#------------------------------------------------------------------------------
#$Date: 2016-04-03 04:57:59 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181207 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/86/2228655.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2228655_Fobs
loop_
_publ_author_name
'Kriel, Frederik H.'
'Fernandes, Manuel A.'
'Coates, Judy'
_publ_section_title
;
 [\m-1,2-Bis(diphenylphosphanyl)-1,2-dimethylhydrazine-\k^2^<i>P</i>:<i>P</i>']bis[chloridogold(I)]
;
_journal_coeditor_code           BR2152
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m42
_journal_volume                  67
_journal_year                    2011
_space_group_IT_number           92
_symmetry_space_group_name_Hall  'P 4abw 2nw'
_symmetry_space_group_name_H-M   'P 41 21 2'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   10.6720
_cell_length_b                   10.6720
_cell_length_c                   23.4391
_exptl_crystal_F_000             1672.00
_reflns_d_resolution_high        0.7498
_cod_data_source_file            br2152Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' 5mml18_a in P4(3)2(1)2'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            545.03
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'x+1/2, -y+1/2, -z+3/4'
'-x+1/2, y+1/2, -z+1/4'
'-y, -x, -z+1/2'
'y, x, -z'
'y+1/2, -x+1/2, z+3/4'
'-y+1/2, x+1/2, z+1/4'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 1 0 104579.29 109968.34 6515.06 o
0 2 0 59492.25 59156.16 2610.51 o
1 2 0 48651.45 49885.85 1113.70 o
2 2 0 891.93 1340.26 109.80 o
1 3 0 9707.29 10534.65 234.88 o
2 3 0 114089.91 118096.29 2726.07 o
3 3 0 5978.91 6552.63 200.85 o
0 4 0 66501.68 69130.33 851.15 o
1 4 0 52171.26 52442.35 815.60 o
2 4 0 18806.46 19455.54 344.37 o
3 4 0 101406.82 100192.16 2236.07 o
4 4 0 1705.00 1538.02 161.08 o
1 5 0 153940.47 158342.52 1881.53 o
2 5 0 14556.50 14845.71 248.31 o
3 5 0 77.28 -16.56 100.24 o
4 5 0 10639.77 10727.66 282.42 o
5 5 0 75093.34 73397.67 1845.64 o
0 6 0 162671.41 161935.44 2067.71 o
1 6 0 1855.43 2050.55 142.16 o
2 6 0 31501.18 31415.85 343.28 o
3 6 0 6356.08 6611.74 193.64 o
4 6 0 21175.59 20692.43 315.70 o
5 6 0 2209.71 2115.34 185.76 o
6 6 0 44807.19 46116.77 1570.01 o
1 7 0 33708.25 33666.77 407.52 o
2 7 0 11064.88 11555.98 280.64 o
3 7 0 257.95 203.65 152.40 o
4 7 0 24438.36 24857.11 762.09 o
5 7 0 32056.34 31506.34 771.28 o
6 7 0 64.47 102.18 285.82 o
7 7 0 7358.62 7675.91 1016.22 o
0 8 0 8300.48 7860.65 433.71 o
1 8 0 14028.32 14406.22 354.34 o
2 8 0 15.75 7.12 182.44 o
3 8 0 33021.41 33037.02 449.73 o
4 8 0 19191.18 19484.48 695.32 o
5 8 0 4834.80 4968.96 336.48 o
6 8 0 5576.85 5718.10 415.60 o
7 8 0 1644.71 1711.13 402.32 o
8 8 0 7117.14 7057.61 746.34 o
1 9 0 709.99 748.44 232.21 o
2 9 0 45135.51 45882.89 665.93 o
3 9 0 7170.48 7213.52 398.58 o
4 9 0 26675.21 26298.75 621.19 o
5 9 0 190.52 47.16 358.97 o
6 9 0 2721.98 2806.92 484.52 o
7 9 0 2960.04 3373.00 524.69 o
8 9 0 15666.94 15465.93 820.89 o
9 9 0 8423.84 10359.28 1193.81 o
0 10 0 24533.48 23557.22 694.32 o
1 10 0 2314.51 2590.84 324.79 o
2 10 0 1834.14 2159.96 331.26 o
3 10 0 18901.75 19329.88 609.27 o
4 10 0 18.64 -93.65 417.53 o
5 10 0 4.18 -61.17 398.33 o
6 10 0 4594.27 4416.66 559.90 o
7 10 0 8123.96 9296.11 655.14 o
8 10 0 9895.61 10462.39 731.80 o
9 10 0 2439.10 2605.77 752.10 o
10 10 0 426.91 796.46 1086.52 o
1 11 0 9997.73 9784.88 478.56 o
2 11 0 1583.88 1498.16 368.37 o
3 11 0 1414.22 1337.65 411.47 o
4 11 0 243.93 -173.94 457.67 o
5 11 0 6130.61 6204.97 596.63 o
6 11 0 381.70 429.03 590.74 o
7 11 0 3947.90 4979.63 651.96 o
8 11 0 390.56 241.33 609.23 o
9 11 0 1146.23 530.92 783.52 o
0 12 0 5676.02 5223.98 997.02 o
1 12 0 6.48 -420.82 420.82 o
2 12 0 1192.74 935.27 483.14 o
3 12 0 146.80 -195.75 509.57 o
4 12 0 854.92 943.24 553.04 o
5 12 0 2454.20 2818.37 701.14 o
6 12 0 3318.86 2978.03 740.82 o
7 12 0 2314.29 1568.75 732.92 o
1 13 0 1537.93 1683.74 543.40 o
2 13 0 921.56 474.64 630.07 o
3 13 0 1657.58 1882.49 665.53 o
4 13 0 2825.21 2458.58 646.70 o
5 13 0 1841.93 1790.60 749.02 o
0 14 0 497.89 43.80 781.78 o
1 14 0 1444.43 1198.76 714.54 o
2 14 0 464.40 1180.05 715.06 o
0 1 1 72404.32 72503.47 2752.98 o
1 1 1 39288.27 39951.84 1155.32 o
-1 2 1 42710.64 44709.09 898.40 o
0 2 1 91887.16 96961.92 3404.07 o
1 2 1 34620.25 35647.47 519.16 o
2 2 1 12946.13 13075.92 402.45 o
-2 3 1 23892.12 25045.40 598.40 o
-1 3 1 129140.07 135608.11 2555.03 o
0 3 1 100455.28 101529.91 4685.93 o
1 3 1 123132.25 131785.14 2318.96 o
2 3 1 23883.67 24491.30 454.68 o
3 3 1 11584.18 11675.66 257.89 o
-3 4 1 11159.43 11792.99 259.64 o
-2 4 1 45997.89 49181.19 898.63 o
-1 4 1 47674.64 48800.58 756.62 o
0 4 1 62158.38 62851.25 2533.58 o
1 4 1 46014.05 46647.85 757.87 o
2 4 1 45732.17 48976.41 798.19 o
3 4 1 8296.59 8537.52 212.90 o
4 4 1 73736.96 70817.97 1148.83 o
-4 5 1 21236.87 21207.89 501.38 o
-3 5 1 87283.51 86236.62 1600.87 o
-2 5 1 43265.96 44542.61 869.85 o
-1 5 1 47728.03 49477.96 779.22 o
0 5 1 565.91 514.86 94.35 o
1 5 1 47105.52 49130.25 698.80 o
2 5 1 43648.56 44304.95 705.80 o
3 5 1 88450.87 86376.20 2003.53 o
4 5 1 20070.60 19671.57 404.80 o
5 5 1 44071.57 42278.78 795.24 o
-5 6 1 7889.14 7759.97 287.45 o
-4 6 1 38270.52 36905.48 796.53 o
-3 6 1 35967.68 35848.85 656.87 o
-2 6 1 31723.39 32187.53 487.55 o
-1 6 1 20571.92 20690.22 330.84 o
0 6 1 2328.55 2266.81 138.28 o
1 6 1 23577.64 23963.90 426.53 o
2 6 1 27834.50 28282.79 340.20 o
3 6 1 37283.24 36658.75 553.10 o
4 6 1 40212.08 39260.44 1057.31 o
5 6 1 7765.20 8164.00 300.00 o
6 6 1 1511.47 1724.54 283.51 o
-6 7 1 14329.20 14170.20 510.53 o
-5 7 1 745.85 546.33 250.44 o
-4 7 1 13429.26 13840.73 351.79 o
-3 7 1 9571.39 9945.86 258.71 o
-2 7 1 23862.56 23774.55 415.22 o
-1 7 1 2375.98 2715.11 192.78 o
0 7 1 18948.83 18822.00 366.40 o
1 7 1 2153.24 2404.96 182.05 o
2 7 1 26619.39 26849.22 495.82 o
3 7 1 11869.37 12620.59 286.80 o
4 7 1 13750.36 13550.96 400.75 o
5 7 1 923.09 839.20 259.55 o
6 7 1 15067.26 15077.09 515.52 o
7 7 1 696.75 823.07 314.36 o
-7 8 1 19429.45 18950.66 826.52 o
-6 8 1 6338.37 6831.83 433.42 o
-5 8 1 10257.08 10575.27 406.83 o
-4 8 1 3600.07 3741.69 327.42 o
-3 8 1 9910.56 10651.10 330.83 o
-2 8 1 739.33 775.41 198.32 o
-1 8 1 19311.15 19302.26 456.05 o
0 8 1 13114.42 13078.99 358.88 o
1 8 1 20732.15 20622.89 381.24 o
2 8 1 379.87 526.95 181.66 o
3 8 1 8729.07 9348.02 334.57 o
4 8 1 3085.51 3052.30 339.09 o
5 8 1 9857.59 10255.54 440.97 o
6 8 1 7063.32 7370.80 448.71 o
7 8 1 20013.57 19834.69 732.03 o
8 8 1 1501.55 2334.44 463.60 o
-8 9 1 1947.88 2126.25 545.01 o
-7 9 1 4080.57 4597.47 551.46 o
-6 9 1 8054.48 8887.59 603.89 o
-5 9 1 21301.55 22072.08 841.65 o
-4 9 1 2656.13 2466.99 330.76 o
-3 9 1 5728.75 5590.93 314.49 o
-2 9 1 3755.64 4123.39 292.10 o
-1 9 1 14143.34 14004.50 407.30 o
0 9 1 20159.70 19933.42 570.50 o
1 9 1 15263.20 14955.34 406.58 o
2 9 1 3890.50 3852.59 328.17 o
3 9 1 5911.85 6753.39 342.59 o
4 9 1 3520.57 4181.84 358.59 o
5 9 1 19202.34 18636.03 790.59 o
6 9 1 6589.71 7771.32 573.93 o
7 9 1 3127.17 3008.72 531.09 o
8 9 1 2174.84 2248.61 543.01 o
9 9 1 3819.32 4305.55 801.63 o
-9 10 1 397.93 105.81 678.17 o
-8 10 1 1703.98 1094.75 556.41 o
-7 10 1 633.44 189.50 511.47 o
-6 10 1 6912.72 6594.80 644.87 o
-5 10 1 1706.02 1498.26 426.92 o
-4 10 1 23562.24 25329.91 1267.76 o
-3 10 1 744.23 769.95 311.03 o
-2 10 1 17433.93 17269.15 545.30 o
-1 10 1 3537.37 3516.85 330.85 o
0 10 1 12383.21 11782.57 423.93 o
1 10 1 2970.15 2762.13 333.16 o
2 10 1 16966.75 17224.92 543.27 o
3 10 1 866.42 725.23 337.26 o
4 10 1 21402.67 22096.63 797.79 o
5 10 1 1686.72 1903.53 426.03 o
6 10 1 7389.93 7791.99 613.25 o
7 10 1 622.71 771.50 516.47 o
8 10 1 2104.10 2515.05 580.90 o
9 10 1 587.08 -64.33 635.52 o
10 10 1 6112.47 6888.94 874.79 o
-9 11 1 3855.66 2706.48 806.87 o
-8 11 1 1533.48 2223.94 639.59 o
-7 11 1 393.43 -553.64 553.64 o
-6 11 1 487.04 298.07 583.75 o
-5 11 1 7484.00 7373.37 625.47 o
-4 11 1 1347.91 1682.53 509.61 o
-3 11 1 10190.21 11098.27 582.46 o
-2 11 1 2833.55 2941.79 397.33 o
-1 11 1 3779.46 3917.41 453.47 o
0 11 1 1554.29 1812.53 413.74 o
1 11 1 3782.53 3886.00 379.61 o
2 11 1 3241.22 3676.54 407.26 o
3 11 1 11210.61 12302.59 645.32 o
4 11 1 1609.45 2363.25 564.08 o
5 11 1 6367.63 6720.09 607.08 o
6 11 1 684.07 508.06 597.60 o
7 11 1 301.34 287.74 566.08 o
8 11 1 1778.73 2031.06 629.52 o
9 11 1 3554.40 2984.66 1132.49 o
-7 12 1 6098.91 5728.73 804.87 o
-6 12 1 948.53 617.57 660.19 o
-5 12 1 1452.28 1583.18 649.46 o
-4 12 1 2912.15 3324.03 594.96 o
-3 12 1 6716.56 6658.19 539.78 o
-2 12 1 1527.55 735.33 482.39 o
-1 12 1 2655.05 3104.14 478.07 o
0 12 1 1798.78 2000.22 463.05 o
1 12 1 3052.50 3121.64 474.67 o
2 12 1 1225.92 1114.05 472.19 o
3 12 1 6979.59 6827.87 679.65 o
4 12 1 3423.67 3545.49 600.94 o
5 12 1 1339.23 -83.99 636.12 o
6 12 1 855.89 482.23 684.63 o
7 12 1 7101.72 7480.04 1092.06 o
-5 13 1 929.03 644.01 702.40 o
-4 13 1 610.11 736.03 613.86 o
-3 13 1 77.88 -616.57 616.57 o
-2 13 1 5759.72 5936.88 745.97 o
-1 13 1 235.37 71.41 527.11 o
0 13 1 2233.01 2164.55 533.32 o
1 13 1 195.85 -240.37 513.34 o
2 13 1 7065.41 5919.75 740.74 o
3 13 1 102.58 -367.69 574.31 o
4 13 1 585.02 857.62 602.88 o
5 13 1 996.83 829.22 737.35 o
-2 14 1 1084.59 403.31 691.36 o
-1 14 1 3396.62 2444.10 632.58 o
0 14 1 489.65 -301.27 539.83 o
1 14 1 2904.52 2466.74 743.23 o
2 14 1 960.74 628.27 698.27 o
0 1 2 110214.91 109216.56 2022.61 o
1 1 2 17126.35 17843.11 850.49 o
-1 2 2 28296.28 30359.80 800.53 o
0 2 2 1008.72 891.50 59.57 o
1 2 2 24200.96 25548.00 476.68 o
2 2 2 59444.53 61465.77 1513.29 o
-2 3 2 1267.07 1724.85 92.83 o
-1 3 2 50743.56 52851.24 938.79 o
0 3 2 142.50 254.16 72.93 o
1 3 2 42186.90 43789.14 596.56 o
2 3 2 1940.32 2470.63 109.62 o
3 3 2 35142.88 35102.99 633.66 o
-3 4 2 4548.61 4804.84 162.40 o
-2 4 2 73181.62 76450.77 1517.02 o
-1 4 2 25212.01 26708.88 512.18 o
0 4 2 18414.30 19427.85 274.72 o
1 4 2 20443.71 21342.99 248.13 o
2 4 2 70890.54 74415.22 1238.24 o
3 4 2 2851.27 3047.90 140.52 o
4 4 2 18751.84 19207.45 397.55 o
-4 5 2 9093.01 9541.72 242.94 o
-3 5 2 10895.94 11141.34 239.86 o
-2 5 2 20160.01 20520.06 283.94 o
-1 5 2 15739.62 16003.66 557.23 o
0 5 2 84208.19 84755.38 1522.18 o
1 5 2 14268.51 14305.99 416.92 o
2 5 2 22124.63 22639.80 354.74 o
3 5 2 10551.60 10703.43 232.74 o
4 5 2 10335.08 10494.38 258.42 o
5 5 2 1745.12 1813.94 172.06 o
-5 6 2 27591.25 26352.58 847.83 o
-4 6 2 9638.23 9674.42 275.91 o
-3 6 2 14655.30 14684.66 396.93 o
-2 6 2 5082.28 5756.42 193.13 o
-1 6 2 33971.52 34129.57 833.32 o
0 6 2 197.51 264.00 116.70 o
1 6 2 29728.43 30556.75 462.08 o
2 6 2 4947.00 5482.41 171.97 o
3 6 2 13749.88 13389.68 240.57 o
4 6 2 8876.27 8526.22 279.04 o
5 6 2 29500.02 28855.39 799.81 o
6 6 2 1412.62 1407.26 285.35 o
-6 7 2 9048.42 10023.97 490.21 o
-5 7 2 16562.92 15866.28 465.85 o
-4 7 2 7451.13 7915.79 283.04 o
-3 7 2 10840.07 11381.88 386.83 o
-2 7 2 9175.06 9739.20 269.83 o
-1 7 2 10848.61 10344.60 294.86 o
0 7 2 19449.99 19538.90 501.98 o
1 7 2 10834.63 10607.40 271.21 o
2 7 2 8013.94 8495.50 249.42 o
3 7 2 11532.26 11193.60 271.00 o
4 7 2 8869.36 9022.15 338.01 o
5 7 2 18923.46 19406.64 579.37 o
6 7 2 8324.85 9049.50 425.05 o
7 7 2 52.71 -45.10 299.33 o
-7 8 2 986.98 1578.12 409.09 o
-6 8 2 9181.60 9332.27 460.72 o
-5 8 2 10396.99 10759.75 418.02 o
-4 8 2 19263.17 18728.64 535.35 o
-3 8 2 3540.76 3866.36 232.94 o
-2 8 2 13189.12 13197.94 350.48 o
-1 8 2 2926.74 3229.07 223.92 o
0 8 2 26337.22 26021.66 431.26 o
1 8 2 1998.09 2008.36 197.86 o
2 8 2 11122.06 11462.09 317.36 o
3 8 2 4730.18 4976.49 273.47 o
4 8 2 18527.46 18963.14 553.63 o
5 8 2 10533.92 10965.22 495.44 o
6 8 2 9998.40 9878.95 522.52 o
7 8 2 1127.45 1337.17 403.40 o
8 8 2 1704.96 1959.46 451.61 o
-8 9 2 5342.71 6652.72 662.66 o
-7 9 2 14179.92 14724.43 729.84 o
-6 9 2 3130.61 3266.78 496.82 o
-5 9 2 12843.97 12679.08 544.06 o
-4 9 2 1357.47 1028.81 317.25 o
-3 9 2 14769.08 15383.04 442.86 o
-2 9 2 528.47 66.96 226.17 o
-1 9 2 35726.60 35525.96 773.36 o
0 9 2 622.19 542.65 227.83 o
1 9 2 37124.66 36508.33 552.14 o
2 9 2 613.23 679.36 253.53 o
3 9 2 15100.41 15169.83 468.01 o
4 9 2 1708.51 1778.21 348.76 o
5 9 2 12361.40 12312.10 584.19 o
6 9 2 3338.44 3114.15 498.15 o
7 9 2 14852.97 14624.24 781.15 o
8 9 2 5166.12 5174.66 583.12 o
9 9 2 2912.12 2748.54 649.30 o
-9 10 2 2174.25 2652.17 735.81 o
-8 10 2 3866.00 4075.00 642.27 o
-7 10 2 8112.32 8296.18 656.23 o
-6 10 2 10990.38 12228.87 838.62 o
-5 10 2 1510.04 935.64 409.16 o
-4 10 2 3071.24 3156.42 491.13 o
-3 10 2 8463.43 8418.88 418.74 o
-2 10 2 14315.67 14367.19 512.80 o
-1 10 2 7698.18 7460.57 362.26 o
0 10 2 23306.54 22167.90 576.95 o
1 10 2 7501.84 7473.55 392.94 o
2 10 2 13517.21 13232.32 499.60 o
3 10 2 8587.33 9271.43 480.75 o
4 10 2 3797.11 3676.67 572.46 o
5 10 2 1701.00 1863.68 438.02 o
6 10 2 10073.16 10862.22 789.76 o
7 10 2 8809.81 9802.69 675.52 o
8 10 2 4492.15 5155.41 618.29 o
9 10 2 2314.30 3382.86 702.55 o
10 10 2 147.60 621.38 742.04 o
-8 11 2 7084.25 8293.40 810.07 o
-7 11 2 3610.28 3752.64 619.15 o
-6 11 2 3718.83 3038.40 633.19 o
-5 11 2 813.59 1453.61 575.58 o
-4 11 2 4848.50 4988.40 727.99 o
-3 11 2 1199.52 1146.64 404.42 o
-2 11 2 15734.38 16276.23 550.66 o
-1 11 2 3899.25 4210.26 447.54 o
0 11 2 5388.45 5562.90 479.79 o
1 11 2 3075.37 3218.34 374.81 o
2 11 2 14556.25 14403.96 651.28 o
3 11 2 1097.54 182.45 531.49 o
4 11 2 4941.07 5815.22 573.43 o
5 11 2 505.22 559.12 490.50 o
6 11 2 3807.54 3624.46 678.51 o
7 11 2 3464.12 3948.97 622.12 o
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-7 12 2 2715.23 3200.63 754.59 o
-6 12 2 1036.24 827.65 655.58 o
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-4 12 2 2008.87 1594.09 559.53 o
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-2 12 2 205.71 77.70 467.90 o
-1 12 2 3093.14 3775.38 489.43 o
0 12 2 413.59 540.14 433.95 o
1 12 2 3211.53 3310.11 483.84 o
2 12 2 180.86 312.13 677.40 o
3 12 2 11796.36 10735.44 783.46 o
4 12 2 1883.22 1692.66 555.84 o
5 12 2 2395.08 2583.81 844.71 o
6 12 2 1163.51 736.84 693.01 o
7 12 2 2807.56 2963.02 758.29 o
-5 13 2 2940.40 2797.79 745.24 o
-4 13 2 4317.72 4050.93 744.65 o
-3 13 2 682.37 193.76 632.19 o
-2 13 2 4233.59 3345.19 576.87 o
-1 13 2 3589.95 3445.09 578.67 o
0 13 2 670.57 698.32 497.38 o
1 13 2 3322.37 3029.91 663.38 o
2 13 2 3975.27 3947.33 701.66 o
3 13 2 665.75 103.16 649.88 o
4 13 2 4957.45 5182.31 684.69 o
5 13 2 2489.68 2046.47 744.59 o
-2 14 2 3644.38 3578.96 752.33 o
-1 14 2 277.43 227.22 621.68 o
0 14 2 10389.02 10402.91 802.21 o
1 14 2 256.69 -478.99 709.09 o
2 14 2 3917.96 3553.51 766.78 o
0 1 3 1319.21 1564.82 48.62 o
1 1 3 48023.77 48924.39 969.85 o
-1 2 3 12380.08 13707.48 280.06 o
0 2 3 10370.30 12660.95 245.80 o
1 2 3 12347.25 13821.80 201.62 o
2 2 3 2836.88 3099.61 84.78 o
-2 3 3 563.28 599.91 84.50 o
-1 3 3 1095.75 1362.02 73.80 o
0 3 3 64152.77 69223.78 1490.28 o
1 3 3 1351.83 1682.68 80.50 o
2 3 3 864.41 857.01 75.17 o
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