#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:59:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181209 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/88/2228854.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2228854_Fobs loop_ _publ_author_name 'Bon, Vladimir V.' 'Orysyk, Svitlana I.' 'Pekhnyo, Vasily I.' _publ_section_title ; Poly[[\m~2~-(1Z,N'E)-2-(1,3-benzothiazol-2-ylsulfanyl)-N'-(2-oxidobenzylidene-\k^2^O:O)acetohydrazidato-\k^2^O,N'](pyridine-\kN)copper(II)] ; _journal_coeditor_code RK2250 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m11 _journal_volume 67 _journal_year 2011 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 21.6256 _cell_length_b 25.3751 _cell_length_c 7.1230 _exptl_crystal_F_000 1976.00 _reflns_d_resolution_high 0.7990 _cod_data_source_file rk2250Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 100 in Pccn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 618.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' 'x+1/2, -y, -z+1/2' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' '-x-1/2, y, z-1/2' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 76238.73 82793.53 2079.31 o 4 0 0 24308.67 25668.66 449.16 o 6 0 0 45361.86 47274.04 808.02 o 8 0 0 46878.10 44870.40 959.86 o 10 0 0 79865.38 78652.45 4325.24 o 12 0 0 27042.12 26838.50 504.54 o 14 0 0 78062.09 78249.69 2581.77 o 16 0 0 4763.67 5019.91 231.72 o 18 0 0 17841.67 18325.38 683.58 o 20 0 0 37431.76 38801.92 1289.92 o 22 0 0 9585.37 9102.83 463.44 o 24 0 0 3307.12 3742.32 347.58 o 26 0 0 6705.45 5951.40 413.24 o 3 1 0 69773.30 71337.20 923.24 o 5 1 0 84.74 124.10 22.30 o 7 1 0 21257.59 21197.15 295.91 o 9 1 0 1420.98 1595.39 54.46 o 11 1 0 3000.03 2468.95 145.49 o 13 1 0 746.64 770.80 52.89 o 15 1 0 26.47 4.63 30.03 o 17 1 0 8613.67 8663.64 218.95 o 19 1 0 658.29 656.13 148.69 o 21 1 0 2889.74 2670.15 185.64 o 23 1 0 1924.23 2014.16 178.86 o 25 1 0 2662.76 3088.11 316.69 o 27 1 0 6.70 -100.52 220.14 o 2 2 0 111054.61 114023.91 2308.38 o 4 2 0 38924.95 40787.65 537.29 o 6 2 0 30644.97 30755.52 414.48 o 8 2 0 82781.15 85223.11 1013.54 o 10 2 0 40133.34 42092.87 521.93 o 12 2 0 28779.19 26374.49 713.51 o 14 2 0 12343.22 12769.31 242.99 o 16 2 0 42186.95 41035.69 769.80 o 18 2 0 9613.05 10645.68 569.65 o 20 2 0 6107.53 6630.33 260.79 o 22 2 0 11642.67 11944.59 865.10 o 24 2 0 2020.42 1919.62 187.31 o 26 2 0 7393.46 7199.53 323.39 o 1 3 0 69524.28 74587.59 2093.23 o 3 3 0 752.07 855.11 44.07 o 5 3 0 37171.46 37260.33 552.68 o 7 3 0 96.40 117.36 21.18 o 9 3 0 108315.87 111521.88 1320.88 o 11 3 0 26359.81 27907.46 361.94 o 13 3 0 433.65 706.51 41.06 o 15 3 0 5057.97 4874.61 113.95 o 17 3 0 14095.32 14035.15 402.47 o 19 3 0 5363.49 5507.89 225.28 o 21 3 0 15.51 -73.38 73.38 o 23 3 0 13237.96 13069.66 421.91 o 25 3 0 1930.15 1923.79 191.16 o 2 4 0 4679.84 5016.64 126.96 o 4 4 0 32160.96 31895.28 554.62 o 6 4 0 2037.19 2434.56 82.79 o 8 4 0 10600.49 10487.89 155.16 o 10 4 0 98517.85 102837.52 1225.96 o 12 4 0 3555.31 3666.42 100.46 o 14 4 0 1541.85 1400.77 62.29 o 16 4 0 5277.15 4990.26 138.84 o 18 4 0 7353.96 7422.36 291.54 o 20 4 0 31.14 -45.69 64.13 o 22 4 0 3368.36 3355.73 215.69 o 24 4 0 6781.69 6571.18 292.05 o 26 4 0 464.22 706.75 200.83 o 1 5 0 39181.19 40003.46 675.41 o 3 5 0 2051.19 2057.13 100.73 o 5 5 0 5407.17 4849.34 102.38 o 7 5 0 33056.48 32128.72 440.88 o 9 5 0 25976.04 26126.88 337.90 o 11 5 0 25455.75 25336.05 334.59 o 13 5 0 32913.38 32718.44 426.72 o 15 5 0 13212.13 12791.36 253.12 o 17 5 0 575.28 551.18 62.99 o 19 5 0 52.97 57.40 47.30 o 21 5 0 13093.01 12019.20 385.05 o 23 5 0 4461.61 4588.41 232.08 o 25 5 0 2560.26 2815.43 312.83 o 0 6 0 1986.55 2143.43 115.86 o 2 6 0 1134.90 1188.02 53.15 o 4 6 0 1284.68 1151.81 54.05 o 6 6 0 55.48 21.26 25.52 o 8 6 0 148.77 217.60 34.07 o 10 6 0 288.80 185.70 27.75 o 12 6 0 470.76 489.47 36.92 o 14 6 0 10.36 -31.42 31.42 o 16 6 0 74.72 29.97 40.21 o 18 6 0 738.29 858.72 74.53 o 20 6 0 1587.90 1768.40 129.40 o 22 6 0 1176.90 1390.33 208.55 o 24 6 0 24.77 112.00 131.31 o 26 6 0 232.49 154.48 146.76 o 1 7 0 35812.86 35822.38 616.62 o 3 7 0 2305.72 2202.93 74.02 o 5 7 0 7546.57 7194.20 141.47 o 7 7 0 32760.46 32518.04 507.62 o 9 7 0 2128.55 1799.04 70.49 o 11 7 0 3678.60 3246.06 85.83 o 13 7 0 41223.50 39508.93 558.09 o 15 7 0 1143.37 1166.01 137.53 o 17 7 0 89.86 88.50 74.57 o 19 7 0 5959.32 6597.90 360.84 o 21 7 0 4438.94 4774.66 330.20 o 23 7 0 2820.62 3282.73 316.69 o 25 7 0 2738.35 2413.78 285.79 o 0 8 0 757.06 845.79 92.69 o 2 8 0 2985.83 2972.90 88.43 o 4 8 0 25608.08 28260.39 503.65 o 6 8 0 13.34 47.62 27.41 o 8 8 0 65.19 51.14 28.84 o 10 8 0 4937.77 4503.71 158.87 o 12 8 0 324.39 293.63 37.97 o 14 8 0 3645.39 3447.14 129.90 o 16 8 0 2249.47 2302.38 124.66 o 18 8 0 79.72 126.34 60.12 o 20 8 0 446.11 510.36 83.43 o 22 8 0 1883.90 2263.16 258.76 o 24 8 0 1863.47 1791.99 247.17 o 26 8 0 117.74 65.65 142.90 o 1 9 0 6738.76 6505.27 207.01 o 3 9 0 16215.56 16091.85 307.39 o 5 9 0 12403.45 11773.05 241.36 o 7 9 0 4387.92 6355.17 159.43 o 9 9 0 4225.90 3280.09 98.58 o 11 9 0 6805.27 6727.53 155.00 o 13 9 0 16520.67 16305.31 355.08 o 15 9 0 4091.23 4233.75 152.58 o 17 9 0 198.63 350.94 64.49 o 19 9 0 3860.22 4086.40 225.67 o 21 9 0 798.95 721.01 97.34 o 23 9 0 2627.01 3421.77 324.41 o 25 9 0 485.07 158.34 142.90 o 0 10 0 6021.72 7275.48 197.30 o 2 10 0 20148.09 20134.80 376.33 o 4 10 0 24417.04 25675.52 470.06 o 6 10 0 1991.05 1827.23 72.12 o 8 10 0 8598.09 8621.29 311.61 o 10 10 0 6005.78 5700.65 141.59 o 12 10 0 15139.81 14299.03 273.29 o 14 10 0 95.60 75.95 79.50 o 16 10 0 3133.18 3287.15 145.34 o 18 10 0 8723.48 8317.98 244.84 o 20 10 0 617.88 716.49 94.59 o 22 10 0 4182.65 4526.31 332.14 o 24 10 0 2931.79 2915.84 308.96 o 1 11 0 258.59 389.88 43.75 o 3 11 0 32952.10 33439.43 598.57 o 5 11 0 21.61 84.59 34.36 o 7 11 0 752.30 555.75 57.86 o 9 11 0 4533.19 4597.27 123.26 o 11 11 0 18417.74 18824.38 337.61 o 13 11 0 120.99 132.92 50.88 o 15 11 0 29.15 38.58 50.13 o 17 11 0 6341.55 6419.86 247.87 o 19 11 0 259.20 301.77 76.98 o 21 11 0 3384.50 3759.21 223.88 o 23 11 0 2192.34 2043.02 258.76 o 25 11 0 891.67 911.44 208.55 o 0 12 0 98854.23 103381.25 2119.42 o 2 12 0 26669.86 27706.27 509.16 o 4 12 0 21760.98 21972.35 417.91 o 6 12 0 521.62 194.92 40.76 o 8 12 0 10230.57 9212.23 193.50 o 10 12 0 16360.33 16162.26 300.62 o 12 12 0 19414.97 19958.49 421.69 o 14 12 0 34265.34 35072.40 683.42 o 16 12 0 1481.27 1528.64 112.13 o 18 12 0 13629.39 13943.66 350.83 o 20 12 0 12495.55 13040.74 503.07 o 22 12 0 4456.51 4974.71 631.44 o 24 12 0 2297.58 2614.60 305.10 o 1 13 0 36.08 -23.17 52.80 o 3 13 0 2339.32 2725.48 146.29 o 5 13 0 9918.34 9406.26 217.63 o 7 13 0 4981.13 4930.27 153.85 o 9 13 0 2343.09 2078.30 90.40 o 11 13 0 509.22 566.80 66.98 o 13 13 0 287.86 237.89 61.53 o 15 13 0 102.38 3.43 52.02 o 17 13 0 541.79 538.30 140.53 o 19 13 0 872.90 959.57 117.92 o 21 13 0 597.51 449.17 208.55 o 0 14 0 33958.20 34729.41 764.69 o 2 14 0 65905.80 68608.93 1186.11 o 4 14 0 23644.96 24291.26 465.86 o 6 14 0 28784.62 27083.23 514.47 o 8 14 0 26981.69 26031.89 443.64 o 10 14 0 2459.72 2800.65 155.72 o 12 14 0 35130.71 35249.28 683.40 o 14 14 0 12287.36 12272.74 307.11 o 16 14 0 8947.13 9284.93 265.24 o 18 14 0 7659.51 8049.42 253.80 o 20 14 0 14975.09 15490.18 464.22 o 22 14 0 5545.35 5944.68 274.44 o 24 14 0 80.63 251.03 154.48 o 1 15 0 2429.73 2754.98 122.08 o 3 15 0 9761.67 10349.44 521.79 o 5 15 0 2916.01 2626.77 108.72 o 7 15 0 8355.06 8413.51 187.59 o 9 15 0 25053.34 25227.02 438.64 o 11 15 0 4116.17 4276.59 157.15 o 13 15 0 180.17 290.65 65.56 o 15 15 0 748.84 702.47 114.80 o 17 15 0 1434.18 1389.21 116.67 o 19 15 0 5764.02 5653.36 252.33 o 21 15 0 794.77 745.64 287.72 o 23 15 0 5718.35 6213.46 330.20 o 0 16 0 48694.78 49069.23 1060.53 o 2 16 0 15391.50 15531.55 328.93 o 4 16 0 34814.72 33465.60 626.02 o 6 16 0 6360.73 6140.17 176.18 o 8 16 0 6672.10 6931.56 172.20 o 10 16 0 40930.36 40239.18 763.14 o 12 16 0 27029.92 26407.09 542.88 o 14 16 0 18505.94 17622.97 406.40 o 16 16 0 351.57 306.90 74.71 o 18 16 0 8597.30 9013.88 278.97 o 20 16 0 3185.45 3232.03 469.24 o 22 16 0 3490.26 3670.46 529.10 o 1 17 0 7372.20 7466.23 162.99 o 3 17 0 20101.57 20651.88 419.18 o 5 17 0 943.68 1026.21 80.63 o 7 17 0 11496.13 11676.56 278.55 o 9 17 0 16873.89 16747.25 324.19 o 11 17 0 21055.54 21527.63 460.76 o 13 17 0 5122.14 4961.73 290.15 o 15 17 0 146.54 141.67 65.23 o 17 17 0 4636.15 5180.68 208.97 o 19 17 0 1364.90 1541.24 155.37 o 21 17 0 4322.35 4320.60 243.56 o 0 18 0 289.96 383.71 83.03 o 2 18 0 23689.06 23833.53 474.40 o 4 18 0 7873.22 7853.45 210.73 o 6 18 0 109.56 82.95 50.12 o 8 18 0 4188.59 4261.97 137.10 o 10 18 0 9408.01 9195.86 251.60 o 12 18 0 10815.52 10400.73 278.59 o 14 18 0 569.26 454.81 79.42 o 16 18 0 6326.79 6834.95 232.00 o 18 18 0 1561.40 1777.22 165.07 o 20 18 0 196.05 152.52 93.50 o 22 18 0 2284.72 2608.53 218.47 o 1 19 0 13890.72 13757.62 312.14 o 3 19 0 350.26 335.33 99.98 o 5 19 0 30137.32 28501.59 561.43 o 7 19 0 21883.78 21465.60 632.74 o 9 19 0 14813.74 14697.73 345.78 o 11 19 0 9083.74 9011.28 253.79 o 13 19 0 13808.84 14281.97 355.34 o 15 19 0 4293.42 4252.93 184.51 o 17 19 0 365.75 351.34 98.31 o 19 19 0 5958.26 5894.43 276.37 o 21 19 0 6456.71 6757.76 504.00 o 0 20 0 9.03 355.31 123.59 o 2 20 0 2.75 17.38 71.00 o 4 20 0 705.31 798.51 79.76 o 6 20 0 494.51 376.50 67.65 o 8 20 0 40.31 72.84 47.66 o 10 20 0 421.03 353.98 68.17 o 12 20 0 1015.68 899.90 94.98 o 14 20 0 1286.73 997.63 106.71 o 16 20 0 51.64 36.36 69.48 o 18 20 0 100.17 91.55 88.59 o 20 20 0 50.98 -36.61 93.50 o 1 21 0 22326.67 22180.57 595.31 o 3 21 0 9685.41 9700.01 334.52 o 5 21 0 1841.30 2098.45 147.79 o 7 21 0 2311.26 2227.01 129.20 o 9 21 0 8572.88 8699.39 248.82 o 11 21 0 5445.15 5554.18 221.98 o 13 21 0 5079.94 5219.58 264.45 o 15 21 0 1822.60 2135.02 176.43 o 17 21 0 1283.10 1805.51 289.65 o 19 21 0 3425.44 3973.73 274.20 o 0 22 0 761.41 706.75 169.93 o 2 22 0 2068.73 2046.63 170.53 o 4 22 0 9570.17 9375.44 335.90 o 6 22 0 2237.89 2101.93 179.99 o 8 22 0 214.00 117.73 61.08 o 10 22 0 1687.71 1734.46 121.99 o 12 22 0 343.47 538.75 138.82 o 14 22 0 19.50 63.27 68.89 o 16 22 0 6805.95 6733.17 286.36 o 18 22 0 674.15 600.44 121.31 o 1 23 0 9002.07 9053.80 335.86 o 3 23 0 469.47 608.03 164.14 o 5 23 0 111.53 -55.64 117.79 o 7 23 0 2408.68 2335.70 154.79 o 9 23 0 653.31 459.37 100.08 o 11 23 0 3679.21 4140.69 256.57 o 13 23 0 1342.69 1388.42 167.04 o 15 23 0 577.92 755.60 128.04 o 17 23 0 1485.72 1823.88 179.02 o 0 24 0 13945.06 13061.42 614.06 o 2 24 0 2221.55 2330.16 214.34 o 4 24 0 8356.84 9332.12 357.71 o 6 24 0 359.66 175.95 102.16 o 8 24 0 963.94 740.02 195.03 o 10 24 0 8745.33 8615.57 417.10 o 12 24 0 37.38 25.61 63.09 o 14 24 0 2739.84 2674.70 199.39 o 16 24 0 2396.56 2268.66 195.79 o 1 25 0 7.03 -90.33 91.21 o 3 25 0 214.80 399.94 158.34 o 5 25 0 237.93 431.05 122.53 o 7 25 0 2268.39 2390.66 197.64 o 9 25 0 4420.61 4832.94 710.62 o 11 25 0 445.86 569.33 133.06 o 13 25 0 177.24 -150.62 150.62 o 15 25 0 311.01 255.40 243.31 o 0 26 0 4734.72 4927.96 370.76 o 2 26 0 3911.94 3730.06 253.80 o 4 26 0 116.67 208.29 119.79 o 6 26 0 8130.78 8631.66 502.07 o 8 26 0 6481.58 6244.92 440.27 o 10 26 0 284.33 70.04 100.93 o 12 26 0 5855.06 7395.81 490.48 o 14 26 0 1489.95 1243.58 270.34 o 1 27 0 452.72 496.58 136.46 o 3 27 0 2645.15 2253.44 214.36 o 5 27 0 3358.18 2746.16 276.14 o 7 27 0 0.06 23.17 158.34 o 9 27 0 1850.98 1664.54 274.20 o 11 27 0 49.85 -38.62 154.48 o 13 27 0 161.70 289.65 193.10 o 0 28 0 20491.88 19584.41 865.10 o 2 28 0 346.20 195.35 158.34 o 4 28 0 1624.81 1976.61 208.79 o 6 28 0 3832.98 3896.80 401.65 o 8 28 0 3424.38 3247.98 366.89 o 10 28 0 4026.03 3966.32 413.24 o 12 28 0 754.45 544.55 220.14 o 1 29 0 58.14 15.20 128.26 o 3 29 0 5307.42 6327.20 482.76 o 5 29 0 29.22 23.17 173.79 o 7 29 0 162.65 305.10 193.10 o 9 29 0 1278.84 946.20 262.62 o 11 29 0 4376.97 4978.17 475.03 o 0 30 0 407.28 502.07 227.86 o 2 30 0 6006.49 6087.73 345.65 o 4 30 0 2035.93 1595.02 285.79 o 6 30 0 1990.79 1861.50 308.96 o 8 30 0 1549.04 1313.09 278.07 o 1 31 0 526.53 298.23 154.28 o 3 31 0 2331.67 2104.69 623.72 o 5 31 0 3998.74 4066.73 420.96 o 1 1 1 1258.15 1231.99 96.55 o 2 1 1 38.43 31.81 25.95 o 3 1 1 11.65 40.45 22.58 o 4 1 1 14855.27 15491.13 175.86 o 5 1 1 660.36 739.70 27.30 o 6 1 1 4646.91 5121.54 68.12 o 7 1 1 225.25 271.53 18.72 o 8 1 1 3.81 14.15 15.03 o 9 1 1 249.39 231.18 18.03 o 10 1 1 5213.21 5120.12 67.04 o 11 1 1 1106.59 1167.31 33.93 o 12 1 1 1122.65 1177.77 37.08 o 13 1 1 1588.00 1653.29 47.74 o 14 1 1 255.99 217.11 25.15 o 15 1 1 2081.01 2126.73 61.54 o 16 1 1 3378.11 3576.37 89.51 o 17 1 1 0.02 -13.65 28.57 o 18 1 1 883.86 788.06 52.18 o 19 1 1 20.68 81.30 37.53 o 20 1 1 9.42 24.30 47.50 o 21 1 1 754.53 869.45 102.57 o 22 1 1 832.82 772.81 88.60 o 23 1 1 152.47 210.92 68.01 o 24 1 1 2045.12 1860.39 216.29 o 25 1 1 638.15 482.76 117.43 o 26 1 1 400.92 622.92 109.25 o 1 2 1 90.01 119.45 23.10 o 2 2 1 37274.57 38322.65 572.50 o 3 2 1 753.22 866.52 28.77 o 4 2 1 2080.73 2356.95 47.90 o 5 2 1 2497.94 2526.70 52.24 o 6 2 1 167.65 188.80 17.36 o 7 2 1 293.50 318.85 22.67 o 8 2 1 10365.87 11123.63 126.23 o 9 2 1 801.74 991.34 42.52 o 10 2 1 2563.26 2626.32 49.97 o 11 2 1 642.24 588.54 25.26 o 12 2 1 10998.01 11564.38 130.51 o 13 2 1 1274.76 1194.22 38.10 o 14 2 1 398.67 403.31 30.88 o 15 2 1 173.79 151.74 26.30 o 16 2 1 787.77 666.82 43.01 o 17 2 1 1145.09 1101.12 53.97 o 18 2 1 5897.56 5873.56 132.55 o 19 2 1 263.27 326.13 63.33 o 20 2 1 719.37 821.69 71.81 o 21 2 1 5.07 -38.15 47.99 o 22 2 1 1662.00 1644.47 110.83 o 23 2 1 1187.59 1172.22 114.08 o 24 2 1 0.53 -1.62 66.74 o 25 2 1 63.11 64.92 75.93 o 26 2 1 483.02 444.89 122.71 o 1 3 1 2635.61 2903.17 72.88 o 2 3 1 3031.34 3082.09 50.87 o 3 3 1 27096.14 27593.22 251.16 o 4 3 1 8758.53 9220.58 100.49 o 5 3 1 6662.33 6509.64 78.60 o 6 3 1 145.50 189.13 16.77 o 7 3 1 2429.03 2407.99 47.03 o 8 3 1 3033.62 2992.36 54.42 o 9 3 1 446.54 493.33 27.94 o 10 3 1 627.45 721.56 58.18 o 11 3 1 1263.29 1408.66 44.65 o 12 3 1 1293.92 1243.94 38.66 o 13 3 1 3152.30 3006.08 64.20 o 14 3 1 161.77 85.56 23.79 o 15 3 1 3099.62 2923.36 73.04 o 16 3 1 164.86 98.37 24.91 o 17 3 1 16.28 -24.60 24.60 o 18 3 1 1578.85 1510.44 74.55 o 19 3 1 129.11 154.46 41.77 o 20 3 1 31.27 38.85 44.19 o 21 3 1 11.69 -19.56 50.08 o 22 3 1 2082.48 2076.41 164.05 o 23 3 1 46.69 85.46 68.47 o 24 3 1 313.30 220.88 98.49 o 25 3 1 23.58 -17.13 73.31 o 26 3 1 613.80 779.94 114.81 o 1 4 1 12545.51 13114.82 185.49 o 2 4 1 1935.22 2181.29 40.48 o 3 4 1 845.68 811.90 26.82 o 4 4 1 6547.70 6478.59 85.04 o 5 4 1 1884.51 1794.48 39.42 o 6 4 1 4.08 -14.90 14.90 o 7 4 1 170.44 203.43 23.72 o 8 4 1 1594.34 1376.58 43.15 o 9 4 1 22.07 17.53 18.08 o 10 4 1 6025.77 6074.53 90.65 o 11 4 1 2886.92 2843.46 78.64 o 12 4 1 1.50 15.49 16.63 o 13 4 1 31.09 48.32 20.39 o 14 4 1 116.97 54.36 21.94 o 15 4 1 2825.83 2663.82 75.07 o 16 4 1 160.09 127.33 28.59 o 17 4 1 22.95 14.26 30.39 o 18 4 1 4976.90 5306.65 137.77 o 19 4 1 1336.58 1297.54 135.91 o 20 4 1 341.22 334.38 55.74 o 21 4 1 2154.22 2035.17 119.20 o 22 4 1 990.99 1039.11 95.25 o 23 4 1 1765.50 1867.59 187.30 o 24 4 1 1102.44 1114.55 163.48 o 25 4 1 596.90 694.42 104.99 o 26 4 1 84.54 53.74 80.93 o 1 5 1 8653.25 9151.52 126.32 o 2 5 1 469.49 508.00 25.97 o 3 5 1 10008.65 9838.50 110.78 o 4 5 1 188.06 205.73 16.61 o 5 5 1 7623.68 7805.42 100.82 o 6 5 1 2983.06 2882.49 53.20 o 7 5 1 8201.64 9109.18 121.48 o 8 5 1 742.64 846.45 35.40 o 9 5 1 1804.76 1652.42 46.17 o 10 5 1 4451.76 4544.70 76.44 o 11 5 1 15639.13 15581.04 197.49 o 12 5 1 10.05 18.53 19.26 o 13 5 1 112.02 81.37 21.76 o 14 5 1 161.45 172.73 25.97 o 15 5 1 1.57 17.86 24.32 o 16 5 1 792.98 866.48 51.10 o 17 5 1 3246.13 3374.31 105.87 o 18 5 1 19.11 -0.46 39.05 o 19 5 1 1203.05 1134.90 75.52 o 20 5 1 1115.84 1168.07 78.88 o 21 5 1 41.02 -43.68 43.68 o 22 5 1 105.03 192.98 67.48 o 23 5 1 4.96 -23.88 64.09 o 24 5 1 674.65 657.57 181.39 o 25 5 1 4362.40 4382.93 221.39 o 26 5 1 317.63 387.65 117.85 o 1 6 1 827.70 1083.69 34.31 o 2 6 1 1179.67 1367.98 38.60 o 3 6 1 5260.57 5462.38 83.28 o 4 6 1 30.70 45.48 20.67 o 5 6 1 1301.62 1394.06 36.71 o 6 6 1 868.60 855.39 31.46 o 7 6 1 1.59 -2.49 17.89 o 8 6 1 19155.02 19292.08 228.58 o 9 6 1 1794.02 1746.65 58.30 o 10 6 1 1500.81 1448.74 57.52 o 11 6 1 508.71 595.97 36.12 o 12 6 1 974.80 996.60 54.58 o 13 6 1 6120.20 5706.69 101.60 o 14 6 1 114.77 86.54 26.23 o 15 6 1 5.23 10.25 25.26 o 16 6 1 703.79 763.62 44.87 o 17 6 1 30.01 26.62 33.91 o 18 6 1 1713.07 1489.39 82.07 o 19 6 1 1503.64 1753.79 91.95 o 20 6 1 0.94 -40.85 41.93 o 21 6 1 2932.52 2823.47 121.70 o 22 6 1 1349.44 1292.37 115.95 o 23 6 1 5236.54 4943.54 198.05 o 24 6 1 2266.76 2062.10 432.55 o 25 6 1 30.24 -84.96 84.96 o 26 6 1 237.88 0.00 101.04 o 1 7 1 13762.01 14181.21 170.81 o 2 7 1 2829.24 3124.07 61.48 o 3 7 1 803.84 745.93 30.96 o 4 7 1 6.48 7.05 17.58 o 5 7 1 2509.84 2700.82 66.02 o 6 7 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63382.48 63294.07 949.89 o 4 7 2 33.58 43.50 16.77 o 5 7 2 26754.01 25043.91 338.51 o 6 7 2 1502.21 1538.06 60.16 o 7 7 2 3055.86 2506.01 65.76 o 8 7 2 1645.36 1639.65 56.50 o 9 7 2 46984.90 46253.70 636.74 o 10 7 2 638.86 756.08 44.83 o 11 7 2 41939.20 41552.67 497.84 o 12 7 2 2946.54 2855.74 73.63 o 13 7 2 16176.70 16035.61 214.32 o 14 7 2 2210.62 2141.49 72.07 o 15 7 2 12189.66 12136.34 202.00 o 16 7 2 246.37 213.91 57.66 o 17 7 2 11509.25 11215.87 196.66 o 18 7 2 1091.91 1124.34 103.13 o 19 7 2 3222.44 3242.89 205.14 o 20 7 2 520.57 588.41 76.83 o 21 7 2 6237.74 6316.91 411.39 o 22 7 2 0.45 -21.64 62.30 o 23 7 2 12691.65 13136.24 348.91 o 24 7 2 1.57 4.56 89.99 o 25 7 2 2235.84 2179.33 200.38 o 0 8 2 7583.01 8072.56 231.02 o 1 8 2 159.31 213.60 47.94 o 2 8 2 923.41 903.26 51.73 o 3 8 2 3483.71 3776.85 86.38 o 4 8 2 9.98 27.26 19.69 o 5 8 2 1282.19 1354.79 54.37 o 6 8 2 5115.27 5136.02 93.16 o 7 8 2 91.45 46.67 20.10 o 8 8 2 7370.72 7855.88 125.23 o 9 8 2 3900.68 3888.71 82.50 o 10 8 2 3.90 26.32 24.45 o 11 8 2 167.21 170.14 31.06 o 12 8 2 2794.32 2675.77 76.08 o 13 8 2 875.17 792.32 47.50 o 14 8 2 1634.62 1609.40 101.92 o 15 8 2 1517.47 1335.79 73.58 o 16 8 2 4.31 16.59 34.97 o 17 8 2 13.80 -27.44 39.97 o 18 8 2 2254.17 2207.38 119.33 o 19 8 2 896.04 857.01 82.93 o 20 8 2 1164.98 1103.18 123.59 o 21 8 2 3.11 -43.79 55.64 o 22 8 2 257.23 193.43 76.28 o 23 8 2 166.57 83.05 76.88 o 24 8 2 118.51 103.26 89.45 o 25 8 2 24.09 -40.58 89.03 o 0 9 2 8391.23 8886.26 191.55 o 1 9 2 31127.77 31312.18 442.50 o 2 9 2 961.23 1093.31 47.88 o 3 9 2 24101.62 24115.68 318.41 o 4 9 2 4384.52 4672.45 90.42 o 5 9 2 14755.09 14591.24 209.84 o 6 9 2 107.72 159.91 18.76 o 7 9 2 23192.49 23079.83 268.08 o 8 9 2 12.21 33.99 21.90 o 9 9 2 21888.11 22525.50 289.35 o 10 9 2 1757.58 1799.99 70.52 o 11 9 2 23214.68 23332.09 287.51 o 12 9 2 17.89 15.52 25.82 o 13 9 2 19752.02 19291.73 273.10 o 14 9 2 716.08 745.63 53.90 o 15 9 2 1976.03 2042.25 82.57 o 16 9 2 205.32 174.97 41.09 o 17 9 2 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2 74.25 162.29 93.78 o 24 10 2 483.10 219.37 88.08 o 0 11 2 284.30 386.75 61.77 o 1 11 2 15841.13 15232.23 215.25 o 2 11 2 14597.99 14930.00 192.54 o 3 11 2 3693.82 4030.64 104.58 o 4 11 2 714.16 755.06 42.60 o 5 11 2 7581.12 7040.41 116.28 o 6 11 2 96.91 159.13 19.16 o 7 11 2 2043.82 1903.40 65.58 o 8 11 2 2413.64 2473.90 82.69 o 9 11 2 950.62 880.49 54.52 o 10 11 2 2044.55 2301.77 85.86 o 11 11 2 2371.62 2360.86 88.22 o 12 11 2 2026.04 2108.14 81.68 o 13 11 2 17946.54 17360.28 257.91 o 14 11 2 2060.29 2067.78 84.16 o 15 11 2 2394.08 2421.55 86.44 o 16 11 2 3416.37 3322.32 116.96 o 17 11 2 217.47 152.34 51.04 o 18 11 2 1351.35 1317.60 89.37 o 19 11 2 3818.83 3981.19 156.62 o 20 11 2 372.97 342.13 72.40 o 21 11 2 1754.65 1988.76 141.17 o 22 11 2 425.62 167.73 163.46 o 23 11 2 208.30 225.29 90.55 o 24 11 2 213.98 133.28 97.85 o 0 12 2 3730.38 3393.43 105.43 o 1 12 2 7.20 -1.87 15.39 o 2 12 2 31848.13 31134.74 371.62 o 3 12 2 3134.84 3074.79 75.12 o 4 12 2 40601.01 40127.10 476.05 o 5 12 2 233.07 185.45 19.50 o 6 12 2 8892.86 8079.30 147.98 o 7 12 2 1461.17 1543.54 111.12 o 8 12 2 17309.56 17171.29 261.10 o 9 12 2 1688.32 1750.64 74.04 o 10 12 2 21644.46 22377.79 327.31 o 11 12 2 2769.60 2884.85 99.01 o 12 12 2 19089.14 18662.75 271.15 o 13 12 2 61.82 44.25 36.16 o 14 12 2 3357.32 3530.79 104.28 o 15 12 2 135.58 89.94 48.61 o 16 12 2 6565.76 6389.60 153.74 o 17 12 2 1738.44 1620.81 95.90 o 18 12 2 8904.03 8329.70 199.29 o 19 12 2 1561.46 1424.15 105.83 o 20 12 2 2116.58 2161.34 144.31 o 21 12 2 557.34 414.91 107.02 o 22 12 2 4396.28 4827.23 266.79 o 23 12 2 174.81 126.41 93.09 o 24 12 2 2991.46 3064.65 396.40 o 0 13 2 7233.71 6482.07 162.34 o 1 13 2 1.67 12.25 16.82 o 2 13 2 132.76 124.96 20.14 o 3 13 2 232.00 346.03 32.34 o 4 13 2 2257.58 2072.81 61.24 o 5 13 2 346.96 422.33 38.82 o 6 13 2 294.48 283.97 31.85 o 7 13 2 880.22 840.97 52.48 o 8 13 2 1561.67 1810.03 94.13 o 9 13 2 2636.34 2727.89 110.54 o 10 13 2 9937.11 9626.80 178.68 o 11 13 2 0.66 69.03 37.19 o 12 13 2 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33.68 o 6 4 3 1196.21 1125.39 45.67 o 7 4 3 136.30 106.96 20.77 o 8 4 3 14.65 46.83 21.70 o 9 4 3 290.95 270.72 29.92 o 10 4 3 608.40 669.87 40.68 o 11 4 3 609.64 662.90 43.19 o 12 4 3 328.37 246.13 31.37 o 13 4 3 9593.28 9459.01 182.20 o 14 4 3 9.90 -6.58 29.10 o 15 4 3 66.13 95.79 32.54 o 16 4 3 859.93 922.81 55.54 o 17 4 3 377.18 419.91 49.37 o 18 4 3 605.97 553.26 58.40 o 19 4 3 20.97 -41.01 41.77 o 20 4 3 452.17 433.78 67.65 o 21 4 3 134.59 117.32 65.03 o 22 4 3 30.72 15.82 72.52 o 23 4 3 2605.18 2548.47 193.37 o 24 4 3 330.36 320.36 107.61 o 25 4 3 3.93 50.21 119.72 o 1 5 3 1168.46 1086.61 53.10 o 2 5 3 15.20 8.36 22.07 o 3 5 3 5329.85 5776.50 114.11 o 4 5 3 3200.55 3628.17 86.41 o 5 5 3 52.16 93.90 27.47 o 6 5 3 5468.50 5234.01 84.52 o 7 5 3 49.24 64.44 18.34 o 8 5 3 8245.87 8045.70 131.49 o 9 5 3 651.10 638.75 40.38 o 10 5 3 240.25 182.79 38.14 o 11 5 3 2786.79 2644.18 72.45 o 12 5 3 322.80 317.03 33.73 o 13 5 3 147.47 98.99 40.15 o 14 5 3 69.48 62.48 31.44 o 15 5 3 2270.25 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56.30 o 7 11 3 30.97 54.19 45.03 o 8 11 3 6029.64 5612.40 162.24 o 9 11 3 19.25 46.77 46.60 o 10 11 3 1.35 58.53 40.97 o 11 11 3 488.51 528.08 59.65 o 12 11 3 145.44 139.58 48.08 o 13 11 3 207.84 164.68 46.91 o 14 11 3 2253.54 2082.21 153.72 o 15 11 3 954.71 973.76 68.72 o 16 11 3 880.83 1075.84 73.11 o 17 11 3 30.80 37.12 48.96 o 18 11 3 95.26 124.26 57.76 o 19 11 3 44.82 39.02 61.16 o 20 11 3 342.04 289.97 84.55 o 21 11 3 65.17 105.16 74.23 o 22 11 3 2046.88 2349.43 190.23 o 23 11 3 137.43 61.13 93.72 o 1 12 3 449.32 473.85 51.86 o 2 12 3 7488.90 7607.27 175.60 o 3 12 3 1703.66 1751.64 102.01 o 4 12 3 1553.51 1468.39 108.70 o 5 12 3 5116.27 5198.27 138.26 o 6 12 3 613.75 633.16 66.67 o 7 12 3 1.66 28.12 44.25 o 8 12 3 3574.08 3723.12 139.92 o 9 12 3 4486.51 4621.74 131.46 o 10 12 3 4.93 -29.27 49.98 o 11 12 3 659.59 751.35 90.93 o 12 12 3 2683.99 2628.12 181.32 o 13 12 3 251.10 318.87 65.44 o 14 12 3 687.54 697.36 98.16 o 15 12 3 17.69 23.87 40.68 o 16 12 3 1275.58 1276.09 77.56 o 17 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