#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/89/2228986.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2228986_Fobs loop_ _publ_author_name 'Zhao, Xi-Zai' 'Jia, Jing-Jing' 'Ou-Yang, Miao' 'Huang, Fu-Ping' 'Jiang, Yi-Min' _publ_section_title ; 1-[2-(Pyrazin-2-ylsulfanyl)ethyl]pyrazine-2(1H)-thione ; _journal_coeditor_code BV2167 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o418 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.628 _cell_angle_gamma 90.000 _cell_length_a 9.7615 _cell_length_b 11.7368 _cell_length_c 10.1289 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.8254 _[local]_cod_data_source_file bv2167Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AA in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 172.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1931.13 2087.64 32.98 o 4 0 0 16886.24 15760.44 210.14 o 6 0 0 2186.41 2187.42 30.50 o 8 0 0 982.08 997.54 16.26 o 10 0 0 131.15 130.03 5.37 o 1 1 0 20.40 25.47 1.14 o 2 1 0 569.87 608.00 6.87 o 3 1 0 14850.29 14753.69 234.00 o 4 1 0 83.27 98.41 3.98 o 5 1 0 160.79 153.89 2.74 o 6 1 0 87.48 93.36 2.01 o 7 1 0 209.93 216.02 4.76 o 8 1 0 29.12 30.83 2.31 o 9 1 0 140.46 149.49 6.05 o 10 1 0 37.79 47.38 2.89 o 11 1 0 19.15 19.89 2.65 o 0 2 0 4710.99 4562.03 77.46 o 1 2 0 409.09 415.63 4.81 o 2 2 0 8.78 10.83 0.55 o 3 2 0 49.13 50.44 1.18 o 4 2 0 0.92 0.81 0.31 o 5 2 0 366.41 384.39 4.51 o 6 2 0 130.74 150.95 2.43 o 7 2 0 17.00 15.90 1.60 o 8 2 0 1.62 0.99 0.59 o 9 2 0 19.48 18.89 2.26 o 10 2 0 75.89 66.00 5.78 o 11 2 0 7.38 5.51 2.10 o 1 3 0 159.06 143.36 2.40 o 2 3 0 1.51 2.20 0.84 o 3 3 0 452.18 465.78 5.74 o 4 3 0 260.32 262.90 4.29 o 5 3 0 1.25 0.37 0.35 o 6 3 0 39.01 38.79 1.29 o 7 3 0 16.83 15.75 1.10 o 8 3 0 152.18 135.73 3.57 o 9 3 0 5.33 5.30 1.14 o 10 3 0 11.15 8.24 2.02 o 11 3 0 3.10 1.75 1.81 o 0 4 0 192.51 203.43 3.98 o 1 4 0 4001.09 3874.66 40.94 o 2 4 0 306.88 333.33 4.14 o 3 4 0 655.67 601.95 8.04 o 4 4 0 188.19 173.35 2.73 o 5 4 0 3035.08 3033.89 44.41 o 6 4 0 249.30 243.62 4.29 o 7 4 0 385.51 376.34 7.51 o 8 4 0 55.98 48.03 2.07 o 9 4 0 66.11 74.32 2.60 o 10 4 0 35.25 43.40 3.00 o 11 4 0 7.04 3.81 1.88 o 1 5 0 118.06 161.86 2.52 o 2 5 0 10446.46 10502.15 211.21 o 3 5 0 1442.61 1499.49 15.96 o 4 5 0 8.78 7.89 0.40 o 5 5 0 34.26 35.28 2.62 o 6 5 0 527.93 491.11 7.61 o 7 5 0 460.37 447.53 8.05 o 8 5 0 301.54 291.81 6.38 o 9 5 0 4.15 4.38 1.14 o 10 5 0 82.72 97.94 3.47 o 11 5 0 55.19 67.95 4.59 o 0 6 0 1789.36 1719.52 30.58 o 1 6 0 37.86 53.58 3.40 o 2 6 0 211.13 253.76 3.22 o 3 6 0 87.07 93.34 1.53 o 4 6 0 388.96 346.15 5.51 o 5 6 0 70.46 80.77 2.24 o 6 6 0 9.64 10.54 1.06 o 7 6 0 5.94 5.81 0.86 o 8 6 0 112.44 111.60 3.15 o 9 6 0 49.51 54.27 6.14 o 10 6 0 7.30 4.05 1.49 o 1 7 0 44.12 70.84 1.67 o 2 7 0 112.49 168.17 2.82 o 3 7 0 98.43 106.85 2.32 o 4 7 0 0.92 1.15 0.59 o 5 7 0 108.50 102.76 2.31 o 6 7 0 102.48 100.85 2.92 o 7 7 0 178.68 163.60 4.44 o 8 7 0 39.04 35.04 3.90 o 9 7 0 1.23 0.12 0.94 o 10 7 0 0.74 0.93 0.96 o 0 8 0 125.54 94.56 2.69 o 1 8 0 307.86 310.98 5.87 o 2 8 0 388.78 422.57 7.23 o 3 8 0 21.75 17.94 1.59 o 4 8 0 47.51 55.37 3.40 o 5 8 0 272.92 260.74 5.35 o 6 8 0 53.53 54.04 1.93 o 7 8 0 0.00 -0.11 0.89 o 8 8 0 1.36 -0.51 0.93 o 9 8 0 10.69 9.49 1.73 o 1 9 0 291.61 279.66 8.00 o 2 9 0 101.85 89.79 2.50 o 3 9 0 1052.56 1019.28 14.52 o 4 9 0 165.68 159.69 3.61 o 5 9 0 586.43 556.00 9.77 o 6 9 0 1.07 -0.01 0.91 o 7 9 0 74.83 74.91 2.90 o 8 9 0 0.30 0.50 0.98 o 9 9 0 2.15 2.33 1.43 o 0 10 0 36.56 16.07 4.15 o 1 10 0 399.47 387.22 7.03 o 2 10 0 42.35 41.03 1.75 o 3 10 0 108.44 96.52 2.83 o 4 10 0 189.63 167.95 3.71 o 5 10 0 579.11 583.83 10.29 o 6 10 0 49.73 48.86 2.57 o 7 10 0 71.03 71.89 2.85 o 8 10 0 8.86 9.07 1.42 o 1 11 0 439.36 416.11 13.09 o 2 11 0 486.89 486.33 9.13 o 3 11 0 51.85 47.97 2.13 o 4 11 0 16.53 20.65 1.66 o 5 11 0 19.36 18.64 1.50 o 6 11 0 110.36 125.48 4.33 o 7 11 0 200.19 204.41 5.36 o 0 12 0 3.75 4.92 2.85 o 1 12 0 9.31 10.11 2.39 o 2 12 0 63.55 57.43 4.12 o 3 12 0 6.07 6.83 1.06 o 4 12 0 134.19 137.32 4.15 o 5 12 0 5.30 6.72 1.30 o 6 12 0 5.35 6.46 1.44 o 1 13 0 33.59 43.21 12.05 o 2 13 0 291.14 280.36 10.95 o 3 13 0 19.53 25.10 3.73 o 4 13 0 4.12 4.26 2.49 o 0 14 0 269.64 287.64 16.58 o 1 14 0 96.22 82.37 18.53 o 2 14 0 4.57 5.18 3.20 o -9 0 1 254.46 259.98 21.51 o -7 0 1 19.58 22.03 2.50 o -5 0 1 553.26 655.69 18.92 o -3 0 1 16057.62 15557.17 206.88 o -1 0 1 2367.36 2449.17 93.81 o 1 0 1 2215.03 2107.56 46.13 o 3 0 1 9370.45 8353.44 496.90 o 5 0 1 1004.34 1031.44 16.11 o 7 0 1 1335.83 1295.83 20.37 o 9 0 1 187.24 180.74 5.37 o 11 0 1 12.74 23.06 5.18 o -11 1 1 52.27 64.78 5.18 o -10 1 1 23.55 29.71 4.51 o -9 1 1 0.03 -0.32 0.62 o -8 1 1 33.96 36.07 2.07 o -7 1 1 102.69 92.90 1.75 o -6 1 1 0.04 0.27 0.32 o -5 1 1 588.46 575.34 6.50 o -4 1 1 769.53 823.64 8.71 o -3 1 1 2737.40 2756.60 28.40 o -2 1 1 10356.06 9747.64 139.83 o -1 1 1 1125.18 1138.75 23.97 o 0 1 1 1148.30 1100.39 15.86 o 1 1 1 4361.21 4034.85 82.91 o 2 1 1 21059.93 18337.05 263.94 o 3 1 1 820.85 845.78 9.14 o 4 1 1 16.47 13.23 0.93 o 5 1 1 246.50 286.99 3.86 o 6 1 1 4737.50 4844.11 47.50 o 7 1 1 341.51 343.70 5.38 o 8 1 1 141.06 149.36 3.86 o 9 1 1 3.80 2.10 1.20 o 10 1 1 233.37 231.93 6.34 o 11 1 1 67.02 66.68 5.45 o -11 2 1 15.50 15.12 2.30 o -10 2 1 6.71 6.39 1.30 o -9 2 1 85.53 83.57 2.74 o -8 2 1 41.66 44.16 4.90 o -7 2 1 179.97 181.90 3.04 o -6 2 1 180.28 179.54 4.26 o -5 2 1 359.23 333.38 4.03 o -4 2 1 947.38 919.83 9.73 o -3 2 1 37.22 33.96 1.17 o -2 2 1 74.38 81.00 1.57 o -1 2 1 1788.18 1790.85 21.75 o 0 2 1 120.93 100.81 1.35 o 1 2 1 1811.35 1954.39 28.33 o 2 2 1 3521.03 3356.44 41.33 o 3 2 1 2265.24 2405.71 23.79 o 4 2 1 9.11 6.65 0.49 o 5 2 1 1253.78 1229.29 12.34 o 6 2 1 178.19 171.51 2.88 o 7 2 1 32.57 31.72 1.50 o 8 2 1 7.28 7.67 1.40 o 9 2 1 640.84 641.12 12.54 o 10 2 1 0.45 -0.76 1.40 o 11 2 1 35.90 41.23 2.84 o -11 3 1 12.31 17.97 5.18 o -10 3 1 0.18 -0.34 1.18 o -9 3 1 105.70 114.70 3.30 o -8 3 1 19.34 20.00 1.45 o -7 3 1 154.98 157.34 3.23 o -6 3 1 94.56 90.95 1.85 o -5 3 1 1048.39 1008.11 10.40 o -4 3 1 124.88 126.86 1.90 o -3 3 1 155.14 143.22 2.10 o -2 3 1 8.75 10.82 0.84 o -1 3 1 10698.47 9598.56 124.94 o 0 3 1 285.38 296.04 3.62 o 1 3 1 867.52 880.95 9.41 o 2 3 1 478.56 491.75 7.13 o 3 3 1 5303.27 5134.48 54.43 o 4 3 1 34.54 34.94 0.96 o 5 3 1 2.19 2.00 0.44 o 6 3 1 3.93 3.25 0.55 o 7 3 1 774.18 756.19 9.17 o 8 3 1 3.82 4.45 1.58 o 9 3 1 38.30 38.43 2.48 o 10 3 1 9.27 15.49 1.81 o 11 3 1 92.02 114.83 5.51 o -11 4 1 1.38 2.38 1.21 o -10 4 1 13.55 14.29 1.50 o -9 4 1 108.24 107.26 3.30 o -8 4 1 201.24 190.49 4.45 o -7 4 1 99.83 102.84 2.82 o -6 4 1 240.49 241.50 3.84 o -5 4 1 738.97 719.81 9.18 o -4 4 1 32.94 34.18 2.73 o -3 4 1 538.94 516.92 7.19 o -2 4 1 170.66 186.73 3.07 o -1 4 1 496.70 524.65 6.80 o 0 4 1 4258.65 4363.10 66.66 o 1 4 1 666.65 638.34 7.14 o 2 4 1 1200.18 1351.16 22.34 o 3 4 1 153.83 174.02 10.59 o 4 4 1 472.01 467.83 5.85 o 5 4 1 738.27 726.24 11.56 o 6 4 1 34.72 36.72 4.13 o 7 4 1 8.71 5.55 0.89 o 8 4 1 133.80 127.13 3.39 o 9 4 1 108.92 108.36 3.63 o 10 4 1 14.41 14.00 2.37 o 11 4 1 11.17 13.03 3.22 o -11 5 1 69.67 70.83 4.15 o -10 5 1 38.87 39.77 4.55 o -9 5 1 0.02 -0.02 0.89 o -8 5 1 9.26 12.68 1.35 o -7 5 1 54.98 52.64 5.32 o -6 5 1 349.29 331.18 4.90 o -5 5 1 87.91 94.03 2.07 o -4 5 1 407.00 417.61 5.89 o -3 5 1 87.33 86.08 2.06 o -2 5 1 12.97 10.09 1.22 o -1 5 1 694.48 816.79 8.94 o 0 5 1 42.16 59.32 1.32 o 1 5 1 247.53 302.73 5.62 o 2 5 1 4.43 5.03 1.31 o 3 5 1 232.03 249.28 3.29 o 4 5 1 508.07 537.51 7.49 o 5 5 1 810.90 807.30 11.71 o 6 5 1 43.91 42.69 4.84 o 7 5 1 30.76 33.14 1.84 o 8 5 1 88.76 86.62 2.67 o 9 5 1 44.08 45.52 3.10 o 10 5 1 0.94 0.63 1.93 o -10 6 1 1.42 2.74 1.09 o -9 6 1 9.48 9.74 1.32 o -8 6 1 101.74 105.63 3.38 o -7 6 1 5.51 5.97 1.35 o -6 6 1 0.35 0.19 0.66 o -5 6 1 5.34 5.14 0.79 o -4 6 1 414.07 399.01 6.27 o -3 6 1 3.85 6.52 0.77 o -2 6 1 34.36 26.00 1.90 o -1 6 1 347.71 390.17 4.85 o 0 6 1 2577.41 2699.28 33.67 o 1 6 1 9.59 9.27 0.73 o 2 6 1 56.36 51.88 3.98 o 3 6 1 163.76 188.64 3.08 o 4 6 1 1665.12 1734.42 23.44 o 5 6 1 54.72 51.71 4.75 o 6 6 1 344.58 340.86 5.85 o 7 6 1 38.81 49.90 3.07 o 8 6 1 355.27 344.67 5.79 o 9 6 1 0.95 -0.94 2.65 o 10 6 1 101.39 95.09 6.00 o -10 7 1 15.24 22.65 1.87 o -9 7 1 40.72 38.27 2.91 o -8 7 1 63.80 57.70 3.81 o -7 7 1 39.39 40.76 2.55 o -6 7 1 423.10 410.44 6.71 o -5 7 1 0.44 -0.43 0.64 o -4 7 1 399.95 396.74 5.72 o -3 7 1 201.37 216.57 3.90 o -2 7 1 1628.28 1534.97 19.84 o -1 7 1 108.31 129.79 1.94 o 0 7 1 771.83 773.52 10.23 o 1 7 1 91.67 122.84 6.35 o 2 7 1 653.50 584.00 11.79 o 3 7 1 223.83 231.25 4.39 o 4 7 1 707.36 664.16 9.41 o 5 7 1 83.18 83.79 2.38 o 6 7 1 363.96 343.57 6.00 o 7 7 1 133.15 117.11 3.18 o 8 7 1 0.22 -0.78 0.97 o 9 7 1 5.50 5.69 1.22 o 10 7 1 1.01 -1.14 1.85 o -9 8 1 8.99 7.48 1.33 o -8 8 1 133.92 132.96 3.64 o -7 8 1 177.07 175.46 4.83 o -6 8 1 8.02 6.96 1.47 o -5 8 1 39.16 39.65 2.58 o -4 8 1 625.04 603.15 9.03 o -3 8 1 719.92 730.11 11.33 o -2 8 1 144.13 130.71 2.31 o -1 8 1 44.14 51.96 1.56 o 0 8 1 678.13 621.00 8.01 o 1 8 1 2354.85 2312.22 42.73 o 2 8 1 390.92 399.10 6.48 o 3 8 1 21.19 22.70 1.19 o 4 8 1 157.85 154.85 3.30 o 5 8 1 286.69 270.46 5.51 o 6 8 1 91.85 90.54 2.93 o 7 8 1 0.08 -0.35 0.96 o 8 8 1 5.46 5.22 1.14 o 9 8 1 26.85 34.48 2.75 o -9 9 1 2.39 4.86 1.30 o -8 9 1 0.49 0.18 0.94 o -7 9 1 125.50 126.66 3.67 o -6 9 1 321.83 317.68 6.12 o -5 9 1 52.82 54.29 3.85 o -4 9 1 18.17 18.87 1.23 o -3 9 1 214.24 215.43 3.63 o -2 9 1 62.41 52.85 1.87 o -1 9 1 25.23 29.48 2.95 o 0 9 1 127.06 126.72 3.01 o 1 9 1 154.48 150.76 3.49 o 2 9 1 356.99 340.99 11.96 o 3 9 1 439.15 449.73 8.25 o 4 9 1 52.62 52.05 6.18 o 5 9 1 3.93 3.71 0.86 o 6 9 1 59.44 55.81 2.28 o 7 9 1 49.93 61.94 2.45 o 8 9 1 94.66 95.35 3.48 o 9 9 1 0.09 -1.47 0.98 o -8 10 1 16.71 15.88 1.78 o -7 10 1 12.15 11.17 1.54 o -6 10 1 16.51 21.69 4.42 o -5 10 1 4.25 3.65 1.29 o -4 10 1 11.96 12.65 1.26 o -3 10 1 87.47 84.71 2.39 o -2 10 1 93.31 93.72 3.38 o -1 10 1 34.93 32.81 2.76 o 0 10 1 103.62 94.07 4.43 o 1 10 1 273.53 268.86 10.53 o 2 10 1 63.69 67.73 2.03 o 3 10 1 0.02 -0.01 0.70 o 4 10 1 0.28 0.83 0.71 o 5 10 1 0.83 -0.11 0.95 o 6 10 1 44.19 45.29 2.99 o 7 10 1 8.54 13.67 1.57 o 8 10 1 2.95 5.63 1.41 o -7 11 1 17.04 19.55 1.73 o -6 11 1 12.42 16.47 2.29 o -5 11 1 118.24 111.86 3.67 o -4 11 1 4.26 4.78 1.03 o -3 11 1 75.66 68.82 3.78 o -2 11 1 120.86 113.73 3.05 o -1 11 1 296.92 294.80 9.02 o 0 11 1 13.53 16.05 3.47 o 1 11 1 76.66 64.05 4.05 o 2 11 1 1.98 0.91 2.02 o 3 11 1 208.56 198.16 4.84 o 4 11 1 109.39 107.96 3.58 o 5 11 1 16.61 18.20 1.49 o 6 11 1 25.85 27.36 2.16 o 7 11 1 49.74 60.09 4.53 o -6 12 1 32.92 39.84 2.10 o -5 12 1 1.81 3.25 1.14 o -4 12 1 454.65 470.86 8.85 o -3 12 1 15.70 22.18 1.42 o -2 12 1 83.79 79.96 4.59 o -1 12 1 47.96 45.41 7.64 o 0 12 1 1054.76 1053.21 26.50 o 1 12 1 1.41 2.70 1.92 o 2 12 1 92.21 84.56 4.27 o 3 12 1 15.56 20.88 2.55 o 4 12 1 591.61 587.96 11.19 o 5 12 1 8.99 14.35 1.57 o 6 12 1 69.53 78.58 4.41 o -4 13 1 26.12 31.66 2.18 o -3 13 1 0.13 0.52 2.85 o -2 13 1 276.45 294.67 9.69 o -1 13 1 4.46 7.47 2.86 o 0 13 1 53.50 57.53 3.94 o 1 13 1 55.87 62.38 7.26 o 2 13 1 239.35 242.94 11.16 o 3 13 1 9.76 8.23 3.17 o 4 13 1 48.91 51.45 4.70 o -1 14 1 1.79 2.30 2.72 o 0 14 1 179.42 183.16 7.83 o 1 14 1 6.02 11.22 3.57 o -10 0 2 29.04 37.06 4.66 o -8 0 2 319.72 315.20 7.08 o -6 0 2 2029.73 2029.71 28.35 o -4 0 2 406.89 394.81 6.21 o -2 0 2 29632.85 25143.66 1051.32 o 2 0 2 141.38 140.98 3.59 o 4 0 2 464.39 505.60 9.21 o 6 0 2 439.63 422.30 12.44 o 8 0 2 1134.59 1111.08 40.53 o 10 0 2 10.32 25.79 6.35 o -11 1 2 20.53 18.92 5.18 o -10 1 2 56.94 62.80 2.33 o -9 1 2 5.78 5.89 0.92 o -8 1 2 105.81 113.99 2.20 o -7 1 2 0.15 0.52 0.40 o -6 1 2 472.44 459.10 5.19 o -5 1 2 609.17 618.93 6.45 o -4 1 2 1044.93 1096.37 10.82 o -3 1 2 914.32 954.44 10.57 o -2 1 2 2836.09 2932.12 33.54 o -1 1 2 2585.23 2395.23 117.08 o 0 1 2 1176.40 1216.04 17.72 o 1 1 2 41.71 43.56 1.28 o 2 1 2 261.14 252.86 3.94 o 3 1 2 34.71 37.33 1.16 o 4 1 2 2011.65 1950.19 20.69 o 5 1 2 1662.32 1768.90 18.22 o 6 1 2 11.85 8.91 0.87 o 7 1 2 4.06 5.43 2.55 o 8 1 2 630.57 612.86 8.99 o 9 1 2 182.78 175.13 4.40 o 10 1 2 33.00 36.97 2.76 o 11 1 2 128.61 125.18 5.67 o -11 2 2 4.74 4.37 1.18 o -10 2 2 0.32 0.62 0.95 o -9 2 2 24.88 25.54 1.61 o -8 2 2 12.37 10.37 0.97 o -7 2 2 4.48 3.77 0.71 o -6 2 2 1.27 1.19 0.40 o -5 2 2 413.31 414.20 4.89 o -4 2 2 751.37 744.88 8.05 o -3 2 2 49.50 40.96 1.95 o -2 2 2 870.15 985.92 11.94 o -1 2 2 227.50 270.72 3.84 o 0 2 2 705.46 741.03 11.33 o 1 2 2 338.69 369.29 6.53 o 2 2 2 130.68 127.59 2.84 o 3 2 2 190.95 185.46 3.75 o 4 2 2 1.19 1.14 0.58 o 5 2 2 209.65 186.17 3.17 o 6 2 2 250.01 224.89 3.65 o 7 2 2 192.28 211.23 5.21 o 8 2 2 231.85 215.90 4.61 o 9 2 2 62.22 63.83 2.90 o 10 2 2 79.09 84.37 4.38 o 11 2 2 21.64 23.66 2.80 o -11 3 2 37.71 41.09 2.34 o -10 3 2 115.71 106.61 4.53 o -9 3 2 23.50 20.86 1.62 o -8 3 2 160.25 152.38 3.29 o -7 3 2 137.91 127.61 3.01 o -6 3 2 410.95 413.11 10.79 o -5 3 2 111.99 115.32 1.74 o -4 3 2 170.42 168.26 2.38 o -3 3 2 8.12 12.43 1.05 o -2 3 2 342.03 319.36 3.93 o -1 3 2 440.07 478.89 5.88 o 0 3 2 1.70 3.35 0.49 o 1 3 2 328.56 367.77 4.77 o 2 3 2 247.40 271.62 5.20 o 3 3 2 760.37 787.83 12.04 o 4 3 2 225.81 219.37 3.92 o 5 3 2 0.25 -0.89 0.65 o 6 3 2 165.20 163.15 3.94 o 7 3 2 71.40 67.07 3.18 o 8 3 2 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