#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:58:32 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181208 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/87/2228722.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2228722_Fobs loop_ _publ_author_name 'Kandiah, Mathivathani' 'Wragg, David Stephen' 'Tilset, Mats' 'Lillerud, Karl Petter' _publ_section_title ; Poly[tris(\m-2-aminobenzene-1,4-dicarboxylato)tetrakis(N,N-dimethylformamide)diyttrium(III)] ; _journal_coeditor_code HB5707 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m44 _journal_page_last m45 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.359 _cell_angle_beta 111.301 _cell_angle_gamma 101.265 _cell_length_a 10.5254 _cell_length_b 11.0339 _cell_length_c 12.8550 _exptl_crystal_F_000 505.00 _reflns_d_resolution_high 1.0548 _cod_data_source_file hb5707Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dsw_mk6 in P1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 178.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11363.61 11516.20 73.78 o 2 0 0 5616.71 5625.75 113.27 o 3 0 0 1024.50 1359.40 26.32 o 4 0 0 2866.37 2789.84 34.84 o 5 0 0 532.52 432.95 14.79 o 6 0 0 10.01 0.96 7.99 o 7 0 0 164.25 206.55 16.08 o 8 0 0 252.28 193.48 16.94 o -9 1 0 614.35 612.42 24.13 o -8 1 0 58.38 66.03 11.78 o -7 1 0 88.22 123.57 11.57 o -6 1 0 281.98 293.93 14.88 o -5 1 0 3978.98 3771.09 50.42 o -4 1 0 2240.11 2762.58 29.65 o -3 1 0 715.45 790.81 16.67 o -2 1 0 1578.77 1519.57 14.78 o -1 1 0 9378.07 7089.38 189.49 o 0 1 0 26956.66 25906.91 139.24 o 1 1 0 703.88 597.52 13.08 o 2 1 0 3666.90 4809.51 41.66 o 3 1 0 3786.63 4602.12 55.07 o 4 1 0 7194.29 7540.86 65.49 o 5 1 0 3095.75 3034.13 32.71 o 6 1 0 512.92 606.72 21.33 o 7 1 0 12.69 15.86 8.48 o 8 1 0 221.79 202.34 14.65 o -9 2 0 668.77 636.44 27.53 o -8 2 0 33.67 27.65 17.32 o -7 2 0 33.94 23.78 8.26 o -6 2 0 1258.80 1330.75 26.49 o -5 2 0 1385.85 1228.97 24.20 o -4 2 0 2824.60 3294.55 31.26 o -3 2 0 139.14 168.09 3.87 o -2 2 0 1745.33 2014.14 29.80 o -1 2 0 273.74 378.90 24.05 o 0 2 0 6066.53 6517.35 56.94 o 1 2 0 1181.48 1577.91 28.83 o 2 2 0 315.22 387.92 11.20 o 3 2 0 3535.64 3864.84 40.79 o 4 2 0 1557.84 1481.09 21.89 o 5 2 0 804.17 730.12 17.31 o 6 2 0 6.23 0.52 7.28 o 7 2 0 191.10 174.25 14.21 o 8 2 0 1418.33 1341.11 34.63 o -9 3 0 340.57 307.08 18.29 o -8 3 0 0.10 1.80 10.50 o -7 3 0 715.00 747.07 23.69 o -6 3 0 1180.74 1197.24 25.94 o -5 3 0 1118.28 970.03 15.95 o -4 3 0 3831.53 3601.35 39.89 o -3 3 0 299.75 286.15 13.61 o -2 3 0 39.36 347.36 10.16 o -1 3 0 445.32 442.01 25.26 o 0 3 0 1389.93 1532.27 38.32 o 1 3 0 788.29 794.30 10.09 o 2 3 0 1179.38 1138.79 15.96 o 3 3 0 5259.03 5732.10 51.73 o 4 3 0 1436.28 1433.94 22.05 o 5 3 0 441.59 462.39 14.24 o 6 3 0 33.03 37.55 9.08 o 7 3 0 910.43 803.46 24.02 o -9 4 0 44.94 41.79 13.77 o -8 4 0 312.26 339.29 18.69 o -7 4 0 1182.58 1198.32 28.29 o -6 4 0 1731.12 1595.55 33.32 o -5 4 0 645.03 703.33 15.37 o -4 4 0 2340.98 2632.02 31.38 o -3 4 0 62.87 130.92 18.67 o -2 4 0 63.15 69.24 6.84 o -1 4 0 381.10 406.98 13.80 o 0 4 0 2894.67 3289.20 26.62 o 1 4 0 918.70 1147.51 22.76 o 2 4 0 3375.87 3428.37 37.74 o 3 4 0 2011.87 2059.84 28.13 o 4 4 0 579.78 592.00 15.97 o 5 4 0 200.27 174.58 9.45 o 6 4 0 1085.34 1208.40 26.78 o 7 4 0 166.28 166.53 21.32 o -9 5 0 14.10 11.03 12.29 o -8 5 0 250.77 281.93 23.98 o -7 5 0 388.83 456.01 18.20 o -6 5 0 215.20 249.15 16.38 o -5 5 0 6.38 10.91 6.19 o -4 5 0 30.37 48.59 6.33 o -3 5 0 1707.70 1928.51 26.74 o -2 5 0 2767.55 3131.35 30.32 o -1 5 0 3764.12 4240.77 50.39 o 0 5 0 3850.29 4320.34 42.69 o 1 5 0 219.10 208.68 10.44 o 2 5 0 721.36 754.26 24.77 o 3 5 0 784.01 763.06 17.27 o 4 5 0 336.31 293.12 11.80 o 5 5 0 335.13 302.56 16.26 o 6 5 0 594.45 609.92 30.18 o -8 6 0 439.32 431.82 20.13 o -7 6 0 459.72 468.60 20.96 o -6 6 0 290.79 335.27 13.72 o -5 6 0 10.50 3.21 6.46 o -4 6 0 60.82 67.33 7.99 o -3 6 0 1519.95 1433.80 22.14 o -2 6 0 1044.19 1088.90 23.31 o -1 6 0 225.77 212.96 15.01 o 0 6 0 93.65 131.70 10.59 o 1 6 0 742.76 691.75 15.79 o 2 6 0 1837.68 1870.83 55.50 o 3 6 0 822.15 821.60 32.52 o 4 6 0 49.54 42.60 10.67 o 5 6 0 207.44 225.71 23.22 o -8 7 0 708.77 758.67 36.59 o -7 7 0 313.58 324.98 17.26 o -6 7 0 62.48 53.91 9.49 o -5 7 0 54.47 56.63 18.82 o -4 7 0 1007.55 1125.10 20.69 o -3 7 0 744.96 734.43 17.46 o -2 7 0 656.68 691.22 23.19 o -1 7 0 40.93 26.86 8.05 o 0 7 0 237.68 258.64 11.96 o 1 7 0 301.64 270.48 17.02 o 2 7 0 701.80 680.66 21.93 o 3 7 0 121.24 125.16 16.63 o 4 7 0 177.13 168.18 14.89 o -7 8 0 681.82 714.46 30.50 o -6 8 0 20.58 14.71 9.15 o -5 8 0 266.00 267.03 16.12 o -4 8 0 309.66 276.92 14.34 o -3 8 0 356.56 368.75 16.16 o -2 8 0 19.60 15.32 7.21 o -1 8 0 222.96 200.99 14.47 o 0 8 0 508.26 465.24 18.27 o 1 8 0 271.36 317.69 17.53 o 2 8 0 693.06 673.60 23.14 o 3 8 0 36.44 28.95 11.75 o -6 9 0 40.63 36.79 11.99 o -5 9 0 538.94 558.85 23.01 o -4 9 0 299.33 335.62 21.68 o -3 9 0 417.32 339.26 24.81 o -2 9 0 18.54 17.16 14.71 o -1 9 0 87.22 117.63 28.92 o 0 9 0 516.97 491.61 26.29 o 1 9 0 458.58 491.14 29.48 o 2 9 0 474.58 433.36 27.46 o -4 10 0 319.65 332.61 25.71 o -3 10 0 237.52 183.44 21.96 o -2 10 0 9.98 5.08 14.14 o -1 10 0 439.64 372.42 27.58 o 0 -10 1 9.81 0.17 14.10 o 1 -10 1 245.65 257.65 24.16 o 2 -10 1 282.52 230.20 22.23 o 3 -10 1 367.73 441.45 28.26 o 4 -10 1 264.16 229.60 20.79 o -2 -9 1 664.49 644.05 39.29 o -1 -9 1 97.81 97.61 18.79 o 0 -9 1 31.35 32.77 15.55 o 1 -9 1 317.17 366.47 23.88 o 2 -9 1 549.51 528.35 43.73 o 3 -9 1 301.03 354.44 22.09 o 4 -9 1 94.99 137.42 14.54 o 5 -9 1 9.16 16.06 11.36 o 6 -9 1 717.68 711.24 25.84 o -4 -8 1 267.14 246.03 27.09 o -3 -8 1 997.13 1065.00 37.60 o -2 -8 1 686.63 638.33 28.99 o -1 -8 1 278.29 333.84 23.20 o 0 -8 1 10.86 7.44 8.50 o 1 -8 1 368.16 324.75 16.92 o 2 -8 1 474.24 491.54 18.36 o 3 -8 1 93.79 90.54 12.13 o 4 -8 1 22.74 15.30 9.87 o 5 -8 1 132.52 138.33 19.17 o 6 -8 1 733.95 768.93 32.76 o 7 -8 1 348.47 377.02 26.09 o -5 -7 1 7.12 9.98 12.03 o -4 -7 1 526.20 538.39 28.41 o -3 -7 1 1438.87 1578.43 47.02 o -2 -7 1 845.47 870.70 23.69 o -1 -7 1 42.72 47.05 7.22 o 0 -7 1 219.57 235.46 10.86 o 1 -7 1 1953.50 2021.94 35.62 o 2 -7 1 625.00 558.95 14.00 o 3 -7 1 70.52 82.59 10.76 o 4 -7 1 286.62 299.35 15.99 o 5 -7 1 166.52 226.93 13.51 o 6 -7 1 330.06 312.17 20.14 o 7 -7 1 309.87 279.66 17.04 o 8 -7 1 5.45 11.62 14.29 o -6 -6 1 48.41 48.29 12.79 o -5 -6 1 205.43 229.95 23.28 o -4 -6 1 2708.76 2795.84 53.25 o -3 -6 1 2310.85 2245.48 37.47 o -2 -6 1 1134.21 1176.44 20.62 o -1 -6 1 8.50 7.85 6.20 o 0 -6 1 3156.09 3125.80 44.84 o 1 -6 1 1280.77 1180.10 22.08 o 2 -6 1 778.32 644.41 17.94 o 3 -6 1 314.91 384.54 13.32 o 4 -6 1 456.30 481.20 21.30 o 5 -6 1 312.08 361.32 13.09 o 6 -6 1 283.04 270.98 14.55 o 7 -6 1 96.48 97.88 13.46 o 8 -6 1 9.89 0.35 10.90 o -6 -5 1 163.58 149.65 12.18 o -5 -5 1 1009.97 966.71 21.65 o -4 -5 1 1087.74 1070.67 20.20 o -3 -5 1 486.07 502.96 15.95 o -2 -5 1 2.10 1.27 5.24 o -1 -5 1 6126.38 6665.24 68.99 o 0 -5 1 11268.01 12332.23 92.03 o 1 -5 1 1976.77 2216.90 33.06 o 2 -5 1 2016.59 2248.62 23.30 o 3 -5 1 27.46 14.12 5.87 o 4 -5 1 755.48 738.37 14.81 o 5 -5 1 65.85 66.17 7.84 o 6 -5 1 243.83 216.74 15.15 o 7 -5 1 1.26 3.20 9.58 o 8 -5 1 198.58 195.96 15.42 o -7 -4 1 205.66 253.03 18.42 o -6 -4 1 487.08 546.01 18.91 o -5 -4 1 327.13 379.13 12.48 o -4 -4 1 1062.30 1144.78 19.82 o -3 -4 1 705.16 747.11 16.28 o -2 -4 1 1034.41 847.92 16.87 o -1 -4 1 3030.85 2728.66 38.73 o 0 -4 1 5353.38 5480.54 42.46 o 1 -4 1 277.68 190.20 10.05 o 2 -4 1 190.37 134.18 10.24 o 3 -4 1 2910.57 2667.10 30.27 o 4 -4 1 4354.43 4368.76 73.49 o 5 -4 1 1224.85 1200.72 19.23 o 6 -4 1 607.83 649.34 19.85 o 7 -4 1 1.22 5.78 9.53 o 8 -4 1 396.92 450.17 22.37 o -8 -3 1 536.70 567.31 24.18 o -7 -3 1 161.79 153.02 15.69 o -6 -3 1 301.92 295.98 11.90 o -5 -3 1 268.23 283.53 11.85 o -4 -3 1 1779.66 1946.46 29.60 o -3 -3 1 1149.74 1047.60 18.49 o -2 -3 1 234.98 264.57 11.71 o -1 -3 1 451.40 362.12 31.75 o 0 -3 1 6446.67 7532.84 126.84 o 1 -3 1 245.63 100.44 6.16 o 2 -3 1 70.17 87.02 10.19 o 3 -3 1 6921.36 6937.75 60.15 o 4 -3 1 6475.99 6831.53 65.66 o 5 -3 1 628.57 529.87 10.73 o 6 -3 1 295.09 273.56 13.65 o 7 -3 1 375.09 384.75 26.53 o 8 -3 1 718.31 792.02 27.86 o -8 -2 1 88.89 84.46 13.07 o -7 -2 1 79.40 105.46 12.74 o -6 -2 1 433.97 405.91 12.14 o -5 -2 1 368.99 410.13 12.68 o -4 -2 1 2811.86 3094.20 34.51 o -3 -2 1 2096.02 2054.76 20.29 o -2 -2 1 107.31 334.51 23.94 o -1 -2 1 268.67 241.21 12.68 o 0 -2 1 6036.81 6097.56 29.35 o 1 -2 1 2045.39 1825.99 24.91 o 2 -2 1 5602.53 6108.67 70.09 o 3 -2 1 5776.60 5387.69 57.37 o 4 -2 1 6645.65 6652.62 78.84 o 5 -2 1 1311.94 1327.46 27.18 o 6 -2 1 167.74 177.05 13.56 o 7 -2 1 267.47 233.02 17.22 o 8 -2 1 493.50 510.31 21.86 o -8 -1 1 132.21 93.67 13.97 o -7 -1 1 748.31 756.53 20.47 o -6 -1 1 1830.65 1740.62 28.69 o -5 -1 1 2555.55 2630.01 30.49 o -4 -1 1 3942.88 4331.05 43.16 o -3 -1 1 2257.79 2273.58 38.24 o -2 -1 1 334.08 216.61 7.51 o -1 -1 1 445.24 450.36 37.71 o 0 -1 1 6784.00 8264.87 56.58 o 1 -1 1 5163.43 3758.50 46.80 o 2 -1 1 6057.18 6741.54 63.96 o 3 -1 1 2798.79 2769.80 36.85 o 4 -1 1 6042.96 6076.53 66.65 o 5 -1 1 122.99 161.54 10.09 o 6 -1 1 654.43 618.05 19.83 o 7 -1 1 172.70 143.26 12.84 o 8 -1 1 492.12 524.83 22.19 o -9 0 1 66.03 20.29 11.72 o -8 0 1 12.55 17.71 6.66 o -7 0 1 100.71 155.16 17.86 o -6 0 1 517.92 498.35 13.13 o -5 0 1 161.61 204.56 19.44 o -4 0 1 1680.21 1717.18 20.54 o -3 0 1 2813.95 3375.87 36.30 o -2 0 1 2853.41 4536.48 52.83 o -1 0 1 31854.39 29344.28 201.34 o 0 0 1 1066.65 1194.43 83.81 o 1 0 1 9.59 2.15 12.95 o 2 0 1 51.96 2.65 5.31 o 3 0 1 1196.23 1290.80 14.23 o 4 0 1 1317.27 1407.37 19.85 o 5 0 1 54.27 44.56 4.47 o 6 0 1 913.13 1017.11 27.20 o 7 0 1 550.54 529.96 18.19 o 8 0 1 760.99 776.29 27.37 o -9 1 1 7.71 9.70 8.97 o -8 1 1 157.59 172.04 32.43 o -7 1 1 394.32 432.48 28.50 o -6 1 1 2082.89 1981.43 27.97 o -5 1 1 516.63 671.16 13.88 o -4 1 1 257.81 213.31 8.75 o -3 1 1 1161.21 1061.81 17.08 o -2 1 1 3229.83 2824.28 27.22 o -1 1 1 183.70 4.22 15.26 o 0 1 1 2700.42 1764.98 11.36 o 1 1 1 4854.24 5393.37 38.41 o 2 1 1 3976.67 4039.28 35.38 o 3 1 1 5503.92 5897.73 61.89 o 4 1 1 2878.52 3010.63 34.86 o 5 1 1 0.86 21.76 8.65 o 6 1 1 640.44 665.17 17.81 o 7 1 1 454.67 544.18 23.35 o 8 1 1 753.93 673.54 37.80 o -9 2 1 52.82 41.91 11.87 o -8 2 1 522.45 490.18 20.76 o -7 2 1 641.92 735.79 21.06 o -6 2 1 558.34 563.70 12.29 o -5 2 1 444.71 597.46 12.16 o -4 2 1 1659.81 1498.14 18.22 o -3 2 1 1586.21 1590.85 20.98 o -2 2 1 5373.11 4190.19 26.82 o -1 2 1 172.78 164.99 4.49 o 0 2 1 3336.91 3853.72 65.92 o 1 2 1 283.31 389.97 13.25 o 2 2 1 5256.07 5287.02 47.09 o 3 2 1 1632.23 1766.07 23.60 o 4 2 1 132.67 128.27 13.71 o 5 2 1 418.61 470.23 13.18 o 6 2 1 1671.99 1535.31 32.67 o 7 2 1 1754.92 1971.12 38.66 o -9 3 1 208.06 231.62 21.67 o -8 3 1 1246.74 1270.38 28.57 o -7 3 1 746.13 727.86 24.04 o -6 3 1 420.95 384.39 12.25 o -5 3 1 159.34 195.24 7.74 o -4 3 1 822.33 519.13 51.69 o -3 3 1 1308.16 745.54 19.96 o -2 3 1 853.34 672.18 20.59 o -1 3 1 35.71 6.82 4.87 o 0 3 1 901.00 859.62 20.57 o 1 3 1 1276.53 1292.19 17.04 o 2 3 1 7671.11 7872.76 76.45 o 3 3 1 357.42 392.61 10.40 o 4 3 1 0.52 2.63 5.72 o 5 3 1 179.14 200.90 9.39 o 6 3 1 3192.39 2856.73 62.99 o 7 3 1 79.74 101.86 13.39 o -9 4 1 626.12 600.10 23.15 o -8 4 1 1601.06 1650.73 35.47 o -7 4 1 739.79 691.32 26.59 o -6 4 1 134.18 148.11 10.06 o -5 4 1 87.63 102.16 16.99 o -4 4 1 1521.80 1560.07 20.43 o -3 4 1 1609.37 1840.01 22.73 o -2 4 1 1178.22 992.64 21.95 o -1 4 1 154.28 153.96 8.73 o 0 4 1 67.96 104.12 6.89 o 1 4 1 4203.23 4691.61 49.86 o 2 4 1 1578.23 1659.86 24.34 o 3 4 1 164.17 166.79 14.59 o 4 4 1 6.37 20.25 7.70 o 5 4 1 942.86 929.36 28.29 o 6 4 1 773.76 655.25 28.64 o -9 5 1 509.27 518.55 37.78 o -8 5 1 727.09 797.69 36.07 o -7 5 1 166.82 159.10 16.46 o -6 5 1 64.14 57.93 18.30 o -5 5 1 1294.45 1363.40 22.68 o -4 5 1 3799.24 3683.99 42.93 o -3 5 1 4804.47 4532.09 62.54 o -2 5 1 432.28 405.56 12.50 o -1 5 1 53.07 65.22 7.33 o 0 5 1 1483.08 1515.50 21.75 o 1 5 1 1108.11 1085.34 18.23 o 2 5 1 1339.51 1405.16 19.76 o 3 5 1 98.41 91.67 11.42 o 4 5 1 225.63 249.55 24.92 o 5 5 1 496.15 509.63 22.92 o 6 5 1 697.07 660.34 31.66 o -8 6 1 701.36 723.03 30.31 o -7 6 1 28.02 35.68 10.43 o -6 6 1 164.28 200.02 11.02 o -5 6 1 1427.52 1310.73 27.58 o -4 6 1 3131.68 2876.87 51.85 o -3 6 1 1387.35 1289.84 24.34 o -2 6 1 146.54 159.21 10.11 o -1 6 1 954.75 941.63 22.97 o 0 6 1 1732.24 1663.78 26.86 o 1 6 1 1470.71 1423.59 28.18 o 2 6 1 806.86 776.38 21.77 o 3 6 1 21.73 17.16 13.29 o 4 6 1 476.19 495.76 20.42 o 5 6 1 479.73 488.22 21.19 o -8 7 1 215.29 258.45 34.12 o -7 7 1 9.52 8.57 10.92 o -6 7 1 272.13 184.23 12.07 o -5 7 1 1829.95 1694.32 33.42 o -4 7 1 718.44 635.29 16.51 o -3 7 1 492.44 379.28 13.43 o -2 7 1 384.04 424.58 13.98 o -1 7 1 1034.62 1168.17 24.51 o 0 7 1 701.62 724.77 23.10 o 1 7 1 319.82 369.14 36.68 o 2 7 1 240.84 297.35 17.33 o 3 7 1 274.41 325.34 18.16 o 4 7 1 838.83 793.97 25.84 o -7 8 1 1.88 2.87 9.72 o -6 8 1 464.89 501.72 18.38 o -5 8 1 523.79 584.07 18.43 o -4 8 1 209.05 265.09 14.99 o -3 8 1 124.42 126.56 10.06 o -2 8 1 248.79 231.80 13.55 o -1 8 1 462.63 437.98 22.90 o 0 8 1 328.14 355.52 17.03 o 1 8 1 61.27 62.48 12.08 o 2 8 1 1.89 3.97 7.43 o 3 8 1 535.19 556.54 25.14 o -6 9 1 523.35 581.03 22.82 o -5 9 1 283.08 270.40 23.70 o -4 9 1 132.31 96.66 17.92 o -3 9 1 71.73 55.27 16.09 o -2 9 1 187.72 186.70 21.23 o -1 9 1 810.71 747.91 32.70 o 0 9 1 374.21 337.99 26.92 o 1 9 1 44.81 56.02 17.65 o -4 10 1 19.22 35.50 17.86 o -3 10 1 2.98 9.12 14.49 o -2 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487.69 428.40 16.74 o -5 6 3 76.89 113.43 10.29 o -4 6 3 2018.65 2132.53 31.10 o -3 6 3 1274.27 1433.04 23.16 o -2 6 3 1057.74 918.60 24.58 o -1 6 3 131.16 172.95 12.83 o 0 6 3 17.77 21.24 9.15 o 1 6 3 749.77 792.19 22.41 o 2 6 3 608.39 668.91 23.07 o 3 6 3 367.15 394.91 19.79 o 4 6 3 17.39 11.80 11.64 o -8 7 3 855.32 886.94 32.37 o -7 7 3 187.22 186.86 13.10 o -6 7 3 9.46 1.04 8.59 o -5 7 3 697.20 730.63 18.09 o -4 7 3 1858.85 1693.91 41.17 o -3 7 3 1617.87 1523.60 30.15 o -2 7 3 767.33 747.45 22.50 o -1 7 3 41.67 19.66 9.35 o 0 7 3 297.59 307.01 17.09 o 1 7 3 1333.98 1411.08 33.75 o 2 7 3 795.95 785.22 30.95 o 3 7 3 260.33 298.54 18.92 o -7 8 3 259.21 188.18 55.50 o -6 8 3 8.15 2.76 8.72 o -5 8 3 81.10 56.20 12.43 o -4 8 3 378.70 375.28 18.89 o -3 8 3 219.16 199.28 16.68 o -2 8 3 18.07 34.24 11.82 o -1 8 3 1369.65 1322.32 32.14 o 0 8 3 1607.05 1626.99 36.71 o 1 8 3 2162.16 2071.67 42.91 o -6 9 3 70.73 49.69 13.39 o -5 9 3 260.47 216.83 20.97 o -4 9 3 863.67 811.14 26.76 o -3 9 3 990.78 996.37 28.52 o -2 9 3 19.81 25.58 12.37 o -1 9 3 147.77 174.36 16.64 o 0 -10 4 33.78 28.62 13.02 o 1 -10 4 158.21 149.00 16.66 o 2 -10 4 594.60 641.84 32.95 o 3 -10 4 753.11 728.70 27.00 o -3 -9 4 450.52 438.86 34.41 o -2 -9 4 371.72 352.50 21.21 o -1 -9 4 58.85 68.94 23.67 o 0 -9 4 33.07 24.05 13.61 o 1 -9 4 882.63 809.32 31.55 o 2 -9 4 383.96 362.93 18.31 o 3 -9 4 250.03 294.93 31.24 o 4 -9 4 2.85 6.66 8.04 o 5 -9 4 647.10 652.66 33.98 o -4 -8 4 771.21 776.57 25.60 o -3 -8 4 369.13 392.98 38.68 o -2 -8 4 260.81 253.99 14.43 o -1 -8 4 20.26 16.96 12.13 o 0 -8 4 179.94 226.40 33.54 o 1 -8 4 801.50 815.43 40.50 o 2 -8 4 308.06 354.73 18.57 o 3 -8 4 6.89 6.82 10.46 o 4 -8 4 0.78 3.37 10.41 o 5 -8 4 936.85 1004.50 53.75 o 6 -8 4 838.16 845.69 36.56 o -5 -7 4 870.42 799.60 25.68 o -4 -7 4 588.89 635.86 37.98 o -3 -7 4 183.02 205.58 14.55 o -2 -7 4 80.30 92.77 11.71 o -1 -7 4 511.09 542.12 21.70 o 0 -7 4 721.40 712.93 23.43 o 1 -7 4 812.32 771.38 21.26 o 2 -7 4 609.15 513.13 27.92 o 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681.42 632.09 15.34 o -5 -2 4 3880.45 3980.84 46.31 o -4 -2 4 612.83 565.79 26.47 o -3 -2 4 520.99 566.56 11.02 o -2 -2 4 2559.82 2812.73 49.95 o -1 -2 4 6789.81 6346.57 86.16 o 0 -2 4 389.51 434.34 15.62 o 1 -2 4 286.85 229.71 7.95 o 2 -2 4 93.29 120.14 8.98 o 3 -2 4 752.44 776.51 15.23 o 4 -2 4 732.36 667.26 21.95 o 5 -2 4 165.72 150.25 13.23 o 6 -2 4 86.12 87.56 11.98 o 7 -2 4 776.94 755.70 39.80 o -9 -1 4 680.36 647.52 30.14 o -8 -1 4 32.67 21.50 11.28 o -7 -1 4 483.14 465.09 14.31 o -6 -1 4 1610.28 1698.71 23.42 o -5 -1 4 411.70 386.51 11.51 o -4 -1 4 214.74 121.65 6.76 o -3 -1 4 262.91 181.50 4.98 o -2 -1 4 4063.21 4055.58 39.37 o -1 -1 4 231.05 269.00 10.30 o 0 -1 4 558.04 707.85 14.14 o 1 -1 4 405.88 484.88 11.08 o 2 -1 4 775.90 706.04 11.97 o 3 -1 4 823.73 869.57 15.53 o 4 -1 4 749.19 717.19 20.74 o 5 -1 4 13.02 13.66 9.08 o 6 -1 4 68.88 82.52 12.80 o 7 -1 4 554.11 536.46 23.66 o -9 0 4 47.92 84.47 16.69 o -8 0 4 82.56 64.08 11.37 o -7 0 4 1188.86 1030.29 18.44 o -6 0 4 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1805.71 24.01 o -3 2 4 1108.10 960.01 16.42 o -2 2 4 3671.07 3778.00 39.53 o -1 2 4 435.43 351.65 10.29 o 0 2 4 450.49 475.70 19.46 o 1 2 4 6079.11 6272.58 106.11 o 2 2 4 229.98 226.57 14.47 o 3 2 4 346.74 329.27 14.21 o 4 2 4 45.91 65.36 9.77 o 5 2 4 511.14 433.31 28.31 o 6 2 4 187.35 190.83 21.07 o -9 3 4 147.95 172.76 18.59 o -8 3 4 743.67 760.47 22.75 o -7 3 4 664.16 650.19 23.82 o -6 3 4 320.91 317.73 12.02 o -5 3 4 61.61 84.95 8.81 o -4 3 4 1043.57 1101.70 21.48 o -3 3 4 610.08 595.84 15.64 o -2 3 4 209.98 195.29 7.84 o -1 3 4 1437.07 1439.16 22.86 o 0 3 4 4834.97 4861.63 75.14 o 1 3 4 5753.81 5853.92 57.34 o 2 3 4 655.21 696.52 16.07 o 3 3 4 172.80 169.76 11.99 o 4 3 4 18.03 16.43 18.99 o 5 3 4 372.54 310.36 23.47 o -9 4 4 145.30 129.77 19.52 o -8 4 4 1654.60 1614.10 32.71 o -7 4 4 98.04 137.82 12.89 o -6 4 4 99.31 127.92 8.93 o -5 4 4 419.82 408.64 11.86 o -4 4 4 3547.08 3529.86 40.86 o -3 4 4 81.76 78.19 8.50 o -2 4 4 59.16 73.85 6.77 o -1 4 4 617.34 592.04 18.17 o 0 4 4 1209.55 1349.71 24.64 o 1 4 4 1495.75 1540.89 31.67 o 2 4 4 19.37 13.86 9.09 o 3 4 4 56.22 40.42 9.99 o 4 4 4 503.30 559.43 28.29 o 5 4 4 835.06 811.13 35.25 o -9 5 4 690.68 692.78 31.10 o -8 5 4 887.94 836.60 46.44 o -7 5 4 137.01 117.93 12.93 o -6 5 4 0.95 8.85 8.59 o -5 5 4 1577.95 1542.29 25.36 o -4 5 4 2107.81 2086.07 27.58 o -3 5 4 135.83 151.79 9.13 o -2 5 4 1.34 1.93 6.94 o -1 5 4 446.24 424.00 15.98 o 0 5 4 843.38 738.47 22.58 o 1 5 4 795.80 816.17 22.86 o 2 5 4 61.53 51.52 10.90 o 3 5 4 146.58 162.46 15.87 o 4 5 4 566.92 618.58 30.54 o -9 6 4 410.96 443.97 27.52 o -8 6 4 997.22 1067.83 49.47 o -7 6 4 46.79 42.59 10.97 o -6 6 4 220.85 225.75 14.28 o -5 6 4 1478.81 1249.96 27.27 o -4 6 4 1767.58 1771.73 27.85 o -3 6 4 289.22 295.48 14.93 o -2 6 4 1.40 7.20 7.69 o -1 6 4 344.54 386.27 17.23 o 0 6 4 1279.84 1390.15 31.73 o 1 6 4 722.42 754.44 23.77 o 2 6 4 15.47 14.89 11.05 o 3 6 4 264.90 283.48 18.23 o -8 7 4 224.28 180.11 15.58 o -7 7 4 107.26 81.65 27.37 o -6 7 4 951.22 1155.88 28.99 o -5 7 4 1726.03 1746.39 51.53 o -4 7 4 2197.30 2146.68 41.29 o -3 7 4 463.81 525.76 20.57 o -2 7 4 4.86 16.37 9.51 o -1 7 4 1212.82 1118.92 29.46 o 0 7 4 1014.21 1018.91 27.88 o 1 7 4 457.81 424.60 21.19 o 2 7 4 0.03 3.88 10.38 o -7 8 4 4.55 13.56 15.81 o -6 8 4 234.82 228.72 16.80 o -5 8 4 271.53 334.59 24.00 o -4 8 4 306.81 335.23 17.66 o -3 8 4 27.37 15.40 10.80 o -2 8 4 2632.90 2603.02 49.00 o -1 8 4 1715.58 1710.13 38.91 o 0 8 4 1712.11 1650.58 79.35 o -5 9 4 555.64 633.83 25.63 o -4 9 4 571.67 610.65 32.54 o -3 9 4 167.74 152.22 16.18 o -2 9 4 467.52 405.81 36.42 o 0 -10 5 132.66 123.67 16.69 o 1 -10 5 461.22 433.72 22.51 o -3 -9 5 67.15 61.23 13.62 o -2 -9 5 42.83 34.87 12.35 o -1 -9 5 469.77 496.51 30.12 o 0 -9 5 867.11 826.35 31.54 o 1 -9 5 329.55 330.55 21.21 o 2 -9 5 23.85 27.56 12.14 o 3 -9 5 13.00 15.58 12.60 o 4 -9 5 487.80 456.34 34.76 o -4 -8 5 257.22 247.17 17.89 o -3 -8 5 27.73 17.86 11.98 o -2 -8 5 10.33 7.11 11.44 o -1 -8 5 973.38 982.83 40.03 o 0 -8 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212.85 275.43 10.88 o -3 -5 5 130.77 111.99 9.28 o -2 -5 5 1293.37 1326.65 27.96 o -1 -5 5 1465.50 1550.88 26.48 o 0 -5 5 663.33 587.61 22.20 o 1 -5 5 111.94 103.11 5.27 o 2 -5 5 1382.52 1294.48 20.47 o 3 -5 5 993.83 1051.36 20.02 o 4 -5 5 467.20 412.69 18.46 o 5 -5 5 276.47 322.20 17.45 o 6 -5 5 3.16 10.45 11.43 o -8 -4 5 169.34 119.53 14.16 o -7 -4 5 664.98 540.25 21.39 o -6 -4 5 722.84 653.23 20.34 o -5 -4 5 941.62 905.60 18.80 o -4 -4 5 2.29 4.40 5.59 o -3 -4 5 2073.19 2191.92 40.99 o -2 -4 5 1706.52 1707.24 25.33 o -1 -4 5 1030.12 1198.84 25.39 o 0 -4 5 1175.08 1288.91 17.86 o 1 -4 5 2318.40 2271.67 30.84 o 2 -4 5 1205.15 1217.72 20.34 o 3 -4 5 751.93 747.97 15.97 o 4 -4 5 888.78 809.72 22.49 o 5 -4 5 56.72 69.22 11.65 o 6 -4 5 11.59 18.86 11.46 o -8 -3 5 538.12 538.73 21.38 o -7 -3 5 1014.69 935.19 43.85 o -6 -3 5 900.67 886.89 23.54 o -5 -3 5 866.18 1019.29 31.99 o -4 -3 5 889.01 790.01 14.93 o -3 -3 5 1046.06 1071.89 18.64 o -2 -3 5 843.58 773.61 13.71 o -1 -3 5 174.61 186.83 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516.65 543.03 116.05 o -4 2 11 238.59 190.18 27.97 o -3 2 11 114.86 136.56 19.74 o -2 2 11 60.95 75.17 18.40 o -4 -3 12 284.57 288.37 33.63 o -3 -3 12 246.91 178.79 20.91 o -5 -2 12 426.56 510.01 43.56 o -4 -2 12 336.91 368.65 20.80 o -3 -2 12 79.48 104.21 15.41 o -2 -2 12 119.37 74.40 27.70 o -5 -1 12 564.79 560.44 51.49 o -4 -1 12 197.73 175.98 17.15 o -3 -1 12 32.73 18.02 13.24 o -4 0 12 1.41 6.60 14.11 o