#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/93/2229316.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229316_Fobs loop_ _publ_author_name 'Saeed, Aamer' 'Mahmood, Shams-ul' 'Bolte, Michael' 'Rauf, Abdul' 'Subhan, Mohammad' _publ_section_title ; (E)-1-(4-Chlorobenzylidene)thiosemicarbazide ; _journal_coeditor_code BG2386 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o649 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.852 _cell_angle_beta 75.373 _cell_angle_gamma 76.353 _cell_length_a 5.7611 _cell_length_b 7.8329 _cell_length_c 11.2016 _exptl_crystal_F_000 220.00 _reflns_d_resolution_high 0.7658 _[local]_cod_data_source_file bg2386Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sa41 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 89.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 145.67 132.30 4.34 o 2 0 0 1300.09 1303.32 22.27 o 3 0 0 435.21 423.96 10.74 o 4 0 0 126.40 129.22 2.75 o 5 0 0 948.90 932.46 4.15 o 6 0 0 202.80 202.11 3.61 o 7 0 0 79.72 80.79 1.39 o -6 1 0 58.04 59.03 1.38 o -5 1 0 293.67 275.88 4.46 o -4 1 0 18.16 18.25 0.41 o -3 1 0 149.77 163.15 3.19 o -2 1 0 13.06 17.23 0.51 o -1 1 0 27.73 31.23 0.75 o 1 1 0 2.07 0.79 0.38 o 2 1 0 64.09 61.65 1.54 o 3 1 0 63.28 60.54 1.23 o 4 1 0 110.56 105.83 2.80 o 5 1 0 466.86 482.01 11.05 o 6 1 0 54.29 55.24 0.67 o 7 1 0 4.68 5.19 0.57 o -6 2 0 98.91 98.61 4.82 o -5 2 0 159.11 154.02 2.91 o -4 2 0 4.66 5.08 0.42 o -3 2 0 392.27 359.17 8.07 o -2 2 0 3211.56 3091.24 139.98 o -1 2 0 1030.25 917.89 29.72 o 0 2 0 8077.35 8496.29 64.71 o 1 2 0 66.37 65.55 1.24 o 2 2 0 146.55 141.31 3.68 o 3 2 0 1653.71 1671.66 23.83 o 4 2 0 106.87 103.09 3.82 o 5 2 0 1511.31 1518.13 41.43 o 6 2 0 48.57 48.99 0.68 o 7 2 0 0.10 1.12 0.67 o -6 3 0 40.87 42.90 0.76 o -5 3 0 132.31 133.23 1.45 o -4 3 0 53.06 45.15 0.86 o -3 3 0 50.32 52.31 2.50 o -2 3 0 2.06 1.07 0.35 o -1 3 0 60.54 67.74 1.63 o 0 3 0 192.05 187.68 4.32 o 1 3 0 69.60 68.90 1.62 o 2 3 0 8.50 9.89 0.38 o 3 3 0 851.87 895.18 18.85 o 4 3 0 0.15 0.34 0.40 o 5 3 0 90.68 92.25 3.56 o 6 3 0 37.65 37.41 2.01 o 7 3 0 0.22 0.95 0.51 o -5 4 0 168.11 169.61 2.18 o -4 4 0 12.60 8.93 0.41 o -3 4 0 140.50 147.77 4.07 o -2 4 0 1402.71 1383.25 4.76 o -1 4 0 28.65 30.62 0.49 o 0 4 0 1675.95 1673.65 34.56 o 1 4 0 203.95 182.76 5.86 o 2 4 0 184.60 174.10 2.69 o 3 4 0 1715.30 1076.26 350.59 o 4 4 0 37.50 33.26 1.51 o 5 4 0 438.32 453.03 9.77 o 6 4 0 148.20 145.49 4.39 o 7 4 0 2.77 2.31 0.53 o -5 5 0 61.71 66.28 1.07 o -4 5 0 103.44 97.59 0.77 o -3 5 0 41.86 38.22 0.69 o -2 5 0 114.29 110.20 3.38 o -1 5 0 0.13 0.45 0.35 o 0 5 0 41.62 51.10 2.27 o 1 5 0 242.28 271.03 3.67 o 2 5 0 9.05 8.61 0.42 o 3 5 0 154.92 165.72 4.45 o 4 5 0 2.16 1.48 0.37 o 5 5 0 37.33 35.71 0.55 o 6 5 0 34.18 35.62 1.10 o -4 6 0 10.83 15.71 0.54 o -3 6 0 48.76 48.57 0.72 o -2 6 0 606.54 602.74 6.40 o -1 6 0 0.97 1.24 0.45 o 0 6 0 370.52 337.58 10.90 o 1 6 0 78.56 67.21 1.51 o 2 6 0 1.41 1.19 0.31 o 3 6 0 1118.06 1179.35 40.94 o 4 6 0 35.91 33.83 1.35 o 5 6 0 96.39 100.05 3.42 o 6 6 0 73.14 76.49 2.02 o -4 7 0 7.72 8.57 0.63 o -3 7 0 41.75 43.15 1.35 o -2 7 0 2.13 2.77 0.49 o -1 7 0 305.20 309.80 14.90 o 0 7 0 23.30 23.02 0.81 o 1 7 0 59.89 63.35 5.86 o 2 7 0 19.04 20.98 0.80 o 3 7 0 98.93 100.35 3.43 o 4 7 0 5.14 5.66 0.39 o 5 7 0 89.27 89.30 2.61 o 6 7 0 0.44 0.53 0.51 o -3 8 0 16.83 17.77 1.04 o -2 8 0 124.77 131.50 4.57 o -1 8 0 6.03 7.86 1.00 o 0 8 0 91.80 93.55 2.99 o 1 8 0 152.18 152.53 4.55 o 2 8 0 10.73 13.72 0.45 o 3 8 0 214.55 228.13 8.47 o 4 8 0 93.98 96.12 4.02 o 5 8 0 18.24 21.26 1.27 o -1 9 0 149.95 139.97 8.55 o 0 9 0 54.24 52.89 2.80 o 1 9 0 8.59 7.55 0.48 o 2 9 0 1.96 2.65 0.51 o 3 9 0 36.81 38.93 2.52 o 4 9 0 118.35 125.81 6.14 o 1 10 0 88.65 88.58 2.09 o 2 10 0 7.10 7.23 0.59 o -1 -10 1 6.00 8.67 1.13 o -4 -9 1 69.87 70.88 3.18 o -3 -9 1 108.60 110.45 5.84 o -2 -9 1 114.53 114.23 3.36 o -1 -9 1 11.09 9.79 0.53 o 0 -9 1 119.57 110.75 2.14 o 1 -9 1 128.42 121.78 4.54 o -5 -8 1 18.17 18.65 0.70 o -4 -8 1 2.41 2.66 0.38 o -3 -8 1 62.44 63.12 2.31 o -2 -8 1 38.31 38.10 1.21 o -1 -8 1 18.35 18.30 0.66 o 0 -8 1 1.96 2.37 0.47 o 1 -8 1 71.95 69.65 2.51 o 2 -8 1 21.12 22.05 1.20 o 3 -8 1 5.69 6.55 0.47 o -6 -7 1 8.10 6.65 1.58 o -5 -7 1 136.47 142.31 5.54 o -4 -7 1 45.17 48.95 1.92 o -3 -7 1 4.52 4.57 0.43 o -2 -7 1 400.80 404.49 14.31 o -1 -7 1 7.02 6.43 0.38 o 0 -7 1 377.61 371.54 7.68 o 1 -7 1 401.96 396.58 6.85 o 2 -7 1 54.85 49.96 1.56 o 3 -7 1 166.33 170.97 3.64 o 4 -7 1 52.30 56.50 1.17 o -6 -6 1 34.17 32.60 0.75 o -5 -6 1 102.55 102.13 2.67 o -4 -6 1 13.43 13.94 0.58 o -3 -6 1 113.70 115.57 4.33 o -2 -6 1 12.71 13.98 0.56 o -1 -6 1 68.75 70.73 1.48 o 0 -6 1 9.76 8.66 0.46 o 1 -6 1 5.17 6.17 0.38 o 2 -6 1 260.47 274.83 12.06 o 3 -6 1 53.54 56.29 1.68 o 4 -6 1 92.15 91.24 3.49 o -6 -5 1 3.88 4.91 0.50 o -5 -5 1 90.09 96.96 2.64 o -4 -5 1 91.38 90.41 1.70 o -3 -5 1 6.43 5.14 0.38 o -2 -5 1 523.83 496.81 9.25 o -1 -5 1 19.20 22.42 0.60 o 0 -5 1 585.78 600.82 16.33 o 1 -5 1 815.91 814.01 12.19 o 2 -5 1 5.21 5.08 0.43 o 3 -5 1 317.58 315.88 4.71 o 4 -5 1 50.46 50.03 1.05 o 5 -5 1 23.16 19.10 0.73 o -6 -4 1 49.08 49.23 2.79 o -5 -4 1 194.98 183.12 3.77 o -4 -4 1 8.33 7.62 0.38 o -3 -4 1 64.18 79.93 1.58 o -2 -4 1 138.81 145.50 5.78 o -1 -4 1 0.19 0.36 0.36 o 0 -4 1 325.54 376.56 15.46 o 1 -4 1 32.99 36.46 1.71 o 2 -4 1 107.95 97.70 0.74 o 3 -4 1 237.56 235.80 2.49 o 4 -4 1 36.90 33.98 1.06 o 5 -4 1 6.62 6.86 0.52 o -7 -3 1 21.33 23.61 0.85 o -6 -3 1 37.42 39.29 0.60 o -5 -3 1 5.86 14.82 5.65 o -4 -3 1 152.06 152.12 2.06 o -3 -3 1 10.32 8.76 0.39 o -2 -3 1 677.20 688.72 20.19 o -1 -3 1 196.47 208.33 6.52 o 0 -3 1 1607.75 1604.70 38.71 o 1 -3 1 518.88 480.82 21.47 o 2 -3 1 32.87 34.65 0.71 o 3 -3 1 205.75 206.66 1.34 o 4 -3 1 420.86 399.24 10.45 o 5 -3 1 201.81 185.03 4.56 o 6 -3 1 226.85 221.63 14.61 o -7 -2 1 77.43 80.27 2.02 o -6 -2 1 19.07 20.59 0.64 o -5 -2 1 10.88 10.46 0.54 o -4 -2 1 545.03 535.47 20.77 o -3 -2 1 2.44 1.47 0.45 o -2 -2 1 217.38 224.90 4.74 o -1 -2 1 55.29 59.79 0.87 o 0 -2 1 299.25 283.48 13.31 o 1 -2 1 73.71 73.53 3.89 o 2 -2 1 135.97 159.12 2.04 o 3 -2 1 42.06 39.30 0.55 o 4 -2 1 98.41 90.32 2.85 o 5 -2 1 9.44 7.93 0.47 o 6 -2 1 96.38 86.83 3.30 o -7 -1 1 1.12 1.26 0.53 o -6 -1 1 0.13 0.19 0.52 o -5 -1 1 52.44 54.63 0.76 o -4 -1 1 308.96 319.80 2.07 o -3 -1 1 229.79 237.02 4.44 o -2 -1 1 1084.20 997.21 21.55 o -1 -1 1 70.32 57.10 0.99 o 0 -1 1 814.68 776.42 8.93 o 1 -1 1 1759.87 1692.00 51.29 o 2 -1 1 31.88 29.85 1.23 o 3 -1 1 377.97 344.71 5.76 o 4 -1 1 405.48 352.27 25.26 o 5 -1 1 98.75 94.13 5.04 o 6 -1 1 54.90 58.75 2.38 o -6 0 1 10.81 12.51 0.55 o -5 0 1 43.68 41.26 0.63 o -4 0 1 345.99 330.25 2.29 o -3 0 1 38.47 32.48 0.80 o -2 0 1 315.38 303.53 7.83 o -1 0 1 265.48 211.29 7.72 o 1 0 1 231.13 218.50 27.55 o 2 0 1 26.24 29.27 0.68 o 3 0 1 253.04 268.57 4.94 o 4 0 1 4.93 4.22 0.39 o 5 0 1 20.98 20.52 0.48 o 6 0 1 90.67 86.90 2.32 o 7 0 1 3.66 2.21 0.52 o -6 1 1 36.38 38.89 0.64 o -5 1 1 34.79 34.21 1.38 o -4 1 1 70.94 73.53 1.59 o -3 1 1 107.69 118.87 2.14 o -2 1 1 201.21 169.92 3.57 o -1 1 1 1242.54 1084.46 97.06 o 1 1 1 647.51 603.36 19.48 o 2 1 1 27.65 28.84 0.52 o 3 1 1 239.05 206.30 4.91 o 4 1 1 575.69 558.27 4.64 o 5 1 1 9.37 8.80 0.41 o 6 1 1 109.62 108.33 0.93 o 7 1 1 1.02 0.78 0.49 o -6 2 1 36.10 37.83 1.36 o -5 2 1 122.89 126.89 3.26 o -4 2 1 129.46 137.62 2.25 o -3 2 1 10.49 7.14 0.48 o -2 2 1 887.52 902.71 15.71 o -1 2 1 64.32 65.18 1.56 o 0 2 1 483.66 466.71 9.08 o 1 2 1 160.31 162.75 5.48 o 2 2 1 78.83 68.17 1.99 o 3 2 1 26.65 27.75 0.50 o 4 2 1 41.13 37.90 0.62 o 5 2 1 27.06 27.82 0.73 o 6 2 1 35.26 36.26 1.79 o 7 2 1 1.82 2.50 0.58 o -6 3 1 2.88 2.80 0.79 o -5 3 1 0.45 1.47 0.35 o -4 3 1 380.63 344.71 6.36 o -3 3 1 36.65 31.74 2.54 o -2 3 1 100.73 79.78 0.72 o -1 3 1 264.00 235.16 9.35 o 0 3 1 53.94 52.83 0.63 o 1 3 1 111.72 89.00 1.90 o 2 3 1 536.41 525.97 10.01 o 3 3 1 347.90 315.17 14.92 o 4 3 1 449.55 438.89 9.20 o 5 3 1 2.60 3.18 0.47 o 6 3 1 0.35 1.20 0.53 o 7 3 1 41.87 43.46 1.62 o -5 4 1 167.83 159.30 4.54 o -4 4 1 63.24 67.20 0.59 o -3 4 1 24.08 24.09 0.46 o -2 4 1 169.63 153.26 0.94 o -1 4 1 347.43 362.45 3.47 o 0 4 1 156.42 147.58 1.76 o 1 4 1 0.62 4.92 1.52 o 2 4 1 23.52 24.51 0.43 o 3 4 1 1.41 1.76 0.33 o 4 4 1 2.96 3.10 0.36 o 5 4 1 95.69 94.17 2.14 o 6 4 1 0.19 0.17 0.44 o 7 4 1 44.92 45.95 1.38 o -5 5 1 66.54 70.55 3.66 o -4 5 1 272.56 263.42 4.86 o -3 5 1 27.43 24.08 0.71 o -2 5 1 13.82 13.19 0.51 o -1 5 1 209.36 196.92 2.94 o 0 5 1 15.44 14.48 0.46 o 1 5 1 1079.17 1067.65 17.24 o 2 5 1 57.57 53.74 2.11 o 3 5 1 49.77 46.58 4.75 o 4 5 1 190.02 180.57 6.63 o 5 5 1 0.05 2.41 1.26 o 6 5 1 2.13 2.45 0.55 o 7 5 1 90.74 87.42 2.94 o -4 6 1 149.97 148.76 5.78 o -3 6 1 0.33 0.23 0.38 o -2 6 1 370.16 347.10 12.24 o -1 6 1 7.41 8.29 0.51 o 0 6 1 34.10 35.33 1.08 o 1 6 1 1.83 10.65 3.51 o 2 6 1 5.91 5.48 0.36 o 3 6 1 3.90 3.78 0.34 o 4 6 1 14.61 15.69 0.42 o 5 6 1 9.88 9.71 0.48 o 6 6 1 44.93 45.48 1.40 o -3 7 1 7.88 8.46 0.44 o -2 7 1 63.25 63.51 1.51 o -1 7 1 149.63 145.90 5.53 o 0 7 1 47.02 46.27 1.36 o 1 7 1 436.30 449.40 13.33 o 2 7 1 110.97 106.23 10.99 o 3 7 1 76.66 78.14 8.73 o 4 7 1 63.91 68.03 2.52 o 5 7 1 0.86 1.41 0.41 o 6 7 1 37.68 40.33 1.97 o -3 8 1 16.97 16.65 1.19 o -2 8 1 85.36 80.92 4.08 o -1 8 1 40.07 40.86 1.40 o 0 8 1 0.15 0.20 0.35 o 1 8 1 113.60 107.88 6.66 o 2 8 1 14.13 13.70 0.76 o 3 8 1 9.64 9.36 0.55 o 4 8 1 38.72 38.74 1.26 o 5 8 1 0.62 0.61 0.44 o -1 9 1 196.40 191.70 7.75 o 0 9 1 29.01 30.37 0.57 o 1 9 1 172.88 169.92 5.40 o 2 9 1 29.25 31.52 1.80 o 3 9 1 41.38 42.42 2.01 o 4 9 1 29.55 33.35 1.65 o 1 10 1 24.48 25.09 1.17 o 2 10 1 2.83 3.05 0.57 o -4 -9 2 28.99 31.74 1.36 o -3 -9 2 109.14 106.62 4.43 o -2 -9 2 45.63 46.66 1.78 o -1 -9 2 46.57 46.52 1.76 o 0 -9 2 22.43 20.84 1.07 o 1 -9 2 2.39 3.16 0.46 o -5 -8 2 3.82 4.53 0.45 o -4 -8 2 62.84 66.48 2.30 o -3 -8 2 29.90 30.16 1.25 o -2 -8 2 89.87 89.75 2.46 o -1 -8 2 33.02 33.83 0.84 o 0 -8 2 15.84 15.25 0.71 o 1 -8 2 130.30 127.07 1.70 o 2 -8 2 73.36 76.08 1.61 o 3 -8 2 98.36 99.90 2.69 o -5 -7 2 22.87 22.94 0.56 o -4 -7 2 68.80 69.12 3.14 o -3 -7 2 402.48 439.18 17.02 o -2 -7 2 274.79 275.98 8.21 o -1 -7 2 74.88 71.98 1.86 o 0 -7 2 65.57 59.02 1.69 o 1 -7 2 29.49 28.73 1.00 o 2 -7 2 310.11 316.28 11.33 o 3 -7 2 0.62 1.25 0.40 o 4 -7 2 5.14 6.15 0.48 o -6 -6 2 2.87 3.87 0.47 o -5 -6 2 14.59 18.31 2.75 o -4 -6 2 61.65 67.58 1.82 o -3 -6 2 17.87 18.54 0.92 o -2 -6 2 205.86 203.01 7.37 o -1 -6 2 250.20 248.91 9.58 o 0 -6 2 14.95 11.03 0.39 o 1 -6 2 199.40 194.17 8.39 o 2 -6 2 67.14 67.37 1.59 o 3 -6 2 90.70 94.75 2.76 o 4 -6 2 148.82 144.77 2.10 o -6 -5 2 58.92 57.97 0.74 o -5 -5 2 5.25 4.57 0.45 o -4 -5 2 576.17 603.99 19.80 o -3 -5 2 77.20 77.48 2.59 o -2 -5 2 518.99 519.01 11.12 o -1 -5 2 19.66 18.46 0.44 o 0 -5 2 149.78 186.57 6.11 o 1 -5 2 7.47 9.88 1.15 o 2 -5 2 617.57 655.64 19.21 o 3 -5 2 89.17 93.16 1.84 o 4 -5 2 16.78 17.80 0.48 o 5 -5 2 3.63 4.73 0.50 o -6 -4 2 14.89 14.36 0.62 o -5 -4 2 32.75 33.01 2.32 o -4 -4 2 191.02 186.45 3.38 o -3 -4 2 10.84 10.18 0.46 o -2 -4 2 916.18 948.56 13.30 o -1 -4 2 191.18 172.18 6.74 o 0 -4 2 99.56 123.80 3.10 o 1 -4 2 759.29 735.95 18.29 o 2 -4 2 217.82 214.12 6.94 o 3 -4 2 339.38 337.43 9.77 o 4 -4 2 167.31 178.17 2.49 o 5 -4 2 58.92 52.71 1.79 o -6 -3 2 160.10 156.20 3.45 o -5 -3 2 20.25 22.33 0.55 o -4 -3 2 433.67 423.24 5.06 o -3 -3 2 108.93 120.12 1.81 o -2 -3 2 828.36 923.12 15.71 o -1 -3 2 485.32 487.21 11.91 o 0 -3 2 733.27 851.86 20.91 o 1 -3 2 427.91 430.38 7.39 o 2 -3 2 71.40 66.44 2.23 o 3 -3 2 2.84 3.33 0.44 o 4 -3 2 0.01 0.36 0.44 o 5 -3 2 32.79 26.02 0.66 o 6 -3 2 15.02 16.45 0.71 o -6 -2 2 22.22 22.15 1.14 o -5 -2 2 80.66 79.06 3.23 o -4 -2 2 409.98 418.61 2.31 o -3 -2 2 170.14 177.88 1.34 o -2 -2 2 1359.46 1465.58 18.24 o -1 -2 2 1384.44 1373.00 29.27 o 0 -2 2 2.34 3.61 0.66 o 1 -2 2 1915.78 1801.00 41.02 o 2 -2 2 707.45 660.12 16.37 o 3 -2 2 463.13 495.58 3.87 o 4 -2 2 355.91 379.16 10.36 o 5 -2 2 238.01 217.80 4.99 o 6 -2 2 128.78 117.37 2.25 o -6 -1 2 138.96 151.03 2.61 o -5 -1 2 14.04 14.56 0.52 o -4 -1 2 747.25 763.24 7.88 o -3 -1 2 157.13 165.58 4.06 o -2 -1 2 1969.66 2033.08 41.70 o -1 -1 2 185.90 203.21 5.15 o 0 -1 2 1094.39 945.54 45.81 o 1 -1 2 228.35 253.71 6.35 o 2 -1 2 342.61 343.21 3.38 o 3 -1 2 224.49 244.78 4.97 o 4 -1 2 2.41 2.43 0.44 o 5 -1 2 48.84 39.02 0.71 o 6 -1 2 9.45 9.19 0.52 o 7 -1 2 12.35 13.61 0.95 o -6 0 2 2.45 2.54 0.45 o -5 0 2 5.13 5.46 0.50 o -4 0 2 1452.00 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43.31 o 2 1 11 8.87 8.58 0.52 o 3 1 11 122.19 135.02 4.00 o 4 1 11 36.12 37.81 1.22 o 5 1 11 10.45 10.40 0.48 o 6 1 11 59.55 58.24 1.85 o -3 2 11 0.08 0.45 1.14 o -2 2 11 0.03 0.82 0.50 o -1 2 11 3.27 2.56 0.39 o 0 2 11 4.99 5.75 0.39 o 1 2 11 0.01 0.59 0.46 o 2 2 11 28.29 27.04 0.59 o 3 2 11 24.43 28.79 0.69 o 4 2 11 27.58 33.99 1.23 o 5 2 11 0.01 0.55 0.51 o 6 2 11 94.47 99.47 5.22 o -2 3 11 104.02 100.66 4.79 o -1 3 11 192.76 189.85 6.28 o 0 3 11 117.25 110.84 1.61 o 1 3 11 554.01 568.12 15.56 o 2 3 11 23.39 22.37 0.91 o 3 3 11 78.77 78.60 3.26 o 4 3 11 41.34 46.17 2.24 o 5 3 11 18.49 20.41 0.80 o 6 3 11 184.63 181.29 1.60 o -2 4 11 11.52 10.79 0.58 o -1 4 11 3.68 4.68 0.47 o 0 4 11 7.25 6.51 0.45 o 1 4 11 3.07 3.69 0.42 o 2 4 11 46.77 43.15 3.61 o 3 4 11 5.87 7.11 0.56 o 4 4 11 76.96 78.67 6.33 o 5 4 11 6.27 6.94 0.78 o -1 5 11 171.50 172.76 4.31 o 0 5 11 161.04 160.44 6.09 o 1 5 11 44.33 45.54 1.76 o 2 5 11 0.63 1.47 0.52 o 3 5 11 38.22 35.11 2.35 o 4 5 11 177.84 173.33 19.69 o 5 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3.51 o 0 0 12 42.64 43.47 1.03 o 1 0 12 42.74 44.91 2.06 o 2 0 12 10.78 11.24 0.60 o 3 0 12 68.49 71.72 2.97 o 4 0 12 23.44 27.64 1.80 o 5 0 12 33.61 38.02 1.51 o -2 1 12 5.97 5.63 0.62 o -1 1 12 34.20 32.06 0.86 o 0 1 12 19.13 19.32 0.52 o 1 1 12 56.47 57.74 0.99 o 2 1 12 18.84 19.19 0.59 o 3 1 12 67.28 69.93 1.67 o 4 1 12 3.64 3.86 0.53 o 5 1 12 2.20 2.89 0.40 o -2 2 12 193.39 176.91 2.10 o -1 2 12 40.60 40.65 0.67 o 0 2 12 30.36 33.02 0.91 o 1 2 12 16.11 17.87 0.61 o 2 2 12 23.93 25.85 0.74 o 3 2 12 35.83 40.32 1.21 o 4 2 12 86.76 93.07 3.53 o 5 2 12 1.00 1.87 0.57 o -1 3 12 37.69 34.65 1.15 o 0 3 12 3.89 3.37 0.39 o 1 3 12 70.78 66.42 3.23 o 2 3 12 3.12 3.57 0.61 o 3 3 12 7.81 8.55 0.66 o 4 3 12 0.73 1.66 0.75 o 5 3 12 8.24 8.66 0.65 o -1 4 12 3.55 4.86 0.54 o 0 4 12 1.94 3.05 1.02 o 1 4 12 142.65 144.34 3.10 o 2 4 12 9.73 12.18 0.63 o 3 4 12 20.40 18.99 1.13 o 4 4 12 17.70 22.51 3.94 o 5 4 12 0.03 0.81 0.73 o 0 5 12 5.19 5.12 0.44 o 1 5 12 11.04 10.13 0.57 o 2 5 12 7.51 7.00 0.45 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