#------------------------------------------------------------------------------ #$Date: 2011-02-15 17:23:33 +0200 (Tue, 15 Feb 2011) $ #$Revision: 11387 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2228724.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2228724_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Hemamalini, Madhukar' Nithinchandra 'Kalluraya, Balakrishna' _publ_section_title ; 4-[(3-Benzamidomethyl-6-phenyl-6,7-dihydro-5H-1,2,4-triazolo[3,4-b][1,3,4]thiadiazin-7-yl)carbonyl]-3-phenyl-1,2,3-oxadiazol-3-ium-5-olate 0.06-hydrate ; _journal_coeditor_code HB5742 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o128 _journal_page_last o129 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 111.235 _cell_angle_beta 93.970 _cell_angle_gamma 101.636 _cell_length_a 15.6242 _cell_length_b 18.7430 _cell_length_c 18.9689 _exptl_crystal_F_000 2245.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file hb5742Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bk53m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 417.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1967.95 2055.48 60.12 o 3 0 0 1106.51 818.92 27.26 o 4 0 0 11720.29 12630.55 280.16 o 5 0 0 2097.41 2183.49 53.63 o 6 0 0 17199.74 17673.04 341.01 o 7 0 0 629.79 762.26 28.80 o 8 0 0 320.98 302.46 25.82 o 9 0 0 1439.73 1542.86 47.18 o 10 0 0 21.53 5.68 11.53 o 11 0 0 18.80 27.23 13.74 o 12 0 0 1470.76 1539.29 67.77 o 13 0 0 199.51 243.82 28.75 o 14 0 0 50.22 41.17 27.09 o 15 0 0 338.29 305.16 51.74 o 16 0 0 202.36 218.15 50.33 o 17 0 0 57.15 75.64 42.26 o -18 1 0 725.93 878.72 89.66 o -17 1 0 410.02 295.41 56.90 o -16 1 0 15.81 -25.79 29.04 o -15 1 0 407.90 502.35 61.97 o -14 1 0 820.03 896.61 191.83 o -13 1 0 31.11 30.01 18.09 o -12 1 0 741.47 899.94 42.71 o -11 1 0 2477.69 2319.53 63.38 o -10 1 0 2926.21 3138.84 75.60 o -9 1 0 3.46 -5.43 9.99 o -8 1 0 1519.36 1626.20 53.21 o -7 1 0 18.35 7.81 9.46 o -6 1 0 12.40 7.72 8.44 o -5 1 0 48.87 21.60 11.59 o -4 1 0 10102.84 9196.40 183.81 o -3 1 0 9390.02 9200.16 181.01 o -2 1 0 3493.75 3967.76 81.20 o 1 1 0 710.41 943.40 38.87 o 2 1 0 282.96 186.94 12.81 o 3 1 0 861.39 847.82 31.92 o 4 1 0 20.19 13.99 7.81 o 5 1 0 280.90 213.50 20.16 o 6 1 0 546.96 650.63 30.03 o 7 1 0 9488.63 9294.15 390.31 o 8 1 0 1561.50 1774.78 51.18 o 9 1 0 866.22 1001.24 36.78 o 10 1 0 395.42 363.74 34.14 o 11 1 0 610.12 633.49 50.63 o 12 1 0 443.81 476.30 34.89 o 13 1 0 763.86 841.37 59.95 o 14 1 0 1777.24 1856.96 94.68 o 15 1 0 1017.57 1213.76 77.98 o 16 1 0 1.27 -21.81 45.29 o 17 1 0 479.01 360.24 87.62 o -18 2 0 12.78 19.49 36.27 o -17 2 0 909.62 943.81 89.28 o -16 2 0 153.40 169.34 45.30 o -15 2 0 813.48 937.82 79.72 o -14 2 0 86.06 66.25 22.34 o -13 2 0 1828.93 1854.04 66.58 o -12 2 0 1550.48 1671.93 51.82 o -11 2 0 816.93 740.87 40.79 o -10 2 0 864.93 934.85 41.54 o -9 2 0 807.52 981.96 36.52 o -8 2 0 11348.52 11945.92 245.54 o -7 2 0 170.58 163.23 15.87 o -6 2 0 13426.07 13800.11 273.28 o -5 2 0 3311.42 3042.04 64.68 o -4 2 0 22361.77 21492.77 369.11 o -3 2 0 23984.17 24893.64 474.58 o -2 2 0 986.22 911.37 38.79 o 1 2 0 12049.98 12245.46 490.46 o 2 2 0 241.78 210.23 23.24 o 3 2 0 927.79 771.27 32.62 o 4 2 0 207.21 241.10 24.41 o 5 2 0 43.95 10.25 7.65 o 6 2 0 1050.47 1119.89 31.03 o 7 2 0 5872.09 6432.60 163.52 o 8 2 0 20.07 -2.85 10.32 o 9 2 0 1645.36 1601.34 48.84 o 10 2 0 1327.42 1252.57 68.79 o 11 2 0 262.17 159.47 26.91 o 12 2 0 2210.52 1981.10 80.75 o 13 2 0 3102.37 3188.76 140.75 o 14 2 0 2741.17 2751.46 133.65 o 15 2 0 6.93 13.55 41.85 o 16 2 0 0.25 0.77 43.06 o 17 2 0 219.75 141.89 66.44 o -18 3 0 0.22 7.07 64.62 o -17 3 0 226.17 172.52 49.01 o -16 3 0 864.51 1176.16 93.95 o -15 3 0 106.96 127.70 31.01 o -14 3 0 211.80 195.61 29.48 o -13 3 0 60.05 19.89 18.38 o -12 3 0 970.88 884.21 44.70 o -11 3 0 564.16 436.96 27.90 o -10 3 0 19.52 2.92 11.79 o -9 3 0 509.61 551.62 28.27 o -8 3 0 3389.82 3369.51 70.58 o -7 3 0 6851.33 7454.49 185.53 o -6 3 0 13.35 -14.02 9.08 o -5 3 0 2683.67 2343.79 54.15 o -4 3 0 62.48 33.73 10.13 o -3 3 0 12118.00 12492.87 364.74 o -2 3 0 373.01 333.13 37.66 o -1 3 0 3704.28 3084.28 102.35 o 0 3 0 0.25 6.74 12.95 o 1 3 0 644.99 787.09 52.55 o 2 3 0 1920.87 2242.94 57.46 o 3 3 0 17415.93 16593.30 456.11 o 4 3 0 6020.30 5602.26 164.26 o 5 3 0 3153.68 3091.71 70.13 o 6 3 0 2773.90 2630.93 56.18 o 7 3 0 9.09 20.84 11.90 o 8 3 0 4192.46 4317.93 102.00 o 9 3 0 629.78 650.00 29.45 o 10 3 0 4.29 25.60 29.58 o 11 3 0 17.61 28.23 22.81 o 12 3 0 98.43 95.09 54.06 o 13 3 0 2916.80 2972.19 138.50 o 14 3 0 713.42 624.48 81.97 o 15 3 0 593.94 437.09 119.83 o 16 3 0 464.19 612.06 76.74 o 17 3 0 16.53 -91.36 46.52 o -18 4 0 9.30 0.66 43.28 o -17 4 0 158.40 202.10 92.69 o -16 4 0 205.72 100.48 40.23 o -15 4 0 524.25 574.37 46.00 o -14 4 0 1390.05 1329.71 60.46 o -13 4 0 563.31 651.77 41.16 o -12 4 0 1383.15 1310.22 52.99 o -11 4 0 1749.11 1768.21 56.42 o -10 4 0 596.99 619.46 31.83 o -9 4 0 139.38 98.41 16.62 o -8 4 0 426.58 575.59 30.21 o -7 4 0 59.28 41.49 12.51 o -5 4 0 3077.31 3480.10 123.83 o -4 4 0 5848.24 5750.73 184.70 o -3 4 0 48398.13 47217.69 1863.26 o -2 4 0 42165.82 39092.48 1051.69 o -1 4 0 1.12 -23.84 31.48 o 0 4 0 117107.66 106064.14 3221.61 o 1 4 0 15120.48 15633.42 448.95 o 2 4 0 425.51 465.37 19.35 o 3 4 0 2330.08 2297.09 120.08 o 4 4 0 1466.32 1294.61 51.26 o 5 4 0 3.49 -7.83 9.37 o 6 4 0 2848.80 3159.36 74.44 o 7 4 0 51.33 42.65 11.52 o 8 4 0 617.91 693.51 32.27 o 9 4 0 616.21 670.21 33.45 o 10 4 0 18.54 9.12 22.60 o 11 4 0 2755.67 2822.26 196.25 o 12 4 0 411.41 532.25 62.30 o 13 4 0 724.30 813.98 76.48 o 14 4 0 105.50 60.93 57.32 o 15 4 0 291.06 418.49 64.62 o 16 4 0 152.63 176.74 50.57 o -18 5 0 12.09 -51.77 35.24 o -17 5 0 1.24 -51.51 39.82 o -16 5 0 31.11 72.71 32.76 o -15 5 0 580.09 531.08 41.25 o -14 5 0 698.19 763.20 46.80 o -13 5 0 1624.71 1825.63 63.87 o -12 5 0 821.00 811.36 44.21 o -11 5 0 998.02 1018.31 47.72 o -10 5 0 284.28 387.28 28.59 o -9 5 0 2.13 8.90 12.28 o -8 5 0 2762.35 2574.74 65.32 o -7 5 0 1572.15 1518.17 44.87 o -6 5 0 903.45 1025.91 47.96 o -4 5 0 1175.60 1351.88 88.37 o -3 5 0 12335.83 11481.51 323.01 o -2 5 0 7502.89 7253.08 226.17 o -1 5 0 404.09 432.46 37.22 o 0 5 0 389.62 448.91 36.82 o 1 5 0 3299.27 3085.40 106.67 o 2 5 0 8147.55 7988.14 164.58 o 3 5 0 2282.19 2500.62 59.20 o 4 5 0 30.65 19.93 27.43 o 5 5 0 166.37 154.27 21.11 o 6 5 0 91.24 133.59 16.89 o 7 5 0 492.02 532.19 27.44 o 8 5 0 204.22 228.17 21.15 o 9 5 0 194.82 182.52 22.37 o 10 5 0 64.77 24.03 36.03 o 11 5 0 1762.23 1666.12 132.87 o 12 5 0 2919.84 2637.72 126.88 o 13 5 0 634.01 777.58 77.40 o 14 5 0 96.40 122.66 47.70 o 15 5 0 148.41 126.37 48.59 o 16 5 0 0.93 -14.16 38.82 o -18 6 0 54.44 53.94 56.41 o -17 6 0 2.09 -0.34 30.57 o -16 6 0 504.16 456.10 53.56 o -15 6 0 5.38 16.18 25.73 o -14 6 0 653.30 697.28 54.38 o -13 6 0 286.91 310.63 36.40 o -12 6 0 1312.51 1448.21 68.59 o -11 6 0 187.70 223.90 29.21 o -10 6 0 2941.58 3108.05 93.09 o -9 6 0 610.49 598.51 40.41 o -8 6 0 4287.92 4242.61 110.80 o -7 6 0 2626.83 2836.16 81.10 o -6 6 0 356.49 386.78 34.28 o -5 6 0 7783.23 8072.08 259.87 o -4 6 0 17072.00 17035.30 476.62 o -3 6 0 1587.01 1574.84 59.92 o -2 6 0 36170.46 35758.19 1019.14 o -1 6 0 20477.94 20448.52 594.17 o 0 6 0 1958.24 2251.84 124.95 o 1 6 0 1632.30 1441.77 64.40 o 2 6 0 6.46 -3.38 7.14 o 3 6 0 78.60 114.54 12.81 o 4 6 0 24.85 24.59 15.73 o 5 6 0 2412.18 2496.55 86.70 o 6 6 0 6328.10 6294.72 200.27 o 7 6 0 4655.74 4546.34 129.11 o 8 6 0 609.25 615.71 36.83 o 9 6 0 47.74 23.83 26.40 o 10 6 0 457.98 431.92 54.21 o 11 6 0 79.20 56.41 36.01 o 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1467.94 104.80 o 13 7 0 1259.28 1118.17 92.87 o 14 7 0 1107.20 1218.44 168.45 o 15 7 0 148.94 125.69 111.31 o -18 8 0 399.61 359.59 56.39 o -17 8 0 218.82 238.13 47.50 o -16 8 0 214.99 265.19 53.46 o -15 8 0 264.07 292.81 59.14 o -14 8 0 179.63 128.78 34.08 o -13 8 0 255.97 267.60 36.05 o -12 8 0 3.95 23.31 20.66 o -11 8 0 437.55 457.38 40.98 o -10 8 0 4062.33 3884.40 112.47 o -9 8 0 115.39 98.88 26.27 o -8 8 0 282.74 301.63 30.36 o -7 8 0 564.47 519.59 36.18 o -6 8 0 959.27 1106.35 92.00 o -5 8 0 3061.18 1823.53 119.78 o -4 8 0 5524.82 5847.82 145.03 o -3 8 0 17.87 45.79 24.22 o -2 8 0 119.37 166.04 29.88 o -1 8 0 702.96 387.95 123.10 o 0 8 0 1747.21 24.14 24.31 o 1 8 0 94.62 158.98 27.65 o 2 8 0 37.85 51.34 8.98 o 3 8 0 158.76 184.71 14.72 o 4 8 0 4.10 3.35 9.14 o 5 8 0 6235.03 5672.36 145.51 o 6 8 0 2405.20 2410.60 148.92 o 7 8 0 7.16 47.95 38.40 o 8 8 0 212.82 108.90 33.13 o 9 8 0 3695.39 3640.26 216.07 o 10 8 0 4303.28 3867.44 157.67 o 11 8 0 219.36 250.92 127.81 o 12 8 0 390.36 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125.16 37.21 o -16 10 0 286.06 343.10 68.79 o -15 10 0 12.06 49.17 29.21 o -14 10 0 628.07 668.64 56.84 o -13 10 0 387.81 496.09 48.28 o -12 10 0 362.26 390.66 42.32 o -11 10 0 297.58 321.91 37.84 o -10 10 0 446.94 485.25 47.93 o -9 10 0 972.72 1018.95 57.50 o -8 10 0 226.93 173.11 39.15 o -7 10 0 139.40 115.74 47.37 o -6 10 0 65.91 54.17 14.60 o -5 10 0 56.92 56.79 15.10 o -4 10 0 2346.33 2290.02 60.72 o -3 10 0 3346.79 3757.30 150.25 o -2 10 0 6255.11 6208.68 217.82 o -1 10 0 649.73 646.02 58.21 o 0 10 0 1264.91 1250.00 105.96 o 1 10 0 4928.25 5096.90 181.87 o 2 10 0 852.40 799.80 29.23 o 3 10 0 769.63 764.46 29.87 o 4 10 0 130.05 119.91 21.23 o 5 10 0 1227.47 1295.16 66.56 o 6 10 0 966.39 841.06 61.11 o 7 10 0 561.99 581.50 68.68 o 8 10 0 444.36 419.45 51.41 o 9 10 0 0.95 -2.71 36.00 o 10 10 0 0.88 -60.05 30.03 o 11 10 0 23.13 -4.81 35.51 o 12 10 0 899.31 690.55 127.07 o 13 10 0 1.41 -76.90 38.45 o -17 11 0 252.86 340.88 49.41 o -16 11 0 14.11 -18.03 27.62 o -15 11 0 3.73 15.21 28.39 o -14 11 0 519.19 493.78 51.98 o -13 11 0 846.79 959.29 65.22 o -12 11 0 433.46 454.31 46.36 o -11 11 0 27.53 35.41 24.40 o -10 11 0 148.99 133.54 29.53 o -9 11 0 3229.83 3384.54 150.26 o -8 11 0 220.82 302.48 66.03 o -7 11 0 488.37 547.09 52.22 o -6 11 0 3476.32 3348.77 94.49 o -5 11 0 1754.85 1807.75 55.62 o -4 11 0 22.57 27.62 14.32 o -3 11 0 7905.19 8173.67 279.52 o -2 11 0 1560.39 1598.15 88.66 o -1 11 0 346.45 456.38 51.35 o 0 11 0 2015.81 1878.80 179.62 o 1 11 0 698.34 764.22 105.82 o 2 11 0 61.20 56.66 11.37 o 3 11 0 359.42 394.03 37.44 o 4 11 0 17.42 5.79 15.69 o 5 11 0 31.51 38.33 21.70 o 6 11 0 1008.51 908.03 64.70 o 7 11 0 899.58 845.43 66.49 o 8 11 0 877.74 798.44 67.93 o 9 11 0 176.70 162.83 77.27 o 10 11 0 383.68 471.90 97.08 o 11 11 0 1.19 29.99 40.29 o 12 11 0 131.86 60.62 45.88 o -17 12 0 66.44 63.13 37.10 o -16 12 0 4.92 58.57 34.31 o -15 12 0 126.54 99.73 33.92 o -14 12 0 1026.80 966.77 69.51 o -13 12 0 738.45 714.18 58.59 o -12 12 0 14.39 -10.02 23.41 o -11 12 0 109.90 165.96 32.58 o -10 12 0 3488.35 3517.87 111.79 o -9 12 0 10.71 3.97 18.53 o -8 12 0 1013.77 646.19 261.90 o -7 12 0 427.75 551.07 46.23 o -6 12 0 91.72 83.52 16.83 o -5 12 0 3944.70 4085.41 127.53 o -4 12 0 5936.92 5504.90 150.95 o -3 12 0 123.90 62.13 31.92 o -2 12 0 406.94 502.57 57.77 o -1 12 0 87.73 197.12 39.55 o 0 12 0 383.56 334.22 47.03 o 1 12 0 109.99 75.16 32.77 o 2 12 0 148.12 191.29 16.10 o 3 12 0 769.83 902.89 34.96 o 4 12 0 407.21 490.20 47.79 o 5 12 0 101.01 24.42 22.80 o 6 12 0 11.34 27.15 25.76 o 7 12 0 65.88 53.06 29.42 o 8 12 0 116.60 156.36 39.82 o 9 12 0 59.84 107.90 40.86 o 10 12 0 275.38 244.41 51.68 o 11 12 0 850.64 867.46 85.87 o 12 12 0 323.55 195.75 56.17 o -16 13 0 59.93 24.14 33.01 o -15 13 0 788.71 918.69 71.12 o -14 13 0 6.75 -24.42 25.27 o -13 13 0 334.90 360.02 45.48 o -12 13 0 20.56 34.93 24.80 o -11 13 0 486.26 530.35 48.55 o -10 13 0 411.42 426.21 53.19 o -9 13 0 7.92 4.31 27.86 o -8 13 0 2549.77 2659.96 143.95 o -7 13 0 91.00 113.44 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