#------------------------------------------------------------------------------ #$Date: 2016-04-03 05:01:52 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181213 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/92/2229223.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229223_Fobs loop_ _publ_author_name 'Pojarov\'a, Michaela' 'Du\tert-butyl-31,32,33,34,35-pentapropoxycalix[5]arene dichloromethane hemisolvate ; _journal_coeditor_code SJ5077 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o296 _journal_page_last o297 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _audit_creation_date 10-12-17 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 91.7460(5) _cell_angle_gamma 90 _cell_length_a 12.3740(2) _cell_length_b 23.9130(2) _cell_length_c 43.6550(5) _cod_data_source_file sj5077Isup2.hkl _cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 1 0 0 83816.51 0.00 2050.56 x 2 0 0 53424.27 0.00 736.82 x 3 0 0 6557.89 5911.82 114.62 o 4 0 0 1531.47 1108.08 41.46 o 5 0 0 309.36 205.03 25.08 o 6 0 0 11641.43 9885.33 254.67 o 7 0 0 9267.58 8225.23 261.28 o 8 0 0 1245.80 1201.98 70.72 o 9 0 0 888.37 971.25 73.86 o 10 0 0 6965.49 6687.14 246.30 o 11 0 0 1000.89 1265.63 78.39 o 12 0 0 2564.77 2450.38 143.53 o 13 0 0 390.88 400.80 90.93 o 14 0 0 0.00 22.20 0.06 o 1 1 0 122158.04 0.00 2056.95 x 2 1 0 22088.45 0.00 229.55 x 3 1 0 7129.05 6165.56 91.64 o 4 1 0 17.59 16.71 28.60 o 5 1 0 204.15 153.18 18.52 o 6 1 0 13603.33 11627.00 204.47 o 7 1 0 13315.57 12490.25 245.63 o 8 1 0 3376.84 3277.81 89.85 o 9 1 0 1069.52 1117.40 50.55 o 10 1 0 191.61 321.44 40.07 o 11 1 0 1776.56 1501.79 75.50 o 12 1 0 -52.08 91.66 55.71 o 13 1 0 22.47 124.37 95.97 o 14 1 0 -71.07 5.95 80.09 o 1 2 0 3247.59 0.00 38.06 x 2 2 0 4142.75 0.00 51.18 x 3 2 0 32461.09 31685.07 324.26 o 4 2 0 5504.74 5708.86 74.27 o 5 2 0 1198.60 1454.45 30.35 o 6 2 0 256.41 387.31 24.38 o 7 2 0 4219.22 5053.60 89.75 o 8 2 0 2282.93 2037.60 69.86 o 9 2 0 909.10 717.45 47.67 o 10 2 0 659.48 747.18 48.16 o 11 2 0 841.51 724.88 54.45 o 12 2 0 289.15 482.27 44.53 o 13 2 0 -22.64 34.77 108.72 o 14 2 0 253.97 242.34 86.40 o 1 3 0 332.70 0.00 10.00 x 2 3 0 41.63 16.17 11.13 o 3 3 0 54026.61 56166.44 524.15 o 4 3 0 3230.87 3418.10 45.13 o 5 3 0 3237.83 4104.94 59.39 o 6 3 0 28049.56 26701.07 392.50 o 7 3 0 767.30 471.02 35.04 o 8 3 0 311.45 295.06 33.14 o 9 3 0 298.21 350.05 38.87 o 10 3 0 278.01 236.25 42.39 o 11 3 0 50.51 7.13 67.42 o 12 3 0 1802.34 1964.86 83.17 o 13 3 0 55.57 92.80 67.46 o 14 3 0 711.74 520.51 85.15 o 0 4 0 7687.68 0.00 109.99 x 1 4 0 15687.33 0.00 167.27 x 2 4 0 9081.02 8286.82 99.49 o 3 4 0 18.99 32.82 19.20 o 4 4 0 3678.01 3849.30 50.87 o 5 4 0 3977.44 3914.72 76.41 o 6 4 0 13370.96 11083.87 213.67 o 7 4 0 6.97 1.95 15.57 o 8 4 0 2809.50 2817.28 79.57 o 9 4 0 386.35 417.48 41.04 o 10 4 0 469.27 627.92 50.64 o 11 4 0 2340.06 2558.79 88.81 o 12 4 0 520.83 431.49 77.90 o 13 4 0 234.98 132.76 73.96 o 14 4 0 66.19 1.10 74.89 o 1 5 0 42981.95 43525.24 415.66 o 2 5 0 37388.90 38344.16 395.44 o 3 5 0 4683.78 5200.46 60.05 o 4 5 0 21721.60 20245.36 233.95 o 5 5 0 78.21 234.98 21.91 o 6 5 0 650.42 495.40 31.15 o 7 5 0 5820.19 6524.60 112.07 o 8 5 0 112.70 75.82 26.09 o 9 5 0 226.97 136.62 39.29 o 10 5 0 1823.59 1632.06 69.50 o 11 5 0 238.64 120.87 54.04 o 12 5 0 -87.09 3.48 67.22 o 13 5 0 -15.68 10.54 108.60 o 0 6 0 121476.27 126344.21 2468.61 o 1 6 0 1608.47 1625.13 23.40 o 2 6 0 135.17 10.27 9.61 o 3 6 0 3746.47 3892.59 51.34 o 4 6 0 469.27 230.54 17.28 o 5 6 0 5775.95 5446.44 131.69 o 6 6 0 3.48 51.84 10.94 o 7 6 0 27.70 53.45 84.08 o 8 6 0 240.38 275.23 41.63 o 9 6 0 212.86 169.77 52.09 o 10 6 0 516.30 552.75 63.25 o 11 6 0 13.94 10.20 75.84 o 12 6 0 116.71 235.92 57.09 o 13 6 0 226.10 214.73 84.27 o 1 7 0 15101.36 14500.52 154.16 o 2 7 0 1912.95 1891.74 27.53 o 3 7 0 5283.52 5931.91 69.77 o 4 7 0 791.34 340.22 22.48 o 5 7 0 6382.83 6274.50 113.85 o 6 7 0 1763.67 1656.10 62.20 o 7 7 0 587.89 565.36 48.53 o 8 7 0 5460.84 5443.58 136.40 o 9 7 0 317.20 255.40 51.52 o 10 7 0 984.52 790.51 80.37 o 11 7 0 -5.40 75.54 74.84 o 12 7 0 1078.93 1140.91 84.21 o 13 7 0 -18.99 20.62 114.27 o 0 8 0 2781.28 3273.35 48.41 o 1 8 0 650.08 501.44 13.83 o 2 8 0 354.65 454.53 12.57 o 3 8 0 2036.28 2196.93 39.57 o 4 8 0 135.17 179.72 15.23 o 5 8 0 389.84 276.39 24.20 o 6 8 0 12457.69 12714.29 248.79 o 7 8 0 2073.03 2257.29 74.31 o 8 8 0 93.89 32.02 43.30 o 9 8 0 468.05 356.17 48.01 o 10 8 0 7662.25 6732.21 227.08 o 11 8 0 1746.95 1968.34 91.63 o 12 8 0 242.65 50.83 61.27 o 13 8 0 107.65 31.22 80.36 o 1 9 0 604.26 856.59 14.41 o 2 9 0 2740.87 3103.94 39.53 o 3 9 0 23045.97 23467.89 285.61 o 4 9 0 2891.55 2578.05 52.22 o 5 9 0 1580.60 1500.65 47.84 o 6 9 0 1465.46 1382.47 44.95 o 7 9 0 862.76 757.27 51.73 o 8 9 0 3172.16 2996.22 109.57 o 9 9 0 1741.55 1751.62 79.19 o 10 9 0 1583.56 1707.26 90.92 o 11 9 0 864.50 1101.51 74.17 o 12 9 0 106.26 4.81 97.05 o 13 9 0 73.33 149.17 69.38 o 0 10 0 19946.61 20694.87 265.28 o 1 10 0 300.13 132.06 11.00 o 2 10 0 11495.46 9973.85 149.21 o 3 10 0 13796.33 13655.06 187.46 o 4 10 0 61.31 0.95 13.85 o 5 10 0 3085.07 3633.44 74.25 o 6 10 0 330.79 312.81 25.92 o 7 10 0 548.87 400.61 38.54 o 8 10 0 325.39 291.67 49.74 o 9 10 0 59.40 1.60 91.45 o 10 10 0 5493.76 5242.19 186.98 o 11 10 0 384.44 346.25 73.55 o 12 10 0 155.20 0.17 91.19 o 13 10 0 95.98 48.50 65.37 o 1 11 0 751.80 843.32 20.73 o 2 11 0 3393.91 2689.91 53.64 o 3 11 0 348.90 283.75 17.12 o 4 11 0 264.42 205.48 16.33 o 5 11 0 -17.42 0.93 48.65 o 6 11 0 212.69 216.05 27.07 o 7 11 0 258.67 215.68 45.48 o 8 11 0 352.21 370.41 44.83 o 9 11 0 1106.28 1226.42 71.67 o 10 11 0 347.86 385.99 61.49 o 11 11 0 -38.15 0.62 62.09 o 12 11 0 240.38 275.04 60.68 o 13 11 0 412.31 329.99 112.58 o 0 12 0 3184.01 2445.19 63.59 o 1 12 0 5452.13 5716.40 80.32 o 2 12 0 57.48 15.60 15.83 o 3 12 0 766.43 642.12 23.15 o 4 12 0 2661.09 2377.85 54.36 o 5 12 0 2982.82 3099.47 68.50 o 6 12 0 -17.24 1.25 53.49 o 7 12 0 157.12 308.22 37.04 o 8 12 0 123.67 163.30 48.30 o 9 12 0 134.47 162.19 57.85 o 10 12 0 29.79 24.58 163.74 o 11 12 0 203.10 294.61 72.95 o 12 12 0 31.18 62.23 281.31 o 1 13 0 31.35 60.49 27.01 o 2 13 0 561.76 584.12 19.97 o 3 13 0 2618.76 2685.67 47.13 o 4 13 0 31.35 35.61 38.78 o 5 13 0 97.20 59.85 19.48 o 6 13 0 1656.37 1816.04 68.41 o 7 13 0 2394.41 2623.45 73.69 o 8 13 0 6316.29 5913.72 177.14 o 9 13 0 1192.85 1227.64 73.53 o 10 13 0 448.02 336.65 71.34 o 11 13 0 580.40 531.26 74.36 o 12 13 0 41.63 10.46 77.43 o 0 14 0 784.55 617.61 31.56 o 1 14 0 1803.56 1846.96 39.05 o 2 14 0 269.47 255.27 17.12 o 3 14 0 4022.56 3979.20 71.47 o 4 14 0 18.99 16.52 27.09 o 5 14 0 117.93 146.39 28.91 o 6 14 0 -12.19 10.64 39.52 o 7 14 0 381.65 422.37 54.06 o 8 14 0 22.47 110.76 57.68 o 9 14 0 121.93 271.34 42.41 o 10 14 0 611.75 502.66 77.26 o 11 14 0 313.19 256.21 71.29 o 12 14 0 17.59 22.83 105.10 o 1 15 0 -1.74 6.44 6.26 o 2 15 0 31.35 43.12 34.82 o 3 15 0 2063.62 2061.80 49.58 o 4 15 0 55.91 80.92 32.69 o 5 15 0 303.26 251.16 26.37 o 6 15 0 1133.97 1183.18 43.64 o 7 15 0 137.44 77.86 43.30 o 8 15 0 1303.81 1627.23 77.10 o 9 15 0 268.08 256.96 49.95 o 10 15 0 469.27 169.02 74.71 o 11 15 0 109.74 31.99 73.77 o 0 16 0 449.23 390.61 27.43 o 1 16 0 64.28 128.68 14.90 o 2 16 0 682.30 652.61 24.02 o 3 16 0 22.47 58.12 48.48 o 4 16 0 1321.92 1128.16 45.65 o 5 16 0 1722.56 1758.37 53.58 o 6 16 0 651.12 800.99 37.12 o 7 16 0 346.29 499.49 33.14 o 8 16 0 1865.40 1794.39 63.24 o 9 16 0 286.19 213.70 53.82 o 10 16 0 155.20 185.26 70.59 o 11 16 0 228.54 202.75 77.75 o 1 17 0 198.92 184.95 20.92 o 2 17 0 194.74 146.66 22.26 o 3 17 0 -15.85 6.72 38.47 o 4 17 0 99.46 40.31 23.66 o 5 17 0 469.27 523.75 31.61 o 6 17 0 886.80 955.24 44.92 o 7 17 0 18.99 80.20 60.70 o 8 17 0 648.68 737.82 59.39 o 9 17 0 242.30 338.28 44.59 o 10 17 0 132.56 142.91 69.80 o 11 17 0 48.42 149.49 78.35 o 0 18 0 149.45 143.55 42.69 o 1 18 0 394.71 391.23 34.63 o 2 18 0 1711.93 1625.89 57.16 o 3 18 0 753.54 861.93 36.45 o 4 18 0 665.75 759.92 38.81 o 5 18 0 1025.28 1212.03 44.29 o 6 18 0 868.86 882.38 45.41 o 7 18 0 52.08 61.62 19.34 o 8 18 0 756.68 715.29 49.40 o 9 18 0 219.83 323.98 71.19 o 10 18 0 78.39 64.18 61.63 o 1 19 0 53.82 2.66 34.81 o 2 19 0 1145.99 1131.43 54.17 o 3 19 0 102.60 57.05 30.62 o 4 19 0 55.57 96.70 54.63 o 5 19 0 78.39 7.20 41.36 o 6 19 0 846.91 888.44 80.20 o 7 19 0 1630.41 1413.86 93.06 o 8 19 0 696.24 789.64 75.61 o 9 19 0 48.95 93.01 124.04 o 10 19 0 171.93 77.00 84.26 o 0 20 0 296.12 211.13 54.50 o 1 20 0 101.20 52.31 30.80 o 2 20 0 79.95 37.49 28.84 o 3 20 0 315.28 233.88 41.68 o 4 20 0 1970.26 1661.00 93.13 o 5 20 0 2891.72 2614.13 135.07 o 6 20 0 850.74 977.10 72.65 o 7 20 0 90.75 51.69 57.98 o 8 20 0 177.32 199.79 71.01 o 9 20 0 263.37 129.44 95.34 o 1 21 0 2229.63 2478.09 70.78 o 2 21 0 826.18 826.09 48.02 o 3 21 0 132.56 114.33 30.14 o 4 21 0 275.22 215.74 49.74 o 5 21 0 64.45 15.12 51.19 o 6 21 0 381.65 440.36 64.80 o 7 21 0 204.15 265.84 56.59 o 8 21 0 85.53 64.24 92.19 o 9 21 0 194.92 218.10 78.91 o 0 22 0 3578.55 3734.47 148.72 o 1 22 0 93.89 110.71 28.60 o 2 22 0 48.77 105.98 52.49 o 3 22 0 121.76 161.17 48.18 o 4 22 0 231.32 209.51 56.20 o 5 22 0 215.65 204.33 55.19 o 6 22 0 314.41 250.81 63.46 o 7 22 0 381.82 359.24 71.13 o 8 22 0 52.26 40.29 88.39 o 1 23 0 2950.60 2817.91 100.00 o 2 23 0 140.75 101.19 49.10 o 3 23 0 724.45 552.36 67.40 o 4 23 0 636.66 716.77 68.68 o 5 23 0 74.90 150.16 53.32 o 6 23 0 120.19 95.27 55.07 o 7 23 0 224.18 131.73 72.31 o 0 24 0 -88.84 9.39 58.64 o 1 24 0 102.95 88.68 58.06 o 2 24 0 379.38 374.46 58.03 o 3 24 0 355.00 499.64 65.46 o 4 24 0 550.44 509.30 66.85 o 5 24 0 240.56 200.68 60.58 o 6 24 0 913.28 813.53 89.72 o 1 25 0 31.18 0.99 86.17 o 2 25 0 -36.58 15.23 54.94 o 3 25 0 -52.26 0.15 86.34 o 4 25 0 45.29 88.43 48.49 o 5 25 0 119.67 109.34 62.13 o 0 26 0 -229.93 17.22 114.62 o 1 26 0 354.65 291.13 93.37 o 2 26 0 46.86 26.21 53.62 o 3 26 0 57.66 5.21 65.53 o 4 26 0 398.02 339.95 77.77 o 1 27 0 -153.64 18.93 73.16 o 2 27 0 38.32 37.21 73.16 o -14 1 1 -39.89 7.43 82.58 o -13 1 1 214.78 210.72 49.55 o -12 1 1 588.41 745.46 52.47 o -11 1 1 304.83 334.89 44.54 o -10 1 1 736.82 624.57 49.93 o -9 1 1 73.16 12.71 46.90 o -8 1 1 354.30 222.89 37.05 o -7 1 1 -1.74 6.17 12.90 o -6 1 1 102.60 1.69 18.65 o -5 1 1 6.97 0.45 13.60 o -4 1 1 6.97 104.76 9.85 o -3 1 1 6838.51 5705.82 82.77 o -2 1 1 30782.07 0.00 307.56 x -1 1 1 21.08 0.00 5.96 x 1 1 1 13226.73 0.00 144.28 x 2 1 1 1305.03 0.00 21.19 x 3 1 1 24354.30 24338.06 260.51 o 4 1 1 69.68 71.28 12.07 o 5 1 1 3016.27 3104.73 59.61 o 6 1 1 9490.37 9620.00 167.21 o 7 1 1 128.55 157.75 27.10 o 8 1 1 6.97 0.23 25.33 o 9 1 1 683.00 634.80 45.72 o 10 1 1 67.93 130.49 33.16 o 11 1 1 100.68 101.87 45.86 o 12 1 1 982.60 654.50 70.71 o 13 1 1 26.30 8.92 103.41 o 14 1 1 163.74 115.60 59.35 o -14 2 1 229.93 219.02 96.85 o -13 2 1 553.75 548.68 67.73 o -12 2 1 991.84 991.33 68.45 o -11 2 1 437.91 759.46 48.05 o -10 2 1 34.66 7.82 72.44 o -9 2 1 584.75 559.19 43.69 o -8 2 1 3167.46 2794.34 84.62 o -7 2 1 3264.66 3016.00 76.56 o -6 2 1 17163.41 16648.91 269.81 o -5 2 1 133.95 520.08 18.40 o -4 2 1 2652.21 2742.65 42.99 o -3 2 1 10620.34 10988.20 124.84 o -2 2 1 5176.74 0.00 54.07 x -1 2 1 157.99 0.00 5.17 x 0 2 1 50464.96 0.00 1038.88 x 1 2 1 4635.36 0.00 56.90 x 2 2 1 2694.89 0.00 39.15 x 3 2 1 1682.67 2585.58 29.12 o 4 2 1 2806.37 3090.31 44.22 o 5 2 1 13.94 100.20 29.13 o 6 2 1 15917.26 13714.61 243.04 o 7 2 1 1366.34 1465.54 43.98 o 8 2 1 180.98 345.10 30.70 o 9 2 1 2773.10 2253.16 83.53 o 10 2 1 982.78 687.45 56.80 o 11 2 1 -107.82 6.16 38.34 o 12 2 1 85.35 46.47 47.20 o 13 2 1 -10.28 0.82 101.16 o 14 2 1 271.04 377.66 101.03 o -14 3 1 93.71 12.46 66.19 o -13 3 1 341.59 331.28 77.60 o -12 3 1 140.92 132.62 67.27 o -11 3 1 362.31 312.58 51.73 o -10 3 1 726.37 994.47 49.50 o -9 3 1 62.88 58.53 32.22 o -8 3 1 1543.32 1545.08 50.75 o -7 3 1 788.21 718.40 35.37 o -6 3 1 45956.59 42547.10 638.72 o -5 3 1 5293.27 5951.31 82.68 o -4 3 1 3452.44 2974.04 49.27 o -3 3 1 8289.16 8345.04 95.05 o -2 3 1 725.85 631.45 13.73 o -1 3 1 7239.14 0.00 78.09 x 0 3 1 45.29 0.00 3.82 x 1 3 1 35096.75 0.00 344.02 x 2 3 1 3003.38 2908.95 38.98 o 3 3 1 44813.91 44232.67 470.92 o 4 3 1 3400.88 2889.37 51.18 o 5 3 1 21177.09 22544.01 279.77 o 6 3 1 3417.95 3776.54 73.33 o 7 3 1 273.48 135.91 28.62 o 8 3 1 174.36 126.18 34.00 o 9 3 1 231.67 276.76 34.86 o 10 3 1 86.75 1.81 47.01 o 11 3 1 22.64 19.71 87.98 o 12 3 1 129.07 75.58 44.51 o 13 3 1 29.44 0.35 138.34 o 14 3 1 6.97 24.56 50.45 o -14 4 1 392.27 292.13 105.56 o -13 4 1 244.56 320.27 55.74 o -12 4 1 48.95 0.03 57.00 o -11 4 1 187.43 101.71 44.64 o -10 4 1 120.02 19.87 39.66 o -9 4 1 149.63 154.67 31.19 o -8 4 1 1243.89 1231.80 45.74 o -7 4 1 17.42 3.44 44.48 o -6 4 1 6906.61 6551.00 121.73 o -5 4 1 2038.89 2777.29 49.18 o -4 4 1 15232.35 15537.76 170.07 o -3 4 1 582.66 579.54 14.17 o -2 4 1 50.51 2.47 7.14 o -1 4 1 19933.55 0.00 213.77 x 0 4 1 11331.90 0.00 120.62 x 1 4 1 8299.96 0.00 91.62 x 2 4 1 49383.59 47980.26 500.93 o 3 4 1 15709.46 16126.69 167.75 o 4 4 1 2850.26 3585.74 47.31 o 5 4 1 1510.57 1996.63 40.84 o 6 4 1 346.46 137.84 25.99 o 7 4 1 165.31 214.01 26.16 o 8 4 1 1716.81 1993.85 62.20 o 9 4 1 1090.95 1155.68 53.70 o 10 4 1 111.48 161.30 43.26 o 11 4 1 369.28 66.69 66.94 o 12 4 1 460.38 353.11 71.60 o 13 4 1 59.22 1.24 69.08 o 14 4 1 -8.71 2.14 98.29 o -13 5 1 12.37 4.83 82.03 o -12 5 1 455.33 382.07 75.26 o -11 5 1 71.42 12.06 59.21 o -10 5 1 121.93 88.42 34.69 o -9 5 1 8.71 19.83 34.54 o -8 5 1 1484.09 1417.56 49.96 o -7 5 1 1063.43 897.55 39.61 o -6 5 1 16148.76 15837.01 255.50 o -5 5 1 12530.32 11608.24 189.00 o -4 5 1 6227.62 4930.16 79.38 o -3 5 1 4535.55 4543.27 59.06 o -2 5 1 8796.40 9728.82 101.86 o -1 5 1 18165.71 18241.62 181.47 o 0 5 1 144799.55 141011.09 2784.94 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