#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/86/2228610.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2228610_Fobs loop_ _publ_author_name 'Song, Jing-Jing' 'Zhang, Kou-Lin' 'Ng, Seik Weng' _publ_section_title ; catena-Poly[[tetraaqua[\m~2~-1,4-bis(1,2,4-triazol-1-yl)butane-\k^2^N^4^:N^4'^]cadmium(II)] sulfate] ; _journal_coeditor_code XU5081 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1529 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.227 _cell_angle_gamma 90.000 _cell_length_a 12.1858 _cell_length_b 10.9733 _cell_length_c 12.4916 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file xu5081Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 337.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 21319.45 19000.17 357.27 o 4 0 0 734.96 531.62 15.76 o 6 0 0 136.89 163.85 9.70 o 8 0 0 25238.44 24487.47 468.33 o 10 0 0 1110.34 1059.52 32.18 o 12 0 0 4606.32 4346.98 125.04 o 14 0 0 776.56 753.56 58.32 o 1 1 0 4575.34 4859.88 81.74 o 3 1 0 15858.96 13918.66 204.17 o 5 1 0 1565.41 1459.79 24.09 o 7 1 0 685.61 798.01 22.88 o 9 1 0 451.64 486.90 17.25 o 11 1 0 535.29 571.41 19.06 o 13 1 0 418.05 412.33 24.37 o 15 1 0 40.71 30.69 9.66 o 0 2 0 47235.13 36046.09 1165.79 o 2 2 0 51297.51 49335.50 1593.15 o 4 2 0 11891.20 11511.15 156.29 o 6 2 0 16045.99 14230.47 282.78 o 8 2 0 4538.65 4390.15 66.14 o 10 2 0 3935.35 3775.14 67.09 o 12 2 0 961.67 919.84 25.70 o 14 2 0 2032.21 2081.21 57.27 o 1 3 0 17714.72 17608.63 280.70 o 3 3 0 5961.07 6289.75 87.01 o 5 3 0 840.00 708.58 14.50 o 7 3 0 1.23 2.82 3.40 o 9 3 0 576.17 522.93 19.32 o 11 3 0 172.15 169.92 11.92 o 13 3 0 68.32 69.07 9.52 o 15 3 0 0.19 10.33 8.67 o 0 4 0 39256.26 37336.10 853.38 o 2 4 0 17259.24 17191.70 269.35 o 4 4 0 14822.44 14684.41 199.24 o 6 4 0 9344.71 8932.25 124.94 o 8 4 0 4399.42 4491.84 85.07 o 10 4 0 3038.50 3019.23 56.63 o 12 4 0 2030.33 2000.17 50.06 o 14 4 0 1025.52 1013.35 34.25 o 1 5 0 880.60 741.15 13.71 o 3 5 0 1858.10 2130.93 33.14 o 5 5 0 290.37 320.07 8.96 o 7 5 0 101.15 125.93 8.80 o 9 5 0 188.80 198.33 11.90 o 11 5 0 69.44 86.95 12.96 o 13 5 0 7.24 6.25 8.01 o 0 6 0 29001.75 27971.01 1099.03 o 2 6 0 11058.71 10309.85 222.69 o 4 6 0 8667.79 8594.46 132.22 o 6 6 0 937.20 939.58 26.29 o 8 6 0 7970.01 7733.54 163.99 o 10 6 0 2809.24 2790.05 62.52 o 12 6 0 2599.42 2488.00 59.81 o 14 6 0 188.92 180.43 17.46 o 1 7 0 474.18 500.38 13.45 o 3 7 0 2312.75 2267.28 40.89 o 5 7 0 257.54 227.00 13.60 o 7 7 0 710.97 703.43 23.89 o 9 7 0 255.48 268.27 17.14 o 11 7 0 177.40 146.32 14.52 o 13 7 0 137.12 128.77 14.49 o 0 8 0 70.14 63.82 10.41 o 2 8 0 6878.95 6900.99 139.93 o 4 8 0 7582.45 7414.99 226.25 o 6 8 0 10163.75 10068.66 272.60 o 8 8 0 1166.57 1119.16 38.75 o 10 8 0 1837.73 1697.04 45.47 o 12 8 0 703.27 729.55 37.56 o 1 9 0 24.49 15.50 5.91 o 3 9 0 2.26 -2.66 8.82 o 5 9 0 79.07 95.03 13.00 o 7 9 0 72.79 62.86 9.75 o 9 9 0 22.85 16.54 8.02 o 11 9 0 16.70 4.80 8.45 o 0 10 0 3311.79 3172.61 92.27 o 2 10 0 3732.55 3504.61 84.30 o 4 10 0 1167.89 1216.06 40.59 o 6 10 0 3483.54 3314.85 84.37 o 8 10 0 1672.14 1705.76 56.28 o 10 10 0 996.29 1013.10 43.81 o 1 11 0 0.04 -9.99 6.66 o 3 11 0 536.92 476.11 26.36 o 5 11 0 35.97 38.42 11.61 o 7 11 0 28.30 65.80 17.96 o 9 11 0 136.86 128.60 23.50 o 0 12 0 4383.96 4242.92 185.48 o 2 12 0 1037.59 862.69 36.36 o 4 12 0 989.45 953.80 37.85 o 6 12 0 442.43 420.07 76.21 o 8 12 0 1695.52 1711.64 63.54 o 1 13 0 46.26 37.77 24.12 o 3 13 0 99.30 80.73 15.53 o 5 13 0 364.80 318.27 34.57 o 0 14 0 83.05 46.31 25.48 o 2 14 0 1316.24 1179.66 104.41 o -15 1 1 579.22 522.44 25.76 o -13 1 1 2341.72 2473.90 66.88 o -11 1 1 3046.73 2985.67 56.12 o -9 1 1 14404.39 14017.92 194.29 o -7 1 1 12945.58 12734.03 260.61 o -5 1 1 16329.12 16423.74 243.39 o -3 1 1 55.25 19.38 2.87 o -1 1 1 20862.45 22851.99 425.17 o 3 1 1 94566.12 80016.15 2589.98 o 5 1 1 7957.80 7628.32 116.04 o 7 1 1 6410.56 6678.21 95.65 o 9 1 1 2473.01 2419.58 41.10 o 11 1 1 7432.44 7560.24 123.54 o 13 1 1 1792.41 1795.08 46.81 o 15 1 1 991.02 947.99 33.94 o -14 2 1 43.81 35.38 9.33 o -12 2 1 6.15 1.69 6.57 o -10 2 1 222.18 182.74 11.55 o -8 2 1 2098.02 2174.70 36.44 o -6 2 1 3967.32 4040.84 64.97 o -4 2 1 823.99 536.80 10.82 o -2 2 1 2579.10 2794.52 44.31 o 0 2 1 26221.69 24490.26 619.65 o 2 2 1 283.99 295.65 9.69 o 4 2 1 1123.46 1126.33 21.39 o 6 2 1 3708.15 3436.79 51.76 o 8 2 1 194.18 177.49 8.79 o 10 2 1 76.79 76.00 8.21 o 12 2 1 458.27 417.35 17.42 o 14 2 1 110.54 125.99 14.01 o -15 3 1 1096.62 1100.18 37.45 o -13 3 1 746.47 740.19 30.90 o -11 3 1 5760.16 5837.35 121.41 o -9 3 1 2236.33 2091.12 62.12 o -7 3 1 12917.05 12889.11 195.96 o -5 3 1 21987.17 23716.53 318.40 o -3 3 1 41150.09 39708.82 580.00 o -1 3 1 37.63 44.69 3.69 o 1 3 1 17971.46 17995.91 263.95 o 3 3 1 21284.72 20712.54 277.56 o 5 3 1 24719.70 24173.89 328.80 o 7 3 1 5607.67 5208.31 95.21 o 9 3 1 10261.93 9907.06 155.61 o 11 3 1 1173.24 1168.44 29.32 o 13 3 1 2053.18 1927.59 55.31 o 15 3 1 519.13 508.42 33.29 o -14 4 1 243.48 238.86 18.41 o -12 4 1 87.42 52.01 8.99 o -10 4 1 102.13 108.23 10.43 o -8 4 1 1797.70 1839.39 36.95 o -6 4 1 88.65 94.50 6.91 o -4 4 1 330.63 355.79 20.20 o -2 4 1 6805.02 8076.73 121.80 o 0 4 1 6767.09 7302.43 109.55 o 2 4 1 33.84 58.32 3.71 o 4 4 1 2.30 14.38 3.13 o 6 4 1 995.12 883.22 24.13 o 8 4 1 282.86 301.91 12.72 o 10 4 1 496.69 495.68 17.30 o 12 4 1 339.67 309.02 18.83 o 14 4 1 11.58 -2.16 7.26 o -13 5 1 1188.20 1231.09 37.74 o -11 5 1 2203.13 2267.02 53.72 o -9 5 1 8609.45 8613.89 155.11 o -7 5 1 3430.70 3579.88 76.55 o -5 5 1 15466.09 15965.82 247.31 o -3 5 1 5384.88 5636.63 79.73 o -1 5 1 16216.82 15272.49 226.13 o 1 5 1 9630.25 8511.90 146.08 o 3 5 1 41224.23 39630.01 562.12 o 5 5 1 3593.16 3302.95 66.09 o 7 5 1 3085.98 3116.33 61.90 o 9 5 1 2734.40 2595.36 61.44 o 11 5 1 6557.35 6328.59 121.03 o 13 5 1 665.88 697.24 31.23 o -14 6 1 7.48 10.47 9.31 o -12 6 1 41.12 32.15 9.44 o -10 6 1 193.68 179.47 15.31 o -8 6 1 247.03 279.45 18.11 o -6 6 1 30.98 23.35 6.50 o -4 6 1 471.02 530.16 19.76 o -2 6 1 4268.34 4352.82 69.99 o 0 6 1 8019.31 8066.09 122.07 o 2 6 1 146.17 121.93 5.51 o 4 6 1 85.78 83.45 8.42 o 6 6 1 494.22 525.33 17.35 o 8 6 1 658.70 646.91 23.03 o 10 6 1 114.87 97.83 11.86 o 12 6 1 0.96 -8.68 6.81 o 14 6 1 8.26 9.16 9.17 o -13 7 1 448.73 450.84 24.86 o -11 7 1 1708.06 1641.80 62.50 o -9 7 1 3208.58 3167.62 113.50 o -7 7 1 3373.06 3548.55 72.40 o -5 7 1 10578.10 10648.10 185.72 o -3 7 1 9477.99 9393.36 144.61 o -1 7 1 3789.82 3521.29 59.40 o 1 7 1 8749.33 8275.88 127.23 o 3 7 1 9969.82 9822.06 150.49 o 5 7 1 3666.43 3595.97 70.82 o 7 7 1 3928.78 3957.59 85.61 o 9 7 1 3898.77 3612.33 131.70 o 11 7 1 1669.34 1568.58 46.24 o 13 7 1 509.90 480.05 24.70 o -12 8 1 82.26 71.94 12.57 o -10 8 1 220.64 197.16 16.07 o -8 8 1 176.70 159.53 13.79 o -6 8 1 43.91 47.71 13.35 o -4 8 1 5.24 1.67 8.18 o -2 8 1 2625.75 2493.86 55.28 o 0 8 1 1261.64 1245.91 30.36 o 2 8 1 164.84 188.26 11.61 o 4 8 1 65.87 61.81 8.04 o 6 8 1 861.95 863.97 31.41 o 8 8 1 801.28 768.17 28.03 o 10 8 1 18.92 12.41 8.38 o 12 8 1 9.79 4.66 8.73 o -11 9 1 1135.02 1136.81 47.73 o -9 9 1 791.85 796.25 28.67 o -7 9 1 4196.12 3956.87 100.29 o -5 9 1 1573.88 1538.35 46.98 o -3 9 1 11102.05 10749.55 218.69 o -1 9 1 4610.53 4630.84 175.38 o 1 9 1 4420.67 4283.08 81.80 o 3 9 1 299.94 282.64 19.24 o 5 9 1 8446.67 7901.69 174.33 o 7 9 1 2272.52 2290.76 89.16 o 9 9 1 2286.61 2324.19 60.74 o 11 9 1 243.49 189.31 16.99 o -10 10 1 7.38 -2.96 9.95 o -8 10 1 403.39 413.84 32.36 o -6 10 1 633.78 700.00 30.97 o -4 10 1 0.89 -7.93 6.81 o -2 10 1 34.02 25.59 8.53 o 0 10 1 1067.23 1016.59 28.70 o 2 10 1 40.93 44.15 11.75 o 4 10 1 13.60 13.43 8.45 o 6 10 1 1166.12 1120.05 40.74 o 8 10 1 0.29 1.56 9.49 o 10 10 1 11.87 8.20 11.52 o -9 11 1 1826.48 1884.19 96.99 o -7 11 1 1058.46 1042.24 40.41 o -5 11 1 1431.42 1380.75 58.09 o -3 11 1 976.34 935.70 53.78 o -1 11 1 4310.16 4039.30 113.59 o 1 11 1 3815.01 3616.89 148.41 o 3 11 1 3362.45 3203.11 81.05 o 5 11 1 910.23 738.88 81.70 o 7 11 1 1394.18 1378.39 78.67 o 9 11 1 344.52 286.60 24.81 o -8 12 1 94.79 68.83 23.89 o -6 12 1 16.70 4.83 9.28 o -4 12 1 2.41 -5.45 8.64 o -2 12 1 119.14 141.81 16.38 o 0 12 1 26.66 1.18 22.93 o 2 12 1 10.81 20.55 9.65 o 4 12 1 279.14 309.37 31.97 o 6 12 1 0.06 7.77 10.37 o 8 12 1 1.54 -2.37 9.96 o -5 13 1 686.68 707.44 35.37 o -3 13 1 1059.33 1028.96 40.53 o -1 13 1 1414.29 1301.98 60.69 o 1 13 1 1657.78 1485.64 65.89 o 3 13 1 1123.25 1022.14 62.12 o 5 13 1 1166.99 1150.83 44.86 o -2 14 1 22.79 36.56 22.70 o 0 14 1 12.65 32.65 15.92 o 2 14 1 91.40 58.59 31.76 o -14 0 2 1791.23 1829.04 68.28 o -12 0 2 764.57 795.54 38.29 o -10 0 2 9944.85 10125.01 203.68 o -8 0 2 5780.56 5442.89 112.77 o -6 0 2 14395.68 13608.86 262.53 o -4 0 2 1344.76 1058.93 25.53 o -2 0 2 114112.43 112283.32 2108.75 o 0 0 2 2082.13 2150.59 55.80 o 2 0 2 30086.47 30753.43 584.20 o 4 0 2 49096.86 49315.81 1138.10 o 6 0 2 62446.54 56766.63 1068.91 o 8 0 2 40.82 34.28 11.60 o 10 0 2 1914.15 1998.04 53.88 o 12 0 2 838.07 866.90 43.04 o 14 0 2 2746.43 2672.24 90.11 o -15 1 2 73.76 76.77 15.46 o -13 1 2 73.79 63.95 11.92 o -11 1 2 161.37 168.11 11.41 o -9 1 2 864.51 849.17 22.53 o -7 1 2 411.99 335.52 18.90 o -5 1 2 1649.14 1319.60 22.18 o -3 1 2 7067.04 6179.18 213.00 o -1 1 2 120.39 332.11 7.79 o 1 1 2 2302.80 2856.87 40.39 o 3 1 2 31420.39 31196.80 415.03 o 5 1 2 8.97 1.21 2.75 o 7 1 2 2471.93 2404.30 39.23 o 9 1 2 3417.06 3261.38 71.96 o 11 1 2 1479.43 1441.10 29.73 o 13 1 2 0.06 6.10 7.09 o 15 1 2 20.20 4.59 7.89 o -14 2 2 1035.64 1029.23 64.86 o -12 2 2 1926.46 1937.86 47.90 o -10 2 2 1821.44 1886.76 38.87 o -8 2 2 11321.07 11511.37 198.78 o -6 2 2 11452.74 10539.12 178.97 o -4 2 2 15769.85 15727.76 233.29 o -2 2 2 27495.13 27152.64 444.66 o 0 2 2 45684.95 42047.69 608.99 o 2 2 2 7741.25 8957.26 193.54 o 4 2 2 31936.10 31737.77 514.91 o 6 2 2 32037.06 31562.36 464.18 o 8 2 2 6170.46 6096.29 97.71 o 10 2 2 137.10 131.82 9.13 o 12 2 2 2433.01 2281.34 47.72 o 14 2 2 1122.36 1158.10 36.94 o -15 3 2 6.13 3.56 9.10 o -13 3 2 5.58 3.14 11.67 o -11 3 2 125.91 110.65 9.71 o -9 3 2 97.71 90.24 8.24 o -7 3 2 1414.00 1513.23 30.56 o -5 3 2 420.98 368.61 11.34 o -3 3 2 6929.99 7003.49 106.57 o -1 3 2 101.47 42.41 4.76 o 1 3 2 1291.39 977.20 17.96 o 3 3 2 2573.47 2768.58 41.31 o 5 3 2 471.91 464.27 11.86 o 7 3 2 1500.29 1479.20 27.30 o 9 3 2 37.34 50.39 8.61 o 11 3 2 89.55 105.99 9.90 o 13 3 2 11.90 6.94 6.54 o 15 3 2 7.95 2.76 8.30 o -14 4 2 1189.19 1125.11 78.14 o -12 4 2 1798.31 1790.08 49.67 o -10 4 2 1598.79 1709.76 55.32 o -8 4 2 5588.13 5971.24 103.90 o -6 4 2 10929.52 10703.98 163.93 o -4 4 2 15951.33 16927.19 252.07 o -2 4 2 17569.18 18520.21 272.35 o 0 4 2 15367.17 14458.45 195.14 o 2 4 2 20844.00 22294.20 299.03 o 4 4 2 20760.21 20288.34 273.65 o 6 4 2 7776.95 7254.76 103.66 o 8 4 2 5299.46 5345.09 89.04 o 10 4 2 2063.66 1946.59 73.81 o 12 4 2 1514.60 1533.60 36.83 o 14 4 2 790.06 737.30 27.23 o -13 5 2 0.35 -0.90 7.77 o -11 5 2 176.41 172.78 14.41 o -9 5 2 465.88 462.79 25.03 o -7 5 2 167.18 181.21 10.09 o -5 5 2 24.43 27.84 4.55 o -3 5 2 3533.47 3573.32 58.11 o -1 5 2 1309.15 1542.44 32.46 o 1 5 2 365.83 322.15 9.53 o 3 5 2 933.84 1024.73 18.98 o 5 5 2 78.22 104.91 6.61 o 7 5 2 649.09 615.13 17.89 o 9 5 2 7.16 0.02 4.90 o 11 5 2 11.84 8.39 6.68 o 13 5 2 49.33 45.61 10.51 o -14 6 2 1241.31 1323.06 41.41 o -12 6 2 667.58 726.18 39.83 o -10 6 2 2868.05 3026.93 66.22 o -8 6 2 1383.40 1290.44 34.27 o -6 6 2 13478.56 13731.07 235.19 o -4 6 2 8094.52 8450.40 147.79 o -2 6 2 13084.97 13199.14 222.83 o 0 6 2 5907.40 6147.57 127.16 o 2 6 2 23751.74 22907.10 338.51 o 4 6 2 3563.27 3820.38 107.95 o 6 6 2 8879.47 8744.81 137.51 o 8 6 2 1735.07 1666.45 41.22 o 10 6 2 3893.70 3667.45 77.22 o 12 6 2 611.95 573.23 25.07 o 14 6 2 1191.64 1224.20 40.13 o -13 7 2 63.06 62.48 11.86 o -11 7 2 273.20 265.45 25.81 o -9 7 2 320.04 338.68 18.64 o -7 7 2 19.08 18.78 7.17 o -5 7 2 1532.80 1516.52 36.81 o -3 7 2 2298.99 2401.81 59.32 o -1 7 2 97.70 135.48 7.91 o 1 7 2 190.42 219.53 12.84 o 3 7 2 5389.17 5328.67 85.95 o 5 7 2 1653.84 1732.00 40.25 o 7 7 2 70.67 66.65 10.46 o 9 7 2 1258.79 1213.88 39.57 o 11 7 2 407.21 469.40 23.22 o 13 7 2 0.05 -3.86 8.59 o -12 8 2 626.82 591.36 26.57 o -10 8 2 179.51 167.66 15.23 o -8 8 2 5066.13 5025.50 99.21 o -6 8 2 4522.28 4374.35 86.09 o -4 8 2 7277.99 7268.83 131.54 o -2 8 2 3572.43 3397.94 66.79 o 0 8 2 12184.41 12072.36 205.78 o 2 8 2 2818.51 2897.80 68.34 o 4 8 2 5602.35 5329.12 116.58 o 6 8 2 1592.49 1575.12 39.47 o 8 8 2 4943.71 5008.52 98.77 o 10 8 2 1127.10 1182.16 40.96 o 12 8 2 1335.15 1364.91 42.14 o -11 9 2 5.99 6.15 10.41 o -9 9 2 34.19 49.75 10.25 o -7 9 2 25.83 6.24 6.87 o -5 9 2 76.07 78.08 9.85 o -3 9 2 182.17 162.99 15.48 o -1 9 2 410.67 448.20 22.17 o 1 9 2 29.24 18.34 13.98 o 3 9 2 1225.05 1207.15 38.48 o 5 9 2 156.58 134.76 14.93 o 7 9 2 68.93 68.51 16.71 o 9 9 2 121.76 122.77 16.57 o 11 9 2 34.57 32.25 10.22 o -10 10 2 521.71 540.94 31.59 o -8 10 2 2349.98 2367.67 67.99 o -6 10 2 1892.97 1986.65 117.01 o -4 10 2 3377.24 3220.70 80.52 o -2 10 2 2763.52 2720.66 69.79 o 0 10 2 4918.45 4707.21 106.85 o 2 10 2 1480.06 1577.56 38.90 o 4 10 2 2776.85 2534.01 67.28 o 6 10 2 1785.54 1655.70 54.11 o 8 10 2 1561.12 1547.64 60.80 o 10 10 2 845.56 846.65 38.83 o -9 11 2 5.73 2.87 10.60 o -7 11 2 41.43 41.92 15.47 o -5 11 2 93.95 104.97 15.08 o -3 11 2 742.37 710.12 30.67 o -1 11 2 1.55 -2.25 7.73 o 1 11 2 132.22 138.05 13.29 o 3 11 2 720.37 685.40 30.00 o 5 11 2 90.92 91.45 14.40 o 7 11 2 7.85 5.62 13.33 o 9 11 2 56.37 33.39 13.17 o -8 12 2 924.29 902.04 40.20 o -6 12 2 2046.19 2076.39 63.68 o -4 12 2 517.54 613.57 42.74 o -2 12 2 2245.99 2264.44 64.30 o 0 12 2 685.99 594.46 37.98 o 2 12 2 1416.38 1338.56 85.38 o 4 12 2 994.19 963.26 38.29 o 6 12 2 2531.29 2445.17 71.40 o 8 12 2 444.90 444.74 39.65 o -5 13 2 137.83 152.34 19.23 o -3 13 2 46.76 42.21 12.90 o -1 13 2 41.17 40.49 16.44 o 1 13 2 333.06 354.23 34.99 o 3 13 2 290.63 259.10 30.49 o 5 13 2 63.63 68.14 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