Crystallography Open Database

Information card for entry 2228984

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Structure parameters

Chemical name	Bis(μ~2~-quinoline-2-carboxylato)-κ^3^<i>N</i>,<i>O</i>^1^:<i>O</i>^1^; κ^3^<i>O</i>^1^:<i>N</i>,<i>O</i>^1^-bis[(acetato-κ<i>O</i>)(ethanol- κ<i>O</i>)lead(II)]
Formula	C28 H30 N2 O10 Pb2
Calculated formula	C28 H30 N2 O10 Pb2
SMILES	C(=O)(c1ccc2ccccc2[n]12)[O]1[Pb]2(OC(=O)C)[O](C(=O)c2ccc3ccccc3[n]23)[Pb]13OC(=O)C.OCC.OCC
Title of publication	Bis(μ~2~-quinoline-2-carboxylato)-κ^3^<i>N</i>,<i>O</i>^1^:<i>O</i>^1^;κ^3^<i>O</i>^1^:<i>N</i>,<i>O</i>^1^-bis[(acetato-κ<i>O</i>)(ethanol-κ<i>O</i>)lead(II)]
Authors of publication	Najafi, Ezzatollah; Amini, Mostafa M.; Ng, Seik Weng
Journal of publication	Acta Crystallographica Section E
Year of publication	2011
Journal volume	67
Journal issue	2
Pages of publication	m264
a	7.3419 ± 0.0001 Å
b	8.4004 ± 0.0001 Å
c	23.8008 ± 0.0004 Å
α	90°
β	93.722 ± 0.001°
γ	90°
Cell volume	1464.82 ± 0.04 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0336
Residual factor for significantly intense reflections	0.0294
Weighted residual factors for significantly intense reflections	0.0699
Weighted residual factors for all reflections included in the refinement	0.0732
Goodness-of-fit parameter for all reflections included in the refinement	1.081
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

Version history

Revision	Date	Message	Files
181210 (current)	2016-04-03	hkl/2/22/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22/89.	2228984.cif 2228984.hkl
176789	2016-02-20	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22.	2228984.cif 2228984.hkl
120072	2014-07-11	Adding DOIs to range 2 structures.	2228984.cif 2228984.hkl
88064	2013-08-29	Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet.	2228984.cif 2228984.hkl
26848	2011-09-28	cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree.	2228984.cif 2228984.hkl
14261	2011-03-09	Adding the Fobs data for the recenty deposited IUCr structrures.	2228984.cif 2228984.hkl
12002	2011-03-04	../uploads/cif-deposit/cod/cif Adding structures of 2228984 via cif-deposit CGI script.	2228984.cif