#------------------------------------------------------------------------------ #$Date: 2011-02-15 17:23:33 +0200 (Tue, 15 Feb 2011) $ #$Revision: 11387 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2228693.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2228693_Fobs loop_ _publ_author_name 'Shahwar, Durre' 'Tahir, M. Nawaz' 'Raza, Muhammad Asam' 'Ahmad, Naeem' 'Aslam, Saherish' _publ_section_title ; 3-Benzyl-2-sulfanylidene-1,3-thiazolidin-4-one ; _journal_coeditor_code DN2634 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o133 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.812 _cell_angle_gamma 90.000 _cell_length_a 13.3271 _cell_length_b 5.9025 _cell_length_c 13.0396 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.8331 _[local]_cod_data_source_file dn2634Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a08 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 60.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 52.08 37.14 0.57 o 4 0 0 1710.13 1750.57 41.88 o 5 0 0 1298.64 1335.83 12.35 o 6 0 0 2215.49 2237.07 38.78 o 7 0 0 877.12 822.47 13.47 o 8 0 0 2866.17 2943.33 41.35 o 9 0 0 15.18 20.32 1.62 o 10 0 0 152.30 174.11 4.02 o 11 0 0 20.21 14.01 1.10 o 12 0 0 62.51 54.08 1.50 o 13 0 0 0.02 -0.75 0.65 o 14 0 0 2.07 0.21 1.06 o 15 0 0 0.87 -1.58 1.05 o 2 1 0 1294.36 1329.78 22.93 o 5 1 0 198.45 182.70 1.50 o 6 1 0 10.18 16.00 0.41 o 7 1 0 0.92 0.62 0.20 o 8 1 0 784.90 788.91 7.61 o 9 1 0 687.57 676.12 6.67 o 10 1 0 2.76 0.36 0.39 o 11 1 0 88.36 90.64 1.91 o 12 1 0 3.61 1.74 0.69 o 13 1 0 41.24 41.90 1.82 o 14 1 0 0.94 -0.67 0.64 o 15 1 0 5.21 4.96 0.96 o 0 2 0 325.68 331.23 7.73 o 1 2 0 798.25 797.45 9.39 o 2 2 0 990.27 973.35 8.70 o 3 2 0 1876.66 2005.63 23.61 o 4 2 0 345.01 351.04 3.21 o 6 2 0 1563.56 1621.84 13.95 o 7 2 0 38.40 38.78 1.11 o 8 2 0 78.58 73.58 1.22 o 9 2 0 57.99 53.21 1.00 o 10 2 0 80.02 76.50 1.48 o 11 2 0 38.84 33.61 1.00 o 12 2 0 4.70 3.43 0.60 o 13 2 0 13.42 8.93 0.95 o 14 2 0 6.16 4.44 1.04 o 15 2 0 10.98 12.01 1.87 o 1 3 0 50.01 63.18 1.15 o 2 3 0 1106.50 1186.35 11.52 o 3 3 0 133.71 137.84 2.13 o 4 3 0 159.75 157.66 1.86 o 5 3 0 58.65 57.05 1.00 o 6 3 0 0.67 -0.03 0.53 o 7 3 0 563.03 549.54 6.28 o 8 3 0 361.07 358.78 4.26 o 9 3 0 10.91 10.58 0.96 o 10 3 0 150.28 134.23 3.01 o 11 3 0 76.31 73.05 1.81 o 12 3 0 25.41 28.63 1.13 o 13 3 0 83.43 82.18 2.02 o 14 3 0 33.12 33.40 1.65 o 0 4 0 94.10 85.86 5.48 o 1 4 0 0.41 0.38 0.43 o 2 4 0 188.39 186.21 2.90 o 3 4 0 521.78 552.86 11.05 o 4 4 0 88.30 83.27 1.32 o 5 4 0 47.76 46.54 1.06 o 6 4 0 12.67 13.32 0.53 o 7 4 0 95.99 85.16 1.55 o 8 4 0 118.25 107.23 2.32 o 9 4 0 20.79 24.24 1.27 o 10 4 0 223.93 227.46 3.98 o 11 4 0 98.11 97.53 2.46 o 12 4 0 44.24 38.09 1.74 o 13 4 0 24.47 26.99 1.46 o 1 5 0 41.83 40.04 3.50 o 2 5 0 0.24 -0.18 0.69 o 3 5 0 102.40 105.01 2.82 o 4 5 0 272.82 269.59 5.20 o 5 5 0 67.79 67.25 2.43 o 6 5 0 12.86 16.30 1.14 o 7 5 0 109.94 112.12 2.14 o 8 5 0 22.02 22.07 1.22 o 9 5 0 11.74 8.99 0.94 o 10 5 0 1.23 0.49 0.77 o 11 5 0 1.01 0.11 0.78 o 0 6 0 0.07 1.31 1.57 o 1 6 0 19.69 18.13 1.88 o 2 6 0 0.29 -0.91 1.14 o 3 6 0 0.60 0.22 1.13 o 4 6 0 0.01 0.71 1.04 o 5 6 0 9.11 10.62 0.96 o 6 6 0 44.04 42.55 1.43 o 7 6 0 1.21 1.35 0.69 o 8 6 0 7.26 7.35 0.92 o 1 7 0 6.37 6.51 1.61 o 2 7 0 1.54 2.51 2.06 o -15 1 1 5.29 4.90 0.94 o -14 1 1 0.66 -0.34 0.66 o -13 1 1 3.43 1.89 0.69 o -12 1 1 57.21 55.26 1.43 o -11 1 1 523.93 531.44 5.55 o -10 1 1 270.02 272.52 3.47 o -9 1 1 30.28 27.72 0.88 o -8 1 1 146.39 159.91 1.92 o -7 1 1 31.24 34.81 0.77 o -6 1 1 10.87 14.53 0.41 o -5 1 1 138.87 126.09 1.20 o -4 1 1 249.85 248.32 2.12 o -2 1 1 231.08 230.93 2.26 o 1 1 1 68.36 68.68 0.90 o 2 1 1 1150.90 1150.31 13.06 o 3 1 1 79.64 76.28 0.81 o 4 1 1 500.43 487.08 4.05 o 5 1 1 2553.29 2674.17 63.66 o 6 1 1 14.64 15.14 0.43 o 7 1 1 0.20 -0.36 0.24 o 8 1 1 33.07 28.92 0.75 o 9 1 1 9.23 7.56 0.52 o 10 1 1 4.15 4.48 0.44 o 11 1 1 37.65 33.84 0.96 o 12 1 1 50.66 50.04 1.19 o 13 1 1 0.12 -0.86 0.57 o 14 1 1 67.26 68.48 1.92 o 15 1 1 46.36 53.05 2.03 o -15 2 1 30.40 34.55 2.10 o -14 2 1 63.68 72.35 2.85 o -13 2 1 106.22 107.33 3.10 o -12 2 1 146.41 138.22 2.38 o -11 2 1 5.02 3.65 0.45 o -10 2 1 322.72 309.91 3.23 o -9 2 1 81.13 73.31 1.13 o -8 2 1 582.84 577.94 7.90 o -7 2 1 1398.54 1403.67 11.49 o -6 2 1 1976.54 1982.71 20.55 o -5 2 1 9.87 4.65 0.43 o -4 2 1 4.94 6.33 0.33 o -3 2 1 669.85 663.41 5.72 o -2 2 1 2466.29 2529.15 40.44 o -1 2 1 20.58 14.64 0.53 o 0 2 1 1617.66 1574.79 14.82 o 1 2 1 1713.56 1721.39 14.74 o 2 2 1 394.35 404.45 4.11 o 3 2 1 55.10 64.46 0.72 o 4 2 1 266.15 273.66 2.53 o 5 2 1 8.07 5.66 0.49 o 6 2 1 17.85 17.86 0.75 o 7 2 1 132.77 118.06 1.25 o 8 2 1 142.80 136.82 1.95 o 9 2 1 26.75 26.73 0.76 o 10 2 1 126.99 125.69 1.79 o 11 2 1 142.77 135.69 1.95 o 12 2 1 67.50 73.58 1.45 o 13 2 1 14.48 13.85 0.94 o 14 2 1 0.92 -0.23 1.13 o 15 2 1 77.77 71.22 2.78 o -14 3 1 30.71 29.38 1.59 o -13 3 1 36.03 41.26 1.75 o -12 3 1 7.69 8.33 0.82 o -11 3 1 242.08 257.87 3.19 o -10 3 1 187.29 185.67 2.26 o -9 3 1 188.82 173.68 2.44 o -8 3 1 482.46 485.15 5.00 o -7 3 1 349.94 331.63 4.11 o -6 3 1 1480.99 1541.60 15.66 o -5 3 1 1334.52 1378.41 15.25 o -4 3 1 558.42 507.89 5.31 o -3 3 1 16.46 10.18 0.66 o -2 3 1 326.55 310.50 3.90 o -1 3 1 29.86 26.58 0.72 o 0 3 1 23.43 31.93 0.82 o 1 3 1 520.69 525.02 5.46 o 2 3 1 814.10 862.87 8.53 o 3 3 1 113.24 119.69 1.68 o 4 3 1 14.80 10.72 0.46 o 5 3 1 197.41 213.94 1.96 o 6 3 1 78.48 75.03 1.05 o 7 3 1 237.99 246.77 2.72 o 8 3 1 0.92 -0.74 0.82 o 9 3 1 229.02 217.68 3.27 o 10 3 1 36.13 35.92 1.57 o 11 3 1 19.79 12.62 1.50 o 12 3 1 13.49 10.32 0.85 o 13 3 1 4.89 2.05 0.71 o 14 3 1 29.57 33.27 1.70 o -13 4 1 0.01 -0.32 0.82 o -12 4 1 20.54 20.83 1.18 o -11 4 1 5.47 2.93 0.74 o -10 4 1 60.48 61.07 1.89 o -9 4 1 49.77 55.91 1.74 o -8 4 1 458.45 459.73 6.54 o -7 4 1 461.34 452.90 5.62 o -6 4 1 154.41 159.17 2.18 o -5 4 1 46.21 41.76 0.81 o -4 4 1 95.49 97.46 1.47 o -3 4 1 408.35 402.32 9.41 o -2 4 1 287.26 290.03 4.51 o -1 4 1 286.61 304.69 4.66 o 0 4 1 20.85 20.20 1.03 o 1 4 1 1.72 2.62 0.65 o 2 4 1 597.45 643.41 9.74 o 3 4 1 2.46 1.99 0.59 o 4 4 1 112.29 102.75 1.43 o 5 4 1 2.62 1.74 0.25 o 6 4 1 219.73 207.95 2.15 o 7 4 1 34.23 31.07 1.09 o 8 4 1 102.72 106.90 2.32 o 9 4 1 1.25 0.16 0.61 o 10 4 1 32.68 24.55 1.31 o 11 4 1 0.06 -0.97 0.91 o 12 4 1 0.77 1.31 0.79 o 13 4 1 51.23 64.24 2.16 o -11 5 1 38.25 41.23 1.80 o -10 5 1 6.49 8.63 0.98 o -9 5 1 20.09 14.63 1.08 o -8 5 1 14.79 13.96 1.00 o -7 5 1 35.07 33.87 1.47 o -6 5 1 4.16 4.81 0.63 o -5 5 1 48.88 46.52 1.01 o -4 5 1 353.89 359.98 8.07 o -3 5 1 16.95 17.11 1.67 o -2 5 1 162.09 171.87 4.70 o -1 5 1 279.51 281.55 6.49 o 0 5 1 279.71 278.82 6.73 o 1 5 1 201.58 199.95 5.28 o 2 5 1 70.40 68.74 2.75 o 3 5 1 24.87 19.77 1.64 o 4 5 1 48.85 47.12 1.03 o 5 5 1 536.92 544.99 8.75 o 6 5 1 14.63 18.77 0.78 o 7 5 1 9.51 11.88 0.81 o 8 5 1 0.07 -0.44 0.59 o 9 5 1 2.96 3.41 0.77 o 10 5 1 59.40 73.15 2.16 o 11 5 1 53.91 55.23 2.26 o -8 6 1 13.45 12.29 1.09 o -7 6 1 0.04 -0.72 0.63 o -6 6 1 3.52 1.56 0.63 o -5 6 1 5.02 5.10 0.57 o -4 6 1 54.65 58.33 2.33 o -3 6 1 164.88 165.73 4.04 o -2 6 1 34.72 34.43 2.42 o -1 6 1 6.02 5.22 1.33 o 0 6 1 1.31 2.12 1.29 o 1 6 1 233.45 246.58 6.54 o 2 6 1 312.18 319.71 8.38 o 3 6 1 15.48 19.05 1.89 o 4 6 1 28.23 33.25 2.17 o 5 6 1 7.08 8.41 1.05 o 6 6 1 0.55 0.81 0.63 o 7 6 1 82.89 88.69 2.48 o 8 6 1 79.68 84.42 2.29 o -2 7 1 14.05 11.79 2.77 o -1 7 1 21.52 24.42 3.18 o 0 7 1 41.34 48.18 3.00 o 1 7 1 40.69 47.96 3.01 o 2 7 1 0.02 1.68 1.87 o -15 0 2 281.97 335.66 7.91 o -14 0 2 217.66 224.66 6.31 o -13 0 2 102.65 108.69 3.60 o -12 0 2 1.50 1.33 0.89 o -11 0 2 907.74 931.15 14.21 o -10 0 2 106.95 111.67 2.69 o -9 0 2 130.73 121.83 2.72 o -8 0 2 922.99 892.81 15.69 o -7 0 2 226.44 208.65 3.72 o -6 0 2 34.18 32.66 1.06 o -5 0 2 69.43 56.57 1.15 o -4 0 2 212.96 241.53 2.95 o 0 0 2 12.18 8.99 0.92 o 1 0 2 277.73 252.55 4.55 o 3 0 2 453.67 485.74 5.38 o 5 0 2 2029.38 2091.81 35.82 o 6 0 2 1970.98 1978.23 27.91 o 7 0 2 0.04 0.92 0.42 o 8 0 2 179.66 198.46 3.67 o 9 0 2 227.73 220.14 3.53 o 10 0 2 770.98 770.18 10.20 o 11 0 2 542.00 523.60 7.40 o 12 0 2 301.48 317.79 5.83 o 13 0 2 71.97 90.65 2.66 o 14 0 2 29.95 34.97 1.85 o 15 0 2 7.75 7.75 1.47 o -15 1 2 0.12 1.25 0.95 o -14 1 2 148.05 155.59 3.22 o -13 1 2 261.52 293.34 4.39 o -12 1 2 344.03 355.93 4.51 o -11 1 2 192.43 195.12 2.83 o -10 1 2 58.56 59.68 1.25 o -9 1 2 1.10 1.12 0.36 o -8 1 2 486.29 492.13 5.12 o -7 1 2 470.26 447.08 4.63 o -6 1 2 540.74 509.95 4.49 o -5 1 2 2.00 2.61 0.25 o -4 1 2 158.88 162.58 3.50 o -2 1 2 636.86 630.16 6.91 o 0 1 2 536.80 546.14 5.49 o 1 1 2 798.24 802.69 9.11 o 3 1 2 1964.35 2019.94 27.64 o 4 1 2 1021.62 1158.18 8.02 o 5 1 2 35.97 41.87 0.57 o 6 1 2 0.21 0.32 0.17 o 7 1 2 2729.21 2803.44 33.98 o 8 1 2 705.60 665.69 6.55 o 9 1 2 370.38 352.95 3.80 o 10 1 2 137.70 137.70 1.89 o 11 1 2 14.69 14.64 0.75 o 12 1 2 82.90 89.39 1.58 o 13 1 2 120.80 121.33 2.24 o 14 1 2 46.90 46.12 1.68 o 15 1 2 79.83 94.89 2.64 o -15 2 2 22.05 21.48 3.42 o -14 2 2 1.17 1.36 0.93 o -13 2 2 6.57 5.00 1.06 o -12 2 2 14.58 11.73 0.82 o -11 2 2 96.63 95.09 1.55 o -10 2 2 594.53 587.57 6.00 o -9 2 2 447.08 439.01 4.58 o -8 2 2 84.78 90.36 1.21 o -7 2 2 4.50 3.21 0.33 o -6 2 2 3321.29 3508.55 48.49 o -5 2 2 392.01 392.36 5.65 o -4 2 2 37.08 47.33 0.81 o -3 2 2 229.81 220.35 3.05 o -2 2 2 52.75 59.75 0.93 o -1 2 2 419.79 424.77 4.98 o 1 2 2 0.26 0.53 0.24 o 2 2 2 659.12 691.53 5.52 o 3 2 2 0.99 1.86 0.25 o 4 2 2 1305.96 1382.84 11.48 o 5 2 2 217.62 201.77 1.89 o 6 2 2 887.25 894.46 7.21 o 7 2 2 40.83 28.31 0.60 o 8 2 2 11.55 7.48 0.65 o 9 2 2 39.60 35.78 1.01 o 10 2 2 264.31 258.57 2.99 o 11 2 2 95.52 94.01 2.29 o 12 2 2 34.77 35.50 1.24 o 13 2 2 38.91 40.26 1.43 o 14 2 2 26.45 29.59 1.62 o 15 2 2 0.18 -0.82 0.81 o -14 3 2 25.89 27.61 2.41 o -13 3 2 19.46 19.61 1.55 o -12 3 2 17.76 15.79 1.36 o -11 3 2 6.40 4.82 0.76 o -10 3 2 0.34 0.91 0.48 o -9 3 2 1248.55 1243.41 12.93 o -8 3 2 494.81 479.79 6.40 o -7 3 2 116.72 115.14 2.96 o -6 3 2 80.71 78.21 1.25 o -5 3 2 20.67 23.09 0.65 o -4 3 2 89.82 102.97 1.30 o -3 3 2 1293.47 1286.60 15.73 o -2 3 2 726.79 681.27 8.77 o -1 3 2 2013.98 2148.67 22.51 o 0 3 2 148.23 142.06 2.44 o 1 3 2 2.71 3.83 0.39 o 2 3 2 530.65 537.73 5.19 o 3 3 2 1422.57 1459.23 12.13 o 4 3 2 99.33 77.82 0.83 o 5 3 2 274.31 259.62 2.56 o 6 3 2 206.60 208.55 2.12 o 7 3 2 80.98 77.79 1.22 o 8 3 2 6.15 4.80 0.52 o 9 3 2 0.07 -0.71 0.47 o 10 3 2 85.71 90.87 1.94 o 11 3 2 32.29 34.81 1.29 o 12 3 2 60.35 52.27 1.77 o 13 3 2 4.75 4.88 1.08 o 14 3 2 7.55 4.40 0.98 o -13 4 2 9.46 8.53 1.08 o -12 4 2 117.93 105.00 2.68 o -11 4 2 160.45 149.92 2.80 o -10 4 2 2.49 2.26 0.64 o -9 4 2 23.24 17.54 0.87 o -8 4 2 117.65 112.62 2.15 o -7 4 2 5.08 4.39 0.60 o -6 4 2 434.34 443.60 7.14 o -5 4 2 1453.53 1483.76 15.88 o -4 4 2 255.91 265.80 2.87 o -3 4 2 40.31 36.27 1.33 o -2 4 2 9.44 9.62 0.71 o -1 4 2 391.11 412.63 5.77 o 0 4 2 904.81 925.00 11.82 o 1 4 2 213.33 202.10 3.39 o 2 4 2 444.36 439.51 7.29 o 3 4 2 833.23 867.27 11.06 o 4 4 2 0.28 0.83 0.30 o 5 4 2 258.07 251.90 2.32 o 6 4 2 1.72 0.64 0.33 o 7 4 2 12.48 11.56 0.73 o 8 4 2 150.89 143.79 2.42 o 9 4 2 168.03 157.23 3.02 o 10 4 2 0.10 -0.91 0.62 o 11 4 2 0.02 -0.97 0.65 o 12 4 2 11.37 9.41 1.02 o -11 5 2 22.63 18.30 1.12 o -10 5 2 14.50 14.01 0.98 o -9 5 2 18.73 15.64 1.11 o -8 5 2 73.91 70.39 1.96 o -7 5 2 0.30 0.06 0.56 o -6 5 2 56.99 54.21 1.53 o -5 5 2 0.09 -0.53 0.53 o -4 5 2 273.43 283.53 4.93 o -3 5 2 308.63 325.38 7.41 o -2 5 2 235.64 230.43 5.76 o -1 5 2 63.20 55.56 2.51 o 0 5 2 136.72 141.38 4.03 o 1 5 2 18.98 17.74 2.13 o 2 5 2 1.44 -0.15 1.09 o 3 5 2 0.11 -1.18 0.79 o 4 5 2 217.13 222.15 4.27 o 5 5 2 83.69 82.91 1.56 o 6 5 2 123.20 116.80 2.35 o 7 5 2 35.15 33.81 1.22 o 8 5 2 23.88 18.12 1.25 o 9 5 2 11.76 9.66 0.97 o 10 5 2 24.80 26.46 1.48 o 11 5 2 9.87 9.80 1.09 o -8 6 2 0.26 -0.50 0.68 o -7 6 2 67.05 68.73 1.95 o -6 6 2 10.45 7.28 0.78 o -5 6 2 0.00 -0.71 0.47 o -4 6 2 2.98 1.66 1.20 o -3 6 2 8.57 9.59 1.54 o -2 6 2 6.62 6.75 1.12 o -1 6 2 0.43 -0.66 1.05 o 0 6 2 155.50 167.40 5.11 o 1 6 2 16.58 16.47 1.86 o 2 6 2 41.66 37.09 2.45 o 3 6 2 89.06 89.34 3.41 o 4 6 2 10.94 8.59 1.24 o 5 6 2 2.48 2.17 0.87 o 6 6 2 0.98 0.56 0.66 o 7 6 2 0.20 -1.01 1.24 o 8 6 2 10.34 9.07 1.14 o -1 7 2 3.33 2.75 1.41 o 0 7 2 38.46 40.57 2.80 o 1 7 2 0.44 1.50 1.98 o -15 1 3 0.59 0.21 0.89 o -14 1 3 13.89 12.27 1.11 o -13 1 3 55.85 47.91 2.79 o -12 1 3 5.46 4.86 0.71 o -11 1 3 106.08 102.74 1.90 o -10 1 3 15.82 13.25 0.72 o -9 1 3 132.16 128.85 1.90 o -8 1 3 85.20 81.51 1.37 o -7 1 3 499.22 508.95 5.23 o -6 1 3 60.89 61.19 0.97 o -5 1 3 966.35 1025.52 10.61 o -4 1 3 4.00 0.88 0.18 o -2 1 3 499.72 505.12 4.18 o 1 1 3 808.45 850.53 7.24 o 2 1 3 628.56 655.46 5.01 o 3 1 3 95.30 106.94 0.93 o 4 1 3 325.17 325.73 2.70 o 5 1 3 392.71 395.40 3.17 o 6 1 3 452.97 430.17 4.07 o 7 1 3 386.86 373.76 3.24 o 8 1 3 117.78 114.47 1.23 o 9 1 3 22.15 18.77 0.55 o 10 1 3 79.12 76.78 1.16 o 11 1 3 0.40 0.46 0.37 o 12 1 3 12.47 13.75 0.69 o 13 1 3 1.96 0.77 0.61 o 14 1 3 217.92 217.39 3.35 o 15 1 3 6.60 7.19 1.06 o -15 2 3 34.55 37.43 2.48 o -14 2 3 3.08 2.81 1.01 o -13 2 3 18.75 15.84 1.42 o -12 2 3 238.91 234.49 3.57 o -11 2 3 42.49 39.33 1.06 o -10 2 3 0.34 -0.44 0.37 o -9 2 3 13.86 13.58 0.60 o -8 2 3 21.51 19.49 0.63 o -7 2 3 203.33 205.56 2.44 o -6 2 3 89.88 85.28 1.21 o -5 2 3 13.27 9.00 0.34 o -3 2 3 636.68 676.66 6.47 o -2 2 3 47.94 39.79 0.63 o -1 2 3 80.15 85.88 1.01 o 0 2 3 295.41 316.09 3.66 o 1 2 3 591.01 612.33 5.01 o 2 2 3 665.72 672.34 5.45 o 3 2 3 1238.80 1140.11 8.92 o 4 2 3 1649.17 1688.18 13.97 o 5 2 3 473.95 463.48 3.91 o 6 2 3 345.22 341.35 2.86 o 7 2 3 15.91 21.67 0.65 o 8 2 3 23.11 24.68 0.79 o 9 2 3 149.50 142.96 1.72 o 10 2 3 334.19 324.30 3.27 o 11 2 3 241.66 240.99 2.88 o 12 2 3 4.06 3.18 0.61 o 13 2 3 127.41 122.03 3.43 o 14 2 3 28.87 22.61 1.47 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