Crystallography Open Database

Information card for entry 2229315

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Structure parameters

Chemical name	Chloridonitrosyl[<i>meso</i>-5,10,15,20-tetrakis(<i>p</i>-tolyl)porphyrinato- κ^4^<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>''')osmium(II) tetrahydrofuran tetrasolvate
Formula	C64 H68 Cl N5 O5 Os
Calculated formula	C64 H68 Cl0.997 N4.997 O4.997 Os
Title of publication	Chloridonitrosyl[<i>meso</i>-5,10,15,20-tetrakis(<i>p</i>-tolyl)porphyrinato-κ^4^<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>''']osmium(II) tetrahydrofuran tetrasolvate
Authors of publication	Chen, Li; Xu, Nan; Powell, Douglas R.; Richter-Addo, George B.
Journal of publication	Acta Crystallographica Section E
Year of publication	2011
Journal volume	67
Journal issue	2
Pages of publication	m224
a	16.905 ± 0.002 Å
b	16.905 Å
c	9.622 ± 0.0019 Å
α	90°
β	90°
γ	90°
Cell volume	2749.8 ± 0.6 Å³
Cell temperature	188 ± 2 K
Ambient diffraction temperature	188 ± 2 K
Number of distinct elements	6
Space group number	85
Hermann-Mauguin space group symbol	P 4/n :2
Hall space group symbol	-P 4a
Residual factor for all reflections	0.023
Residual factor for significantly intense reflections	0.0215
Weighted residual factors for significantly intense reflections	0.0569
Weighted residual factors for all reflections included in the refinement	0.058
Goodness-of-fit parameter for all reflections included in the refinement	0.968
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
181214 (current)	2016-04-03	hkl/2/22/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22/93.	2229315.cif 2229315.hkl
176789	2016-02-20	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22.	2229315.cif 2229315.hkl
120072	2014-07-11	Adding DOIs to range 2 structures.	2229315.cif 2229315.hkl
88064	2013-08-29	Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet.	2229315.cif 2229315.hkl
26848	2011-09-28	cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree.	2229315.cif 2229315.hkl
17966	2011-04-13	hkl/: adding the rest of Fobs files for the recent IUCr deposit.	2229315.cif 2229315.hkl
17357	2011-04-07	../uploads/cif-deposit/cod/cif Adding structures of 2229315 via cif-deposit CGI script.	2229315.cif