5.36 o 1 8 0 477.70 487.75 9.26 o 2 8 0 0.90 1.99 2.38 o 3 8 0 10.60 11.40 2.34 o 4 8 0 0.73 -1.33 1.97 o 5 8 0 10.28 7.12 2.75 o -4 9 0 47.11 43.71 3.64 o -3 9 0 12.28 10.16 2.06 o -2 9 0 257.89 227.44 6.15 o -1 9 0 115.61 104.09 5.15 o 0 9 0 0.74 1.01 1.45 o 1 9 0 99.16 104.23 5.11 o 2 9 0 76.21 69.62 3.57 o 3 9 0 37.59 33.36 5.95 o 4 9 0 31.09 38.55 5.28 o -3 10 0 140.27 120.97 6.62 o -2 10 0 20.68 14.76 3.02 o -1 10 0 85.07 85.09 5.15 o 0 10 0 248.07 265.34 8.65 o 1 10 0 222.03 213.68 7.63 o 2 10 0 60.49 57.47 5.51 o 3 10 0 123.02 123.99 6.13 o -2 11 0 416.06 426.97 18.47 o -1 11 0 157.25 166.92 7.46 o 0 11 0 82.97 90.31 5.83 o 1 11 0 0.71 1.09 2.22 o 2 11 0 92.61 117.37 9.12 o -1 -11 1 6.30 3.68 2.74 o 0 -11 1 64.44 61.29 13.29 o 1 -11 1 445.71 462.57 22.36 o -3 -10 1 69.59 67.27 5.18 o -2 -10 1 73.12 85.11 8.23 o -1 -10 1 371.15 395.99 11.21 o 0 -10 1 520.65 536.24 13.69 o 1 -10 1 410.67 401.25 11.52 o 2 -10 1 15.47 17.07 3.20 o 3 -10 1 14.08 12.60 2.44 o -4 -9 1 94.58 101.44 5.90 o -3 -9 1 124.07 114.75 5.78 o -2 -9 1 323.86 323.08 7.68 o -1 -9 1 319.85 328.74 9.56 o 0 -9 1 219.85 219.32 6.75 o 1 -9 1 12.98 13.71 3.17 o 2 -9 1 0.93 1.20 1.50 o 3 -9 1 259.39 252.04 6.97 o 4 -9 1 246.84 255.99 17.86 o -4 -8 1 119.28 109.89 5.66 o -3 -8 1 197.47 185.09 6.84 o -2 -8 1 157.40 157.05 4.84 o -1 -8 1 189.24 174.75 6.25 o 0 -8 1 61.92 73.31 4.25 o 1 -8 1 487.89 499.19 7.48 o 2 -8 1 2014.51 1924.61 27.95 o 3 -8 1 1631.62 1555.25 37.58 o 4 -8 1 334.85 326.89 8.28 o -5 -7 1 7.46 6.66 2.71 o -4 -7 1 240.34 225.08 7.71 o -3 -7 1 172.58 194.14 6.64 o -2 -7 1 337.89 361.03 7.51 o -1 -7 1 486.18 537.73 10.21 o 0 -7 1 2319.10 2315.01 37.71 o 1 -7 1 1532.94 1459.35 17.43 o 2 -7 1 1349.71 1273.64 17.73 o 3 -7 1 630.94 608.96 10.25 o 4 -7 1 226.06 223.34 6.41 o 5 -7 1 113.28 114.19 5.02 o -5 -6 1 710.17 727.64 16.59 o -4 -6 1 184.33 190.27 6.69 o -3 -6 1 269.98 303.73 9.05 o -2 -6 1 1904.66 1931.59 27.27 o -1 -6 1 1881.98 1845.17 26.01 o 0 -6 1 1333.10 1249.76 16.44 o 1 -6 1 1470.32 1410.63 19.67 o 2 -6 1 323.44 336.37 6.21 o 3 -6 1 80.37 78.32 2.91 o 4 -6 1 243.89 231.73 6.28 o 5 -6 1 287.62 309.82 8.39 o -6 -5 1 607.09 645.24 22.81 o -5 -5 1 535.39 575.34 13.72 o -4 -5 1 676.78 682.17 14.66 o -3 -5 1 967.19 966.17 14.98 o -2 -5 1 73.61 59.41 2.49 o -1 -5 1 22.45 18.90 1.01 o 0 -5 1 847.32 864.77 11.63 o 1 -5 1 3104.55 3147.83 34.53 o 2 -5 1 800.55 764.35 11.07 o 3 -5 1 1568.18 1532.65 22.38 o 4 -5 1 1230.72 1198.19 22.12 o 5 -5 1 357.98 388.01 10.54 o 6 -5 1 567.49 575.95 18.30 o -6 -4 1 159.63 162.65 10.01 o -5 -4 1 77.38 81.53 6.84 o -4 -4 1 217.05 227.97 7.62 o -3 -4 1 2.90 1.76 0.92 o -2 -4 1 383.38 380.99 8.07 o -1 -4 1 6408.17 6750.32 74.38 o 0 -4 1 2005.15 1984.17 24.23 o 1 -4 1 2834.03 2707.62 27.97 o 2 -4 1 1641.33 1541.83 19.75 o 3 -4 1 1863.22 1868.63 26.26 o 4 -4 1 551.76 543.14 10.05 o 5 -4 1 306.26 295.08 8.61 o 6 -4 1 149.66 131.50 8.68 o -6 -3 1 290.30 286.13 13.13 o -5 -3 1 16.43 16.64 2.48 o -4 -3 1 206.76 207.08 4.98 o -3 -3 1 1197.02 1197.00 17.34 o -2 -3 1 4723.49 4872.33 63.15 o -1 -3 1 3967.80 3972.53 44.79 o 0 -3 1 235.51 204.89 3.31 o 1 -3 1 4992.36 5065.88 53.83 o 2 -3 1 1037.15 1083.60 14.11 o 3 -3 1 44.18 48.66 2.29 o 4 -3 1 82.67 72.31 5.23 o 5 -3 1 103.22 105.35 6.79 o -6 -2 1 327.28 321.18 13.68 o -5 -2 1 516.21 516.63 13.68 o -4 -2 1 3849.22 3955.58 52.64 o -3 -2 1 3294.52 3305.33 37.32 o -2 -2 1 19.46 8.07 0.62 o -1 -2 1 1461.74 1740.45 23.08 o 0 -2 1 137.01 118.92 1.91 o 1 -2 1 1175.72 1312.00 14.53 o 2 -2 1 3624.65 3851.46 49.65 o 3 -2 1 1405.82 1379.50 24.06 o 4 -2 1 480.17 512.30 15.69 o 5 -2 1 39.80 45.39 4.78 o 6 -2 1 159.87 174.33 9.23 o -6 -1 1 535.14 548.56 13.85 o -5 -1 1 452.52 446.26 10.65 o -4 -1 1 330.38 344.40 5.61 o -3 -1 1 5.53 4.18 0.67 o -2 -1 1 61.26 95.73 1.90 o -1 -1 1 206.82 207.16 2.82 o 0 -1 1 2840.02 2831.66 50.07 o 1 -1 1 270.62 313.35 4.81 o 2 -1 1 8366.26 8543.86 132.32 o 3 -1 1 1007.87 1013.59 30.82 o 4 -1 1 595.56 586.41 11.96 o 5 -1 1 175.07 158.20 7.79 o 6 -1 1 3.13 2.19 1.66 o -6 0 1 43.75 43.68 3.81 o -5 0 1 7.03 6.51 1.30 o -4 0 1 268.49 284.66 4.97 o -3 0 1 34.32 24.19 1.28 o -2 0 1 721.39 648.10 8.06 o -1 0 1 3305.50 3415.14 42.87 o 0 0 1 4491.58 4534.97 73.86 o 1 0 1 597.57 670.28 15.46 o 2 0 1 2610.19 2576.55 40.32 o 4 0 1 1.31 0.78 1.00 o 5 0 1 266.73 264.90 21.69 o 6 0 1 231.44 220.20 7.71 o 7 0 1 1.66 0.78 2.43 o -6 1 1 0.82 0.33 2.67 o -5 1 1 188.97 172.16 4.15 o -4 1 1 2.69 1.90 1.00 o -3 1 1 2156.11 2318.49 30.91 o -2 1 1 2174.40 2265.17 36.06 o -1 1 1 22.13 16.35 1.01 o 0 1 1 406.68 441.13 5.79 o 1 1 1 445.47 479.64 8.13 o 2 1 1 341.00 389.79 7.34 o 3 1 1 501.35 539.61 9.48 o 4 1 1 0.98 4.28 3.03 o 5 1 1 3.06 1.00 1.26 o 6 1 1 19.75 24.19 3.56 o 7 1 1 38.32 46.61 6.67 o -6 2 1 79.85 76.34 9.68 o -5 2 1 1.70 1.10 1.44 o -4 2 1 88.97 68.19 3.49 o -3 2 1 631.11 719.16 13.68 o -2 2 1 219.25 262.24 6.82 o -1 2 1 0.91 2.33 0.50 o 0 2 1 308.78 328.07 3.64 o 1 2 1 594.97 721.86 9.01 o 2 2 1 311.12 351.30 5.61 o 3 2 1 1984.66 2068.73 23.93 o 4 2 1 1144.45 1164.95 21.72 o 5 2 1 459.66 471.98 13.63 o 6 2 1 9.62 11.56 2.67 o -6 3 1 24.31 13.07 2.51 o -5 3 1 60.08 54.32 4.08 o -4 3 1 227.42 239.32 6.95 o -3 3 1 834.83 914.27 13.93 o -2 3 1 8.96 4.89 0.83 o -1 3 1 810.96 774.43 11.06 o 0 3 1 190.39 205.28 2.68 o 1 3 1 346.97 325.70 4.62 o 2 3 1 36.40 43.42 1.46 o 3 3 1 1426.14 1493.93 17.72 o 4 3 1 1.85 1.49 2.22 o 5 3 1 35.94 33.01 3.18 o 6 3 1 158.87 149.64 6.35 o -6 4 1 7.30 4.78 3.23 o -5 4 1 0.88 0.56 1.63 o -4 4 1 6.43 3.86 1.30 o -3 4 1 57.32 66.31 2.99 o -2 4 1 778.66 764.18 11.56 o -1 4 1 14.26 8.87 0.94 o 0 4 1 78.77 66.76 1.50 o 1 4 1 402.07 418.03 5.87 o 2 4 1 89.50 98.55 3.61 o 3 4 1 0.78 1.60 0.71 o 4 4 1 1.01 0.92 1.37 o 5 4 1 16.40 17.50 3.11 o 6 4 1 33.95 29.20 8.68 o -6 5 1 178.81 199.25 10.68 o -5 5 1 27.35 22.81 4.23 o -4 5 1 29.16 30.69 3.06 o -3 5 1 494.30 504.36 11.17 o -2 5 1 4.14 3.23 0.90 o -1 5 1 151.34 151.36 2.70 o 0 5 1 293.10 332.27 4.15 o 1 5 1 132.33 149.92 2.99 o 2 5 1 442.79 472.48 7.87 o 3 5 1 40.40 43.33 5.28 o 4 5 1 897.23 851.48 17.38 o 5 5 1 277.12 273.39 8.48 o 6 5 1 105.84 105.82 5.80 o -6 6 1 165.36 186.53 7.86 o -5 6 1 1.46 -1.49 1.49 o -4 6 1 403.20 382.90 8.34 o -3 6 1 1458.57 1420.76 21.19 o -2 6 1 261.55 253.45 5.01 o -1 6 1 239.24 253.98 4.78 o 0 6 1 717.74 715.11 8.78 o 1 6 1 1058.26 1038.50 12.09 o 2 6 1 618.54 551.29 29.91 o 3 6 1 12.04 14.61 2.12 o 4 6 1 183.38 192.66 12.13 o 5 6 1 15.88 17.34 2.91 o 6 6 1 115.93 117.83 6.17 o -5 7 1 112.46 112.42 5.65 o -4 7 1 1.41 0.10 1.50 o -3 7 1 84.63 81.29 4.14 o -2 7 1 6.46 8.19 1.27 o -1 7 1 547.01 529.48 10.85 o 0 7 1 846.35 834.36 10.29 o 1 7 1 756.58 753.97 12.65 o 2 7 1 205.36 185.91 8.36 o 3 7 1 7.17 9.85 2.04 o 4 7 1 33.83 28.04 3.15 o 5 7 1 0.95 -0.22 2.12 o -5 8 1 187.12 195.67 6.55 o -4 8 1 289.41 280.48 7.43 o -3 8 1 272.22 274.79 6.66 o -2 8 1 9.13 9.63 1.49 o -1 8 1 322.78 313.63 5.33 o 0 8 1 0.96 0.19 1.13 o 1 8 1 56.98 56.44 2.75 o 2 8 1 84.73 80.17 3.32 o 3 8 1 3.88 1.50 2.45 o 4 8 1 160.62 162.18 6.61 o 5 8 1 680.52 672.83 23.03 o -4 9 1 48.37 41.40 4.14 o -3 9 1 7.08 10.17 2.02 o -2 9 1 279.05 257.54 7.11 o -1 9 1 104.03 107.60 3.33 o 0 9 1 265.56 271.06 7.00 o 1 9 1 1322.67 1312.75 20.18 o 2 9 1 630.98 614.27 14.00 o 3 9 1 533.79 517.46 15.52 o 4 9 1 578.13 565.97 14.31 o -3 10 1 35.01 32.60 2.94 o -2 10 1 14.46 14.52 1.86 o -1 10 1 231.01 230.13 8.84 o 0 10 1 880.41 903.37 25.20 o 1 10 1 563.92 561.59 14.02 o 2 10 1 1280.73 1260.88 72.15 o 3 10 1 1255.88 1189.42 54.90 o 4 10 1 28.31 27.59 4.84 o -2 11 1 926.06 931.23 43.11 o -1 11 1 231.37 224.75 8.96 o 0 11 1 214.13 223.54 8.18 o 1 11 1 266.25 272.89 13.13 o 2 11 1 510.39 502.20 13.17 o 3 11 1 23.18 27.81 6.84 o -1 12 1 1.02 0.22 3.78 o 0 12 1 275.86 264.82 20.53 o 1 12 1 232.02 244.86 13.02 o 0 -11 2 226.16 248.88 9.48 o -2 -10 2 1050.69 1085.12 32.48 o -1 -10 2 1232.67 1281.43 26.00 o 0 -10 2 681.88 683.25 16.48 o 1 -10 2 94.11 103.13 5.96 o 2 -10 2 31.93 34.75 4.12 o -3 -9 2 465.21 488.76 17.30 o -2 -9 2 562.95 555.46 13.69 o -1 -9 2 571.18 579.21 14.00 o 0 -9 2 235.84 236.90 8.14 o 1 -9 2 50.55 48.47 10.51 o 2 -9 2 152.16 156.91 6.80 o 3 -9 2 252.67 247.08 7.12 o -4 -8 2 145.53 142.33 8.62 o -3 -8 2 46.09 38.52 3.70 o -2 -8 2 87.62 92.19 3.90 o -1 -8 2 16.86 29.43 3.15 o 0 -8 2 185.10 182.39 7.23 o 1 -8 2 429.02 419.35 8.55 o 2 -8 2 1118.83 1131.66 18.13 o 3 -8 2 331.28 330.59 8.00 o 4 -8 2 579.31 607.24 13.34 o -5 -7 2 135.55 128.72 9.23 o -4 -7 2 1.25 -1.08 1.88 o -3 -7 2 274.53 294.57 7.11 o -2 -7 2 303.95 326.55 10.47 o -1 -7 2 516.40 518.16 13.91 o 0 -7 2 1812.84 1711.03 30.56 o 1 -7 2 472.33 468.47 7.02 o 2 -7 2 57.75 69.11 2.87 o 3 -7 2 243.66 244.72 6.46 o 4 -7 2 334.08 349.63 14.55 o 5 -7 2 10.71 7.41 2.24 o -5 -6 2 814.13 800.66 25.92 o -4 -6 2 470.06 474.71 11.79 o -3 -6 2 215.37 215.50 5.52 o -2 -6 2 62.38 56.12 3.47 o -1 -6 2 518.32 487.17 10.86 o 0 -6 2 704.00 697.72 11.03 o 1 -6 2 140.55 144.91 3.08 o 2 -6 2 8.34 10.41 1.38 o 3 -6 2 8.89 13.81 1.68 o 4 -6 2 86.83 73.06 3.78 o 5 -6 2 54.20 61.45 4.10 o -6 -5 2 532.98 551.68 20.58 o -5 -5 2 1007.68 987.89 29.48 o -4 -5 2 440.38 409.58 10.29 o -3 -5 2 23.77 34.80 4.08 o -2 -5 2 104.41 128.38 3.75 o -1 -5 2 90.59 92.18 3.66 o 0 -5 2 1.40 2.58 0.70 o 1 -5 2 890.26 857.14 10.67 o 2 -5 2 46.50 49.15 2.15 o 3 -5 2 257.70 259.09 5.38 o 4 -5 2 182.33 182.06 5.38 o 5 -5 2 341.16 344.55 9.83 o 6 -5 2 24.50 26.37 5.23 o -6 -4 2 68.32 73.87 7.56 o -5 -4 2 20.18 19.69 4.00 o -4 -4 2 19.56 23.93 3.30 o -3 -4 2 197.11 216.40 5.03 o -2 -4 2 247.89 252.38 5.24 o -1 -4 2 161.14 162.52 2.92 o 0 -4 2 188.43 157.88 3.39 o 1 -4 2 524.70 518.75 6.82 o 2 -4 2 10.35 12.63 1.21 o 3 -4 2 596.34 575.52 8.99 o 4 -4 2 43.53 43.72 2.83 o 5 -4 2 24.37 26.03 3.10 o 6 -4 2 39.15 47.06 6.23 o -6 -3 2 4.49 5.45 3.45 o -5 -3 2 124.55 113.81 7.45 o -4 -3 2 314.07 303.34 7.14 o -3 -3 2 224.39 234.96 5.07 o -2 -3 2 412.18 398.84 6.93 o -1 -3 2 25.32 46.57 1.85 o 0 -3 2 102.81 87.32 2.19 o 1 -3 2 450.33 470.07 5.68 o 2 -3 2 7.68 6.55 0.84 o 3 -3 2 367.59 371.51 7.07 o 4 -3 2 194.50 185.94 5.90 o 5 -3 2 15.02 17.47 2.56 o 6 -3 2 77.96 82.21 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