#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:58:32 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181208 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/87/2228723.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2228723_Fobs loop_ _publ_author_name 'Nurco, Daniel J.' 'Conklin, Douglas E.' 'Shapiro, Nathan S.' 'Tran, Elaine' _publ_section_title ; The absolute structure of ptilosarcenone 2.5-hydrate, a diterpenoid briarane from the orange sea pen Ptilosarcus gurneyi (Gray) ; _journal_coeditor_code HB5711 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o181 _journal_page_last o182 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.8505 _cell_length_b 13.5256 _cell_length_c 39.3169 _exptl_crystal_F_000 2199.79 _reflns_d_resolution_high 0.7419 _cod_data_source_file hb5711Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 250XG2 P 21 21 21 R = 0.07' _shelx_refln_list_code 4 _shelx_f_calc_maximum 287.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4864.52 4514.20 22.35 o 4 0 0 6191.39 6305.94 29.99 o 6 0 0 12653.95 11855.37 50.37 o 8 0 0 589.09 632.97 21.44 o 10 0 0 82.09 120.95 15.19 o 12 0 0 306.73 298.62 29.19 o 1 1 0 19163.62 14553.32 88.88 o 2 1 0 5410.23 7892.65 54.81 o 3 1 0 4789.69 4886.46 35.38 o 4 1 0 5149.07 5172.18 35.80 o 5 1 0 2860.68 2618.45 18.07 o 6 1 0 741.58 772.89 9.97 o 7 1 0 2450.87 2396.69 17.73 o 8 1 0 1.34 31.73 7.57 o 9 1 0 91.49 121.33 9.90 o 10 1 0 146.58 133.99 10.83 o 11 1 0 86.64 92.23 12.75 o 12 1 0 39.13 52.73 14.84 o 13 1 0 125.38 108.32 17.94 o 0 2 0 1817.10 737.67 8.78 o 1 2 0 11624.62 10076.88 76.14 o 2 2 0 968.88 530.28 5.85 o 3 2 0 26167.36 27414.77 128.99 o 4 2 0 689.55 1426.85 14.55 o 5 2 0 9606.71 10453.95 44.18 o 6 2 0 52.74 109.38 8.39 o 7 2 0 538.28 599.22 11.52 o 8 2 0 3541.29 3678.25 31.59 o 9 2 0 2310.46 2033.82 33.57 o 10 2 0 436.05 450.59 15.51 o 11 2 0 458.06 400.51 22.27 o 12 2 0 4.80 11.08 14.05 o 13 2 0 526.68 691.48 29.22 o 1 3 0 31815.04 37011.02 226.66 o 2 3 0 1200.05 2145.93 12.49 o 3 3 0 3954.46 4594.37 25.10 o 4 3 0 8442.83 9059.92 57.44 o 5 3 0 14.29 50.81 4.08 o 6 3 0 58.94 64.02 4.77 o 7 3 0 5.35 14.23 4.56 o 8 3 0 15.92 21.14 6.02 o 9 3 0 438.21 428.93 14.18 o 10 3 0 0.35 5.61 9.42 o 11 3 0 77.77 90.98 12.62 o 12 3 0 1017.77 913.86 30.10 o 13 3 0 82.23 113.37 18.56 o 0 4 0 925.44 850.73 18.08 o 1 4 0 0.65 36.83 2.80 o 2 4 0 933.46 911.17 29.00 o 3 4 0 624.90 597.63 13.74 o 4 4 0 12450.10 12798.38 44.65 o 5 4 0 100.18 232.12 6.92 o 6 4 0 11.82 36.89 4.66 o 7 4 0 3356.17 3427.04 53.27 o 8 4 0 197.32 205.52 9.39 o 9 4 0 623.86 584.40 15.94 o 10 4 0 51.04 39.16 10.71 o 11 4 0 68.62 63.41 12.23 o 12 4 0 122.25 132.13 15.42 o 1 5 0 3748.39 3522.77 28.17 o 2 5 0 57.90 116.93 4.64 o 3 5 0 2412.64 2679.52 27.01 o 4 5 0 345.75 722.52 23.67 o 5 5 0 977.32 808.43 11.19 o 6 5 0 787.12 818.55 11.95 o 7 5 0 637.71 585.50 12.54 o 8 5 0 54.65 106.79 8.18 o 9 5 0 51.02 93.91 9.57 o 10 5 0 90.78 87.35 12.02 o 11 5 0 853.83 876.48 27.66 o 12 5 0 278.76 275.00 20.61 o 0 6 0 29048.20 28291.76 220.20 o 1 6 0 4508.65 4096.67 26.10 o 2 6 0 2466.77 2873.78 32.00 o 3 6 0 226.16 934.55 38.36 o 4 6 0 35.70 85.45 5.19 o 5 6 0 4547.06 4506.90 34.05 o 6 6 0 519.50 567.05 11.08 o 7 6 0 628.95 631.98 13.40 o 8 6 0 163.59 238.68 10.65 o 9 6 0 307.54 318.53 15.68 o 10 6 0 226.32 233.55 17.54 o 11 6 0 266.63 208.04 18.42 o 12 6 0 267.87 348.38 22.64 o 1 7 0 2360.90 2197.47 29.65 o 2 7 0 3350.96 3397.45 25.92 o 3 7 0 7920.79 7193.73 55.22 o 4 7 0 43.39 67.43 5.14 o 5 7 0 1853.37 1764.33 19.64 o 6 7 0 1143.11 1225.34 16.40 o 7 7 0 1021.32 883.01 17.53 o 8 7 0 543.85 587.96 16.66 o 9 7 0 68.18 66.67 13.02 o 10 7 0 312.76 306.79 19.74 o 11 7 0 52.98 53.34 14.75 o 12 7 0 0.03 43.84 15.50 o 0 8 0 4990.23 4279.74 41.50 o 1 8 0 1270.08 1328.56 25.17 o 2 8 0 1713.20 1991.84 30.26 o 3 8 0 2700.07 2297.02 24.43 o 4 8 0 380.13 454.52 9.80 o 5 8 0 869.73 844.68 13.09 o 6 8 0 14.05 26.90 6.63 o 7 8 0 681.20 625.83 16.18 o 8 8 0 2009.52 1860.80 34.70 o 9 8 0 112.76 203.00 14.32 o 10 8 0 395.54 353.77 21.04 o 11 8 0 201.07 232.32 20.58 o 1 9 0 54.42 225.52 16.10 o 2 9 0 330.72 364.06 8.54 o 3 9 0 53.57 116.28 7.38 o 4 9 0 533.76 657.01 13.59 o 5 9 0 2541.03 1958.72 21.79 o 6 9 0 151.71 198.39 10.19 o 7 9 0 322.46 287.76 12.89 o 8 9 0 238.85 257.42 14.65 o 9 9 0 234.78 277.83 16.13 o 10 9 0 254.09 269.53 19.85 o 11 9 0 494.99 459.84 24.96 o 0 10 0 791.92 750.49 33.59 o 1 10 0 2431.93 2447.16 21.93 o 2 10 0 24.16 19.26 5.70 o 3 10 0 1358.07 1335.26 18.11 o 4 10 0 31.59 103.37 8.15 o 5 10 0 244.17 191.17 10.20 o 6 10 0 902.80 762.12 16.43 o 7 10 0 1823.77 1408.64 23.53 o 8 10 0 185.98 191.33 14.47 o 9 10 0 171.29 147.29 14.29 o 10 10 0 62.38 98.82 18.24 o 11 10 0 124.75 130.09 19.04 o 1 11 0 485.02 528.07 12.58 o 2 11 0 764.32 760.39 14.80 o 3 11 0 93.49 75.43 7.75 o 4 11 0 0.74 287.48 33.13 o 5 11 0 146.56 518.75 16.21 o 6 11 0 877.93 842.18 17.75 o 7 11 0 36.45 59.77 11.36 o 8 11 0 242.11 348.13 17.57 o 9 11 0 2.50 21.24 12.16 o 10 11 0 62.07 78.31 16.86 o 0 12 0 89.72 81.80 13.07 o 1 12 0 17.63 30.90 7.93 o 2 12 0 162.64 205.29 10.24 o 3 12 0 2.59 285.22 12.59 o 4 12 0 1570.77 1537.27 22.50 o 5 12 0 21.94 67.91 9.26 o 6 12 0 215.39 207.58 12.12 o 7 12 0 295.40 431.31 18.89 o 8 12 0 77.85 60.96 13.14 o 9 12 0 673.15 905.44 29.87 o 1 13 0 156.94 392.53 14.95 o 2 13 0 466.88 413.85 14.82 o 3 13 0 499.40 418.70 13.80 o 4 13 0 5.80 388.51 39.43 o 5 13 0 8.65 11.21 8.52 o 6 13 0 582.56 444.49 19.00 o 7 13 0 66.48 38.62 13.47 o 8 13 0 731.29 788.68 28.05 o 9 13 0 327.18 268.92 21.35 o 0 14 0 2603.08 2672.70 44.68 o 1 14 0 19.42 44.61 10.55 o 2 14 0 809.16 571.14 19.27 o 3 14 0 239.61 196.96 17.64 o 4 14 0 218.98 283.71 16.09 o 5 14 0 37.75 77.90 10.88 o 6 14 0 127.81 390.31 25.15 o 7 14 0 188.56 284.13 18.27 o 8 14 0 72.28 73.71 17.05 o 1 15 0 60.22 70.38 13.54 o 2 15 0 1044.85 849.07 25.81 o 3 15 0 71.13 50.84 13.38 o 4 15 0 104.97 90.43 15.02 o 5 15 0 129.61 136.86 16.26 o 6 15 0 318.05 333.29 30.18 o 7 15 0 130.05 128.43 17.81 o 0 16 0 19.82 24.66 20.26 o 1 16 0 339.84 312.28 20.23 o 2 16 0 63.22 46.32 14.25 o 3 16 0 130.00 189.14 17.93 o 4 16 0 99.13 123.04 16.91 o 5 16 0 126.21 131.32 20.19 o 6 16 0 16.69 113.78 24.37 o 1 17 0 844.31 884.18 29.11 o 2 17 0 213.73 264.85 20.33 o 3 17 0 123.54 121.05 17.32 o 4 17 0 124.10 45.95 15.82 o 0 18 0 225.40 747.01 40.90 o 1 18 0 76.54 146.40 18.95 o 2 18 0 758.12 783.16 42.68 o 1 0 1 1547.97 2432.04 25.29 o 2 0 1 8303.62 10105.51 89.75 o 3 0 1 189.29 294.42 6.67 o 4 0 1 1735.40 2119.22 12.35 o 5 0 1 2509.53 2265.52 14.25 o 6 0 1 1607.99 1379.04 12.68 o 7 0 1 237.00 189.29 6.97 o 8 0 1 211.53 290.78 12.12 o 9 0 1 1359.86 1299.98 21.15 o 10 0 1 14.86 31.54 8.76 o 11 0 1 1345.03 1323.70 27.70 o 12 0 1 4.24 66.59 15.25 o 13 0 1 757.19 860.71 31.33 o -13 1 1 14.04 9.92 14.94 o -12 1 1 837.66 830.02 29.06 o -11 1 1 4.41 10.50 10.29 o -10 1 1 1372.85 1341.25 23.16 o -9 1 1 491.95 493.19 14.84 o -8 1 1 3548.81 3517.22 30.39 o -7 1 1 63.63 81.46 5.24 o -6 1 1 2337.16 2757.14 22.82 o -5 1 1 659.84 702.84 8.60 o -4 1 1 2777.90 3100.02 20.84 o -3 1 1 4763.93 5737.63 37.33 o -2 1 1 5208.85 5423.73 36.69 o -1 1 1 2921.66 3195.67 35.00 o 1 1 1 2890.74 3099.09 15.33 o 2 1 1 5257.78 5620.27 50.10 o 3 1 1 4750.23 5750.49 34.40 o 4 1 1 2756.60 3016.65 22.46 o 5 1 1 654.68 698.17 8.54 o 6 1 1 2285.90 2684.01 19.34 o 7 1 1 61.52 85.38 5.47 o 8 1 1 3560.74 3607.37 32.27 o 9 1 1 497.69 508.09 15.32 o 10 1 1 1368.16 1353.06 23.31 o 11 1 1 4.53 13.65 10.39 o 12 1 1 859.07 871.92 29.23 o 13 1 1 15.59 24.14 15.79 o -13 2 1 546.74 594.89 28.21 o -12 2 1 171.35 204.42 18.74 o -11 2 1 623.95 669.10 21.89 o -10 2 1 87.83 121.87 10.81 o -9 2 1 289.75 298.30 12.91 o -8 2 1 2879.67 2755.89 23.90 o -7 2 1 5994.50 6008.98 61.87 o -6 2 1 5911.74 5612.43 25.57 o -5 2 1 1885.11 2005.38 14.49 o -4 2 1 61.01 126.90 4.62 o -3 2 1 15337.67 16083.05 122.40 o -2 2 1 5886.57 7360.49 42.91 o -1 2 1 1495.95 1976.97 26.10 o 0 2 1 5799.16 5870.17 25.62 o 1 2 1 1502.08 2037.61 19.14 o 2 2 1 5882.36 7374.72 31.15 o 3 2 1 15321.74 16026.01 150.62 o 4 2 1 55.93 121.16 4.81 o 5 2 1 1940.60 2076.48 19.85 o 6 2 1 5978.59 5670.10 27.42 o 7 2 1 5986.54 5928.36 27.99 o 8 2 1 2855.17 2710.43 37.95 o 9 2 1 298.17 305.32 14.95 o 10 2 1 81.31 121.86 10.88 o 11 2 1 631.92 643.23 21.36 o 12 2 1 180.40 183.89 18.74 o 13 2 1 534.29 557.12 27.29 o -13 3 1 60.21 61.62 17.41 o -12 3 1 22.59 52.18 13.29 o -11 3 1 700.05 621.95 21.52 o -10 3 1 33.56 37.39 10.24 o -9 3 1 30.29 48.17 8.18 o -8 3 1 636.83 607.40 12.90 o -7 3 1 469.04 498.64 11.32 o -6 3 1 3071.74 3388.54 22.81 o -5 3 1 3334.64 3551.11 26.75 o -4 3 1 81.41 72.21 5.46 o -3 3 1 18050.75 18032.77 79.04 o -2 3 1 3610.45 3578.01 16.42 o -1 3 1 14806.05 14938.74 72.91 o 0 3 1 10277.73 10032.48 67.45 o 1 3 1 14583.94 15042.30 69.74 o 2 3 1 3627.09 3628.27 19.29 o 3 3 1 17969.91 17916.19 60.17 o 4 3 1 82.94 87.59 5.68 o 5 3 1 3441.64 3648.37 22.54 o 6 3 1 3028.34 3366.84 31.32 o 7 3 1 480.96 521.99 10.24 o 8 3 1 652.98 635.86 13.22 o 9 3 1 33.61 49.30 8.38 o 10 3 1 35.97 30.23 8.85 o 11 3 1 721.57 657.49 21.60 o 12 3 1 23.01 54.96 14.78 o 13 3 1 61.67 59.19 17.10 o -12 4 1 29.87 33.90 12.88 o -11 4 1 394.63 371.79 18.44 o -10 4 1 138.70 147.63 12.75 o -9 4 1 50.09 59.21 8.82 o -8 4 1 99.12 106.66 7.97 o -7 4 1 4691.07 4878.02 42.78 o -6 4 1 1284.72 1334.40 15.00 o -5 4 1 332.85 270.48 7.08 o -4 4 1 2639.17 2831.28 30.51 o -3 4 1 18747.24 20482.30 117.57 o -2 4 1 12733.58 13539.91 95.36 o -1 4 1 2543.08 2287.78 16.39 o 0 4 1 2631.77 1909.13 13.83 o 1 4 1 2455.87 2186.10 14.82 o 2 4 1 12762.48 13544.66 78.09 o 3 4 1 18769.49 20468.70 131.33 o 4 4 1 2712.49 2913.86 17.44 o 5 4 1 342.04 273.91 7.27 o 6 4 1 1300.60 1346.76 13.21 o 7 4 1 4745.97 4930.66 32.59 o 8 4 1 104.28 113.26 8.01 o 9 4 1 52.05 54.04 8.65 o 10 4 1 123.85 142.94 13.19 o 11 4 1 392.56 371.14 18.29 o 12 4 1 28.22 42.63 13.12 o -12 5 1 354.82 385.94 22.64 o -11 5 1 23.70 60.39 12.37 o -10 5 1 257.34 262.87 15.30 o -9 5 1 405.66 438.20 16.81 o -8 5 1 1336.31 1459.82 19.16 o -7 5 1 675.91 755.46 13.74 o -6 5 1 105.37 160.03 7.39 o -5 5 1 1754.24 1749.40 15.26 o -4 5 1 10006.16 10326.57 55.37 o -3 5 1 593.31 711.72 13.11 o -2 5 1 4982.35 5040.31 23.38 o -1 5 1 1683.44 1795.82 18.63 o 0 5 1 618.34 632.27 12.50 o 1 5 1 1653.11 1736.77 17.08 o 2 5 1 5105.09 5158.59 29.57 o 3 5 1 569.96 693.99 12.23 o 4 5 1 10016.91 10446.39 73.76 o 5 5 1 1776.69 1796.41 18.52 o 6 5 1 103.65 157.24 6.55 o 7 5 1 656.81 728.77 12.29 o 8 5 1 1386.86 1546.67 19.72 o 9 5 1 397.18 435.23 14.80 o 10 5 1 252.54 256.22 15.31 o 11 5 1 24.95 57.33 13.46 o 12 5 1 355.54 375.47 22.94 o -12 6 1 213.79 241.56 20.50 o -11 6 1 121.83 135.69 16.51 o -10 6 1 813.62 808.05 26.06 o -9 6 1 447.22 466.04 17.41 o -8 6 1 339.48 332.46 11.67 o -7 6 1 645.41 633.92 14.69 o -6 6 1 378.50 393.35 10.67 o -5 6 1 84.00 205.92 13.31 o -4 6 1 1116.07 1008.73 11.81 o -3 6 1 9866.30 10093.24 66.97 o -2 6 1 6647.04 6558.15 41.69 o -1 6 1 132.17 222.14 7.51 o 0 6 1 1964.05 1975.72 39.52 o 1 6 1 133.53 221.99 9.86 o 2 6 1 6681.79 6596.33 76.18 o 3 6 1 9906.11 10069.48 66.67 o 4 6 1 1075.48 943.73 11.76 o 5 6 1 84.81 209.02 13.17 o 6 6 1 382.77 394.20 8.67 o 7 6 1 638.50 601.63 11.72 o 8 6 1 359.33 353.68 11.79 o 9 6 1 446.44 493.17 15.59 o 10 6 1 830.81 742.53 24.97 o 11 6 1 115.99 123.81 15.99 o 12 6 1 220.96 253.79 20.44 o -12 7 1 330.10 325.97 22.89 o -11 7 1 12.05 19.93 14.18 o -10 7 1 193.45 227.23 18.06 o -9 7 1 271.48 290.88 18.53 o -8 7 1 158.63 256.70 12.24 o -7 7 1 590.86 663.09 15.59 o -6 7 1 927.47 1029.51 15.79 o -5 7 1 2558.19 2479.69 19.59 o -4 7 1 501.41 475.75 9.37 o -3 7 1 1227.49 1575.94 24.53 o -2 7 1 4008.89 3663.97 32.11 o -1 7 1 11037.79 10520.24 35.13 o 0 7 1 1805.01 1683.17 20.69 o 1 7 1 11095.83 10708.19 82.70 o 2 7 1 4058.35 3650.63 30.66 o 3 7 1 1215.39 1584.06 17.48 o 4 7 1 480.53 440.78 9.19 o 5 7 1 2552.29 2475.19 19.86 o 6 7 1 909.85 1035.60 14.58 o 7 7 1 586.61 656.25 14.33 o 8 7 1 161.12 249.90 12.23 o 9 7 1 259.59 262.33 14.84 o 10 7 1 188.81 223.25 17.80 o 11 7 1 10.43 9.91 13.42 o 12 7 1 319.34 294.02 22.22 o -11 8 1 121.22 120.66 17.29 o -10 8 1 1.07 24.08 12.90 o -9 8 1 798.98 735.72 24.98 o -8 8 1 122.35 178.44 12.85 o -7 8 1 265.87 288.42 12.83 o -6 8 1 934.85 933.52 16.05 o -5 8 1 265.46 271.87 10.26 o -4 8 1 236.28 335.71 9.17 o -3 8 1 44.43 104.01 5.84 o -2 8 1 3329.59 3118.42 36.38 o -1 8 1 2169.16 2092.83 16.95 o 0 8 1 3084.38 2975.25 51.20 o 1 8 1 2162.62 2057.20 30.57 o 2 8 1 3348.80 3147.77 21.37 o 3 8 1 39.49 96.19 5.63 o 4 8 1 240.15 348.61 9.26 o 5 8 1 270.37 282.03 9.58 o 6 8 1 874.81 849.47 15.51 o 7 8 1 253.46 283.79 14.22 o 8 8 1 114.70 169.51 11.17 o 9 8 1 791.01 754.09 21.31 o 10 8 1 0.83 27.98 13.53 o 11 8 1 126.59 120.26 17.08 o -11 9 1 36.19 57.61 16.26 o -10 9 1 512.74 479.65 23.57 o -9 9 1 557.59 484.44 19.08 o -8 9 1 422.88 369.17 16.65 o -7 9 1 420.66 430.07 14.91 o -6 9 1 415.06 382.07 12.51 o -5 9 1 209.82 298.07 11.27 o -4 9 1 1215.26 1111.52 16.52 o -3 9 1 1159.04 1184.53 16.02 o -2 9 1 885.80 810.74 11.12 o -1 9 1 2901.20 2510.99 18.50 o 0 9 1 6.83 43.21 4.81 o 1 9 1 2933.44 2571.47 18.96 o 2 9 1 890.60 845.10 12.62 o 3 9 1 1130.46 1179.88 14.05 o 4 9 1 1208.76 1118.78 17.19 o 5 9 1 217.33 307.07 11.51 o 6 9 1 412.32 390.51 12.62 o 7 9 1 430.16 427.19 14.86 o 8 9 1 415.78 368.90 16.53 o 9 9 1 559.53 501.99 19.59 o 10 9 1 510.52 484.82 23.95 o 11 9 1 33.49 59.85 15.82 o -11 10 1 11.42 49.67 16.32 o -10 10 1 528.73 471.82 24.13 o -9 10 1 220.34 198.67 15.26 o -8 10 1 100.89 91.20 12.24 o -7 10 1 599.16 712.06 20.50 o -6 10 1 97.17 316.44 12.59 o -5 10 1 246.12 199.77 10.07 o -4 10 1 1527.32 1358.17 18.78 o -3 10 1 1181.03 1192.79 21.85 o -2 10 1 502.31 500.62 12.08 o -1 10 1 570.27 628.07 11.62 o 0 10 1 1294.23 1117.69 27.22 o 1 10 1 574.72 657.19 16.68 o 2 10 1 472.39 445.74 11.35 o 3 10 1 1163.56 1183.19 18.91 o 4 10 1 1597.74 1434.50 20.09 o 5 10 1 241.21 189.31 10.20 o 6 10 1 98.82 306.46 12.54 o 7 10 1 594.87 714.67 18.36 o 8 10 1 106.71 103.98 12.68 o 9 10 1 222.65 183.21 15.22 o 10 10 1 533.22 500.28 24.60 o 11 10 1 13.09 56.15 17.14 o -10 11 1 313.45 297.51 22.09 o -9 11 1 252.50 316.42 18.04 o -8 11 1 492.61 438.00 19.09 o -7 11 1 227.09 256.36 15.43 o -6 11 1 6.55 123.22 10.06 o -5 11 1 2335.32 2131.54 24.81 o -4 11 1 3418.49 2935.37 34.37 o -3 11 1 226.54 242.52 10.18 o -2 11 1 876.99 827.34 17.26 o -1 11 1 270.33 257.23 10.39 o 0 11 1 1059.87 1032.48 22.78 o 1 11 1 284.32 252.92 10.24 o 2 11 1 882.30 832.26 15.13 o 3 11 1 235.99 239.87 10.68 o 4 11 1 3421.42 3081.79 38.53 o 5 11 1 2379.31 2189.10 25.10 o 6 11 1 8.05 115.59 9.89 o 7 11 1 225.00 257.77 13.95 o 8 11 1 491.58 460.33 19.20 o 9 11 1 252.98 293.39 17.70 o 10 11 1 314.32 327.89 22.71 o -9 12 1 1120.36 1037.71 30.86 o -8 12 1 190.05 224.03 18.10 o -7 12 1 1232.03 1188.91 26.58 o -6 12 1 83.47 126.49 10.64 o -5 12 1 319.53 356.23 13.76 o -4 12 1 2658.69 2553.53 27.26 o -3 12 1 1131.00 1033.56 25.86 o -2 12 1 172.01 175.63 9.77 o -1 12 1 316.19 296.99 12.75 o 0 12 1 104.82 113.00 9.78 o 1 12 1 292.81 294.63 12.82 o 2 12 1 179.42 179.45 9.76 o 3 12 1 1124.85 1026.79 17.92 o 4 12 1 2641.83 2472.67 28.55 o 5 12 1 328.86 375.09 13.86 o 6 12 1 84.00 143.96 11.05 o 7 12 1 1242.46 1231.60 27.17 o 8 12 1 193.67 236.55 16.72 o 9 12 1 1120.23 1034.05 27.50 o -9 13 1 102.08 111.14 18.00 o -8 13 1 22.91 188.01 18.01 o -7 13 1 31.25 57.29 14.42 o -6 13 1 39.19 107.28 14.80 o -5 13 1 369.95 363.17 14.47 o -4 13 1 2254.71 1857.58 33.11 o -3 13 1 98.42 124.24 9.71 o -2 13 1 327.54 373.58 14.57 o -1 13 1 1653.61 1644.73 34.31 o 0 13 1 49.82 53.91 9.23 o 1 13 1 1669.51 1712.99 25.00 o 2 13 1 325.88 345.32 14.21 o 3 13 1 99.93 134.35 10.94 o 4 13 1 2238.53 1938.94 25.10 o 5 13 1 364.67 362.07 14.18 o 6 13 1 41.11 87.18 10.46 o 7 13 1 32.79 45.05 13.77 o 8 13 1 26.79 229.89 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