#------------------------------------------------------------------------------ #$Date: 2011-03-09 10:38:09 +0200 (Wed, 09 Mar 2011) $ #$Revision: 14261 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2229289.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229289_Fobs loop_ _publ_author_name 'Wang, Wei-Juan' 'Yue, Jun-Ming' 'Niu, Yun-Yin' 'Ng, Seik Weng' _publ_section_title ; 1,1'-Di-n-butyl-4,4'-bipyridinium 2.375-bromido-1.625-chloridocadmate ; _journal_coeditor_code XU5137 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m158 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.936 _cell_angle_gamma 90.000 _cell_length_a 8.6969 _cell_length_b 16.6024 _cell_length_c 16.6881 _exptl_crystal_F_000 1227.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file xu5137Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c C18H26N2 Cd-1.625Cl-2.375Br' _shelx_refln_list_code 4 _shelx_f_calc_maximum 342.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 53780.93 47766.39 1877.34 o 2 0 0 111.54 148.30 12.66 o 3 0 0 2698.18 3511.81 102.29 o 4 0 0 456.89 562.63 33.96 o 5 0 0 31959.29 30897.59 818.93 o 6 0 0 22901.23 21582.29 1023.56 o 7 0 0 4835.27 4913.96 288.72 o 8 0 0 4927.16 4941.27 259.12 o 9 0 0 403.37 358.77 86.54 o 10 0 0 507.63 390.74 98.28 o 1 1 0 5002.31 5088.19 95.84 o 2 1 0 6693.28 6745.89 138.49 o 3 1 0 770.14 891.87 29.16 o 4 1 0 7137.46 6508.84 134.34 o 5 1 0 10083.94 10339.81 201.27 o 6 1 0 464.69 493.22 29.07 o 7 1 0 538.59 646.76 44.58 o 8 1 0 51.96 85.51 38.59 o 9 1 0 332.61 379.56 61.24 o 10 1 0 1432.34 1493.82 108.62 o 0 2 0 35357.87 33680.91 883.51 o 1 2 0 4524.07 4409.13 124.82 o 2 2 0 2992.88 2594.57 52.87 o 3 2 0 1376.48 1118.92 30.13 o 4 2 0 1581.84 1599.41 41.57 o 5 2 0 516.22 446.21 25.30 o 6 2 0 3876.38 3907.64 88.65 o 7 2 0 300.74 322.85 32.27 o 8 2 0 1314.88 1329.36 101.83 o 9 2 0 19.21 94.92 83.87 o 10 2 0 232.07 357.97 76.29 o 1 3 0 29554.63 29764.70 615.90 o 2 3 0 33758.46 30672.25 670.52 o 3 3 0 22527.52 22743.50 423.90 o 4 3 0 26002.43 26175.56 489.67 o 5 3 0 8439.88 8034.96 158.32 o 6 3 0 1251.73 1148.20 64.46 o 7 3 0 2011.79 2021.02 67.37 o 8 3 0 1628.93 1740.10 122.78 o 9 3 0 839.30 828.03 74.61 o 10 3 0 167.27 309.76 69.07 o 0 4 0 14540.04 14301.61 377.34 o 1 4 0 1132.73 1039.96 29.36 o 2 4 0 87.98 104.70 9.24 o 3 4 0 2009.57 2105.65 47.63 o 4 4 0 11926.13 11771.79 225.09 o 5 4 0 7049.95 6522.95 130.68 o 6 4 0 25.29 31.53 22.83 o 7 4 0 1880.22 1965.90 72.63 o 8 4 0 233.09 255.19 44.32 o 9 4 0 21.67 88.32 55.68 o 10 4 0 1595.59 1699.90 107.40 o 1 5 0 4287.34 4174.03 102.28 o 2 5 0 36220.35 35354.04 656.86 o 3 5 0 28621.45 25837.46 618.44 o 4 5 0 203.76 297.26 27.32 o 5 5 0 2729.81 2709.36 63.63 o 6 5 0 364.45 427.44 30.33 o 7 5 0 57.86 23.12 27.47 o 8 5 0 1872.96 1959.74 103.54 o 9 5 0 129.38 210.14 59.29 o 10 5 0 2658.93 2763.29 144.10 o 0 6 0 6861.93 6645.31 181.08 o 1 6 0 7314.93 7512.85 161.50 o 2 6 0 35296.71 33159.04 688.07 o 3 6 0 1500.30 1382.26 36.80 o 4 6 0 25904.80 24983.32 507.41 o 5 6 0 300.02 387.72 27.43 o 6 6 0 333.46 298.85 37.58 o 7 6 0 10920.20 11171.33 241.34 o 8 6 0 1278.35 1342.47 65.85 o 9 6 0 4697.73 4969.50 193.86 o 10 6 0 3099.27 3471.04 162.77 o 1 7 0 42.11 54.85 13.04 o 2 7 0 338.95 400.65 21.33 o 3 7 0 3213.10 2950.09 65.46 o 4 7 0 1682.08 1746.18 46.11 o 5 7 0 5717.75 5326.39 123.08 o 6 7 0 471.24 485.18 33.29 o 7 7 0 2191.81 2279.56 75.02 o 8 7 0 2046.27 2154.75 138.16 o 9 7 0 1039.83 1103.13 131.98 o 10 7 0 27.43 99.12 102.10 o 0 8 0 147.37 243.11 18.68 o 1 8 0 4963.60 4686.22 107.55 o 2 8 0 16837.19 16138.16 340.97 o 3 8 0 2992.82 3081.24 69.11 o 4 8 0 8663.63 8165.86 162.13 o 5 8 0 550.03 488.02 30.52 o 6 8 0 423.87 415.73 35.28 o 7 8 0 3622.56 3846.22 122.57 o 8 8 0 228.37 266.58 61.91 o 9 8 0 3205.27 3126.97 175.28 o 10 8 0 1457.56 1456.22 133.76 o 1 9 0 246.76 257.98 21.64 o 2 9 0 19244.66 18716.42 395.22 o 3 9 0 24425.18 23658.48 495.38 o 4 9 0 20.19 -7.42 18.36 o 5 9 0 10853.33 10472.11 225.83 o 6 9 0 1557.59 1596.03 72.58 o 7 9 0 2137.39 2157.40 90.35 o 8 9 0 12448.76 12490.78 367.51 o 9 9 0 1464.06 1312.53 118.78 o 0 10 0 26865.10 27450.84 933.69 o 1 10 0 4928.95 4723.31 110.76 o 2 10 0 95.04 95.68 21.22 o 3 10 0 524.48 547.00 31.04 o 4 10 0 1.35 3.76 30.70 o 5 10 0 525.68 536.68 45.87 o 6 10 0 250.44 179.42 42.98 o 7 10 0 3219.79 3287.93 132.27 o 8 10 0 14.47 54.79 63.35 o 9 10 0 3.01 88.53 87.60 o 1 11 0 522.52 549.71 31.27 o 2 11 0 269.26 226.49 25.86 o 3 11 0 554.80 554.56 33.45 o 4 11 0 4640.05 4306.75 213.71 o 5 11 0 24.00 1.77 38.20 o 6 11 0 750.74 699.50 56.28 o 7 11 0 405.82 477.55 55.75 o 8 11 0 1621.46 1646.69 133.71 o 9 11 0 1536.74 1388.73 128.02 o 0 12 0 9113.05 8687.98 329.91 o 1 12 0 2145.08 2038.31 69.08 o 2 12 0 3106.51 2962.84 83.25 o 3 12 0 1729.46 1601.48 57.81 o 4 12 0 4652.19 4387.86 303.49 o 5 12 0 9112.17 9219.21 238.62 o 6 12 0 5063.97 5274.51 159.71 o 7 12 0 52.85 43.99 75.59 o 8 12 0 1160.84 1129.63 184.65 o 9 12 0 345.28 376.33 103.51 o 1 13 0 380.18 428.47 45.81 o 2 13 0 19.40 -39.42 26.28 o 3 13 0 1118.43 1030.44 66.94 o 4 13 0 4.45 20.22 39.98 o 5 13 0 277.05 352.68 67.85 o 6 13 0 153.33 163.67 52.52 o 7 13 0 166.14 182.51 69.78 o 8 13 0 21.07 -0.37 73.70 o 0 14 0 21166.13 21042.04 1061.23 o 1 14 0 1134.41 1041.45 109.61 o 2 14 0 4337.11 4118.75 130.91 o 3 14 0 29.40 30.85 54.43 o 4 14 0 602.55 567.53 53.82 o 5 14 0 13624.61 14012.18 453.63 o 6 14 0 5905.46 5976.78 181.11 o 7 14 0 1108.78 1074.64 94.83 o 8 14 0 730.67 682.41 93.51 o 1 15 0 4691.01 4738.90 147.29 o 2 15 0 27.99 43.11 43.38 o 3 15 0 4278.87 3852.89 192.14 o 4 15 0 3818.55 3990.89 165.79 o 5 15 0 3504.39 3688.67 165.97 o 6 15 0 2340.45 2585.22 114.60 o 7 15 0 3355.67 3523.53 164.03 o 0 16 0 2686.91 2530.42 259.65 o 1 16 0 1460.43 1426.70 76.06 o 2 16 0 16.23 9.66 60.94 o 3 16 0 139.73 91.67 69.33 o 4 16 0 78.04 -51.26 71.10 o 5 16 0 20.96 110.68 79.26 o 6 16 0 403.58 459.24 92.06 o 7 16 0 766.00 871.55 149.10 o 1 17 0 6388.94 6312.65 188.89 o 2 17 0 4803.37 4741.51 185.29 o 3 17 0 956.19 820.49 106.15 o 4 17 0 526.60 576.07 91.14 o 5 17 0 6.76 148.31 86.86 o 6 17 0 3180.29 3487.67 174.67 o 0 18 0 1508.25 1536.57 155.85 o 1 18 0 123.60 188.12 60.57 o 2 18 0 5.35 13.19 77.42 o 3 18 0 174.54 138.76 83.40 o 4 18 0 104.86 51.64 84.64 o 5 18 0 1225.82 1274.13 172.16 o 6 18 0 434.20 468.53 105.79 o 1 19 0 180.76 191.68 96.67 o 2 19 0 472.78 512.68 113.95 o 3 19 0 222.42 315.57 92.55 o 4 19 0 65.74 62.85 90.75 o 5 19 0 242.75 349.60 101.88 o 0 20 0 116.34 128.09 99.83 o 1 20 0 586.77 518.06 320.66 o 2 20 0 2166.99 2015.77 321.16 o 3 20 0 41.10 81.24 93.86 o 4 20 0 3391.89 3164.89 337.03 o 1 21 0 64.01 63.19 109.48 o 2 21 0 2562.84 2908.99 267.78 o -11 1 1 451.51 589.85 82.84 o -10 1 1 3575.10 3829.58 166.38 o -9 1 1 595.49 723.68 70.17 o -8 1 1 2156.67 2422.58 84.27 o -7 1 1 17604.18 18137.43 376.96 o -6 1 1 12950.37 12908.61 250.49 o -5 1 1 6032.55 6089.82 123.95 o -4 1 1 2840.99 2452.66 56.08 o -3 1 1 9269.72 9771.32 186.21 o -2 1 1 8093.86 8438.81 172.59 o -1 1 1 18046.31 18719.30 375.66 o 0 1 1 1936.94 1601.24 86.79 o 1 1 1 6412.10 6202.00 126.23 o 2 1 1 5195.00 5034.43 97.60 o 3 1 1 684.19 827.71 27.99 o 4 1 1 10669.89 10442.85 216.93 o 5 1 1 4430.73 4413.68 113.27 o 6 1 1 8041.57 8162.98 177.15 o 7 1 1 14457.31 14210.98 276.55 o 8 1 1 1716.35 1976.72 105.02 o 9 1 1 2494.42 2640.36 130.72 o 10 1 1 1263.63 1330.85 97.53 o -10 2 1 1104.56 978.10 84.42 o -9 2 1 985.97 1038.43 176.62 o -8 2 1 5436.94 5527.98 133.97 o -7 2 1 7.89 52.68 26.96 o -6 2 1 23762.45 24070.38 455.80 o -5 2 1 19396.78 19096.10 361.96 o -4 2 1 5080.42 5152.58 112.62 o -3 2 1 11705.76 12015.23 232.02 o -2 2 1 19261.29 19937.40 401.53 o -1 2 1 23478.47 25006.38 564.60 o 0 2 1 53589.37 50958.33 1993.59 o 1 2 1 6413.78 6239.39 156.70 o 2 2 1 8775.38 8474.00 203.12 o 3 2 1 1640.41 1643.09 39.37 o 4 2 1 19800.87 18952.07 405.68 o 5 2 1 35224.06 35492.07 717.33 o 6 2 1 490.92 444.39 27.74 o 7 2 1 3600.16 3652.46 95.53 o 8 2 1 52.12 22.26 48.32 o 9 2 1 1.41 23.25 61.96 o 10 2 1 1565.26 1435.45 101.05 o -10 3 1 152.81 175.94 64.00 o -9 3 1 1088.20 1116.40 81.80 o -8 3 1 325.88 323.27 37.05 o -7 3 1 1029.10 969.65 58.64 o -6 3 1 6445.94 6425.60 141.67 o -5 3 1 7189.33 7300.24 145.59 o -4 3 1 4701.59 4976.96 101.10 o -3 3 1 73.32 99.10 16.70 o -2 3 1 12462.12 13403.27 272.13 o -1 3 1 189.71 334.87 18.34 o 0 3 1 178.90 193.14 7.93 o 1 3 1 25012.51 25539.98 474.41 o 2 3 1 83766.30 80770.02 2460.45 o 3 3 1 91.73 64.37 11.30 o 4 3 1 11997.54 11290.57 216.04 o 5 3 1 314.95 302.98 21.55 o 6 3 1 1417.10 1292.71 48.35 o 7 3 1 10111.01 9965.89 234.51 o 8 3 1 817.20 742.71 64.83 o 9 3 1 3647.04 3830.76 161.89 o 10 3 1 15.60 52.63 66.12 o -10 4 1 2698.69 3068.62 148.14 o -9 4 1 667.82 600.67 67.54 o -8 4 1 27.92 93.68 36.32 o -7 4 1 1300.93 1247.07 54.29 o -6 4 1 3186.34 3243.06 84.02 o -5 4 1 4608.40 4334.83 91.44 o -4 4 1 7192.21 7424.73 158.42 o -3 4 1 13.31 40.64 17.09 o -2 4 1 6303.10 5894.03 113.91 o -1 4 1 4548.36 5117.19 98.93 o 0 4 1 1453.61 1448.11 32.09 o 1 4 1 21022.06 21422.71 511.27 o 2 4 1 218.19 152.53 10.19 o 3 4 1 10335.13 9681.84 185.57 o 4 4 1 6787.87 6434.69 128.02 o 5 4 1 7250.82 7113.49 142.11 o 6 4 1 15203.26 15072.92 314.87 o 7 4 1 7969.17 7822.21 175.46 o 8 4 1 1149.01 1000.83 72.77 o 9 4 1 1920.37 1999.27 116.80 o 10 4 1 816.62 840.64 85.97 o -10 5 1 371.18 288.67 68.26 o -9 5 1 308.32 456.75 63.78 o -8 5 1 6050.67 6341.98 151.31 o -7 5 1 815.15 784.06 57.65 o -6 5 1 124.61 113.68 24.86 o -5 5 1 791.21 888.12 36.58 o -4 5 1 1287.84 1323.57 43.88 o -3 5 1 19367.05 18852.42 382.94 o -2 5 1 33032.41 30706.00 571.30 o -1 5 1 1834.86 1703.13 37.99 o 0 5 1 2423.45 2565.89 52.72 o 1 5 1 10.01 33.10 10.00 o 2 5 1 8441.38 8243.37 158.31 o 3 5 1 18410.83 16800.02 317.10 o 4 5 1 2535.52 2545.72 70.91 o 5 5 1 2125.92 2138.55 55.08 o 6 5 1 1709.51 1622.57 56.57 o 7 5 1 508.26 594.70 52.44 o 8 5 1 1323.16 1371.26 106.09 o 9 5 1 1813.04 1813.44 127.28 o 10 5 1 215.95 221.07 71.64 o -10 6 1 917.17 1032.26 88.71 o -9 6 1 223.91 292.50 55.77 o -8 6 1 5.56 64.79 33.93 o -7 6 1 154.78 188.04 31.10 o -6 6 1 169.44 156.30 28.83 o -5 6 1 332.66 349.63 25.88 o -4 6 1 2351.21 2395.55 63.69 o -3 6 1 6362.96 6647.98 130.91 o -2 6 1 1106.85 1182.93 34.12 o -1 6 1 14789.29 15012.09 314.95 o 0 6 1 2516.18 2462.19 52.20 o 1 6 1 2504.35 2214.33 55.37 o 2 6 1 5568.65 5439.18 117.11 o 3 6 1 11881.65 11873.32 231.04 o 4 6 1 2842.44 3024.96 68.30 o 5 6 1 339.68 353.77 41.92 o 6 6 1 6928.32 6912.51 155.96 o 7 6 1 6464.64 6504.48 170.71 o 8 6 1 788.23 788.62 114.78 o 9 6 1 495.45 558.90 66.05 o 10 6 1 48.00 27.56 102.26 o -10 7 1 1758.42 1775.23 168.26 o -9 7 1 5521.57 5685.14 187.19 o -8 7 1 12185.51 11877.86 259.49 o -7 7 1 899.83 1009.70 82.54 o -6 7 1 3.00 -25.34 24.18 o -5 7 1 9354.04 9313.28 200.49 o -4 7 1 5181.22 5116.39 116.17 o -3 7 1 90187.26 91339.95 2079.28 o -2 7 1 13251.75 12618.96 239.55 o -1 7 1 698.29 768.67 35.50 o 0 7 1 373.90 313.18 22.54 o 1 7 1 2344.25 2231.11 57.94 o 2 7 1 82262.26 81373.82 1676.11 o 3 7 1 28537.29 27724.17 611.71 o 4 7 1 193.10 192.57 17.30 o 5 7 1 6027.05 5811.64 132.93 o 6 7 1 2004.98 1789.19 61.75 o 7 7 1 2574.67 2517.21 91.30 o 8 7 1 4875.94 4673.98 160.09 o 9 7 1 298.42 391.76 91.68 o 10 7 1 455.55 556.21 122.52 o -10 8 1 667.35 823.45 169.01 o -9 8 1 693.52 582.04 116.33 o -8 8 1 3993.52 4247.28 134.27 o -7 8 1 2101.13 2181.74 74.33 o -6 8 1 2551.28 2484.44 74.87 o -5 8 1 916.82 946.59 41.08 o -4 8 1 2855.05 2856.78 66.10 o -3 8 1 398.22 403.71 18.85 o -2 8 1 24993.73 24479.12 511.17 o -1 8 1 1329.71 1357.61 45.48 o 0 8 1 575.87 632.81 27.66 o 1 8 1 12565.69 11671.21 249.10 o 2 8 1 23732.08 23915.99 501.00 o 3 8 1 232.77 270.04 22.16 o 4 8 1 91.26 154.12 17.49 o 5 8 1 1597.87 1628.31 55.53 o 6 8 1 2637.29 2611.84 78.35 o 7 8 1 3185.82 3386.38 110.19 o 8 8 1 76.91 52.71 71.66 o 9 8 1 1570.04 1446.85 123.68 o -10 9 1 85.79 77.83 92.09 o -9 9 1 751.54 766.59 99.70 o -8 9 1 1637.31 1747.03 122.03 o -7 9 1 812.48 736.41 67.58 o -6 9 1 689.99 627.64 48.73 o -5 9 1 8.54 -6.86 22.41 o -4 9 1 3750.37 3374.29 85.04 o -3 9 1 46.04 68.14 14.60 o -2 9 1 479.78 425.52 24.91 o -1 9 1 1429.35 1237.11 62.54 o 0 9 1 3450.82 3561.55 86.12 o 1 9 1 2047.48 1975.64 56.93 o 2 9 1 566.57 667.23 31.00 o 3 9 1 5400.79 5286.99 137.06 o 4 9 1 7730.79 7599.11 153.63 o 5 9 1 1086.97 1194.27 59.71 o 6 9 1 1551.05 1506.46 109.75 o 7 9 1 31.83 86.15 56.47 o 8 9 1 1153.92 975.50 101.26 o 9 9 1 3498.23 4156.86 263.03 o -9 10 1 959.89 831.63 136.77 o -8 10 1 410.16 386.31 69.05 o -7 10 1 4364.58 4364.32 136.01 o -6 10 1 4259.27 4390.89 133.52 o -5 10 1 3291.89 3300.25 107.39 o -4 10 1 12432.38 12357.91 301.38 o -3 10 1 386.99 363.28 27.03 o -2 10 1 14120.06 13792.06 296.44 o -1 10 1 28235.39 26725.45 624.01 o 0 10 1 13438.31 13316.70 284.87 o 1 10 1 11879.99 11954.75 257.34 o 2 10 1 7658.46 7302.42 164.94 o 3 10 1 1450.64 1510.19 91.19 o 4 10 1 7652.23 7704.61 198.90 o 5 10 1 3842.53 3853.09 120.12 o 6 10 1 232.77 216.94 45.13 o 7 10 1 0.87 50.39 58.47 o 8 10 1 159.27 163.91 80.46 o 9 10 1 1237.84 1073.25 116.82 o -9 11 1 2.98 56.07 86.44 o -8 11 1 73.37 113.01 76.55 o -7 11 1 33.81 40.62 47.61 o -6 11 1 801.62 818.74 58.76 o -5 11 1 1.10 -0.31 36.69 o -4 11 1 10125.76 10624.80 316.64 o -3 11 1 8973.70 9010.27 202.01 o -2 11 1 353.10 335.58 33.28 o -1 11 1 1407.15 1489.67 64.05 o 0 11 1 1900.16 1685.76 67.99 o 1 11 1 5438.36 5680.23 132.69 o 2 11 1 16916.38 16136.49 345.59 o 3 11 1 18.59 16.30 24.60 o 4 11 1 550.32 529.23 44.74 o 5 11 1 3192.36 3202.58 110.43 o 6 11 1 381.61 382.52 64.30 o 7 11 1 1260.72 1236.48 169.03 o 8 11 1 482.92 449.41 90.83 o 9 11 1 1161.17 1206.94 125.92 o -9 12 1 614.99 502.73 103.63 o -8 12 1 1136.55 1049.55 93.99 o -7 12 1 171.91 265.61 54.94 o -6 12 1 4956.62 4976.48 152.27 o -5 12 1 2170.91 2182.80 112.77 o -4 12 1 1489.35 1469.44 101.74 o -3 12 1 3888.69 3685.56 98.96 o -2 12 1 402.51 362.50 29.97 o -1 12 1 18320.73 18082.12 443.30 o 0 12 1 10772.07 10375.46 265.22 o 1 12 1 792.32 779.43 37.52 o 2 12 1 21.27 41.71 25.87 o 3 12 1 162.93 95.66 28.87 o 4 12 1 7656.60 7745.44 246.62 o 5 12 1 8741.76 8464.78 224.09 o 6 12 1 456.02 482.24 56.50 o 7 12 1 1814.79 1630.10 102.84 o 8 12 1 434.19 403.07 145.17 o -8 13 1 160.00 139.46 76.41 o -7 13 1 1622.43 1615.00 149.90 o -6 13 1 16.91 50.94 48.07 o -5 13 1 13645.51 13666.82 405.59 o -4 13 1 6555.93 6552.80 179.96 o -3 13 1 802.15 757.24 50.99 o -2 13 1 7387.88 7479.24 233.79 o -1 13 1 12837.17 12506.96 317.38 o 0 13 1 528.55 493.40 44.69 o 1 13 1 4795.00 4658.45 150.47 o 2 13 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