#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/85/2228593.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228593_Fobs loop_ _publ_author_name 'Huang, Hua-Rong' 'Wen-Jiao, Guo' 'Du, Zhi-Yun' 'Fang, Yan-Xiong' 'Zhang, Kun' _publ_section_title ; 1,3-Bis[4-(methoxycarbonyl)benzyl]benzimidazolium bromide monohydrate ; _journal_coeditor_code WN2412 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3064 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.006 _cell_angle_gamma 90.000 _cell_length_a 13.6044 _cell_length_b 9.3537 _cell_length_c 18.9616 _exptl_crystal_F_000 1056.00 _reflns_d_resolution_high 0.7809 _[local]_cod_data_source_file wn2412Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' l09261m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 221.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 15770.42 18216.38 345.49 o 3 0 0 6555.59 6870.76 102.34 o 4 0 0 8688.90 9703.54 143.42 o 5 0 0 75.73 47.52 12.12 o 6 0 0 15967.47 16961.35 199.72 o 7 0 0 14304.80 14537.79 179.84 o 8 0 0 49021.14 50464.27 548.78 o 9 0 0 8869.17 8919.12 130.04 o 10 0 0 80.68 83.30 26.82 o 11 0 0 760.06 632.63 58.21 o 12 0 0 94.22 187.87 61.48 o 13 0 0 288.21 176.26 72.42 o 14 0 0 1158.32 1188.79 120.13 o 15 0 0 4759.60 4532.73 198.50 o 16 0 0 1003.54 1098.09 138.72 o 1 1 0 77.84 83.37 6.06 o 2 1 0 4235.42 4224.68 47.48 o 3 1 0 11788.54 12484.85 124.29 o 4 1 0 148.57 110.79 13.03 o 5 1 0 253.49 188.23 18.87 o 6 1 0 1269.97 1316.38 29.88 o 7 1 0 480.32 538.21 23.81 o 8 1 0 52.37 32.61 15.24 o 9 1 0 3677.11 3462.40 49.73 o 10 1 0 172.96 166.46 27.16 o 11 1 0 7772.13 7565.49 140.77 o 12 1 0 15.67 -0.70 43.20 o 13 1 0 50.84 74.26 45.04 o 14 1 0 47.95 34.57 50.62 o 15 1 0 27.12 -18.98 59.60 o 16 1 0 380.08 316.95 74.79 o 0 2 0 1515.12 1539.98 26.88 o 1 2 0 15711.54 17283.66 149.54 o 2 2 0 2907.20 3066.75 41.72 o 3 2 0 5619.36 5582.52 65.95 o 4 2 0 482.20 442.71 17.84 o 5 2 0 1900.68 2026.96 37.10 o 6 2 0 1236.34 1255.52 27.61 o 7 2 0 558.24 497.44 24.44 o 8 2 0 1521.94 1650.28 36.48 o 9 2 0 159.91 129.70 25.46 o 10 2 0 166.08 87.63 24.59 o 11 2 0 12.87 -26.13 40.57 o 12 2 0 561.29 543.58 137.15 o 13 2 0 15.30 -37.43 37.43 o 14 2 0 407.36 390.19 66.11 o 15 2 0 258.83 257.23 66.53 o 16 2 0 0.57 92.03 99.84 o 1 3 0 469.44 485.42 15.98 o 2 3 0 12839.86 13720.06 185.20 o 3 3 0 1273.63 1334.37 26.29 o 4 3 0 392.30 338.15 25.65 o 5 3 0 4007.19 4180.95 61.20 o 6 3 0 306.12 256.05 26.96 o 7 3 0 686.17 660.40 25.42 o 8 3 0 1854.80 1818.09 45.37 o 9 3 0 227.02 320.32 39.59 o 10 3 0 2867.41 2736.21 73.74 o 11 3 0 1260.53 1194.21 56.57 o 12 3 0 1214.56 1150.07 56.56 o 13 3 0 826.36 900.38 83.40 o 14 3 0 668.61 737.56 169.89 o 15 3 0 594.35 680.09 110.78 o 16 3 0 228.06 146.27 107.44 o 0 4 0 1664.39 1621.29 44.41 o 1 4 0 10538.45 11001.70 109.64 o 2 4 0 8687.66 9160.41 95.90 o 3 4 0 2015.22 1951.39 35.78 o 4 4 0 1758.70 1737.06 34.90 o 5 4 0 637.92 565.38 19.88 o 6 4 0 3481.55 3385.87 49.54 o 7 4 0 2172.16 2047.44 46.07 o 8 4 0 1520.57 1541.52 43.75 o 9 4 0 2091.22 2072.79 52.40 o 10 4 0 1978.50 1961.08 86.76 o 11 4 0 241.14 287.78 54.58 o 12 4 0 349.28 285.15 61.63 o 13 4 0 34.40 10.71 60.82 o 14 4 0 457.95 382.46 82.35 o 15 4 0 37.00 -76.42 88.95 o 1 5 0 42.48 10.49 14.70 o 2 5 0 30.82 -2.89 14.02 o 3 5 0 137.47 110.04 20.76 o 4 5 0 323.02 295.50 29.65 o 5 5 0 1318.66 1238.77 34.28 o 6 5 0 594.91 588.26 40.67 o 7 5 0 38.38 76.71 30.47 o 8 5 0 198.09 199.92 62.68 o 9 5 0 11.03 32.58 33.07 o 10 5 0 132.76 97.20 47.96 o 11 5 0 589.22 319.65 61.55 o 12 5 0 36.40 53.73 58.32 o 13 5 0 51.09 29.85 65.01 o 14 5 0 127.14 72.81 72.54 o 15 5 0 59.43 84.60 79.66 o 0 6 0 5750.45 5789.48 126.65 o 1 6 0 2098.90 2044.04 61.81 o 2 6 0 4509.68 4502.12 66.55 o 3 6 0 8373.74 8856.66 105.26 o 4 6 0 3271.65 3273.97 59.78 o 5 6 0 4869.57 4748.71 120.60 o 6 6 0 2470.64 2442.07 61.67 o 7 6 0 403.13 437.01 38.42 o 8 6 0 1095.78 1150.99 54.65 o 9 6 0 2148.04 2253.10 112.15 o 10 6 0 1582.65 1617.25 88.38 o 11 6 0 948.00 960.96 124.42 o 12 6 0 791.53 894.99 91.73 o 13 6 0 25.64 19.26 67.72 o 14 6 0 132.56 99.50 77.39 o 1 7 0 33.21 22.50 24.95 o 2 7 0 1420.02 1378.09 53.08 o 3 7 0 403.71 402.76 41.58 o 4 7 0 1431.72 1481.29 49.53 o 5 7 0 886.97 927.31 46.26 o 6 7 0 10.98 12.48 29.06 o 7 7 0 511.76 472.78 54.18 o 8 7 0 352.16 392.24 47.66 o 9 7 0 881.60 993.86 125.55 o 10 7 0 849.36 893.82 88.37 o 11 7 0 539.37 566.42 80.35 o 12 7 0 345.29 343.98 78.88 o 13 7 0 19.53 29.89 76.66 o 0 8 0 479.86 297.10 50.29 o 1 8 0 102.98 97.47 31.50 o 2 8 0 208.43 201.49 35.07 o 3 8 0 189.82 114.84 34.82 o 4 8 0 18.79 -29.77 38.66 o 5 8 0 622.35 603.06 56.02 o 6 8 0 2134.66 2079.15 79.61 o 7 8 0 379.76 343.78 44.40 o 8 8 0 9.47 -0.56 44.72 o 9 8 0 19.74 25.45 49.64 o 10 8 0 1.43 -57.00 64.97 o 11 8 0 37.48 75.19 74.12 o 12 8 0 286.36 115.83 81.90 o 1 9 0 16.09 28.24 33.41 o 2 9 0 28.90 23.47 44.29 o 3 9 0 410.18 356.37 54.99 o 4 9 0 187.68 101.51 48.69 o 5 9 0 1336.99 1373.85 73.28 o 6 9 0 32.59 24.95 51.77 o 7 9 0 312.77 404.57 84.28 o 8 9 0 257.32 307.53 102.87 o 9 9 0 653.71 518.56 131.89 o 10 9 0 248.10 199.27 122.54 o 0 10 0 1360.57 1474.97 90.02 o 1 10 0 236.80 325.75 57.64 o 2 10 0 2107.58 2219.97 88.58 o 3 10 0 1927.42 2065.56 105.08 o 4 10 0 1281.05 1342.71 77.10 o 5 10 0 745.37 834.86 122.31 o 6 10 0 824.00 949.68 155.11 o 7 10 0 239.39 303.52 69.86 o 8 10 0 945.08 1065.82 116.02 o 9 10 0 106.10 124.08 129.83 o 1 11 0 107.05 69.92 61.11 o 2 11 0 1.00 8.78 59.18 o 3 11 0 265.99 147.36 71.57 o 4 11 0 52.54 15.60 67.99 o 5 11 0 37.99 -33.68 64.41 o 6 11 0 114.89 136.36 73.94 o -16 1 1 864.17 933.96 94.46 o -15 1 1 1485.67 1460.44 90.36 o -14 1 1 907.87 950.17 82.43 o -13 1 1 507.63 514.30 62.56 o -12 1 1 1021.12 977.98 56.87 o -11 1 1 1718.42 1596.42 47.95 o -10 1 1 87.04 75.09 20.60 o -9 1 1 178.85 158.72 17.58 o -8 1 1 2670.53 2729.22 50.98 o -7 1 1 5991.36 6448.07 94.55 o -6 1 1 20.53 -2.11 17.52 o -5 1 1 3648.05 4122.15 73.31 o -4 1 1 29592.57 31756.27 419.01 o -3 1 1 11122.64 12488.74 143.65 o -2 1 1 360.52 342.85 52.95 o -1 1 1 1703.38 1726.72 34.59 o 0 1 1 28.45 18.77 4.10 o 1 1 1 208.56 215.10 10.46 o 2 1 1 486.31 484.17 10.31 o 3 1 1 33825.07 37237.50 306.31 o 4 1 1 17945.38 19901.43 173.14 o 5 1 1 11171.48 11838.27 112.56 o 6 1 1 112.79 162.40 19.82 o 7 1 1 302.45 243.71 18.20 o 8 1 1 605.05 530.46 53.55 o 9 1 1 5403.74 5343.95 76.52 o 10 1 1 2713.82 2545.17 67.69 o 11 1 1 5551.85 5429.64 108.96 o 12 1 1 1835.85 1817.55 73.86 o 13 1 1 665.69 759.45 72.04 o 14 1 1 330.14 495.10 90.29 o 15 1 1 392.57 582.46 133.20 o 16 1 1 200.37 284.93 72.49 o -16 2 1 404.19 301.01 108.62 o -15 2 1 1313.30 1355.40 90.70 o -14 2 1 1307.77 1260.25 79.81 o -13 2 1 1426.82 1392.04 69.61 o -12 2 1 2045.73 1820.68 66.18 o -11 2 1 1890.97 1758.50 72.47 o -10 2 1 5811.34 5793.07 90.83 o -9 2 1 961.24 926.36 35.81 o -8 2 1 4356.67 4253.79 83.73 o -7 2 1 4352.13 4619.14 95.22 o -6 2 1 10763.83 11010.18 136.91 o -5 2 1 10516.11 11068.50 137.62 o -4 2 1 13138.79 13577.92 160.85 o -3 2 1 4039.85 4162.08 52.56 o -2 2 1 43519.95 47710.00 477.81 o -1 2 1 1072.07 1153.13 25.60 o 0 2 1 8610.17 9403.81 96.89 o 1 2 1 1372.17 1583.02 52.17 o 2 2 1 5821.03 6213.19 73.69 o 3 2 1 11852.75 12844.95 106.59 o 4 2 1 6960.17 7030.40 66.59 o 5 2 1 389.05 316.89 27.55 o 6 2 1 8378.85 9101.75 95.28 o 7 2 1 81.69 40.77 14.48 o 8 2 1 1603.76 1547.10 36.17 o 9 2 1 412.41 399.80 26.97 o 10 2 1 629.77 623.28 81.55 o 11 2 1 792.12 831.37 50.27 o 12 2 1 19.68 70.32 37.50 o 13 2 1 246.99 211.12 74.95 o 14 2 1 213.24 204.36 57.27 o 15 2 1 222.79 208.82 88.08 o 16 2 1 213.70 256.33 99.74 o -16 3 1 2.09 -34.36 96.40 o -15 3 1 41.86 143.91 99.74 o -14 3 1 108.48 100.13 63.45 o -13 3 1 16.21 -37.53 37.53 o -12 3 1 0.07 15.59 36.22 o -11 3 1 6.41 -10.49 31.17 o -10 3 1 891.10 803.03 39.32 o -9 3 1 78.85 54.46 22.90 o -8 3 1 14.22 10.70 24.13 o -7 3 1 0.06 -2.49 16.22 o -6 3 1 56.66 35.96 14.55 o -5 3 1 6264.99 6943.62 85.57 o -4 3 1 3123.05 3286.23 66.89 o -3 3 1 23.60 19.06 9.17 o -2 3 1 11134.46 12160.19 117.05 o -1 3 1 623.90 669.05 17.34 o 0 3 1 220.20 219.12 10.30 o 1 3 1 822.89 794.94 22.31 o 2 3 1 3121.97 3301.98 49.92 o 3 3 1 610.31 658.86 15.84 o 4 3 1 88.75 78.21 12.65 o 5 3 1 6512.19 7209.55 78.61 o 6 3 1 65.44 10.37 13.70 o 7 3 1 14.14 -14.81 14.81 o 8 3 1 175.75 168.28 26.88 o 9 3 1 4.74 -6.03 22.10 o 10 3 1 367.18 383.49 50.70 o 11 3 1 184.06 180.74 37.07 o 12 3 1 106.43 104.96 61.36 o 13 3 1 479.06 337.28 68.37 o 14 3 1 4.51 -41.30 70.23 o 15 3 1 169.20 75.70 94.76 o -15 4 1 19.09 -49.82 91.06 o -14 4 1 1136.59 1172.16 102.12 o -13 4 1 182.59 176.64 61.35 o -12 4 1 1224.53 1197.80 76.62 o -11 4 1 1939.69 1749.63 86.18 o -10 4 1 1897.65 1818.55 64.44 o -9 4 1 382.79 387.99 37.41 o -8 4 1 4719.79 4767.57 77.80 o -7 4 1 773.97 736.33 40.29 o -6 4 1 3224.39 2901.15 52.14 o -5 4 1 7191.81 7646.94 87.50 o -4 4 1 2351.98 2283.36 46.31 o -3 4 1 2149.72 2045.56 36.37 o -2 4 1 5524.83 5717.72 78.16 o -1 4 1 6874.87 7076.80 77.00 o 0 4 1 483.07 454.12 14.87 o 1 4 1 7407.37 7887.59 123.92 o 2 4 1 106.50 82.92 13.24 o 3 4 1 8248.12 8552.64 105.79 o 4 4 1 1497.17 1484.11 26.48 o 5 4 1 1058.53 1040.21 24.58 o 6 4 1 55.70 56.54 16.28 o 7 4 1 2465.51 2555.29 46.10 o 8 4 1 218.58 222.59 26.00 o 9 4 1 598.65 636.20 56.91 o 10 4 1 82.44 43.75 47.30 o 11 4 1 70.78 39.06 47.33 o 12 4 1 54.75 18.25 50.82 o 13 4 1 0.53 14.32 64.33 o 14 4 1 14.95 116.74 73.24 o 15 4 1 176.12 277.33 83.67 o -15 5 1 22.88 90.17 79.26 o -14 5 1 126.15 142.96 71.33 o -13 5 1 99.87 37.95 68.49 o -12 5 1 1180.25 1175.43 96.25 o -11 5 1 1.46 -46.60 50.18 o -10 5 1 28.48 -11.34 41.77 o -9 5 1 4.09 -1.24 32.80 o -8 5 1 139.27 124.54 33.12 o -7 5 1 233.88 216.44 67.18 o -6 5 1 203.03 125.91 39.35 o -5 5 1 1248.97 1265.54 38.39 o -4 5 1 6254.94 6534.89 81.40 o -3 5 1 8708.93 9093.71 133.34 o -2 5 1 731.07 798.34 25.90 o -1 5 1 4399.77 4460.23 59.21 o 0 5 1 3368.92 3354.00 42.80 o 1 5 1 3478.41 3481.09 58.70 o 2 5 1 633.89 578.38 25.38 o 3 5 1 1318.02 1224.77 32.47 o 4 5 1 43.87 22.11 16.65 o 5 5 1 8377.77 8629.13 102.17 o 6 5 1 4328.40 4480.55 68.51 o 7 5 1 4320.85 4408.36 97.61 o 8 5 1 2338.06 2282.28 74.42 o 9 5 1 926.28 938.52 49.75 o 10 5 1 2848.82 2861.77 106.66 o 11 5 1 74.63 47.42 54.96 o 12 5 1 1820.43 1988.42 187.28 o 13 5 1 2253.06 2311.52 147.30 o 14 5 1 1053.70 1089.59 148.48 o -14 6 1 509.18 474.89 174.34 o -13 6 1 275.91 211.94 102.84 o -12 6 1 385.40 370.29 75.59 o -11 6 1 591.13 687.30 78.67 o -10 6 1 334.08 293.27 87.10 o -9 6 1 114.40 81.82 54.27 o -8 6 1 192.53 164.52 40.12 o -7 6 1 100.46 30.74 32.72 o -6 6 1 1343.59 1264.22 112.93 o -5 6 1 290.81 259.66 30.83 o -4 6 1 1961.59 1943.50 44.29 o -3 6 1 4498.21 4813.39 69.44 o -2 6 1 24.85 22.58 17.66 o -1 6 1 1438.31 1495.37 35.54 o 0 6 1 813.64 911.70 29.50 o 1 6 1 1726.75 1678.10 43.99 o 2 6 1 69.66 43.59 18.40 o 3 6 1 981.57 897.55 32.65 o 4 6 1 15.44 -16.07 19.80 o 5 6 1 2769.13 2746.16 61.52 o 6 6 1 77.77 59.88 27.67 o 7 6 1 162.11 198.93 33.44 o 8 6 1 3.67 8.37 33.54 o 9 6 1 24.75 24.30 57.37 o 10 6 1 272.20 215.22 61.63 o 11 6 1 159.75 48.78 59.21 o 12 6 1 1.36 -50.00 62.31 o 13 6 1 0.44 8.14 70.51 o 14 6 1 54.59 52.60 80.55 o -13 7 1 1.86 -15.03 74.82 o -12 7 1 48.71 38.95 70.31 o -11 7 1 182.63 135.16 132.81 o -10 7 1 78.98 64.12 66.43 o -9 7 1 558.54 496.08 57.30 o -8 7 1 404.05 401.73 64.97 o -7 7 1 18.41 48.49 33.77 o -6 7 1 806.39 815.04 47.61 o -5 7 1 305.89 244.37 33.73 o -4 7 1 732.37 690.23 82.46 o -3 7 1 87.38 42.12 26.32 o -2 7 1 8.47 1.68 24.04 o -1 7 1 6.19 22.25 25.22 o 0 7 1 46.65 36.65 26.77 o 1 7 1 320.57 336.56 50.93 o 2 7 1 774.24 769.84 61.45 o 3 7 1 991.18 971.24 37.10 o 4 7 1 738.75 794.02 36.57 o 5 7 1 2532.11 2511.11 65.26 o 6 7 1 249.67 192.41 53.25 o 7 7 1 449.95 463.55 42.97 o 8 7 1 14.39 1.42 40.42 o 9 7 1 1074.41 1144.59 91.20 o 10 7 1 22.89 31.26 60.53 o 11 7 1 1139.14 1230.92 199.06 o 12 7 1 34.73 65.92 73.69 o 13 7 1 1497.37 1514.68 114.86 o -12 8 1 800.05 817.29 96.71 o -11 8 1 262.21 268.69 75.79 o -10 8 1 521.18 505.59 75.18 o -9 8 1 676.06 909.16 71.12 o -8 8 1 700.66 847.66 86.89 o -7 8 1 5619.50 5918.59 235.81 o -6 8 1 3588.38 3572.02 101.25 o -5 8 1 4512.37 4634.94 113.51 o -4 8 1 1884.18 1934.64 74.06 o -3 8 1 884.42 1057.88 63.76 o -2 8 1 1351.02 1492.75 54.14 o -1 8 1 102.28 57.20 30.16 o 0 8 1 4220.51 4195.48 85.45 o 1 8 1 4034.70 4040.93 188.44 o 2 8 1 6145.53 6152.12 187.94 o 3 8 1 2281.53 2227.08 73.65 o 4 8 1 346.06 368.74 48.57 o 5 8 1 145.82 132.89 44.13 o 6 8 1 333.36 300.41 56.69 o 7 8 1 11.25 -9.16 35.46 o 8 8 1 770.88 767.41 93.39 o 9 8 1 1056.25 1142.88 210.36 o 10 8 1 1139.57 1230.36 122.64 o 11 8 1 253.29 143.91 78.13 o 12 8 1 57.19 105.76 78.44 o -11 9 1 90.03 -113.40 113.40 o -10 9 1 141.09 102.15 111.76 o -9 9 1 3.20 -65.14 65.14 o -8 9 1 80.26 66.94 69.89 o -7 9 1 615.33 816.78 110.47 o -6 9 1 17.81 -18.28 47.64 o -5 9 1 353.52 337.62 56.85 o -4 9 1 232.12 149.86 49.61 o -3 9 1 12.82 49.27 42.08 o -2 9 1 137.23 107.81 43.08 o -1 9 1 264.50 210.81 39.68 o 0 9 1 182.50 154.38 39.06 o 1 9 1 427.76 500.72 59.64 o 2 9 1 539.20 514.10 47.14 o 3 9 1 17.47 -18.06 42.03 o 4 9 1 38.14 6.44 43.15 o 5 9 1 387.10 407.44 120.77 o 6 9 1 151.06 156.86 69.50 o 7 9 1 493.25 542.59 65.66 o 8 9 1 272.34 314.94 67.06 o 9 9 1 124.41 70.46 103.54 o 10 9 1 69.99 208.57 119.82 o -9 10 1 92.11 93.17 118.18 o -8 10 1 892.82 1064.49 111.48 o -7 10 1 8.62 18.26 73.41 o -6 10 1 336.96 212.61 63.30 o -5 10 1 12.10 -36.57 51.81 o -4 10 1 419.08 411.77 62.91 o -3 10 1 101.82 41.29 51.39 o -2 10 1 189.64 117.86 53.65 o -1 10 1 114.52 144.08 52.18 o 0 10 1 442.84 494.25 56.98 o 1 10 1 15.65 22.44 52.42 o 2 10 1 259.25 233.60 58.36 o 3 10 1 6.30 -21.70 51.10 o 4 10 1 424.88 388.16 117.09 o 5 10 1 224.04 233.33 62.02 o 6 10 1 56.30 8.14 59.75 o 7 10 1 22.95 47.24 62.91 o 8 10 1 14.75 -57.66 65.48 o -6 11 1 17.20 -30.48 67.93 o -5 11 1 339.52 335.03 73.76 o -4 11 1 29.35 52.74 64.15 o -3 11 1 384.37 235.71 67.83 o -2 11 1 56.60 14.93 60.70 o -1 11 1 209.53 188.10 63.36 o 0 11 1 13.77 -72.17 75.03 o 1 11 1 10.01 -31.38 55.33 o 2 11 1 817.17 982.06 157.62 o 3 11 1 954.83 1341.68 95.82 o 4 11 1 619.72 667.58 80.77 o 5 11 1 526.47 645.68 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