#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/90/2229024.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229024_Fobs loop_ _publ_author_name 'Komarsamy, Lynette' 'Bala, Muhammad D.' 'Friedrich, Holger B.' 'Omondi, Bernard' _publ_section_title ; 2,6-Bis(tosyloxymethyl)pyridine ; _journal_coeditor_code DN2643 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o302 _journal_volume 67 _journal_year 2011 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 21.0320 _cell_length_b 6.2243 _cell_length_c 15.4048 _exptl_crystal_F_000 936.00 _reflns_d_resolution_high 0.7476 _[local]_cod_data_source_file dn2643Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Lynette1 in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 260.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 453.99 400.71 21.15 o 4 0 0 25489.61 23999.94 516.92 o 6 0 0 68016.34 67372.64 1249.02 o 8 0 0 3534.36 3039.12 65.60 o 10 0 0 6835.98 6670.69 132.90 o 12 0 0 0.51 27.19 15.43 o 14 0 0 22.92 -13.53 16.83 o 16 0 0 2842.43 2770.94 69.14 o 18 0 0 6348.58 6616.71 140.84 o 20 0 0 193.72 230.73 28.28 o 22 0 0 4824.81 5354.71 123.73 o 24 0 0 170.57 170.56 36.80 o 26 0 0 626.02 631.66 48.63 o 28 0 0 2.90 27.17 44.61 o 1 1 0 11485.24 13960.69 178.52 o 3 1 0 11042.32 12032.43 160.60 o 5 1 0 53348.55 52734.38 692.93 o 7 1 0 9364.34 8663.63 130.08 o 9 1 0 3871.72 3916.53 61.09 o 11 1 0 12858.19 12772.13 174.20 o 13 1 0 2.29 3.80 11.54 o 15 1 0 2025.09 2036.12 39.52 o 17 1 0 1339.30 1519.28 37.14 o 19 1 0 516.48 475.16 23.93 o 21 1 0 617.18 611.01 26.56 o 23 1 0 926.00 942.15 34.62 o 25 1 0 12.34 6.24 20.56 o 27 1 0 253.76 294.92 27.83 o 0 2 0 6059.92 6852.60 124.93 o 2 2 0 5184.97 6478.69 83.92 o 4 2 0 5079.68 5194.34 71.42 o 6 2 0 1199.05 1368.53 25.92 o 8 2 0 1989.47 1744.77 31.50 o 10 2 0 20.70 58.51 12.10 o 12 2 0 5497.14 5177.15 81.14 o 14 2 0 48.47 34.82 13.69 o 16 2 0 3292.24 3231.60 56.20 o 18 2 0 861.82 894.28 29.05 o 20 2 0 231.51 259.72 20.90 o 22 2 0 406.32 386.28 24.81 o 24 2 0 43.41 27.82 21.91 o 26 2 0 368.17 413.57 28.25 o 1 3 0 2611.23 3463.72 52.30 o 3 3 0 106.25 132.16 11.78 o 5 3 0 1356.66 1518.71 29.57 o 7 3 0 1197.31 1196.73 26.57 o 9 3 0 80.87 72.23 12.02 o 11 3 0 1157.70 1235.39 27.80 o 13 3 0 6.49 -0.58 14.60 o 15 3 0 180.79 195.78 18.70 o 17 3 0 1186.06 1143.44 32.84 o 19 3 0 105.05 119.67 19.61 o 21 3 0 746.15 696.74 29.78 o 23 3 0 1134.05 1203.39 40.30 o 25 3 0 166.58 152.56 26.86 o 0 4 0 609.28 858.23 34.71 o 2 4 0 808.42 1172.27 28.03 o 4 4 0 312.75 462.71 18.15 o 6 4 0 471.39 542.36 22.11 o 8 4 0 418.67 486.58 19.93 o 10 4 0 0.84 -12.67 12.54 o 12 4 0 12.84 22.50 13.77 o 14 4 0 542.63 483.10 23.29 o 16 4 0 0.91 3.38 17.07 o 18 4 0 301.34 360.47 31.25 o 20 4 0 142.56 140.43 22.90 o 22 4 0 28.06 13.45 22.90 o 24 4 0 0.00 38.41 26.44 o 1 5 0 312.46 319.31 21.29 o 3 5 0 258.61 332.53 18.96 o 5 5 0 120.95 107.30 20.60 o 7 5 0 169.80 184.40 17.63 o 9 5 0 450.40 451.27 21.82 o 11 5 0 0.28 -28.26 14.66 o 13 5 0 855.21 815.86 33.27 o 15 5 0 31.62 2.76 19.32 o 17 5 0 5.77 -8.13 20.26 o 19 5 0 122.28 119.94 25.56 o 21 5 0 26.26 -19.05 26.02 o 0 6 0 216.17 296.91 31.49 o 2 6 0 271.62 251.51 20.69 o 4 6 0 2568.09 2610.00 50.68 o 6 6 0 615.16 637.56 27.49 o 8 6 0 268.52 298.19 23.38 o 10 6 0 16.32 0.83 17.46 o 12 6 0 436.95 414.95 27.60 o 14 6 0 5.43 -11.87 21.81 o 16 6 0 146.37 85.33 26.30 o 18 6 0 67.38 95.16 36.51 o 1 7 0 886.37 942.60 42.06 o 3 7 0 323.05 358.66 29.34 o 5 7 0 1860.12 1726.10 64.65 o 7 7 0 445.74 429.90 32.67 o 9 7 0 727.44 721.32 39.34 o 11 7 0 264.76 270.96 30.60 o 13 7 0 90.60 109.43 28.00 o 15 7 0 391.09 333.64 36.37 o 0 8 0 1436.02 1630.51 81.33 o 2 8 0 21.73 13.41 23.94 o 4 8 0 1142.09 1238.41 56.01 o 6 8 0 17.43 -15.53 26.35 o 1 1 1 138.87 189.15 5.23 o 2 1 1 465.59 558.62 8.37 o 3 1 1 17915.15 19649.67 176.66 o 4 1 1 1392.65 1528.18 18.54 o 5 1 1 129.02 114.36 6.69 o 6 1 1 545.61 470.86 9.87 o 7 1 1 629.29 555.33 11.50 o 8 1 1 7473.08 7575.00 77.49 o 9 1 1 2120.68 2183.42 26.47 o 10 1 1 158.47 191.83 9.08 o 11 1 1 296.08 243.32 9.92 o 12 1 1 56.84 54.75 8.58 o 13 1 1 107.10 89.14 9.34 o 14 1 1 479.05 478.40 14.95 o 15 1 1 332.99 367.57 13.18 o 16 1 1 692.09 622.35 16.50 o 17 1 1 3.66 8.75 10.78 o 18 1 1 159.34 131.21 12.28 o 19 1 1 165.38 156.11 12.52 o 20 1 1 240.38 262.36 14.60 o 21 1 1 74.14 95.19 13.31 o 22 1 1 100.10 66.85 13.70 o 23 1 1 48.58 59.65 14.34 o 24 1 1 7.09 9.33 14.18 o 25 1 1 13.61 33.70 15.38 o 26 1 1 382.15 442.02 20.43 o 27 1 1 17.10 61.81 17.48 o 0 2 1 3.80 -6.54 9.47 o 1 2 1 5752.38 6951.32 67.07 o 2 2 1 4425.25 5462.64 51.72 o 3 2 1 964.64 1317.48 17.17 o 4 2 1 2933.82 3210.46 32.68 o 5 2 1 2678.12 2656.47 28.13 o 6 2 1 188.95 161.50 7.91 o 7 2 1 1446.54 1710.04 21.53 o 8 2 1 3.36 11.28 6.98 o 9 2 1 2599.58 2973.12 34.26 o 10 2 1 1467.04 1644.89 23.61 o 11 2 1 82.40 71.35 9.18 o 12 2 1 1571.46 1507.63 23.38 o 13 2 1 5.94 4.48 9.28 o 14 2 1 1132.17 1119.33 20.31 o 15 2 1 1607.00 1647.58 25.51 o 16 2 1 165.50 124.72 11.83 o 17 2 1 3042.83 2907.93 37.50 o 18 2 1 1350.09 1300.71 24.36 o 19 2 1 463.09 459.93 16.62 o 20 2 1 13.19 18.33 12.40 o 21 2 1 1233.86 1234.89 25.63 o 22 2 1 15.91 0.40 12.99 o 23 2 1 32.34 -5.66 13.75 o 24 2 1 146.62 154.81 16.06 o 25 2 1 520.13 560.34 21.07 o 26 2 1 2.42 7.93 16.05 o 27 2 1 31.39 8.89 17.89 o 1 3 1 1212.75 1708.68 22.35 o 2 3 1 41.30 106.01 8.18 o 3 3 1 14.37 23.26 7.41 o 4 3 1 1094.92 1159.10 17.35 o 5 3 1 2575.54 3212.40 34.34 o 6 3 1 89.71 57.77 8.08 o 7 3 1 1947.95 2333.40 27.25 o 8 3 1 1787.42 1842.50 23.98 o 9 3 1 0.69 -4.02 7.90 o 10 3 1 3196.03 3113.84 35.19 o 11 3 1 54.11 37.70 8.40 o 12 3 1 391.35 393.69 12.78 o 13 3 1 0.59 9.13 10.13 o 14 3 1 2371.03 2231.96 31.56 o 15 3 1 933.36 925.29 21.02 o 16 3 1 364.28 345.69 15.34 o 17 3 1 316.49 316.38 15.13 o 18 3 1 1408.95 1336.08 25.66 o 19 3 1 589.62 551.10 18.36 o 20 3 1 9.71 22.45 13.16 o 21 3 1 31.76 46.25 14.09 o 22 3 1 278.84 291.74 17.51 o 23 3 1 253.89 285.40 18.13 o 24 3 1 80.91 136.83 17.41 o 25 3 1 7.20 3.03 16.79 o 26 3 1 181.76 165.93 19.87 o 0 4 1 30.91 71.56 13.74 o 1 4 1 364.20 440.90 13.13 o 2 4 1 39.68 51.64 9.09 o 3 4 1 12.71 33.94 8.77 o 4 4 1 23.56 18.46 8.61 o 5 4 1 1692.68 1812.44 24.83 o 6 4 1 24.41 12.17 8.90 o 7 4 1 8.64 15.41 9.28 o 8 4 1 101.79 114.54 10.27 o 9 4 1 3283.57 3232.77 37.64 o 10 4 1 127.85 166.36 11.21 o 11 4 1 281.42 291.04 12.58 o 12 4 1 774.52 813.22 17.66 o 13 4 1 3910.70 3662.15 44.58 o 14 4 1 114.36 113.51 12.56 o 15 4 1 423.91 354.40 15.50 o 16 4 1 693.01 658.24 19.47 o 17 4 1 999.86 954.03 23.10 o 18 4 1 35.23 41.05 13.89 o 19 4 1 98.53 108.04 14.87 o 20 4 1 70.15 52.19 14.66 o 21 4 1 384.82 419.45 20.98 o 22 4 1 210.43 211.96 18.86 o 23 4 1 21.31 10.95 16.85 o 24 4 1 441.95 443.26 26.42 o 1 5 1 114.34 170.51 12.42 o 2 5 1 2044.56 2247.71 30.09 o 3 5 1 43.61 40.38 10.60 o 4 5 1 77.90 103.39 11.10 o 5 5 1 166.17 169.60 12.14 o 6 5 1 1841.27 1946.77 28.05 o 7 5 1 322.76 370.56 14.25 o 8 5 1 746.78 746.03 17.85 o 9 5 1 122.47 77.94 11.25 o 10 5 1 1425.43 1462.80 25.01 o 11 5 1 799.22 770.24 19.18 o 12 5 1 870.01 859.74 22.10 o 13 5 1 14.21 7.05 12.79 o 14 5 1 47.62 36.44 13.29 o 15 5 1 138.54 117.84 14.71 o 16 5 1 251.82 269.46 17.32 o 17 5 1 9.06 -6.86 14.73 o 18 5 1 47.23 62.08 16.59 o 19 5 1 153.44 108.94 17.79 o 20 5 1 169.90 158.47 19.03 o 21 5 1 18.74 7.59 17.88 o 22 5 1 488.26 506.19 25.08 o 0 6 1 1341.42 1531.10 44.51 o 1 6 1 1245.68 1521.46 28.28 o 2 6 1 14.29 29.88 12.34 o 3 6 1 1291.81 1455.10 27.49 o 4 6 1 247.10 291.96 15.07 o 5 6 1 541.40 648.16 19.75 o 6 6 1 298.17 321.75 16.09 o 7 6 1 264.68 269.05 15.25 o 8 6 1 316.01 352.66 16.21 o 9 6 1 397.67 396.58 16.74 o 10 6 1 26.02 21.79 13.11 o 11 6 1 11.65 -0.25 13.94 o 12 6 1 4.54 16.24 15.03 o 13 6 1 150.90 189.53 17.72 o 14 6 1 54.60 82.23 16.70 o 15 6 1 134.56 130.68 17.61 o 16 6 1 25.22 29.38 17.10 o 17 6 1 382.70 402.12 22.78 o 18 6 1 30.44 49.75 19.08 o 19 6 1 80.41 85.29 20.06 o 1 7 1 5.51 5.53 14.58 o 2 7 1 182.72 194.24 17.50 o 3 7 1 86.18 78.15 16.11 o 4 7 1 91.01 87.06 16.53 o 5 7 1 670.86 650.63 23.99 o 6 7 1 1057.12 1094.37 29.41 o 7 7 1 38.00 39.80 15.44 o 8 7 1 6.27 23.57 15.36 o 9 7 1 20.14 9.08 15.48 o 10 7 1 403.82 418.15 22.68 o 11 7 1 411.75 376.18 22.37 o 12 7 1 360.70 380.65 23.45 o 13 7 1 4.09 -16.24 17.90 o 14 7 1 1.66 -8.50 18.27 o 15 7 1 0.26 10.53 22.80 o 0 8 1 6.01 24.53 25.99 o 1 8 1 58.93 54.70 18.70 o 2 8 1 327.59 396.58 23.61 o 3 8 1 18.67 -7.91 17.93 o 4 8 1 356.49 428.98 28.11 o 5 8 1 318.14 313.13 23.63 o 6 8 1 46.36 54.68 19.84 o 7 8 1 12.84 -5.30 30.47 o 0 0 2 7956.58 7361.13 166.14 o 1 0 2 8.45 7.94 4.61 o 2 0 2 4419.17 4341.84 46.31 o 3 0 2 11674.43 10920.04 114.92 o 4 0 2 40844.26 38474.73 485.25 o 5 0 2 12942.24 12948.06 165.19 o 6 0 2 6433.75 6668.89 84.50 o 7 0 2 186.13 147.92 9.10 o 8 0 2 353.09 438.54 12.63 o 9 0 2 510.16 379.74 12.40 o 10 0 2 1444.44 1326.13 25.03 o 11 0 2 8412.42 8577.63 114.43 o 12 0 2 2276.10 2389.85 38.74 o 13 0 2 1593.48 1799.17 32.42 o 14 0 2 22.44 33.05 11.01 o 15 0 2 204.17 225.49 14.46 o 16 0 2 33.45 23.40 15.20 o 17 0 2 265.64 259.23 16.16 o 18 0 2 2574.52 2575.25 48.32 o 19 0 2 26.96 20.47 16.03 o 20 0 2 851.59 848.74 28.72 o 21 0 2 0.67 -7.38 16.81 o 22 0 2 1028.84 1050.94 39.05 o 23 0 2 54.14 38.95 20.32 o 24 0 2 276.81 275.64 25.66 o 25 0 2 142.43 105.19 24.05 o 26 0 2 305.48 343.78 40.46 o 27 0 2 2.97 -19.72 23.49 o 28 0 2 26.65 50.58 72.33 o 1 1 2 19805.22 20863.24 163.81 o 2 1 2 10932.16 11535.69 95.74 o 3 1 2 7163.90 7248.22 63.20 o 4 1 2 2809.70 2855.78 29.22 o 5 1 2 77.37 130.72 6.71 o 6 1 2 411.58 464.87 10.65 o 7 1 2 4147.74 3959.74 40.75 o 8 1 2 1866.54 1949.46 23.90 o 9 1 2 761.22 679.40 13.04 o 10 1 2 1390.57 1437.56 19.96 o 11 1 2 630.79 510.30 12.18 o 12 1 2 2563.01 2682.38 31.68 o 13 1 2 170.43 173.75 9.94 o 14 1 2 1164.89 1054.31 19.11 o 15 1 2 1952.52 1828.84 25.06 o 16 1 2 468.77 501.26 14.16 o 17 1 2 38.33 31.87 10.29 o 18 1 2 7.25 -2.88 10.15 o 19 1 2 1700.16 1789.44 27.03 o 20 1 2 1147.94 1138.85 23.03 o 21 1 2 134.00 123.73 13.76 o 22 1 2 36.56 43.59 13.67 o 23 1 2 297.09 307.08 17.32 o 24 1 2 54.02 50.10 14.87 o 25 1 2 105.33 117.03 16.63 o 26 1 2 50.77 61.24 17.16 o 27 1 2 237.30 274.27 21.30 o 0 2 2 9.21 -6.73 8.97 o 1 2 2 58.70 50.37 6.44 o 2 2 2 45.81 56.33 6.51 o 3 2 2 550.55 653.26 11.83 o 4 2 2 1087.23 1150.81 16.02 o 5 2 2 709.95 703.20 12.04 o 6 2 2 1653.86 1798.33 22.05 o 7 2 2 1310.31 1405.68 19.04 o 8 2 2 8552.86 8950.48 85.93 o 9 2 2 677.60 603.71 12.74 o 10 2 2 1389.21 1511.69 21.62 o 11 2 2 9.34 2.31 7.51 o 12 2 2 2461.12 2338.87 30.82 o 13 2 2 158.27 138.74 10.56 o 14 2 2 2025.36 2131.96 29.58 o 15 2 2 213.01 219.80 12.12 o 16 2 2 801.82 747.76 18.04 o 17 2 2 0.33 3.20 10.84 o 18 2 2 66.68 68.30 11.82 o 19 2 2 0.02 13.07 11.61 o 20 2 2 2.02 -4.64 11.56 o 21 2 2 12.24 25.75 12.40 o 22 2 2 73.48 78.03 14.03 o 23 2 2 29.50 9.24 13.83 o 24 2 2 6.58 20.09 15.08 o 25 2 2 79.49 110.87 17.18 o 26 2 2 87.62 117.09 18.82 o 27 2 2 49.01 50.97 17.78 o 1 3 2 238.98 265.92 9.68 o 2 3 2 33.99 50.86 7.57 o 3 3 2 1217.53 1393.01 19.01 o 4 3 2 137.75 156.07 8.36 o 5 3 2 381.99 501.79 11.46 o 6 3 2 1865.00 2124.19 24.92 o 7 3 2 2503.82 2559.37 29.67 o 8 3 2 0.02 -4.37 7.64 o 9 3 2 26.89 13.25 8.04 o 10 3 2 82.99 86.32 8.93 o 11 3 2 474.34 449.43 12.82 o 12 3 2 1224.18 1261.14 21.30 o 13 3 2 9.31 10.23 9.19 o 14 3 2 48.56 50.40 11.41 o 15 3 2 584.25 612.81 17.39 o 16 3 2 444.81 415.02 15.30 o 17 3 2 280.77 272.66 14.57 o 18 3 2 3.82 17.69 12.02 o 19 3 2 107.54 119.44 14.20 o 20 3 2 0.08 12.71 13.28 o 21 3 2 2.17 -8.11 13.18 o 22 3 2 158.22 182.43 16.10 o 23 3 2 125.61 130.03 16.47 o 24 3 2 10.33 22.09 16.22 o 25 3 2 67.83 79.80 17.96 o 26 3 2 2.49 -22.21 20.18 o 0 4 2 150.14 187.45 14.81 o 1 4 2 100.34 89.90 9.46 o 2 4 2 254.39 279.83 11.26 o 3 4 2 3.45 2.76 8.35 o 4 4 2 104.24 117.61 9.78 o 5 4 2 35.84 61.53 9.05 o 6 4 2 615.49 681.06 14.96 o 7 4 2 19.29 16.45 9.05 o 8 4 2 60.77 83.57 10.02 o 9 4 2 949.43 988.65 18.91 o 10 4 2 18.26 -1.24 9.54 o 11 4 2 210.19 186.21 11.64 o 12 4 2 173.28 166.71 11.75 o 13 4 2 1.42 -18.27 10.63 o 14 4 2 33.61 49.05 11.99 o 15 4 2 595.51 561.55 18.44 o 16 4 2 10.04 8.38 12.60 o 17 4 2 77.74 72.55 13.80 o 18 4 2 105.73 95.08 14.55 o 19 4 2 420.67 419.72 18.86 o 20 4 2 32.73 36.18 14.93 o 21 4 2 8.47 -16.04 14.96 o 22 4 2 181.95 185.16 17.94 o 23 4 2 10.54 9.49 16.95 o 24 4 2 427.06 435.76 24.88 o 1 5 2 37.10 58.34 11.15 o 2 5 2 808.35 931.97 19.63 o 3 5 2 1587.34 1707.22 25.92 o 4 5 2 46.93 62.57 11.01 o 5 5 2 253.73 293.49 13.25 o 6 5 2 19.58 6.36 10.19 o 7 5 2 1203.58 1268.41 22.55 o 8 5 2 1.56 -12.89 10.30 o 9 5 2 208.90 207.06 13.32 o 10 5 2 36.65 35.74 11.35 o 11 5 2 70.23 76.94 12.20 o 12 5 2 838.17 833.71 20.53 o 13 5 2 3.41 -7.94 12.47 o 14 5 2 155.10 154.74 15.26 o 15 5 2 91.84 110.25 15.06 o 16 5 2 40.81 65.51 15.28 o 17 5 2 356.91 318.22 22.33 o 18 5 2 111.50 131.22 17.28 o 19 5 2 37.32 40.08 16.84 o 20 5 2 101.85 94.85 18.52 o 21 5 2 72.03 61.48 19.30 o 22 5 2 242.50 301.55 22.59 o 0 6 2 608.49 700.67 27.99 o 1 6 2 31.74 27.94 12.57 o 2 6 2 176.37 210.18 14.76 o 3 6 2 97.83 111.71 13.46 o 4 6 2 91.73 115.34 13.70 o 5 6 2 152.59 144.56 13.63 o 6 6 2 2.57 -14.51 11.87 o 7 6 2 739.70 807.17 21.80 o 8 6 2 1151.92 1211.14 26.12 o 9 6 2 69.88 66.95 13.99 o 10 6 2 14.13 -9.24 13.11 o 11 6 2 5.96 -2.65 13.23 o 12 6 2 184.81 163.19 16.63 o 13 6 2 36.52 30.53 15.42 o 14 6 2 579.90 593.66 23.63 o 15 6 2 0.24 4.53 15.95 o 16 6 2 96.57 85.19 17.70 o 17 6 2 34.23 34.10 17.31 o 18 6 2 99.83 97.62 19.32 o 19 6 2 34.12 37.83 19.95 o 1 7 2 207.11 243.49 17.63 o 2 7 2 126.55 138.21 16.25 o 3 7 2 124.35 115.96 16.66 o 4 7 2 1.71 6.22 14.92 o 5 7 2 710.64 748.16 24.26 o 6 7 2 158.90 187.70 17.50 o 7 7 2 1.31 -11.72 14.76 o 8 7 2 136.19 131.93 17.71 o 9 7 2 158.90 114.19 17.00 o 10 7 2 0.11 -5.34 16.38 o 11 7 2 54.18 21.85 17.11 o 12 7 2 0.12 -21.99 17.16 o 13 7 2 27.87 39.91 19.38 o 14 7 2 4.11 -7.92 21.32 o 0 8 2 361.21 468.79 32.82 o 1 8 2 3.45 -4.92 17.78 o 2 8 2 0.89 -5.96 18.16 o 3 8 2 89.84 81.87 19.06 o 4 8 2 206.55 233.88 21.13 o 5 8 2 3.80 -22.12 18.51 o 6 8 2 0.37 -36.29 18.15 o 7 8 2 119.51 133.31 45.99 o 1 1 3 450.54 504.38 8.12 o 2 1 3 10076.76 10488.20 101.61 o 3 1 3 7934.07 8247.19 69.13 o 4 1 3 3417.92 3502.35 32.37 o 5 1 3 1588.01 1648.94 18.50 o 6 1 3 1025.58 950.61 14.32 o 7 1 3 72.62 80.59 6.46 o 8 1 3 147.64 166.26 7.66 o 9 1 3 10.57 15.28 6.90 o 10 1 3 363.21 405.59 10.73 o 11 1 3 596.65 618.09 12.51 o 12 1 3 129.99 162.13 8.89 o 13 1 3 19.84 -9.39 7.88 o 14 1 3 518.32 538.49 13.41 o 15 1 3 1927.19 1843.79 25.29 o 16 1 3 837.68 842.75 17.41 o 17 1 3 183.52 176.36 11.44 o 18 1 3 12.75 22.87 10.30 o 19 1 3 702.31 713.76 17.66 o 20 1 3 150.88 155.16 13.39 o 21 1 3 118.65 119.10 13.73 o 22 1 3 0.06 -11.82 13.02 o 23 1 3 49.35 58.01 14.47 o 24 1 3 171.47 209.20 17.50 o 25 1 3 19.57 -11.06 15.63 o 26 1 3 90.63 140.81 19.74 o 27 1 3 35.00 58.48 19.54 o 0 2 3 2080.79 2137.71 30.95 o 1 2 3 2508.56 2592.53 25.48 o 2 2 3 624.31 592.48 10.11 o 3 2 3 4732.27 5131.78 46.98 o 4 2 3 568.62 616.00 10.51 o 5 2 3 250.43 255.56 8.16 o 6 2 3 2686.16 2972.66 32.06 o 7 2 3 2297.76 2355.98 26.88 o 8 2 3 1765.90 1682.96 21.55 o 9 2 3 148.29 115.58 7.94 o 10 2 3 35.51 25.26 7.59 o 11 2 3 350.82 355.27 11.34 o 12 2 3 102.78 96.18 9.86 o 13 2 3 258.52 282.75 13.58 o 14 2 3 2962.63 2976.65 37.10 o 15 2 3 2.99 -19.74 9.87 o 16 2 3 2503.10 2366.30 32.21 o 17 2 3 129.57 124.27 11.77 o 18 2 3 140.57 146.09 12.25 o 19 2 3 150.56 143.09 12.59 o 20 2 3 50.17 45.64 12.21 o 21 2 3 508.74 500.65 17.57 o 22 2 3 448.24 494.51 19.31 o 23 2 3 0.45 27.63 14.50 o 24 2 3 199.87 203.77 18.19 o 25 2 3 171.74 219.60 18.85 o 26 2 3 23.00 -2.11 17.93 o 27 2 3 25.78 71.40 49.51 o 1 3 3 510.45 600.71 11.85 o 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7 5171.52 5285.34 62.12 o 2 1 7 7.49 -14.76 7.38 o 3 1 7 4697.99 5255.29 62.30 o 4 1 7 2004.29 1857.37 25.25 o 5 1 7 1814.04 1724.14 21.37 o 6 1 7 27.42 22.27 5.84 o 7 1 7 370.72 422.23 9.74 o 8 1 7 5.20 17.53 6.92 o 9 1 7 219.50 266.58 9.25 o 10 1 7 12.47 6.29 6.75 o 11 1 7 32.19 20.25 7.15 o 12 1 7 268.17 267.40 10.10 o 13 1 7 94.78 109.21 9.98 o 14 1 7 663.86 593.92 15.96 o 15 1 7 277.09 292.04 13.24 o 16 1 7 128.73 131.72 12.74 o 17 1 7 143.82 151.51 13.32 o 18 1 7 332.22 335.68 16.07 o 19 1 7 20.03 29.65 12.95 o 20 1 7 1.62 6.84 14.06 o 21 1 7 146.33 166.37 16.51 o 22 1 7 0.00 6.84 15.08 o 23 1 7 485.11 565.49 23.56 o 24 1 7 70.96 55.48 17.73 o 25 1 7 7.95 9.04 17.64 o 26 1 7 1.51 17.96 18.53 o 0 2 7 7997.65 7853.31 104.33 o 1 2 7 973.22 898.17 13.70 o 2 2 7 5368.05 5735.39 55.25 o 3 2 7 0.48 -11.89 5.94 o 4 2 7 1245.66 1121.22 15.83 o 5 2 7 607.26 615.94 12.35 o 6 2 7 92.37 98.85 8.09 o 7 2 7 1.09 1.77 8.15 o 8 2 7 7756.27 7581.10 81.24 o 9 2 7 27.97 19.29 8.20 o 10 2 7 53.46 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