#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/92/2229299.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229299_Fobs loop_ _publ_author_name 'Ali, Qamar' 'Anis, Itrat' 'Raza Shah, M.' 'Ng, Seik Weng' _publ_section_title ; tert-Butyl 2-(4-nitrophenoxy)acetate ; _journal_coeditor_code XU5151 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o532 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.682 _cell_angle_gamma 90.000 _cell_length_a 19.2761 _cell_length_b 12.1131 _cell_length_c 11.7267 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file xu5151Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 293.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 29691.81 27938.98 155.60 o 4 0 0 18669.59 18715.86 170.50 o 6 0 0 85971.13 95804.68 861.29 o 8 0 0 6916.43 7487.86 69.78 o 10 0 0 14425.50 15412.28 104.85 o 12 0 0 173.69 276.46 37.07 o 14 0 0 0.92 120.30 27.34 o 16 0 0 98.44 229.52 39.93 o 18 0 0 894.43 1045.90 90.05 o 20 0 0 913.30 1274.85 106.74 o 22 0 0 144.05 323.33 59.25 o 3 1 0 23.14 20.54 2.59 o 5 1 0 28394.60 28364.10 178.08 o 7 1 0 2531.97 2454.94 41.77 o 9 1 0 231.74 218.52 13.77 o 11 1 0 19.39 22.79 5.54 o 13 1 0 116.28 143.78 12.28 o 15 1 0 1.75 8.21 6.98 o 17 1 0 63.34 41.15 12.27 o 19 1 0 183.81 154.10 59.62 o 21 1 0 2.73 2.95 6.60 o 0 2 0 2246.64 2205.12 54.19 o 2 2 0 976.52 887.81 14.56 o 4 2 0 3134.65 2901.81 35.17 o 6 2 0 17.42 19.47 2.83 o 8 2 0 3314.56 3373.60 80.95 o 10 2 0 332.31 348.99 19.69 o 12 2 0 109.40 94.71 11.11 o 14 2 0 11.10 11.48 4.96 o 16 2 0 46.93 40.88 12.30 o 18 2 0 13.09 9.10 8.21 o 20 2 0 111.88 118.82 24.45 o 22 2 0 2.28 -17.17 11.44 o 1 3 0 34681.97 33170.25 146.53 o 3 3 0 2905.75 2866.23 29.41 o 5 3 0 9640.35 9284.47 62.52 o 7 3 0 324.06 331.40 13.62 o 9 3 0 1343.72 1333.58 20.69 o 11 3 0 1546.52 1527.48 45.09 o 13 3 0 465.48 470.41 26.71 o 15 3 0 249.68 322.32 23.40 o 17 3 0 22.13 7.07 6.41 o 19 3 0 18.50 17.88 7.44 o 21 3 0 0.90 7.79 11.47 o 0 4 0 19846.25 20082.33 237.56 o 2 4 0 16747.33 17162.43 140.48 o 4 4 0 439.28 494.88 15.09 o 6 4 0 1171.03 1074.32 23.90 o 8 4 0 5205.69 5508.05 63.53 o 10 4 0 1342.50 1248.84 43.61 o 12 4 0 975.16 968.71 38.97 o 14 4 0 381.42 403.62 26.78 o 16 4 0 427.40 396.76 37.39 o 18 4 0 171.19 208.58 29.06 o 20 4 0 843.75 917.72 65.91 o 22 4 0 75.43 82.13 31.44 o 1 5 0 9591.77 9287.21 94.99 o 3 5 0 1004.77 1054.86 26.52 o 5 5 0 332.74 264.31 13.46 o 7 5 0 2306.50 2417.33 45.34 o 9 5 0 1584.76 1615.67 38.35 o 11 5 0 93.79 92.67 11.76 o 13 5 0 6537.64 6872.19 112.01 o 15 5 0 47.35 71.21 12.64 o 17 5 0 227.51 213.48 31.19 o 19 5 0 966.28 923.31 64.86 o 21 5 0 515.90 425.16 46.93 o 0 6 0 785.77 1002.26 65.61 o 2 6 0 136.47 120.57 9.94 o 4 6 0 379.16 322.90 16.23 o 6 6 0 461.42 542.03 26.70 o 8 6 0 1791.50 1795.88 45.13 o 10 6 0 75.41 67.13 9.25 o 12 6 0 267.15 303.95 23.99 o 14 6 0 590.79 616.37 35.69 o 16 6 0 45.53 37.31 11.99 o 18 6 0 23.80 9.74 10.45 o 20 6 0 0.92 -11.95 10.19 o 1 7 0 2720.94 2730.40 60.29 o 3 7 0 0.63 2.71 2.64 o 5 7 0 459.86 409.12 24.48 o 7 7 0 759.58 761.71 34.39 o 9 7 0 17.01 15.51 5.05 o 11 7 0 834.62 878.07 33.52 o 13 7 0 23.65 23.44 7.20 o 15 7 0 75.48 79.09 13.54 o 17 7 0 0.31 -5.95 9.22 o 19 7 0 39.07 34.35 18.30 o 0 8 0 12753.04 13501.16 168.23 o 2 8 0 11.13 4.02 3.51 o 4 8 0 422.61 376.10 20.00 o 6 8 0 539.69 523.01 30.05 o 8 8 0 95.27 128.44 20.19 o 10 8 0 2285.93 2256.04 66.84 o 12 8 0 130.55 154.49 18.83 o 14 8 0 61.07 52.38 14.98 o 16 8 0 8.85 35.99 13.67 o 18 8 0 110.60 107.80 33.72 o 1 9 0 2387.99 2634.76 132.21 o 3 9 0 99.10 216.35 29.32 o 5 9 0 1112.79 1073.83 44.60 o 7 9 0 1322.61 1301.02 50.58 o 9 9 0 132.15 151.94 17.92 o 11 9 0 277.91 267.71 30.51 o 13 9 0 42.40 30.60 14.53 o 15 9 0 404.54 387.34 39.45 o 17 9 0 224.94 202.04 42.44 o 19 9 0 193.09 211.82 46.07 o 0 10 0 8571.80 8733.93 190.33 o 2 10 0 1753.38 1746.58 57.63 o 4 10 0 745.63 786.48 39.72 o 6 10 0 2361.81 2505.75 72.44 o 8 10 0 495.02 533.66 35.67 o 10 10 0 304.92 355.45 28.88 o 12 10 0 132.78 141.36 23.71 o 14 10 0 0.64 1.91 14.43 o 16 10 0 2.86 1.48 7.10 o 1 11 0 4777.75 4845.34 145.76 o 3 11 0 1.43 5.99 6.56 o 5 11 0 993.23 1029.39 47.97 o 7 11 0 2200.67 2187.03 71.66 o 9 11 0 0.19 -2.87 6.69 o 11 11 0 60.32 61.49 18.01 o 13 11 0 19.78 8.08 8.17 o 15 11 0 0.93 0.16 20.83 o 0 12 0 2022.07 2113.32 144.34 o 2 12 0 97.27 107.42 23.90 o 4 12 0 11.75 30.64 14.60 o 6 12 0 69.57 92.42 22.93 o 8 12 0 94.12 84.26 21.71 o 10 12 0 206.25 199.32 48.51 o 12 12 0 9.25 48.38 25.26 o 14 12 0 8.79 -2.51 11.74 o 1 13 0 1570.14 1663.39 95.35 o 3 13 0 0.66 -1.90 14.54 o 5 13 0 173.95 235.11 37.20 o 7 13 0 198.26 204.44 34.55 o 9 13 0 15.00 33.52 15.42 o 11 13 0 345.89 388.42 68.62 o 13 13 0 26.71 21.22 19.19 o 0 14 0 116.94 144.94 42.84 o 2 14 0 0.63 -2.70 11.88 o 4 14 0 174.95 197.96 39.72 o 6 14 0 91.97 149.66 30.86 o 8 14 0 24.73 44.49 18.59 o 1 15 0 252.21 282.49 44.26 o 3 15 0 26.31 61.75 22.98 o 5 15 0 283.04 292.41 62.75 o 7 15 0 78.14 64.63 37.07 o -23 1 1 0.81 -10.29 24.08 o -21 1 1 0.43 0.83 19.57 o -19 1 1 80.40 65.11 22.84 o -17 1 1 121.72 104.42 19.56 o -15 1 1 270.38 286.67 28.54 o -13 1 1 4247.77 4595.76 189.66 o -11 1 1 387.38 367.79 18.02 o -9 1 1 7034.37 7042.43 72.86 o -7 1 1 19534.96 19750.59 213.88 o -5 1 1 51747.54 54730.85 587.64 o -3 1 1 5838.21 5795.75 32.27 o -1 1 1 9.30 9.93 3.92 o 1 1 1 5137.38 4817.08 50.47 o 3 1 1 5744.49 5556.87 35.04 o 5 1 1 20.38 24.67 2.77 o 7 1 1 10229.12 10278.37 111.18 o 9 1 1 962.58 1039.79 26.23 o 11 1 1 429.90 449.68 22.83 o 13 1 1 632.54 607.92 27.66 o 15 1 1 458.20 566.10 43.36 o 17 1 1 28.44 26.34 24.60 o 19 1 1 57.41 74.46 18.45 o 21 1 1 623.94 680.30 59.71 o -22 2 1 6.33 23.77 11.29 o -20 2 1 208.45 201.35 29.20 o -18 2 1 163.75 179.35 25.71 o -16 2 1 263.09 249.75 40.79 o -14 2 1 1724.78 1838.35 48.53 o -12 2 1 92.71 82.70 10.15 o -10 2 1 8931.67 8922.79 95.45 o -8 2 1 4506.37 4435.96 65.03 o -6 2 1 2003.88 1945.64 27.24 o -4 2 1 9890.08 9698.11 99.37 o -2 2 1 1900.38 1907.35 52.36 o 0 2 1 39116.67 37135.79 266.19 o 2 2 1 50.82 64.70 4.70 o 4 2 1 2659.06 2546.60 30.26 o 6 2 1 5191.02 5282.72 56.59 o 8 2 1 2045.78 1971.67 30.68 o 10 2 1 1001.59 1117.72 26.32 o 12 2 1 88.77 140.91 13.96 o 14 2 1 52.07 67.89 11.88 o 16 2 1 93.33 107.49 25.41 o 18 2 1 4.82 3.38 6.58 o 20 2 1 30.59 20.23 26.27 o 22 2 1 154.39 207.60 49.77 o -23 3 1 178.78 123.98 36.23 o -21 3 1 430.38 455.95 51.53 o -19 3 1 0.33 -9.22 8.26 o -17 3 1 64.68 66.04 15.68 o -15 3 1 124.99 131.43 14.31 o -13 3 1 475.96 447.49 25.04 o -11 3 1 4007.20 4053.29 70.83 o -9 3 1 1380.47 1435.38 26.96 o -7 3 1 1494.91 1465.63 25.16 o -5 3 1 483.40 485.44 14.26 o -3 3 1 3354.81 3126.20 45.35 o -1 3 1 13974.26 13760.92 176.68 o 1 3 1 6898.68 6709.54 54.06 o 3 3 1 3.08 4.46 2.61 o 5 3 1 7853.90 7755.09 84.49 o 7 3 1 4930.66 4843.08 56.70 o 9 3 1 939.61 872.47 39.62 o 11 3 1 1500.81 1397.09 33.38 o 13 3 1 44.43 36.36 7.95 o 15 3 1 39.14 34.27 11.76 o 17 3 1 17.76 2.52 14.08 o 19 3 1 14.61 5.94 8.64 o 21 3 1 0.02 -5.10 8.68 o -22 4 1 16.65 5.71 7.74 o -20 4 1 281.61 307.29 38.91 o -18 4 1 153.22 197.15 27.88 o -16 4 1 64.90 49.64 13.61 o -14 4 1 28.16 46.71 9.20 o -12 4 1 158.82 159.50 15.72 o -10 4 1 400.97 369.07 19.15 o -8 4 1 88.65 91.88 7.97 o -6 4 1 7.40 7.03 2.43 o -4 4 1 58.39 59.77 7.32 o -2 4 1 164.83 154.37 8.71 o 0 4 1 1050.24 984.97 51.72 o 2 4 1 8.57 12.52 3.13 o 4 4 1 299.47 270.12 13.74 o 6 4 1 229.00 265.35 17.25 o 8 4 1 1304.35 1364.48 33.24 o 10 4 1 803.98 807.82 30.07 o 12 4 1 2.61 8.01 4.88 o 14 4 1 728.57 732.36 37.57 o 16 4 1 181.31 200.77 28.06 o 18 4 1 3.65 1.01 7.94 o 20 4 1 13.67 6.46 7.90 o -21 5 1 10.88 5.77 7.79 o -19 5 1 13.86 11.06 21.47 o -17 5 1 192.96 166.85 44.78 o -15 5 1 0.63 5.09 6.21 o -13 5 1 1742.87 1776.12 55.20 o -11 5 1 1577.73 1654.14 45.52 o -9 5 1 886.99 858.57 27.20 o -7 5 1 3259.61 3053.26 54.66 o -5 5 1 1170.60 1063.39 22.30 o -3 5 1 1006.32 1008.00 25.19 o -1 5 1 1432.88 1525.14 35.72 o 1 5 1 600.31 727.66 27.83 o 3 5 1 328.97 305.34 14.85 o 5 5 1 577.79 560.82 28.83 o 7 5 1 407.11 425.15 24.12 o 9 5 1 1654.06 1593.97 39.46 o 11 5 1 236.99 217.01 14.90 o 13 5 1 0.10 -5.28 5.37 o 15 5 1 436.86 449.59 31.48 o 17 5 1 14.70 -3.66 8.32 o 19 5 1 0.01 8.39 8.40 o 21 5 1 14.43 32.31 20.49 o -20 6 1 32.12 32.39 13.89 o -18 6 1 714.98 711.60 53.61 o -16 6 1 511.22 514.72 33.52 o -14 6 1 466.10 442.79 32.49 o -12 6 1 569.59 570.90 24.68 o -10 6 1 2469.39 2542.84 51.13 o -8 6 1 219.04 164.10 12.77 o -6 6 1 3529.02 3404.37 60.11 o -4 6 1 5266.91 5497.59 60.20 o -2 6 1 181.90 151.69 28.26 o 0 6 1 3042.44 3332.70 88.79 o 2 6 1 7185.17 7385.31 86.50 o 4 6 1 178.91 167.46 17.31 o 6 6 1 6725.44 6509.18 113.95 o 8 6 1 4772.05 5098.94 78.09 o 10 6 1 611.13 579.38 26.10 o 12 6 1 913.71 917.43 52.38 o 14 6 1 116.45 105.94 15.27 o 16 6 1 243.33 255.53 35.65 o 18 6 1 269.61 289.53 36.91 o 20 6 1 51.86 17.18 18.03 o -19 7 1 117.87 90.91 28.12 o -17 7 1 98.17 79.67 18.02 o -15 7 1 11.68 7.51 5.25 o -13 7 1 1396.78 1364.89 52.48 o -11 7 1 1541.52 1532.12 43.39 o -9 7 1 1399.96 1447.94 40.68 o -7 7 1 22.63 29.65 5.48 o -5 7 1 279.43 235.54 14.49 o -3 7 1 1295.25 1269.58 49.52 o -1 7 1 4588.17 4651.86 136.45 o 1 7 1 560.28 556.84 28.48 o 3 7 1 534.09 512.19 35.02 o 5 7 1 238.97 224.68 18.08 o 7 7 1 411.69 389.10 24.63 o 9 7 1 212.10 191.91 16.01 o 11 7 1 179.89 189.93 16.30 o 13 7 1 37.30 35.77 9.64 o 15 7 1 28.14 22.62 8.17 o 17 7 1 163.84 186.64 29.45 o 19 7 1 11.54 21.07 17.11 o -20 8 1 141.09 101.36 30.14 o -18 8 1 101.61 102.60 30.46 o -16 8 1 67.67 60.72 16.76 o -14 8 1 43.81 34.77 9.52 o -12 8 1 3.05 10.57 5.67 o -10 8 1 225.09 188.61 15.92 o -8 8 1 4.91 3.68 4.11 o -6 8 1 1187.42 1111.71 43.96 o -4 8 1 127.01 125.01 11.92 o -2 8 1 19.70 18.24 3.75 o 0 8 1 13.29 18.15 5.82 o 2 8 1 114.00 150.47 14.74 o 4 8 1 201.88 203.01 18.52 o 6 8 1 362.69 349.54 24.41 o 8 8 1 47.34 37.33 9.21 o 10 8 1 426.50 440.10 29.81 o 12 8 1 22.48 13.04 9.31 o 14 8 1 12.87 17.16 7.35 o 16 8 1 0.19 -18.42 12.28 o 18 8 1 49.02 68.42 26.55 o -19 9 1 11.60 17.33 15.57 o -17 9 1 0.61 -5.17 10.26 o -15 9 1 20.42 25.62 21.62 o -13 9 1 407.00 401.32 38.48 o -11 9 1 103.36 122.95 16.48 o -9 9 1 217.35 206.69 20.75 o -7 9 1 420.83 400.96 28.81 o -5 9 1 91.86 109.29 20.11 o -3 9 1 2690.69 2685.38 52.14 o -1 9 1 26.48 17.01 6.69 o 1 9 1 3211.71 3420.53 70.18 o 3 9 1 1417.23 1442.58 47.83 o 5 9 1 92.59 85.54 12.81 o 7 9 1 2596.98 2776.72 98.31 o 9 9 1 7.99 6.83 6.52 o 11 9 1 0.31 0.22 7.96 o 13 9 1 21.60 24.32 10.81 o 15 9 1 21.30 37.74 12.80 o 17 9 1 3.53 12.33 15.22 o -18 10 1 46.16 78.33 27.58 o -16 10 1 345.54 341.25 39.02 o -14 10 1 831.91 851.44 58.85 o -12 10 1 138.02 123.39 22.67 o -10 10 1 2963.60 3037.17 104.49 o -8 10 1 1427.93 1585.90 60.16 o -6 10 1 70.59 64.45 12.84 o -4 10 1 1.48 0.34 5.62 o -2 10 1 21.93 34.68 9.80 o 0 10 1 3772.34 4008.16 76.91 o 2 10 1 1825.79 1869.35 56.15 o 4 10 1 543.70 526.18 31.55 o 6 10 1 1734.98 1804.08 60.81 o 8 10 1 39.65 21.32 9.02 o 10 10 1 1115.75 1018.79 48.97 o 12 10 1 70.47 55.56 15.86 o 14 10 1 334.27 334.08 38.25 o 16 10 1 81.64 38.77 22.31 o -17 11 1 190.61 179.22 42.01 o -15 11 1 2.67 -13.35 9.60 o -13 11 1 307.82 294.03 36.05 o -11 11 1 72.27 31.28 23.47 o -9 11 1 151.89 162.26 21.00 o -7 11 1 1282.32 1346.63 57.60 o -5 11 1 2687.75 2690.45 80.23 o -3 11 1 335.94 381.63 30.47 o -1 11 1 133.76 125.92 18.00 o 1 11 1 79.66 74.39 20.13 o 3 11 1 2.21 11.14 7.66 o 5 11 1 116.19 88.41 22.30 o 7 11 1 582.50 631.85 38.52 o 9 11 1 45.74 53.55 12.46 o 11 11 1 6.41 -6.09 8.86 o 13 11 1 9.78 18.97 10.75 o 15 11 1 81.14 48.20 16.28 o -14 12 1 5.33 18.72 10.75 o -12 12 1 135.94 159.25 27.21 o -10 12 1 265.71 238.27 26.01 o -8 12 1 11.16 6.52 9.04 o -6 12 1 240.13 225.89 38.79 o -4 12 1 154.23 214.80 33.85 o -2 12 1 204.59 294.36 79.96 o 0 12 1 565.77 591.98 54.56 o 2 12 1 26.82 35.78 17.20 o 4 12 1 2.90 15.16 13.72 o 6 12 1 0.00 7.05 12.11 o 8 12 1 35.30 65.57 20.10 o 10 12 1 0.43 72.59 28.07 o 12 12 1 135.73 157.12 44.60 o 14 12 1 38.01 27.96 23.50 o -13 13 1 128.72 104.59 36.11 o -11 13 1 21.19 24.16 25.00 o -9 13 1 9.07 16.97 15.01 o -7 13 1 83.16 83.10 22.21 o -5 13 1 96.44 92.64 35.14 o -3 13 1 117.63 132.21 26.99 o -1 13 1 13.18 18.15 14.50 o 1 13 1 34.89 42.66 15.81 o 3 13 1 137.86 127.49 42.25 o 5 13 1 54.49 89.76 22.92 o 7 13 1 5.84 24.18 14.36 o 9 13 1 220.34 296.84 60.08 o 11 13 1 3.74 13.88 16.99 o -10 14 1 91.59 75.41 32.12 o -8 14 1 52.57 46.51 20.10 o -6 14 1 373.65 474.78 53.87 o -4 14 1 115.09 107.11 50.97 o -2 14 1 13.94 66.87 34.90 o 0 14 1 2.55 9.55 12.14 o 2 14 1 123.39 151.35 30.87 o 4 14 1 103.64 168.22 33.12 o 6 14 1 58.68 62.63 31.77 o 8 14 1 65.44 84.60 32.97 o -7 15 1 70.16 132.51 45.40 o -5 15 1 13.86 44.56 28.58 o -3 15 1 22.01 69.67 27.95 o -1 15 1 234.86 286.83 45.37 o 1 15 1 67.39 128.38 30.13 o 3 15 1 1.41 4.41 19.20 o 5 15 1 21.93 -7.99 16.75 o -22 0 2 185.94 206.98 45.30 o -20 0 2 1202.03 1064.08 92.00 o -18 0 2 665.11 662.28 66.89 o -16 0 2 1189.11 1211.97 83.05 o -14 0 2 1509.06 1524.31 85.71 o -12 0 2 27819.72 28339.77 435.54 o -10 0 2 38430.30 39682.66 422.39 o -8 0 2 1908.04 1914.86 40.90 o -6 0 2 63487.25 67476.58 593.58 o -4 0 2 46523.94 46907.14 162.88 o -2 0 2 11667.86 11011.28 127.55 o 0 0 2 17120.62 15599.13 117.84 o 2 0 2 14616.31 13852.10 95.85 o 4 0 2 7544.30 7357.50 103.38 o 6 0 2 425.78 484.33 22.99 o 8 0 2 443.66 399.75 27.32 o 10 0 2 1853.37 2253.30 102.92 o 12 0 2 1768.52 2116.51 58.43 o 14 0 2 945.03 798.93 73.88 o 16 0 2 4063.60 4358.52 186.29 o 18 0 2 16.79 13.72 13.89 o 20 0 2 2.90 13.59 18.87 o -23 1 2 16.53 10.77 12.70 o -21 1 2 30.05 21.55 12.70 o -19 1 2 73.47 55.36 14.38 o -17 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30.74 o 4 2 2 5.72 3.99 2.22 o 6 2 2 16.64 20.48 4.12 o 8 2 2 172.01 189.37 13.57 o 10 2 2 146.20 131.90 11.71 o 12 2 2 51.26 36.54 8.01 o 14 2 2 17.86 6.62 12.17 o 16 2 2 0.98 -2.66 12.09 o 18 2 2 39.28 29.56 11.13 o 20 2 2 0.59 9.64 14.24 o -23 3 2 9.00 12.50 10.80 o -21 3 2 0.18 -5.76 11.66 o -19 3 2 59.46 34.55 11.34 o -17 3 2 2.58 -0.60 11.55 o -15 3 2 49.60 70.14 10.76 o -13 3 2 93.20 103.81 12.31 o -11 3 2 3863.17 3617.17 68.68 o -9 3 2 6.78 6.91 2.33 o -7 3 2 3.86 3.68 1.96 o -5 3 2 1318.84 1209.17 20.11 o -3 3 2 647.54 570.11 29.31 o -1 3 2 86.73 116.72 18.42 o 1 3 2 2866.01 2637.49 34.76 o 3 3 2 2519.32 2619.01 36.30 o 5 3 2 1596.44 1582.74 34.30 o 7 3 2 89.35 104.31 9.34 o 9 3 2 1532.42 1478.70 36.95 o 11 3 2 197.54 229.17 19.71 o 13 3 2 119.55 100.61 14.12 o 15 3 2 0.61 12.88 7.61 o 17 3 2 60.75 80.90 19.82 o 19 3 2 0.05 -11.21 14.15 o 21 3 2 10.70 16.41 17.82 o -22 4 2 29.96 21.72 11.93 o -20 4 2 105.00 115.65 22.07 o -18 4 2 363.37 344.97 35.06 o -16 4 2 3320.10 3230.48 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