#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/89/2228939.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2228939_Fobs loop_ _publ_author_name 'Ang, Li' _publ_section_title ; 2,7-Dimethyl-2,7-diazoniapyrene bis(hexafluorophosphate) ; _journal_coeditor_code BG2385 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o508 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.028 _cell_angle_gamma 90.000 _cell_length_a 6.7654 _cell_length_b 10.6528 _cell_length_c 13.4222 _exptl_crystal_F_000 524.00 _reflns_d_resolution_high 0.8301 _[local]_cod_data_source_file bg2385Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TREF in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13948.19 14110.70 244.19 o 4 0 0 8794.66 8865.78 142.30 o 6 0 0 31.21 24.99 1.81 o 8 0 0 3.89 -1.35 2.05 o 1 1 0 445.03 463.70 2.42 o 2 1 0 14.52 15.14 0.60 o 3 1 0 52.54 55.92 1.69 o 4 1 0 36.81 22.80 1.20 o 5 1 0 89.93 76.53 2.02 o 6 1 0 0.52 0.05 0.66 o 7 1 0 41.11 38.45 1.19 o 8 1 0 50.68 47.30 2.36 o 0 2 0 583.84 554.09 15.74 o 1 2 0 13143.15 13985.04 169.69 o 2 2 0 9.76 7.70 0.67 o 3 2 0 674.62 584.44 3.94 o 4 2 0 60.00 47.99 1.16 o 5 2 0 742.86 770.94 8.86 o 6 2 0 1.35 1.41 0.76 o 7 2 0 15.26 19.71 1.38 o 8 2 0 0.01 -1.07 1.58 o 1 3 0 14.39 13.24 1.70 o 2 3 0 29.14 32.54 1.59 o 3 3 0 1.18 0.56 0.84 o 4 3 0 135.39 110.08 2.03 o 5 3 0 47.43 51.17 1.57 o 6 3 0 1.85 1.83 1.10 o 7 3 0 0.43 1.97 1.13 o 0 4 0 235.93 181.58 2.72 o 1 4 0 212.97 224.33 2.56 o 2 4 0 939.49 896.53 6.13 o 3 4 0 2.48 4.51 0.76 o 4 4 0 402.90 389.14 3.92 o 5 4 0 209.32 215.06 3.40 o 6 4 0 144.45 155.71 4.07 o 7 4 0 2.88 1.34 2.16 o 1 5 0 6.99 4.93 0.88 o 2 5 0 1058.57 1241.53 10.39 o 3 5 0 20.78 21.97 1.08 o 4 5 0 98.91 127.43 2.43 o 5 5 0 96.20 97.61 2.49 o 6 5 0 185.24 199.36 4.47 o 7 5 0 1.29 6.51 5.15 o 0 6 0 32.64 58.86 2.55 o 1 6 0 43.17 56.00 1.50 o 2 6 0 9.11 16.73 1.45 o 3 6 0 52.19 60.77 2.09 o 4 6 0 1.24 2.96 1.33 o 5 6 0 508.26 474.02 6.02 o 6 6 0 68.02 67.08 2.51 o 7 6 0 32.67 36.58 3.05 o 1 7 0 30.63 34.99 3.00 o 2 7 0 7.40 8.82 1.40 o 3 7 0 15.97 28.44 1.45 o 4 7 0 43.77 57.97 1.99 o 5 7 0 5.82 8.50 1.34 o 6 7 0 12.39 15.28 2.01 o 0 8 0 896.87 1087.61 15.91 o 1 8 0 116.27 127.21 2.81 o 2 8 0 271.34 342.80 4.50 o 3 8 0 20.21 11.96 1.45 o 4 8 0 283.98 315.75 5.11 o 5 8 0 0.37 -0.58 1.42 o 6 8 0 4.91 1.99 1.63 o 1 9 0 53.59 49.88 3.15 o 2 9 0 1.87 1.51 1.35 o 3 9 0 83.84 71.18 2.33 o 4 9 0 10.58 11.69 1.84 o 5 9 0 10.20 11.58 1.75 o 0 10 0 201.54 212.05 5.68 o 1 10 0 191.79 191.82 4.78 o 2 10 0 1.37 4.43 1.81 o 3 10 0 103.57 118.51 2.97 o 4 10 0 18.10 12.90 2.02 o 5 10 0 32.78 30.54 3.44 o 1 11 0 1.28 2.53 1.66 o 2 11 0 5.23 3.75 1.78 o 3 11 0 3.61 5.20 1.74 o 4 11 0 22.68 13.40 2.06 o 0 12 0 21.77 11.35 3.63 o 1 12 0 2.00 6.04 1.95 o 2 12 0 19.92 11.35 2.25 o -7 0 1 29.67 26.88 2.35 o -5 0 1 1564.41 1510.91 21.96 o -3 0 1 8647.01 7949.41 118.70 o -1 0 1 1409.96 1742.08 15.52 o 1 0 1 12304.11 12456.47 288.51 o 3 0 1 865.59 1037.13 11.05 o 5 0 1 229.07 213.16 2.96 o 7 0 1 28.92 19.87 6.21 o -8 1 1 3.10 5.25 2.14 o -7 1 1 25.91 17.04 2.14 o -6 1 1 2.48 1.12 0.83 o -5 1 1 18.44 18.65 1.22 o -4 1 1 7.60 13.46 0.81 o -3 1 1 464.02 435.98 4.98 o -2 1 1 8.39 1.14 0.49 o -1 1 1 1148.15 1188.87 9.92 o 1 1 1 5474.01 5802.71 43.17 o 2 1 1 82.73 91.28 1.05 o 3 1 1 364.15 322.28 4.55 o 4 1 1 245.29 189.05 3.30 o 5 1 1 249.92 226.13 2.55 o 6 1 1 0.93 0.01 0.59 o 7 1 1 29.52 37.34 2.36 o 8 1 1 26.23 21.83 1.46 o -8 2 1 29.02 30.58 2.52 o -7 2 1 32.34 27.52 2.57 o -6 2 1 74.53 80.06 2.34 o -5 2 1 0.11 -0.79 0.79 o -4 2 1 3691.54 3525.12 37.42 o -3 2 1 0.53 -0.14 0.48 o -2 2 1 103.64 92.44 1.44 o -1 2 1 690.12 642.49 6.54 o 0 2 1 11320.00 11961.47 137.37 o 1 2 1 58.36 39.62 1.55 o 2 2 1 51.33 55.46 2.18 o 3 2 1 0.84 -0.46 0.46 o 4 2 1 389.08 384.42 3.40 o 5 2 1 4.49 5.44 0.89 o 6 2 1 10.54 14.64 1.16 o 7 2 1 6.39 4.67 1.13 o 8 2 1 14.71 9.44 2.35 o -7 3 1 19.55 22.84 2.26 o -6 3 1 110.29 106.45 3.85 o -5 3 1 266.56 294.06 4.28 o -4 3 1 1.51 2.73 0.93 o -3 3 1 79.79 68.68 1.11 o -2 3 1 497.54 491.98 4.26 o -1 3 1 75.10 82.83 1.52 o 0 3 1 100.55 99.04 1.57 o 1 3 1 42.99 52.06 1.14 o 2 3 1 147.54 165.93 1.46 o 3 3 1 0.66 4.54 0.65 o 4 3 1 282.69 250.15 2.73 o 5 3 1 527.53 492.44 5.77 o 6 3 1 3.65 6.47 1.19 o 7 3 1 36.64 38.31 2.66 o -7 4 1 9.09 9.38 1.92 o -6 4 1 180.33 174.85 6.30 o -5 4 1 687.42 671.71 6.90 o -4 4 1 9.39 7.65 0.91 o -3 4 1 95.53 82.02 1.71 o -2 4 1 337.00 394.55 4.72 o -1 4 1 206.70 214.51 2.49 o 0 4 1 4.85 1.56 0.74 o 1 4 1 552.78 717.36 6.11 o 2 4 1 649.83 669.05 4.96 o 3 4 1 156.18 174.78 1.88 o 4 4 1 44.43 47.63 1.71 o 5 4 1 7.76 14.85 1.56 o 6 4 1 39.67 39.75 3.92 o 7 4 1 0.37 4.73 1.79 o -7 5 1 6.28 7.93 3.20 o -6 5 1 72.33 83.10 3.56 o -5 5 1 11.23 18.32 1.41 o -4 5 1 27.65 25.20 3.27 o -3 5 1 110.98 117.87 1.90 o -2 5 1 0.06 0.35 0.80 o -1 5 1 27.57 45.75 2.43 o 0 5 1 67.54 71.81 1.63 o 1 5 1 733.43 889.82 7.10 o 2 5 1 16.59 6.47 0.86 o 3 5 1 38.87 30.42 1.09 o 4 5 1 416.25 366.06 3.55 o 5 5 1 260.61 251.25 3.92 o 6 5 1 197.13 201.35 4.29 o 7 5 1 0.13 3.82 2.12 o -7 6 1 6.83 4.25 1.66 o -6 6 1 3.12 2.89 1.55 o -5 6 1 4.74 4.23 1.21 o -4 6 1 196.10 235.68 3.03 o -3 6 1 7.11 8.51 1.11 o -2 6 1 615.98 436.07 4.53 o -1 6 1 34.61 26.40 1.53 o 0 6 1 298.05 266.14 3.35 o 1 6 1 5.05 3.44 1.11 o 2 6 1 1.93 3.74 0.90 o 3 6 1 5.25 5.08 0.92 o 4 6 1 219.99 198.88 2.89 o 5 6 1 103.49 112.72 2.35 o 6 6 1 33.56 30.46 2.14 o 7 6 1 4.35 4.06 2.50 o -6 7 1 1.70 3.25 1.89 o -5 7 1 1.54 4.11 1.40 o -4 7 1 8.10 7.05 1.29 o -3 7 1 0.31 0.78 0.95 o -2 7 1 26.80 31.27 1.67 o -1 7 1 66.10 77.94 2.06 o 0 7 1 87.70 83.37 1.92 o 1 7 1 506.16 512.78 5.60 o 2 7 1 7.50 11.14 1.09 o 3 7 1 92.47 100.01 2.20 o 4 7 1 57.70 72.56 2.00 o 5 7 1 243.07 245.85 3.75 o 6 7 1 6.19 8.68 1.92 o -6 8 1 0.12 0.43 1.31 o -5 8 1 107.46 127.80 3.08 o -4 8 1 0.83 1.06 1.26 o -2 8 1 5.72 7.56 1.74 o -1 8 1 382.71 511.04 6.29 o 0 8 1 24.72 19.94 1.96 o 1 8 1 272.28 334.96 5.33 o 2 8 1 4.43 6.15 1.26 o 3 8 1 168.67 165.72 2.95 o 4 8 1 1.48 3.40 1.47 o 5 8 1 77.74 62.01 2.79 o 6 8 1 6.60 9.09 1.58 o -5 9 1 5.29 8.01 2.12 o -4 9 1 88.78 83.85 2.72 o -3 9 1 87.40 95.49 3.06 o -2 9 1 23.12 28.96 3.56 o -1 9 1 236.56 276.47 4.91 o 0 9 1 1089.12 1132.56 12.05 o 1 9 1 286.90 302.78 4.25 o 2 9 1 41.81 37.66 2.10 o 3 9 1 80.03 82.11 3.15 o 4 9 1 158.34 145.40 3.03 o 5 9 1 36.15 31.83 2.73 o -5 10 1 8.18 7.13 2.14 o -4 10 1 49.45 61.30 4.18 o -3 10 1 0.38 2.46 1.53 o -2 10 1 103.45 107.40 3.40 o -1 10 1 219.90 229.29 4.85 o 0 10 1 210.79 216.24 3.98 o 1 10 1 5.24 5.77 1.69 o 2 10 1 95.22 99.22 2.72 o 3 10 1 35.41 35.18 4.88 o 4 10 1 53.27 54.92 6.44 o 5 10 1 0.24 1.29 1.91 o -4 11 1 3.75 5.03 2.03 o -3 11 1 3.25 5.98 1.84 o -2 11 1 2.40 0.99 1.93 o -1 11 1 34.45 32.69 2.91 o 0 11 1 30.45 34.57 2.60 o 1 11 1 17.08 10.56 2.10 o 2 11 1 4.45 2.61 1.60 o 3 11 1 0.45 0.47 1.80 o 4 11 1 13.08 14.73 3.49 o -2 12 1 0.11 -0.47 1.68 o -1 12 1 48.14 28.17 2.71 o 0 12 1 5.69 5.07 2.39 o 1 12 1 26.27 20.20 2.51 o 2 12 1 0.14 2.14 1.82 o -8 0 2 131.58 132.08 16.29 o -6 0 2 117.51 129.06 2.75 o -4 0 2 2994.99 2868.59 38.82 o -2 0 2 2112.58 2193.45 37.14 o 0 0 2 372.77 350.45 2.15 o 2 0 2 501.22 509.32 4.59 o 4 0 2 53.80 84.56 2.82 o 6 0 2 23.75 24.94 2.23 o 8 0 2 0.21 1.21 1.59 o -8 1 2 25.59 30.94 2.36 o -7 1 2 6.45 3.79 1.02 o -6 1 2 8.22 9.26 1.08 o -5 1 2 220.72 222.12 6.58 o -4 1 2 196.24 145.62 1.86 o -3 1 2 818.12 711.97 7.60 o -2 1 2 111.73 104.60 1.14 o -1 1 2 9871.35 10338.94 115.06 o 0 1 2 233.86 344.23 1.75 o 1 1 2 4839.11 5320.82 38.60 o 2 1 2 50.72 39.88 0.62 o 3 1 2 180.86 189.51 2.12 o 4 1 2 218.84 173.70 2.01 o 5 1 2 350.23 336.23 2.66 o 6 1 2 36.81 30.37 1.83 o 7 1 2 24.40 26.63 1.27 o 8 1 2 19.90 14.05 1.66 o -8 2 2 14.67 13.97 2.10 o -7 2 2 11.83 10.33 1.13 o -6 2 2 0.02 0.83 0.95 o -5 2 2 571.80 597.78 9.93 o -4 2 2 89.55 72.13 2.09 o -3 2 2 878.01 883.47 10.49 o -2 2 2 270.04 207.08 3.12 o -1 2 2 399.14 361.91 2.73 o 0 2 2 23.36 15.46 0.70 o 1 2 2 1373.31 1286.20 7.23 o 2 2 2 41.44 38.62 0.75 o 3 2 2 35.36 47.15 0.90 o 4 2 2 49.06 53.94 1.40 o 5 2 2 35.86 41.70 1.25 o 6 2 2 1.07 -0.08 0.70 o 7 2 2 0.59 0.80 1.22 o -7 3 2 3.51 3.41 1.41 o -6 3 2 152.38 143.26 3.31 o -5 3 2 15.35 14.03 1.48 o -4 3 2 75.33 61.96 1.64 o -3 3 2 20.70 30.10 1.21 o -2 3 2 1014.01 1078.82 8.47 o -1 3 2 22.10 17.25 0.92 o 0 3 2 2267.07 2216.38 17.03 o 1 3 2 286.54 227.65 1.79 o 2 3 2 2.44 10.10 0.65 o 3 3 2 28.48 17.07 1.46 o 4 3 2 481.58 418.12 3.34 o 5 3 2 473.42 457.49 4.84 o 6 3 2 39.40 45.20 1.67 o 7 3 2 8.25 5.82 1.16 o -7 4 2 0.95 2.12 2.02 o -6 4 2 177.70 169.89 6.57 o -5 4 2 36.42 34.44 1.92 o -4 4 2 61.55 67.36 2.28 o -3 4 2 287.31 305.32 3.34 o -2 4 2 2517.35 2455.31 21.66 o -1 4 2 11.74 10.74 0.94 o 0 4 2 797.45 638.28 5.00 o 1 4 2 972.05 1003.48 7.00 o 2 4 2 379.85 397.62 3.46 o 3 4 2 51.85 55.60 1.87 o 4 4 2 819.23 877.90 7.57 o 5 4 2 502.14 511.16 4.98 o 6 4 2 95.34 122.48 4.23 o 7 4 2 2.59 0.18 2.14 o -7 5 2 12.45 11.74 3.40 o -6 5 2 27.27 17.52 2.37 o -5 5 2 3.88 1.31 1.66 o -4 5 2 27.10 36.72 1.56 o -3 5 2 156.45 167.14 2.29 o -2 5 2 8.84 2.28 1.13 o -1 5 2 117.77 110.99 1.93 o 0 5 2 516.01 390.05 4.22 o 1 5 2 529.51 488.41 4.40 o 2 5 2 162.53 197.34 5.11 o 3 5 2 114.45 103.50 2.89 o 4 5 2 1167.21 1122.41 9.32 o 5 5 2 443.97 422.89 4.39 o 6 5 2 1.25 3.21 1.43 o 7 5 2 9.70 10.74 4.54 o -7 6 2 35.28 43.59 2.30 o -6 6 2 236.68 241.89 4.76 o -5 6 2 31.78 35.69 1.80 o -4 6 2 35.58 41.46 1.87 o -3 6 2 77.58 111.69 2.84 o -2 6 2 96.47 96.53 3.71 o -1 6 2 15.32 23.74 1.27 o 0 6 2 0.33 0.50 0.91 o 1 6 2 168.31 145.37 4.00 o 2 6 2 17.94 19.62 1.20 o 3 6 2 28.05 28.30 1.18 o 4 6 2 5.68 3.09 1.18 o 5 6 2 1.17 -0.04 1.17 o 6 6 2 0.10 -1.13 1.66 o 7 6 2 0.53 4.44 4.24 o -6 7 2 28.79 21.85 3.80 o -5 7 2 7.81 9.05 1.45 o -4 7 2 84.33 87.49 2.64 o -3 7 2 57.97 82.17 3.72 o -2 7 2 0.69 -0.10 1.23 o -1 7 2 116.01 128.40 2.51 o 0 7 2 315.60 348.69 4.06 o 1 7 2 177.57 176.85 2.78 o 2 7 2 149.15 153.36 4.32 o 3 7 2 114.68 139.36 3.04 o 4 7 2 138.78 147.86 3.21 o 5 7 2 164.71 162.92 3.04 o 6 7 2 63.20 58.23 2.10 o -6 8 2 47.83 47.08 3.35 o -5 8 2 32.84 42.41 2.85 o -4 8 2 425.61 417.75 6.18 o -3 8 2 3.82 1.95 1.49 o -2 8 2 258.98 314.71 4.82 o -1 8 2 48.47 51.58 2.40 o 0 8 2 1049.71 1125.23 10.59 o 1 8 2 7.65 6.55 1.18 o 2 8 2 36.01 47.27 1.77 o 3 8 2 2.90 2.75 1.16 o 4 8 2 36.29 30.40 3.61 o 5 8 2 0.02 0.26 1.18 o 6 8 2 11.69 9.86 1.94 o -5 9 2 0.46 0.65 1.34 o -4 9 2 6.17 12.39 2.05 o -3 9 2 66.37 86.86 3.18 o -2 9 2 1.81 -0.38 1.30 o -1 9 2 77.33 79.85 4.34 o 0 9 2 10.23 9.37 2.05 o 1 9 2 124.60 118.03 3.82 o 2 9 2 2.02 1.10 1.31 o 3 9 2 35.26 34.88 2.34 o 4 9 2 17.97 21.88 1.96 o 5 9 2 18.84 14.32 1.87 o -5 10 2 105.86 98.94 3.91 o -4 10 2 13.99 13.88 1.95 o -3 10 2 114.14 109.12 4.39 o -2 10 2 0.43 0.64 1.64 o -1 10 2 439.84 453.08 6.49 o 0 10 2 104.72 117.11 3.06 o 1 10 2 95.04 110.42 2.65 o 2 10 2 1.83 0.85 1.60 o 3 10 2 36.23 35.37 2.30 o 4 10 2 7.28 9.13 2.13 o -4 11 2 39.72 47.85 2.79 o -3 11 2 11.59 10.68 1.96 o -2 11 2 13.30 15.76 2.11 o -1 11 2 8.56 10.96 2.39 o 0 11 2 88.65 89.09 5.41 o 1 11 2 14.81 12.15 2.46 o 2 11 2 6.80 5.27 1.64 o 3 11 2 5.06 6.78 1.88 o 4 11 2 6.11 8.14 1.91 o -2 12 2 29.49 24.34 3.05 o -1 12 2 1.59 3.02 2.20 o 0 12 2 55.13 48.54 2.74 o 1 12 2 0.69 -0.70 1.85 o 2 12 2 6.82 5.35 2.08 o -7 0 3 44.95 54.65 4.81 o -5 0 3 590.16 676.69 13.44 o -3 0 3 1209.40 1200.47 19.11 o -1 0 3 13558.98 13905.93 236.35 o 1 0 3 1282.98 1465.41 34.97 o 3 0 3 1069.42 1243.56 10.40 o 5 0 3 9.85 16.55 1.46 o 7 0 3 100.62 105.95 2.69 o -8 1 3 5.99 11.26 2.13 o -7 1 3 34.96 40.98 2.66 o -6 1 3 32.78 43.05 3.03 o -5 1 3 1253.70 1255.50 20.88 o -4 1 3 3228.57 3318.68 30.09 o -3 1 3 2820.24 2677.52 32.82 o -2 1 3 786.02 691.16 4.78 o -1 1 3 14660.04 15196.17 170.33 o 0 1 3 12911.75 13468.41 130.96 o 1 1 3 3155.70 3621.35 37.36 o 2 1 3 580.25 577.88 3.47 o 3 1 3 13.96 17.35 1.00 o 4 1 3 109.58 106.51 1.75 o 5 1 3 95.95 90.43 1.37 o 6 1 3 85.62 72.91 1.84 o 7 1 3 1.53 -0.30 1.11 o -7 2 3 0.97 1.78 2.03 o -6 2 3 12.38 8.77 0.92 o -5 2 3 15.58 18.72 1.11 o -4 2 3 242.74 231.99 2.55 o -3 2 3 17.81 9.57 1.65 o -2 2 3 1.84 2.22 0.92 o -1 2 3 66.62 79.21 1.11 o 0 2 3 89.53 58.61 0.83 o 1 2 3 22.93 17.30 0.58 o 2 2 3 0.04 2.59 0.99 o 3 2 3 53.24 50.45 1.28 o 4 2 3 5.90 3.68 0.85 o 5 2 3 39.09 45.99 2.39 o 6 2 3 19.09 23.92 1.08 o 7 2 3 0.31 0.78 0.80 o -7 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