#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:57:59 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181207 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/86/2228697.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2228697_Fobs loop_ _publ_author_name 'Fu, Jun-Dan' 'Wen, Yi-Hang' _publ_section_title ; 2-[4-(Carboxymethyl)phenoxy]acetic acid ; _journal_coeditor_code DS2074 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o167 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.4640 _cell_length_b 10.7798 _cell_length_c 16.2550 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.7654 _cod_data_source_file ds2074Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 96.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 240.65 214.36 10.27 o 4 0 0 7.64 6.01 0.53 o 6 0 0 3.85 2.82 0.95 o 1 1 0 801.67 770.43 15.86 o 2 1 0 500.65 449.23 14.90 o 3 1 0 0.93 1.79 0.20 o 4 1 0 3.23 4.71 0.32 o 5 1 0 70.66 74.26 1.97 o 6 1 0 46.90 45.65 1.88 o 7 1 0 0.30 -0.10 0.28 o 0 2 0 7.26 7.14 0.63 o 1 2 0 438.65 449.65 7.61 o 2 2 0 431.56 410.78 6.68 o 3 2 0 176.11 182.94 2.95 o 4 2 0 28.15 29.12 0.81 o 5 2 0 123.53 126.01 2.98 o 6 2 0 107.08 118.34 3.69 o 7 2 0 0.57 0.00 0.31 o 1 3 0 245.14 177.54 26.16 o 2 3 0 122.41 141.90 2.45 o 3 3 0 1050.41 1075.75 17.30 o 4 3 0 74.01 68.59 1.45 o 5 3 0 91.40 103.68 2.84 o 6 3 0 22.47 23.96 1.24 o 1 4 0 1089.50 1080.41 19.18 o 2 4 0 301.60 327.21 5.82 o 3 4 0 34.41 37.44 0.87 o 4 4 0 79.55 80.28 1.65 o 5 4 0 3.42 0.81 0.52 o 6 4 0 27.56 29.11 1.51 o 1 5 0 420.20 429.35 6.52 o 2 5 0 16.29 18.59 0.44 o 3 5 0 31.68 35.64 0.98 o 4 5 0 30.39 28.06 0.83 o 5 5 0 8.48 11.92 0.84 o 6 5 0 14.51 14.81 1.33 o 1 6 0 0.18 0.04 0.07 o 2 6 0 473.79 455.41 7.39 o 3 6 0 9.27 6.90 0.67 o 4 6 0 8.59 7.38 0.55 o 5 6 0 20.99 24.12 1.17 o 6 6 0 5.36 5.97 0.87 o 1 7 0 201.70 208.47 3.81 o 2 7 0 25.36 25.59 0.82 o 3 7 0 31.02 36.27 0.93 o 4 7 0 0.72 0.36 0.19 o 5 7 0 17.49 12.85 0.93 o 6 7 0 2.61 1.23 0.58 o 1 8 0 72.86 74.95 4.55 o 2 8 0 7.13 6.86 0.44 o 3 8 0 132.31 108.98 3.61 o 4 8 0 6.38 6.14 0.65 o 5 8 0 4.48 1.38 0.84 o 1 9 0 14.77 14.37 0.66 o 2 9 0 10.45 11.71 0.59 o 3 9 0 6.52 9.93 0.62 o 4 9 0 2.75 3.74 0.57 o 5 9 0 1.00 0.30 0.29 o 0 10 0 5.68 7.09 0.98 o 1 10 0 0.24 -0.43 0.71 o 2 10 0 0.28 1.06 0.33 o 3 10 0 8.57 7.65 0.64 o 4 10 0 1.89 0.44 0.32 o 5 10 0 28.30 37.69 2.54 o 1 11 0 23.73 25.28 1.52 o 2 11 0 14.95 12.50 1.52 o 3 11 0 12.13 13.13 0.81 o 4 11 0 5.74 3.41 1.35 o 0 12 0 143.29 160.08 6.18 o 1 12 0 92.28 89.58 3.32 o 2 12 0 20.44 24.29 3.26 o 3 12 0 1.24 0.52 0.41 o 1 13 0 31.42 28.78 1.80 o 2 13 0 2.04 3.22 0.95 o 0 14 0 34.22 39.87 3.79 o 1 0 1 2220.40 2063.81 29.22 o 2 0 1 1050.90 894.83 18.56 o 3 0 1 187.33 187.46 2.82 o 4 0 1 119.17 113.01 2.16 o 5 0 1 130.37 133.10 2.81 o 6 0 1 103.27 115.91 3.64 o 7 0 1 0.87 -0.20 0.32 o 0 1 1 0.09 0.36 0.15 o 1 1 1 3922.67 3791.73 56.71 o 2 1 1 9.35 10.09 0.56 o 3 1 1 311.46 304.17 3.18 o 4 1 1 52.06 52.72 0.78 o 5 1 1 257.42 267.55 4.22 o 6 1 1 19.56 22.70 1.00 o 7 1 1 9.95 2.95 3.46 o 0 2 1 8.31 9.81 0.42 o 1 2 1 229.12 201.61 2.37 o 2 2 1 515.55 499.04 12.95 o 3 2 1 13.28 14.61 0.32 o 4 2 1 9.77 9.30 0.29 o 5 2 1 44.59 46.60 1.11 o 6 2 1 15.90 14.61 0.74 o 7 2 1 15.05 4.49 5.05 o 0 3 1 118.32 126.70 2.01 o 1 3 1 1791.74 1816.10 19.44 o 2 3 1 805.25 751.09 14.08 o 3 3 1 519.71 563.37 6.29 o 4 3 1 92.03 90.60 1.23 o 5 3 1 23.52 23.11 0.73 o 6 3 1 9.06 11.41 0.69 o 0 4 1 1018.83 992.27 28.62 o 1 4 1 136.64 143.30 1.63 o 2 4 1 57.30 73.53 0.96 o 3 4 1 4.67 5.03 0.23 o 4 4 1 29.97 28.82 0.60 o 5 4 1 9.67 9.82 0.57 o 6 4 1 1.69 0.65 0.37 o 0 5 1 134.13 103.45 29.88 o 1 5 1 332.53 340.67 3.87 o 2 5 1 169.12 176.11 2.06 o 3 5 1 156.50 155.68 2.27 o 4 5 1 20.91 23.04 0.57 o 5 5 1 6.10 7.05 0.54 o 6 5 1 1.78 0.93 0.51 o 0 6 1 5.92 5.25 0.29 o 1 6 1 323.17 335.09 3.76 o 2 6 1 158.61 163.06 2.21 o 3 6 1 136.45 130.97 2.07 o 4 6 1 25.34 24.69 0.76 o 5 6 1 3.78 4.10 0.44 o 6 6 1 4.00 4.32 0.60 o 0 7 1 201.89 201.76 5.51 o 1 7 1 55.85 55.11 0.89 o 2 7 1 56.97 61.61 1.05 o 3 7 1 17.45 15.61 0.45 o 4 7 1 58.05 47.15 1.00 o 5 7 1 9.04 10.38 0.60 o 6 7 1 15.06 19.16 0.93 o 0 8 1 76.37 73.47 1.76 o 1 8 1 49.99 52.98 1.17 o 2 8 1 23.09 20.08 0.91 o 3 8 1 60.33 59.78 1.20 o 4 8 1 12.19 10.54 0.52 o 5 8 1 0.47 0.24 0.20 o 0 9 1 60.94 62.33 1.69 o 1 9 1 179.54 187.03 2.59 o 2 9 1 245.06 245.24 3.07 o 3 9 1 1.22 0.71 0.19 o 4 9 1 1.16 0.09 0.15 o 5 9 1 2.55 0.89 0.48 o 0 10 1 26.45 27.06 1.21 o 1 10 1 53.41 56.93 1.46 o 2 10 1 48.49 50.08 0.92 o 3 10 1 5.54 6.71 0.42 o 4 10 1 0.96 0.54 0.18 o 5 10 1 3.45 4.94 0.85 o 0 11 1 339.33 358.61 8.63 o 1 11 1 9.80 11.15 0.77 o 2 11 1 0.40 0.21 0.33 o 3 11 1 4.89 3.46 0.35 o 4 11 1 1.47 0.75 0.31 o 0 12 1 4.65 5.99 0.81 o 1 12 1 21.42 23.69 1.11 o 2 12 1 0.01 0.00 0.50 o 3 12 1 9.05 3.87 2.12 o 0 13 1 18.56 17.72 1.88 o 1 13 1 14.18 16.23 1.00 o 2 13 1 11.10 10.87 0.90 o 0 14 1 4.49 5.26 3.06 o 1 0 2 910.10 836.91 15.64 o 2 0 2 0.29 0.37 0.12 o 3 0 2 847.84 855.46 12.07 o 4 0 2 332.27 325.94 5.22 o 5 0 2 152.76 158.72 3.28 o 6 0 2 44.14 42.42 1.81 o 7 0 2 1.68 0.02 0.30 o 0 1 2 33.99 28.05 1.27 o 1 1 2 6608.50 6241.14 78.77 o 2 1 2 888.26 853.41 17.59 o 3 1 2 63.70 72.81 1.03 o 4 1 2 99.23 100.72 1.26 o 5 1 2 72.59 80.50 1.47 o 6 1 2 10.96 12.02 0.63 o 7 1 2 0.77 -0.16 0.22 o 0 2 2 73.66 86.90 1.77 o 1 2 2 4624.16 4546.13 42.97 o 2 2 2 2438.30 2475.21 23.54 o 3 2 2 153.12 153.22 2.00 o 4 2 2 87.45 96.28 1.22 o 5 2 2 14.56 14.45 0.60 o 6 2 2 50.25 54.90 1.42 o 7 2 2 7.62 9.88 1.66 o 0 3 2 670.11 620.55 11.96 o 1 3 2 1397.05 1325.63 18.05 o 2 3 2 598.46 612.52 6.71 o 3 3 2 108.66 111.11 1.57 o 4 3 2 22.24 23.65 0.49 o 5 3 2 27.64 30.85 0.92 o 6 3 2 4.33 5.67 0.55 o 1 4 2 97.48 100.26 1.27 o 2 4 2 188.79 190.40 2.19 o 3 4 2 31.02 28.86 0.57 o 4 4 2 40.84 41.30 1.43 o 5 4 2 55.20 51.52 2.33 o 6 4 2 20.79 21.39 0.94 o 0 5 2 334.56 253.73 40.93 o 1 5 2 431.17 438.46 4.95 o 2 5 2 628.55 633.71 6.76 o 3 5 2 41.03 46.57 0.77 o 4 5 2 149.60 152.71 2.17 o 5 5 2 8.30 7.73 0.58 o 6 5 2 16.20 21.37 1.09 o 0 6 2 37.82 39.59 1.15 o 1 6 2 168.20 178.75 2.29 o 2 6 2 40.86 45.35 0.68 o 3 6 2 46.67 50.08 0.83 o 4 6 2 13.49 15.69 0.60 o 5 6 2 28.49 28.27 1.00 o 6 6 2 4.28 4.38 0.68 o 0 7 2 611.47 478.26 79.19 o 1 7 2 411.97 405.75 4.69 o 2 7 2 5.57 5.42 0.24 o 3 7 2 0.70 0.12 0.08 o 4 7 2 54.18 54.60 1.28 o 5 7 2 8.07 8.81 0.60 o 6 7 2 0.91 0.55 0.35 o 0 8 2 132.26 125.58 3.22 o 1 8 2 0.88 1.78 0.18 o 2 8 2 28.97 35.10 0.62 o 3 8 2 16.35 15.88 0.51 o 4 8 2 5.84 5.76 0.44 o 5 8 2 3.64 2.36 0.49 o 0 9 2 3.82 3.52 0.45 o 1 9 2 10.49 12.69 0.45 o 2 9 2 12.86 13.59 0.41 o 3 9 2 35.62 34.71 0.87 o 4 9 2 72.17 72.79 1.64 o 5 9 2 1.37 0.46 0.40 o 0 10 2 63.46 64.81 2.07 o 1 10 2 123.64 121.56 2.56 o 2 10 2 7.49 5.90 0.38 o 3 10 2 22.18 22.11 0.66 o 4 10 2 4.39 4.86 0.79 o 0 11 2 150.88 156.80 4.20 o 1 11 2 68.40 69.94 2.75 o 2 11 2 2.31 2.51 0.43 o 3 11 2 1.90 1.89 0.31 o 4 11 2 2.92 1.63 0.56 o 0 12 2 32.80 34.54 1.54 o 1 12 2 57.13 56.97 1.90 o 2 12 2 2.15 2.11 0.56 o 3 12 2 0.51 0.60 0.33 o 0 13 2 41.18 43.08 2.47 o 1 13 2 2.92 2.51 0.62 o 2 13 2 3.72 3.26 0.63 o 1 0 3 917.10 807.30 12.79 o 2 0 3 614.80 580.35 8.30 o 3 0 3 150.71 164.70 2.83 o 4 0 3 67.66 67.72 1.33 o 5 0 3 208.46 218.07 4.32 o 6 0 3 24.05 24.50 1.36 o 7 0 3 3.35 0.94 2.32 o 0 1 3 135.81 131.19 2.28 o 1 1 3 2328.60 2161.13 22.11 o 2 1 3 46.76 50.45 2.03 o 3 1 3 84.15 92.71 1.21 o 4 1 3 131.20 138.02 2.01 o 5 1 3 27.92 29.00 0.71 o 6 1 3 22.98 22.36 0.81 o 7 1 3 0.71 -0.15 0.22 o 0 2 3 9359.26 8931.22 125.65 o 1 2 3 3376.70 3389.48 34.57 o 2 2 3 996.62 1007.33 12.16 o 3 2 3 38.56 31.84 0.56 o 4 2 3 129.14 137.00 1.64 o 5 2 3 6.47 6.79 0.43 o 6 2 3 15.94 16.47 0.76 o 0 3 3 19.50 20.06 1.45 o 1 3 3 3760.48 3734.17 36.29 o 2 3 3 359.73 382.95 4.51 o 3 3 3 123.34 127.87 1.78 o 4 3 3 99.93 91.29 1.83 o 5 3 3 6.99 5.77 0.44 o 6 3 3 10.18 11.45 0.67 o 0 4 3 1269.02 1208.82 23.89 o 1 4 3 18.83 24.22 0.44 o 2 4 3 492.76 464.26 5.34 o 3 4 3 65.75 66.60 1.10 o 4 4 3 25.16 26.79 0.58 o 5 4 3 8.19 7.46 0.56 o 6 4 3 43.65 53.27 1.91 o 0 5 3 166.03 185.90 3.26 o 1 5 3 156.63 150.28 1.80 o 2 5 3 154.61 160.33 1.79 o 3 5 3 44.10 43.30 0.79 o 4 5 3 36.17 34.47 1.03 o 5 5 3 7.23 4.56 0.83 o 6 5 3 15.40 13.09 3.54 o 0 6 3 106.17 99.44 2.46 o 1 6 3 503.96 553.12 6.27 o 2 6 3 222.30 218.08 2.54 o 3 6 3 1.69 0.65 0.18 o 4 6 3 10.07 10.14 0.54 o 5 6 3 23.05 23.26 0.99 o 6 6 3 1.95 0.55 0.34 o 0 7 3 255.50 270.84 6.20 o 1 7 3 100.47 99.89 1.50 o 2 7 3 26.25 28.14 0.60 o 3 7 3 1.28 0.72 0.13 o 4 7 3 3.03 1.28 0.39 o 5 7 3 2.34 3.46 0.45 o 6 7 3 8.37 11.06 1.13 o 0 8 3 3.96 3.06 0.32 o 1 8 3 27.27 28.34 0.56 o 2 8 3 26.21 23.52 0.50 o 3 8 3 22.51 20.15 0.58 o 4 8 3 14.27 17.46 0.72 o 5 8 3 29.54 25.24 5.82 o 0 9 3 99.79 99.06 2.43 o 1 9 3 91.86 89.40 1.48 o 2 9 3 51.28 50.49 0.84 o 3 9 3 16.39 16.14 0.57 o 4 9 3 8.36 7.97 0.53 o 5 9 3 2.73 2.54 0.77 o 0 10 3 151.05 152.54 5.32 o 1 10 3 39.12 40.43 1.10 o 2 10 3 0.13 0.12 0.20 o 3 10 3 13.87 12.07 0.52 o 4 10 3 32.52 29.63 4.54 o 0 11 3 2.84 2.60 0.66 o 1 11 3 77.60 78.05 1.89 o 2 11 3 2.77 1.71 0.40 o 3 11 3 10.12 8.53 0.99 o 4 11 3 34.24 29.30 7.26 o 0 12 3 37.39 40.83 2.02 o 1 12 3 1.93 1.39 0.50 o 2 12 3 19.25 21.48 1.11 o 3 12 3 6.44 5.06 1.24 o 0 13 3 27.38 24.56 1.66 o 1 13 3 1.37 1.97 0.58 o 2 13 3 1.85 1.34 0.57 o 0 0 4 76.93 83.08 2.98 o 1 0 4 3322.39 3148.71 40.78 o 2 0 4 99.38 102.18 1.58 o 3 0 4 4.43 4.55 0.48 o 4 0 4 23.06 24.30 0.82 o 5 0 4 3.05 3.33 0.42 o 6 0 4 30.29 35.55 2.33 o 7 0 4 7.98 11.51 2.25 o 0 1 4 870.55 805.29 16.31 o 1 1 4 517.98 559.57 6.43 o 2 1 4 256.18 289.37 3.22 o 3 1 4 73.49 82.06 1.14 o 4 1 4 16.82 16.06 0.38 o 5 1 4 41.51 40.22 0.90 o 6 1 4 6.45 7.14 0.55 o 0 2 4 5542.07 5270.87 67.03 o 1 2 4 527.80 529.58 9.89 o 2 2 4 21.78 20.95 0.43 o 3 2 4 621.77 621.53 6.89 o 4 2 4 177.66 177.89 2.33 o 5 2 4 25.67 24.05 0.65 o 6 2 4 1.64 0.36 0.24 o 0 3 4 13.13 13.26 0.46 o 1 3 4 479.57 475.40 5.37 o 2 3 4 310.43 324.45 3.73 o 3 3 4 112.74 128.34 1.87 o 4 3 4 434.65 459.58 5.58 o 5 3 4 64.74 64.66 2.15 o 6 3 4 17.01 17.27 0.91 o 0 4 4 1406.09 1474.18 22.94 o 1 4 4 119.92 111.53 1.35 o 2 4 4 753.05 767.86 8.13 o 3 4 4 2.79 3.66 0.21 o 4 4 4 173.62 175.95 2.60 o 5 4 4 10.99 11.57 0.66 o 6 4 4 19.08 23.78 1.07 o 0 5 4 48.34 45.77 1.26 o 1 5 4 570.86 581.68 6.73 o 2 5 4 420.54 436.04 4.72 o 3 5 4 91.58 95.72 1.45 o 4 5 4 66.48 65.39 1.71 o 5 5 4 19.67 20.93 0.92 o 6 5 4 4.76 2.66 0.97 o 0 6 4 111.50 107.94 2.65 o 1 6 4 241.89 247.80 4.35 o 2 6 4 57.68 54.41 1.03 o 3 6 4 55.04 55.99 0.95 o 4 6 4 45.92 43.71 2.28 o 5 6 4 2.50 0.28 0.20 o 6 6 4 5.66 3.78 1.47 o 0 7 4 8.15 12.48 0.47 o 1 7 4 47.79 49.77 1.06 o 2 7 4 9.63 9.33 0.42 o 3 7 4 133.96 131.16 2.04 o 4 7 4 33.70 33.17 1.01 o 5 7 4 25.41 31.32 1.96 o 6 7 4 8.73 7.10 2.00 o 0 8 4 0.24 0.16 0.16 o 1 8 4 16.47 14.75 0.43 o 2 8 4 128.46 121.31 1.73 o 3 8 4 44.61 43.44 1.02 o 4 8 4 2.31 1.30 0.38 o 5 8 4 14.44 8.77 3.11 o 0 9 4 31.92 30.80 1.10 o 1 9 4 223.51 223.09 3.38 o 2 9 4 101.99 96.58 1.64 o 3 9 4 13.21 14.77 0.56 o 4 9 4 8.89 10.60 0.63 o 5 9 4 9.23 8.17 1.77 o 0 10 4 9.62 9.70 0.81 o 1 10 4 39.20 41.47 1.04 o 2 10 4 11.12 11.95 0.61 o 3 10 4 41.10 42.88 1.10 o 4 10 4 4.13 2.99 0.65 o 0 11 4 3.29 2.73 0.63 o 1 11 4 42.46 45.01 1.33 o 2 11 4 19.04 21.77 0.83 o 3 11 4 5.72 6.43 1.02 o 4 11 4 3.03 1.40 0.85 o 0 12 4 1.93 0.79 0.72 o 1 12 4 0.33 0.20 0.47 o 2 12 4 1.08 0.83 0.52 o 3 12 4 6.04 3.98 0.88 o 0 13 4 19.35 20.26 1.62 o 1 13 4 7.60 7.44 0.79 o 2 13 4 0.90 0.65 0.61 o 1 0 5 32.35 30.45 0.53 o 2 0 5 11.62 9.65 0.35 o 3 0 5 278.79 303.85 4.53 o 4 0 5 93.81 95.69 1.89 o 5 0 5 1.36 0.96 0.34 o 6 0 5 0.18 0.08 0.22 o 0 1 5 812.75 754.00 12.51 o 1 1 5 23.55 25.34 0.36 o 2 1 5 35.89 41.86 0.75 o 3 1 5 434.92 376.36 22.33 o 4 1 5 19.56 20.61 0.44 o 5 1 5 35.84 36.11 0.81 o 6 1 5 13.07 14.08 0.71 o 0 2 5 823.10 852.35 13.23 o 1 2 5 566.84 556.90 5.79 o 2 2 5 261.74 266.88 3.16 o 3 2 5 19.98 15.49 0.36 o 4 2 5 60.38 61.06 1.03 o 5 2 5 14.22 12.55 0.55 o 6 2 5 9.88 9.54 0.62 o 0 3 5 1004.20 986.79 13.08 o 1 3 5 210.42 202.11 2.34 o 2 3 5 611.00 639.29 7.41 o 3 3 5 185.72 182.65 2.17 o 4 3 5 20.47 21.17 0.60 o 5 3 5 51.72 56.53 1.66 o 6 3 5 7.21 7.23 0.67 o 0 4 5 501.99 553.27 9.38 o 1 4 5 1138.04 1162.17 11.96 o 2 4 5 815.17 829.09 8.82 o 3 4 5 311.39 238.04 22.45 o 4 4 5 23.37 24.72 0.67 o 5 4 5 52.04 56.96 1.88 o 6 4 5 2.00 0.77 0.35 o 0 5 5 654.34 651.52 14.30 o 1 5 5 669.72 651.15 7.52 o 2 5 5 262.97 240.75 2.69 o 3 5 5 16.33 17.88 0.45 o 4 5 5 0.42 0.21 0.15 o 5 5 5 17.96 18.89 0.88 o 6 5 5 0.67 0.07 0.22 o 0 6 5 85.71 88.58 2.25 o 1 6 5 5.12 6.65 0.23 o 2 6 5 112.59 115.22 1.89 o 3 6 5 5.67 5.04 0.29 o 4 6 5 15.72 16.80 0.77 o 5 6 5 9.68 9.18 0.70 o 6 6 5 3.32 2.48 0.94 o 0 7 5 105.08 110.49 2.16 o 1 7 5 158.02 158.50 2.37 o 2 7 5 79.65 79.26 1.26 o 3 7 5 95.04 98.07 2.02 o 4 7 5 53.79 60.96 1.50 o 5 7 5 8.63 4.61 2.07 o 0 8 5 4.17 3.30 0.48 o 1 8 5 443.49 450.06 5.80 o 2 8 5 56.29 54.98 0.99 o 3 8 5 60.64 65.14 1.29 o 4 8 5 18.87 22.33 0.86 o 5 8 5 2.28 0.90 0.52 o 0 9 5 41.65 42.36 1.22 o 1 9 5 111.54 108.32 1.74 o 2 9 5 27.74 28.54 0.74 o 3 9 5 8.70 10.91 0.54 o 4 9 5 9.80 11.43 0.65 o 5 9 5 4.92 1.55 0.59 o 0 10 5 91.60 93.71 4.36 o 1 10 5 34.08 34.05 0.89 o 2 10 5 2.66 1.19 0.30 o 3 10 5 0.73 0.49 0.18 o 4 10 5 5.03 2.52 0.68 o 0 11 5 0.22 -0.25 0.49 o 1 11 5 3.78 4.72 0.55 o 2 11 5 46.01 49.42 1.66 o 3 11 5 0.13 0.11 0.23 o 4 11 5 5.31 2.14 0.97 o 0 12 5 9.07 8.00 1.05 o 1 12 5 0.15 0.66 0.50 o 2 12 5 1.11 0.84 0.59 o 3 12 5 18.38 20.62 1.03 o 0 13 5 6.51 5.41 1.01 o 1 13 5 0.30 0.16 0.56 o 2 13 5 0.51 0.64 0.60 o 0 0 6 22.64 23.36 0.88 o 1 0 6 478.01 558.64 8.86 o 2 0 6 2071.92 2038.53 42.08 o 3 0 6 3.84 4.59 0.31 o 4 0 6 6.68 5.78 0.39 o 5 0 6 0.98 0.54 0.22 o 6 0 6 10.01 10.48 1.13 o 0 1 6 61.93 52.96 0.93 o 1 1 6 6.78 7.33 0.21 o 2 1 6 175.62 176.38 2.12 o 3 1 6 270.70 272.52 3.49 o 4 1 6 44.92 47.60 0.74 o 5 1 6 20.33 20.49 0.64 o 6 1 6 3.37 2.11 0.44 o 0 2 6 539.74 476.46 7.10 o 1 2 6 684.59 701.00 7.14 o 2 2 6 132.23 143.27 1.92 o 3 2 6 105.90 113.82 1.63 o 4 2 6 64.17 61.75 1.08 o 5 2 6 90.36 90.38 2.30 o 6 2 6 12.78 15.21 0.79 o 0 3 6 288.44 318.04 4.47 o 1 3 6 979.80 955.75 11.81 o 2 3 6 177.75 162.31 5.53 o 3 3 6 49.14 47.68 0.86 o 4 3 6 31.92 31.65 0.77 o 5 3 6 33.87 32.91 0.98 o 6 3 6 12.04 11.36 0.79 o 0 4 6 68.41 70.16 1.39 o 1 4 6 619.48 622.14 11.74 o 2 4 6 576.49 573.96 6.19 o 3 4 6 146.02 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2.49 o 0 11 6 0.40 0.95 0.78 o 1 11 6 14.96 16.29 1.01 o 2 11 6 0.66 0.04 0.27 o 3 11 6 0.71 0.71 0.27 o 0 12 6 15.48 16.99 2.20 o 1 12 6 8.23 6.73 0.67 o 2 12 6 20.22 16.36 4.33 o 3 12 6 1.63 0.65 0.34 o 0 13 6 1.46 2.30 0.86 o 1 13 6 2.56 3.31 0.66 o 1 0 7 73.19 79.24 1.32 o 2 0 7 40.35 37.54 0.71 o 3 0 7 45.11 42.28 1.41 o 4 0 7 2.97 3.21 0.33 o 5 0 7 18.88 20.31 0.82 o 6 0 7 9.30 10.63 1.44 o 0 1 7 45.61 43.50 0.74 o 1 1 7 506.95 512.76 4.98 o 2 1 7 436.27 450.24 4.92 o 3 1 7 4.76 3.58 0.19 o 4 1 7 30.02 32.05 0.99 o 5 1 7 17.14 17.96 0.64 o 6 1 7 12.05 11.55 0.80 o 0 2 7 2727.21 2765.21 40.47 o 1 2 7 211.71 229.79 2.36 o 2 2 7 22.90 16.93 0.44 o 3 2 7 109.39 104.39 1.66 o 4 2 7 84.32 81.83 1.26 o 5 2 7 2.04 0.96 0.28 o 6 2 7 3.58 1.27 0.52 o 0 3 7 257.03 282.32 4.25 o 1 3 7 387.53 403.41 4.59 o 2 3 7 158.31 156.64 2.02 o 3 3 7 25.60 22.96 0.56 o 4 3 7 18.98 19.83 0.57 o 5 3 7 10.55 11.76 0.56 o 6 3 7 24.06 19.49 3.57 o 0 4 7 10.79 11.84 0.39 o 1 4 7 86.13 90.57 1.80 o 2 4 7 91.82 93.42 1.31 o 3 4 7 12.47 13.48 0.38 o 4 4 7 1.46 0.62 0.22 o 5 4 7 55.32 55.37 1.38 o 6 4 7 1.66 0.61 0.40 o 0 5 7 94.25 96.74 2.00 o 1 5 7 84.14 85.56 1.25 o 2 5 7 49.16 50.90 0.80 o 3 5 7 307.86 305.34 4.10 o 4 5 7 59.59 62.33 1.87 o 5 5 7 7.09 5.78 1.07 o 6 5 7 3.92 2.07 0.83 o 0 6 7 0.56 0.17 0.09 o 1 6 7 30.95 26.51 0.62 o 2 6 7 230.66 231.61 2.72 o 3 6 7 586.28 587.96 8.38 o 4 6 7 56.55 63.80 3.04 o 5 6 7 5.64 3.81 0.81 o 6 6 7 3.97 4.93 0.91 o 0 7 7 22.59 23.58 0.71 o 1 7 7 70.85 67.58 1.20 o 2 7 7 120.60 121.48 1.88 o 3 7 7 56.37 57.13 1.95 o 4 7 7 7.56 5.86 0.54 o 5 7 7 0.52 0.17 0.15 o 0 8 7 60.49 63.88 2.19 o 1 8 7 30.80 32.98 0.68 o 2 8 7 126.25 124.94 2.05 o 3 8 7 12.05 12.12 0.54 o 4 8 7 10.59 9.95 0.66 o 5 8 7 15.73 7.85 3.87 o 0 9 7 1.82 2.03 0.39 o 1 9 7 77.88 85.73 1.52 o 2 9 7 13.80 15.40 0.69 o 3 9 7 6.44 7.87 0.52 o 4 9 7 9.02 4.48 1.64 o 0 10 7 0.01 -0.44 0.44 o 1 10 7 8.33 7.02 0.51 o 2 10 7 0.13 0.20 0.21 o 3 10 7 15.62 16.99 0.77 o 4 10 7 2.05 0.90 0.45 o 0 11 7 2.21 2.28 0.77 o 1 11 7 3.82 2.30 0.50 o 2 11 7 0.58 0.52 0.25 o 3 11 7 0.70 0.29 0.22 o 0 12 7 6.33 4.75 1.76 o 1 12 7 0.39 0.00 0.44 o 2 12 7 1.98 1.50 0.62 o 0 13 7 3.43 4.84 1.02 o 1 13 7 15.31 16.76 1.19 o 0 0 8 371.53 352.05 9.64 o 1 0 8 746.95 744.37 11.97 o 2 0 8 33.73 34.19 0.70 o 3 0 8 0.15 -0.12 0.12 o 4 0 8 1.26 0.90 0.23 o 5 0 8 26.35 26.92 1.29 o 6 0 8 0.01 -0.36 0.61 o 0 1 8 1249.95 1183.00 19.43 o 1 1 8 191.13 213.43 2.14 o 2 1 8 16.13 21.19 0.52 o 3 1 8 93.37 98.55 1.68 o 4 1 8 20.83 21.17 0.50 o 5 1 8 16.97 15.40 1.34 o 6 1 8 11.06 7.75 2.48 o 0 2 8 3.60 3.54 0.40 o 1 2 8 491.05 504.19 5.07 o 2 2 8 0.55 0.19 0.07 o 3 2 8 26.83 23.13 0.55 o 4 2 8 68.17 67.55 1.07 o 5 2 8 2.01 0.78 0.29 o 6 2 8 10.67 8.40 1.55 o 0 3 8 932.67 976.83 15.20 o 1 3 8 17.28 13.99 0.43 o 2 3 8 23.76 25.24 0.48 o 3 3 8 74.43 68.10 1.15 o 4 3 8 100.56 103.90 1.89 o 5 3 8 16.91 14.65 1.35 o 6 3 8 0.97 0.48 0.46 o 0 4 8 5.76 6.15 0.31 o 1 4 8 375.43 377.74 4.36 o 2 4 8 173.06 169.60 2.22 o 3 4 8 93.71 90.48 1.32 o 4 4 8 18.83 21.66 0.65 o 5 4 8 1.12 0.25 0.19 o 6 4 8 0.64 0.19 0.21 o 0 5 8 276.04 272.74 4.51 o 1 5 8 1.84 1.05 0.14 o 2 5 8 94.23 95.87 1.26 o 3 5 8 258.80 277.46 4.33 o 4 5 8 103.83 113.48 3.33 o 5 5 8 10.97 6.78 1.09 o 6 5 8 4.42 2.83 0.90 o 0 6 8 12.62 12.84 1.28 o 1 6 8 136.62 133.91 1.66 o 2 6 8 180.43 175.96 2.47 o 3 6 8 510.20 520.54 8.28 o 4 6 8 15.69 13.44 0.75 o 5 6 8 13.38 10.27 1.76 o 0 7 8 2.02 1.25 0.26 o 1 7 8 27.57 27.93 0.59 o 2 7 8 610.65 617.60 8.30 o 3 7 8 44.97 47.22 1.37 o 4 7 8 4.23 2.44 0.83 o 5 7 8 9.11 5.35 2.98 o 0 8 8 24.55 24.08 0.81 o 1 8 8 27.69 29.02 0.65 o 2 8 8 7.70 6.02 0.35 o 3 8 8 1.77 0.66 0.36 o 4 8 8 11.11 13.19 0.81 o 5 8 8 7.37 2.88 1.91 o 0 9 8 212.50 203.09 3.85 o 1 9 8 68.19 68.91 1.31 o 2 9 8 0.76 0.18 0.16 o 3 9 8 36.92 37.50 1.34 o 4 9 8 1.19 0.31 0.21 o 0 10 8 6.96 5.76 0.88 o 1 10 8 9.63 10.00 0.64 o 2 10 8 0.62 0.08 0.21 o 3 10 8 5.19 2.13 1.04 o 4 10 8 1.64 1.18 0.44 o 0 11 8 21.57 21.20 1.50 o 1 11 8 0.39 0.03 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6 10 180.91 180.97 3.04 o 1 6 10 13.15 13.73 0.43 o 2 6 10 51.41 52.83 1.32 o 3 6 10 108.51 115.71 2.99 o 4 6 10 0.07 0.01 0.13 o 5 6 10 4.23 1.97 0.78 o 0 7 10 18.61 15.84 0.68 o 1 7 10 38.76 38.23 0.80 o 2 7 10 42.04 43.90 1.17 o 3 7 10 111.23 105.59 2.66 o 4 7 10 12.84 13.19 0.91 o 5 7 10 10.47 3.26 2.76 o 0 8 10 21.85 23.87 0.93 o 1 8 10 19.46 23.45 0.66 o 2 8 10 15.51 16.80 0.65 o 3 8 10 28.01 27.01 1.15 o 4 8 10 29.33 31.71 1.54 o 0 9 10 14.42 14.53 0.78 o 1 9 10 19.14 17.48 0.68 o 2 9 10 6.24 5.84 0.55 o 3 9 10 23.14 15.95 3.61 o 4 9 10 35.62 22.39 7.89 o 0 10 10 30.87 28.69 1.46 o 1 10 10 4.48 6.02 0.55 o 2 10 10 15.00 15.46 0.80 o 3 10 10 2.31 0.81 0.54 o 0 11 10 5.31 6.02 1.87 o 1 11 10 11.39 9.46 0.72 o 2 11 10 9.32 6.23 1.35 o 0 12 10 32.28 39.06 3.66 o 1 12 10 2.96 3.73 0.70 o 1 0 11 289.91 281.73 5.97 o 2 0 11 86.25 83.52 2.29 o 3 0 11 3.99 4.95 0.45 o 4 0 11 21.67 19.67 0.81 o 5 0 11 21.76 21.48 1.10 o 6 0 11 0.39 0.58 0.67 o 0 1 11 40.68 44.47 1.39 o 1 1 11 6.70 4.53 0.27 o 2 1 11 6.68 5.94 0.32 o 3 1 11 182.90 169.14 2.54 o 4 1 11 4.52 4.73 0.40 o 5 1 11 17.89 16.99 0.67 o 6 1 11 3.09 2.72 0.64 o 0 2 11 19.91 16.78 0.82 o 1 2 11 71.67 69.61 1.16 o 2 2 11 84.93 85.71 1.39 o 3 2 11 22.77 20.76 0.51 o 4 2 11 0.08 -0.07 0.16 o 5 2 11 20.36 18.25 0.78 o 6 2 11 4.19 5.01 1.26 o 0 3 11 1.06 0.75 0.27 o 1 3 11 55.19 51.58 1.10 o 2 3 11 390.64 367.47 4.66 o 3 3 11 33.82 31.01 0.79 o 4 3 11 2.67 2.91 0.37 o 5 3 11 30.97 35.29 1.06 o 0 4 11 188.67 198.94 4.48 o 1 4 11 181.34 183.71 2.96 o 2 4 11 30.85 30.18 0.65 o 3 4 11 284.90 294.50 5.98 o 4 4 11 0.56 0.37 0.17 o 5 4 11 2.03 1.49 0.42 o 0 5 11 52.18 48.87 1.49 o 1 5 11 24.00 22.63 0.72 o 2 5 11 96.71 102.85 1.63 o 3 5 11 14.49 17.81 0.79 o 4 5 11 1.15 0.52 0.30 o 5 5 11 5.94 9.02 0.70 o 0 6 11 0.40 0.77 0.28 o 1 6 11 47.55 44.32 1.11 o 2 6 11 155.11 157.12 2.81 o 3 6 11 6.69 6.57 0.53 o 4 6 11 0.46 0.19 0.18 o 5 6 11 0.57 0.03 0.24 o 0 7 11 48.10 39.30 1.13 o 1 7 11 18.50 17.72 0.57 o 2 7 11 2.07 1.30 0.35 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2.95 o 1 3 12 55.18 57.20 1.05 o 2 3 12 81.52 85.49 1.37 o 3 3 12 40.14 39.00 1.36 o 4 3 12 70.00 67.98 1.79 o 5 3 12 4.97 6.30 0.57 o 0 4 12 98.05 97.82 2.48 o 1 4 12 24.68 26.32 0.75 o 2 4 12 70.24 75.90 1.65 o 3 4 12 12.65 11.50 0.62 o 4 4 12 46.45 49.85 1.42 o 5 4 12 7.50 8.11 0.64 o 0 5 12 11.64 8.41 0.56 o 1 5 12 45.19 44.41 1.06 o 2 5 12 97.57 98.59 1.93 o 3 5 12 26.50 28.83 1.13 o 4 5 12 9.83 9.35 0.98 o 5 5 12 5.05 5.30 0.68 o 0 6 12 44.09 46.19 1.25 o 1 6 12 0.14 0.29 0.16 o 2 6 12 28.95 31.96 0.83 o 3 6 12 0.55 0.07 0.17 o 4 6 12 10.57 3.59 2.61 o 5 6 12 1.76 0.76 0.37 o 0 7 12 23.59 17.73 0.84 o 1 7 12 7.53 6.47 0.43 o 2 7 12 1.76 0.68 0.30 o 3 7 12 23.84 24.65 1.01 o 4 7 12 3.59 1.26 1.05 o 0 8 12 6.27 6.06 0.59 o 1 8 12 8.15 10.59 0.57 o 2 8 12 56.59 59.26 1.73 o 3 8 12 18.18 13.07 3.65 o 4 8 12 0.42 0.46 0.28 o 0 9 12 24.67 30.41 1.32 o 1 9 12 43.34 43.71 1.19 o 2 9 12 40.74 23.03 7.45 o 3 9 12 10.25 2.32 1.61 o 0 10 12 2.47 2.36 0.74 o 1 10 12 26.87 33.47 1.14 o 2 10 12 20.52 16.03 2.91 o 0 11 12 4.39 6.04 1.12 o 1 11 12 26.86 30.01 1.53 o 1 0 13 0.77 0.21 0.17 o 2 0 13 39.78 44.39 1.28 o 3 0 13 12.58 11.88 0.76 o 4 0 13 64.65 55.95 2.23 o 5 0 13 0.48 0.50 0.56 o 0 1 13 3.60 3.07 0.46 o 1 1 13 303.28 302.60 3.79 o 2 1 13 11.78 11.81 0.43 o 3 1 13 24.63 26.17 0.86 o 4 1 13 59.08 58.39 1.66 o 5 1 13 23.91 25.74 1.03 o 0 2 13 140.44 141.95 3.09 o 1 2 13 153.90 144.64 2.13 o 2 2 13 61.40 55.84 1.18 o 3 2 13 46.84 48.44 1.14 o 4 2 13 58.91 59.35 1.54 o 5 2 13 11.35 11.42 0.67 o 0 3 13 21.98 23.19 0.94 o 1 3 13 96.78 95.91 1.58 o 2 3 13 10.43 8.50 0.48 o 3 3 13 19.73 18.05 1.22 o 4 3 13 18.20 16.92 0.75 o 5 3 13 0.95 0.44 0.32 o 0 4 13 72.12 71.87 1.88 o 1 4 13 22.30 19.39 0.57 o 2 4 13 12.39 12.72 0.61 o 3 4 13 34.37 35.29 1.36 o 4 4 13 5.12 5.57 0.54 o 5 4 13 1.92 1.17 0.41 o 0 5 13 5.60 4.26 0.47 o 1 5 13 37.32 38.25 0.93 o 2 5 13 27.10 26.14 0.88 o 3 5 13 14.91 14.15 0.71 o 4 5 13 5.34 5.16 0.64 o 5 5 13 5.38 5.84 0.75 o 0 6 13 11.47 12.31 0.66 o 1 6 13 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17.28 0.77 o 1 3 14 6.57 8.19 0.54 o 2 3 14 0.85 0.14 0.18 o 3 3 14 91.80 90.71 3.21 o 4 3 14 0.23 0.36 0.25 o 5 3 14 2.34 2.42 0.42 o 0 4 14 23.55 24.58 0.86 o 1 4 14 6.39 5.89 0.39 o 2 4 14 62.06 60.47 1.70 o 3 4 14 4.18 5.37 0.50 o 4 4 14 8.86 9.56 0.82 o 0 5 14 9.81 7.42 0.67 o 1 5 14 18.30 17.96 0.59 o 2 5 14 30.49 27.93 0.93 o 3 5 14 15.79 15.01 0.75 o 4 5 14 11.70 13.75 1.05 o 0 6 14 8.56 8.55 0.73 o 1 6 14 24.94 22.74 0.85 o 2 6 14 7.19 7.29 0.53 o 3 6 14 0.75 0.23 0.20 o 4 6 14 5.29 6.65 0.76 o 0 7 14 65.55 67.33 2.06 o 1 7 14 17.43 17.37 0.79 o 2 7 14 1.51 0.93 0.28 o 3 7 14 1.50 0.79 0.32 o 4 7 14 13.33 17.67 1.35 o 0 8 14 11.23 11.05 0.87 o 1 8 14 1.58 1.48 0.37 o 2 8 14 10.62 7.75 1.31 o 3 8 14 5.57 2.98 1.64 o 0 9 14 0.25 1.22 0.58 o 1 9 14 8.04 11.09 0.75 o 2 9 14 2.30 1.20 0.84 o 0 10 14 0.02 0.10 0.69 o 1 10 14 16.95 17.61 0.99 o 1 0 15 55.32 53.26 2.39 o 2 0 15 118.28 126.35 4.70 o 3 0 15 9.05 9.67 0.75 o 4 0 15 24.80 29.91 2.04 o 5 0 15 38.41 40.33 2.64 o 0 1 15 69.06 71.38 2.19 o 1 1 15 52.96 54.36 1.25 o 2 1 15 9.91 9.45 0.48 o 3 1 15 15.91 15.71 0.68 o 4 1 15 0.37 0.26 0.20 o 5 1 15 19.11 22.99 2.80 o 0 2 15 1.80 0.85 0.37 o 1 2 15 0.61 0.29 0.11 o 2 2 15 57.36 59.24 1.58 o 3 2 15 5.77 4.51 0.46 o 4 2 15 1.67 0.63 0.23 o 0 3 15 0.59 0.10 0.15 o 1 3 15 17.41 17.49 0.64 o 2 3 15 8.36 7.22 0.53 o 3 3 15 71.63 72.55 2.77 o 4 3 15 5.99 6.76 0.62 o 0 4 15 32.75 30.84 1.97 o 1 4 15 3.89 3.32 0.36 o 2 4 15 18.46 17.07 0.81 o 3 4 15 5.46 5.37 0.54 o 4 4 15 3.01 2.99 0.55 o 0 5 15 1.51 0.37 0.18 o 1 5 15 0.94 0.68 0.21 o 2 5 15 8.65 8.39 0.63 o 3 5 15 3.35 4.55 0.51 o 4 5 15 1.25 0.84 0.45 o 0 6 15 3.57 4.65 0.64 o 1 6 15 8.58 9.11 0.55 o 2 6 15 4.56 4.77 0.48 o 3 6 15 19.15 26.00 1.20 o 4 6 15 15.05 16.00 1.14 o 0 7 15 2.22 4.05 0.66 o 1 7 15 3.55 1.85 0.52 o 2 7 15 3.27 2.93 0.50 o 3 7 15 1.92 0.83 0.40 o 0 8 15 2.52 3.13 0.64 o 1 8 15 4.93 7.02 0.63 o 2 8 15 24.42 21.72 3.31 o 3 8 15 18.82 23.79 2.21 o 0 9 15 7.86 10.64 0.96 o 1 9 15 0.92 0.91 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12.95 13.04 0.82 o 0 4 19 7.85 9.92 0.86 o 1 4 19 6.54 6.57 0.59 o 2 4 19 0.35 0.13 0.20 o 0 5 19 12.61 18.79 1.50 o 1 5 19 1.17 0.48 0.38 o 0 6 19 1.77 0.40 0.51 o 0 0 20 0.18 0.27 0.55 o 1 0 20 21.48 23.06 1.63 o 2 0 20 4.93 6.14 0.87 o 0 1 20 4.36 5.51 0.86 o 1 1 20 1.23 0.51 0.37 o 2 1 20 0.79 0.26 0.20 o 0 2 20 31.65 37.17 2.50 o 1 2 20 2.78 1.43 0.60 o 2 2 20 3.54 2.51 0.59 o 0 3 20 13.75 13.39 1.76 o 1 3 20 15.71 16.19 1.10 o 0 4 20 0.92 0.46 0.62 o 1 4 20 20.06 22.84 1.11 o 1 0 21 2.46 2.73 0.81 o 0 1 21 2.45 0.19 0.36 o 0 2 21 5.35 5.77 1.01 o