#------------------------------------------------------------------------------ #$Date: 2011-04-13 11:12:47 +0300 (Wed, 13 Apr 2011) $ #$Revision: 17966 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2229333.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229333_Fobs loop_ _publ_author_name 'Barryala, Yamna' 'Massip, St\'ephane' 'Lazar, Sa\"id' 'Essassi, El Mokhtar' 'Zouihri, Hafid' _publ_section_title ; Methyl 2-(3-oxo-3,4-dihydro-2H-1,4-benzothiazin-4-yl)acetate ; _journal_coeditor_code BT5472 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o724 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.710 _cell_angle_gamma 90.000 _cell_length_a 17.3470 _cell_length_b 8.7240 _cell_length_c 7.2740 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high 0.8511 _[local]_cod_data_source_file bt5472Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BB10' _shelx_refln_list_code 4 _shelx_f_calc_maximum 102.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8.46 10.00 0.20 o 2 0 0 2957.12 2870.38 19.43 o 3 0 0 1402.07 1142.10 13.28 o 4 0 0 4933.53 4832.31 35.52 o 5 0 0 919.97 857.23 4.12 o 6 0 0 2797.07 2360.53 28.23 o 7 0 0 701.39 682.31 4.41 o 8 0 0 1405.16 1323.43 6.87 o 9 0 0 106.60 98.40 1.85 o 10 0 0 2413.92 2473.87 11.32 o 11 0 0 62.40 36.06 0.95 o 12 0 0 2557.27 2716.18 13.64 o 13 0 0 86.11 79.01 1.65 o 14 0 0 2965.17 3164.63 16.59 o 15 0 0 1089.25 1101.83 9.82 o 16 0 0 0.04 -0.24 2.90 o 17 0 0 2.60 3.22 1.38 o 18 0 0 21.66 25.02 1.23 o 19 0 0 278.60 273.93 4.30 o 20 0 0 69.14 64.10 1.29 o 1 1 0 6.71 10.66 0.24 o 2 1 0 3051.72 3055.41 22.88 o 3 1 0 1544.61 1273.89 15.40 o 4 1 0 123.51 108.35 1.37 o 5 1 0 1645.20 1203.86 18.43 o 6 1 0 1030.14 841.00 4.66 o 7 1 0 668.81 587.23 4.18 o 8 1 0 1810.67 1711.09 8.10 o 9 1 0 116.21 108.94 1.92 o 10 1 0 533.22 500.03 5.03 o 11 1 0 39.08 35.32 0.97 o 12 1 0 271.71 262.38 4.13 o 13 1 0 180.84 162.98 3.15 o 14 1 0 0.73 2.28 1.60 o 15 1 0 288.60 287.57 5.13 o 16 1 0 20.22 23.67 1.21 o 17 1 0 46.11 53.13 1.60 o 18 1 0 0.10 -1.21 1.41 o 19 1 0 48.08 47.33 1.33 o 20 1 0 31.07 35.33 1.00 o 0 2 0 1312.52 1177.92 15.29 o 1 2 0 1987.71 2022.86 20.88 o 2 2 0 3308.89 3331.09 29.21 o 3 2 0 1606.54 1313.85 18.30 o 4 2 0 1551.85 1508.11 5.95 o 5 2 0 107.33 83.47 1.51 o 6 2 0 985.63 922.11 5.27 o 7 2 0 293.54 254.13 2.98 o 8 2 0 1048.98 969.49 6.27 o 9 2 0 212.40 216.10 3.20 o 10 2 0 321.52 315.64 4.17 o 11 2 0 70.72 68.34 1.39 o 12 2 0 62.42 62.41 1.38 o 13 2 0 48.42 47.31 1.31 o 14 2 0 123.60 130.63 2.59 o 15 2 0 33.25 35.51 1.46 o 16 2 0 38.91 35.27 1.43 o 17 2 0 46.94 45.00 1.32 o 18 2 0 35.44 35.57 1.34 o 19 2 0 26.04 26.00 1.08 o 1 3 0 2819.81 2713.63 30.27 o 2 3 0 2529.89 2220.53 27.70 o 3 3 0 197.65 192.94 2.28 o 4 3 0 814.18 834.05 4.99 o 5 3 0 1148.70 1232.35 6.47 o 6 3 0 165.37 169.35 2.52 o 7 3 0 77.58 100.03 1.78 o 8 3 0 79.90 49.94 1.08 o 9 3 0 608.39 626.94 5.81 o 10 3 0 6.05 9.81 0.69 o 11 3 0 10.73 14.85 0.77 o 12 3 0 167.10 167.97 3.22 o 13 3 0 75.67 77.90 1.62 o 14 3 0 0.23 0.00 0.00 o 15 3 0 327.97 343.62 5.63 o 16 3 0 90.45 93.94 1.84 o 17 3 0 22.13 17.24 1.03 o 18 3 0 64.99 70.89 1.55 o 19 3 0 0.25 0.00 0.00 o 0 4 0 379.89 390.52 3.59 o 1 4 0 8.32 8.79 0.48 o 2 4 0 223.39 243.17 2.91 o 3 4 0 1191.87 1231.13 6.83 o 4 4 0 84.85 85.82 1.68 o 5 4 0 72.23 77.43 1.70 o 6 4 0 5.40 5.32 0.53 o 7 4 0 241.51 236.30 3.57 o 8 4 0 128.03 137.59 2.46 o 9 4 0 2.58 2.70 1.08 o 10 4 0 0.33 3.77 1.19 o 11 4 0 83.09 83.81 1.74 o 12 4 0 245.40 263.16 4.68 o 13 4 0 204.88 198.82 3.65 o 14 4 0 28.50 27.11 1.21 o 15 4 0 0.17 -0.69 1.39 o 16 4 0 85.23 87.51 1.69 o 17 4 0 24.20 27.20 1.26 o 18 4 0 16.69 19.86 1.01 o 1 5 0 60.07 74.99 1.60 o 2 5 0 181.64 170.32 2.88 o 3 5 0 27.66 20.09 0.71 o 4 5 0 56.14 65.79 1.34 o 5 5 0 1232.21 1255.92 8.59 o 6 5 0 142.54 157.48 3.08 o 7 5 0 5.05 7.32 0.73 o 8 5 0 27.21 32.21 1.19 o 9 5 0 93.82 84.38 1.70 o 10 5 0 260.20 250.95 4.58 o 11 5 0 353.07 376.77 5.79 o 12 5 0 6.81 8.26 0.97 o 13 5 0 1.08 2.40 1.44 o 14 5 0 72.26 75.39 1.60 o 15 5 0 73.24 74.95 1.66 o 16 5 0 0.28 -0.36 1.25 o 17 5 0 37.28 39.97 1.15 o 0 6 0 1604.76 1629.21 10.28 o 1 6 0 56.20 54.61 1.25 o 2 6 0 151.66 147.80 2.73 o 3 6 0 1343.27 1345.06 9.48 o 4 6 0 383.93 369.46 5.09 o 5 6 0 128.17 123.69 2.42 o 6 6 0 54.34 58.13 1.47 o 7 6 0 459.85 439.81 6.07 o 8 6 0 259.16 233.65 4.42 o 9 6 0 0.09 1.43 1.43 o 10 6 0 159.23 156.23 3.42 o 11 6 0 109.74 136.49 2.67 o 12 6 0 123.95 118.26 2.34 o 13 6 0 23.79 23.74 1.09 o 14 6 0 27.96 29.29 1.17 o 15 6 0 257.25 271.94 4.22 o 16 6 0 58.96 61.28 1.34 o 1 7 0 308.66 289.13 4.95 o 2 7 0 529.12 506.02 6.42 o 3 7 0 14.08 13.41 1.14 o 4 7 0 73.65 73.54 1.62 o 5 7 0 292.03 291.06 5.02 o 6 7 0 142.22 146.60 2.90 o 7 7 0 10.94 6.55 0.97 o 8 7 0 294.32 276.20 4.91 o 9 7 0 102.20 109.88 2.15 o 10 7 0 46.53 44.86 1.38 o 11 7 0 65.84 71.24 1.73 o 12 7 0 44.74 44.93 1.38 o 13 7 0 118.32 121.22 2.25 o 14 7 0 89.53 89.61 1.89 o 0 8 0 5.35 1.70 1.70 o 1 8 0 0.54 8.75 0.97 o 2 8 0 18.00 15.30 1.21 o 3 8 0 307.50 270.19 5.15 o 4 8 0 5.42 4.57 1.68 o 5 8 0 104.04 98.35 1.91 o 6 8 0 0.29 2.33 1.63 o 7 8 0 534.31 510.98 6.70 o 8 8 0 110.04 129.55 2.60 o 9 8 0 12.36 13.69 1.01 o 10 8 0 1.20 2.57 1.28 o 11 8 0 103.67 106.63 2.12 o 12 8 0 14.01 13.26 0.83 o 1 9 0 54.95 52.13 1.50 o 2 9 0 5.86 2.74 1.48 o 3 9 0 8.96 7.85 0.83 o 4 9 0 33.79 35.96 1.21 o 5 9 0 19.63 15.59 1.16 o 6 9 0 73.48 65.13 1.64 o 7 9 0 3.18 2.70 0.84 o 8 9 0 28.62 26.68 1.07 o 9 9 0 10.12 10.01 0.81 o 0 10 0 7.45 4.01 0.86 o 1 10 0 0.21 1.14 0.99 o 2 10 0 2.22 1.67 1.11 o 3 10 0 32.30 24.77 0.94 o 4 10 0 86.10 77.02 1.52 o -20 1 1 20.31 21.85 0.94 o -19 1 1 100.31 103.46 1.92 o -18 1 1 10.83 11.22 1.04 o -17 1 1 27.22 28.24 1.16 o -16 1 1 277.41 260.66 4.91 o -15 1 1 641.48 652.64 7.64 o -14 1 1 914.25 924.16 8.69 o -13 1 1 15.27 15.39 1.03 o -12 1 1 652.75 630.32 6.40 o -11 1 1 124.94 116.77 2.25 o -10 1 1 9.07 5.24 0.55 o -9 1 1 90.22 83.24 1.66 o -8 1 1 280.47 279.84 3.18 o -7 1 1 127.62 107.94 1.81 o -6 1 1 336.02 301.91 2.81 o -5 1 1 1392.77 1511.92 5.90 o -4 1 1 1314.72 1056.69 15.87 o -3 1 1 827.75 926.63 3.79 o -2 1 1 6452.16 8115.45 45.31 o -1 1 1 443.05 439.18 2.28 o 1 1 1 109.87 90.83 1.08 o 2 1 1 260.67 188.09 1.65 o 3 1 1 2170.83 1556.34 19.54 o 4 1 1 432.65 367.55 2.75 o 5 1 1 271.27 234.62 2.38 o 6 1 1 521.25 485.95 3.73 o 7 1 1 1794.59 1826.71 8.18 o 8 1 1 47.56 46.33 0.91 o 9 1 1 370.11 394.83 4.32 o 10 1 1 407.85 398.40 4.70 o 11 1 1 7.21 8.79 0.70 o 12 1 1 414.10 417.03 5.48 o 13 1 1 12.69 15.86 1.10 o 14 1 1 24.71 26.51 1.18 o 15 1 1 0.21 1.22 1.46 o 16 1 1 25.00 25.71 1.18 o 17 1 1 10.00 9.92 1.08 o 18 1 1 0.34 1.29 1.29 o 19 1 1 18.19 22.26 1.02 o -19 2 1 2.66 2.27 1.30 o -18 2 1 51.48 53.31 1.39 o -17 2 1 168.67 176.26 3.39 o -16 2 1 0.72 0.72 1.44 o -15 2 1 42.94 38.35 1.46 o -14 2 1 1447.39 1523.98 11.38 o -13 2 1 425.64 409.76 5.69 o -12 2 1 147.11 141.29 2.73 o -11 2 1 4.58 2.23 1.20 o -10 2 1 1227.05 1207.94 8.16 o -9 2 1 79.31 80.86 1.71 o -8 2 1 525.15 600.10 4.91 o -7 2 1 7.20 8.23 0.49 o -6 2 1 1869.03 1929.37 7.86 o -5 2 1 2446.99 2174.90 28.19 o -4 2 1 2305.48 1989.53 25.20 o -3 2 1 407.24 445.09 3.01 o -2 2 1 10416.49 13370.00 71.77 o -1 2 1 1196.44 1295.47 17.28 o 1 2 1 5048.25 4504.26 37.05 o 2 2 1 939.46 835.50 4.15 o 3 2 1 32.73 25.99 0.56 o 4 2 1 64.65 60.67 1.14 o 5 2 1 449.28 375.81 3.28 o 6 2 1 840.18 846.02 5.37 o 7 2 1 202.07 209.49 2.87 o 8 2 1 598.19 508.88 4.81 o 9 2 1 1038.01 1073.41 7.48 o 10 2 1 9.22 10.09 0.66 o 11 2 1 10.97 9.18 0.75 o 12 2 1 1363.63 1404.13 10.45 o 13 2 1 151.65 168.20 3.44 o 14 2 1 6.17 7.22 0.96 o 15 2 1 597.86 642.75 7.45 o 16 2 1 8.94 8.74 0.92 o 17 2 1 130.69 137.77 2.70 o 18 2 1 0.53 1.38 1.21 o 19 2 1 35.27 32.27 1.07 o -19 3 1 44.14 47.73 1.28 o -18 3 1 27.04 28.00 1.26 o -17 3 1 1.67 1.26 1.26 o -16 3 1 68.76 73.52 1.63 o -15 3 1 421.12 425.21 6.17 o -14 3 1 544.53 529.89 6.89 o -13 3 1 179.42 179.70 3.45 o -12 3 1 482.80 473.28 6.03 o -11 3 1 381.30 373.55 5.05 o -10 3 1 156.01 154.94 2.75 o -9 3 1 705.33 692.14 6.12 o -8 3 1 105.77 71.13 1.35 o -7 3 1 803.64 807.70 5.84 o -6 3 1 0.59 1.69 0.63 o -5 3 1 291.87 266.05 2.99 o -4 3 1 198.56 173.27 2.34 o -3 3 1 66.30 68.20 1.27 o -2 3 1 1274.96 1616.09 6.67 o -1 3 1 653.74 768.13 4.44 o 0 3 1 403.39 539.52 3.68 o 1 3 1 1175.24 1189.69 5.67 o 2 3 1 3.64 2.08 0.39 o 3 3 1 602.40 533.95 4.01 o 4 3 1 3426.90 2787.80 36.16 o 5 3 1 2365.56 2372.28 9.73 o 6 3 1 15.70 21.02 0.69 o 7 3 1 608.88 519.81 4.96 o 8 3 1 20.71 21.38 0.73 o 9 3 1 86.12 71.08 1.49 o 10 3 1 571.15 559.88 6.09 o 11 3 1 47.27 45.05 1.23 o 12 3 1 4.02 11.64 0.90 o 13 3 1 972.15 1027.12 9.43 o 14 3 1 60.31 68.25 1.71 o 15 3 1 230.43 221.30 3.82 o 16 3 1 9.48 8.92 1.09 o 17 3 1 226.76 245.25 4.20 o 18 3 1 34.46 36.53 1.22 o -18 4 1 2.40 2.88 1.21 o -17 4 1 349.33 345.04 4.93 o -16 4 1 8.90 9.02 0.86 o -15 4 1 6.86 6.54 0.93 o -14 4 1 64.21 63.22 1.70 o -13 4 1 26.51 26.96 1.20 o -12 4 1 63.25 66.15 1.61 o -11 4 1 0.40 2.15 1.29 o -10 4 1 1501.19 1511.35 10.56 o -9 4 1 57.59 44.42 1.26 o -8 4 1 304.23 311.08 4.30 o -7 4 1 1584.18 1651.64 9.44 o -6 4 1 116.82 79.71 1.62 o -5 4 1 572.13 606.70 5.10 o -4 4 1 449.85 483.66 4.48 o -3 4 1 803.36 824.29 5.67 o -2 4 1 702.27 770.09 5.29 o -1 4 1 143.78 193.56 2.65 o 0 4 1 48.72 40.60 0.86 o 1 4 1 50.01 36.88 0.82 o 2 4 1 2408.78 2371.21 9.88 o 3 4 1 255.34 264.73 3.31 o 4 4 1 1646.15 1612.52 8.47 o 5 4 1 1369.20 1317.30 7.91 o 6 4 1 1.02 2.73 0.86 o 7 4 1 987.31 1039.19 7.65 o 8 4 1 184.32 161.57 2.82 o 9 4 1 338.92 328.87 4.88 o 10 4 1 0.98 3.36 1.05 o 11 4 1 63.48 68.43 1.59 o 12 4 1 267.87 272.74 5.06 o 13 4 1 55.58 55.81 1.71 o 14 4 1 157.84 174.54 3.58 o 15 4 1 258.36 264.26 4.69 o 16 4 1 32.26 33.79 1.17 o 17 4 1 12.43 14.55 0.97 o 18 4 1 67.23 73.41 1.49 o -17 5 1 5.20 5.89 0.75 o -16 5 1 9.03 7.36 0.92 o -15 5 1 69.52 67.57 1.48 o -14 5 1 44.26 40.83 1.38 o -13 5 1 80.90 82.66 1.69 o -12 5 1 357.36 329.86 5.42 o -11 5 1 2.97 4.02 0.71 o -10 5 1 152.78 154.56 3.17 o -9 5 1 0.15 0.42 1.27 o -8 5 1 135.23 108.80 2.18 o -7 5 1 37.71 35.31 1.10 o -6 5 1 71.83 65.27 1.37 o -5 5 1 2.18 2.09 0.64 o -4 5 1 423.75 410.29 4.66 o -3 5 1 20.39 16.84 0.73 o -2 5 1 227.85 215.40 3.27 o -1 5 1 10.12 14.36 0.69 o 0 5 1 913.88 1028.17 7.17 o 1 5 1 1224.36 1226.86 7.89 o 2 5 1 819.34 756.73 6.30 o 3 5 1 55.36 47.73 1.05 o 4 5 1 4.14 3.16 1.10 o 5 5 1 19.95 24.04 0.84 o 6 5 1 17.68 15.49 0.90 o 7 5 1 58.84 57.01 1.36 o 8 5 1 276.99 289.57 4.63 o 9 5 1 8.84 10.19 0.89 o 10 5 1 227.76 229.80 4.48 o 11 5 1 6.98 7.97 0.97 o 12 5 1 0.12 -0.97 1.45 o 13 5 1 21.95 19.68 1.17 o 14 5 1 99.96 98.25 1.96 o 15 5 1 234.01 244.35 4.28 o 16 5 1 10.31 10.92 0.96 o 17 5 1 53.60 50.64 1.13 o -16 6 1 19.61 18.38 0.98 o -15 6 1 71.31 66.88 1.55 o -14 6 1 8.35 10.15 1.00 o -13 6 1 51.22 51.20 1.32 o -12 6 1 12.69 13.36 0.94 o -11 6 1 1.50 2.42 1.21 o -10 6 1 51.03 52.03 1.46 o -9 6 1 59.80 48.90 1.43 o -8 6 1 222.57 227.86 4.41 o -7 6 1 99.30 94.22 2.00 o -6 6 1 48.81 42.97 1.27 o -5 6 1 30.62 32.43 1.22 o -4 6 1 7.14 8.96 0.78 o -3 6 1 0.30 0.76 1.13 o -2 6 1 11.10 12.75 0.92 o -1 6 1 120.68 126.05 2.57 o 0 6 1 438.17 434.23 5.40 o 1 6 1 79.17 63.11 1.29 o 2 6 1 8.72 10.50 0.94 o 3 6 1 1.22 0.58 1.35 o 4 6 1 137.17 151.71 3.02 o 5 6 1 8.71 11.90 1.04 o 6 6 1 333.70 315.79 5.09 o 7 6 1 0.95 0.68 1.14 o 8 6 1 21.20 25.74 1.18 o 9 6 1 63.66 62.54 1.70 o 10 6 1 0.32 1.94 1.46 o 11 6 1 0.60 1.19 1.19 o 12 6 1 0.00 -1.12 1.35 o 13 6 1 7.62 9.05 0.82 o 14 6 1 18.82 19.26 1.08 o 15 6 1 0.01 2.69 1.04 o -14 7 1 9.49 10.58 0.89 o -13 7 1 17.64 16.75 1.06 o -12 7 1 27.23 22.15 1.00 o -11 7 1 12.26 14.37 1.09 o -10 7 1 1.70 3.23 1.38 o -9 7 1 53.17 56.91 1.43 o -8 7 1 113.20 101.15 1.95 o -7 7 1 117.95 107.61 2.20 o -6 7 1 39.52 38.76 1.44 o -5 7 1 28.49 30.57 1.19 o -4 7 1 52.26 48.76 1.40 o -3 7 1 18.85 21.11 1.15 o -2 7 1 46.40 40.20 1.36 o -1 7 1 326.80 336.73 5.26 o 0 7 1 256.98 251.02 4.67 o 1 7 1 116.16 117.30 2.27 o 2 7 1 9.72 9.14 0.91 o 3 7 1 11.10 13.44 0.93 o 4 7 1 30.57 27.84 1.18 o 5 7 1 78.82 80.25 1.68 o 6 7 1 110.81 112.73 2.19 o 7 7 1 8.72 6.80 0.97 o 8 7 1 29.10 30.28 1.20 o 9 7 1 31.17 36.42 1.40 o 10 7 1 93.38 93.28 2.00 o 11 7 1 18.59 17.23 1.03 o 12 7 1 0.01 1.46 1.10 o 13 7 1 31.56 30.16 1.10 o 14 7 1 6.09 5.10 0.77 o -12 8 1 0.35 0.71 0.99 o -11 8 1 2.40 2.96 1.15 o -10 8 1 112.68 108.77 2.05 o -9 8 1 54.41 58.09 1.42 o -8 8 1 28.51 31.68 1.29 o -7 8 1 219.72 211.28 3.87 o -6 8 1 495.75 484.97 6.65 o -5 8 1 142.47 147.76 2.86 o -4 8 1 97.50 94.12 1.93 o -3 8 1 153.42 145.55 2.92 o -2 8 1 194.36 184.92 3.66 o -1 8 1 43.45 44.70 1.46 o 0 8 1 15.51 13.59 1.21 o 1 8 1 57.05 51.98 1.70 o 2 8 1 354.64 335.12 5.65 o 3 8 1 95.90 85.41 1.93 o 4 8 1 55.18 50.52 1.43 o 5 8 1 125.82 126.17 2.58 o 6 8 1 197.43 195.21 3.67 o 7 8 1 1.31 0.22 3.06 o 8 8 1 235.51 216.61 4.17 o 9 8 1 208.90 220.72 4.03 o 10 8 1 23.31 25.60 1.02 o 11 8 1 11.97 13.32 0.89 o 12 8 1 35.81 35.55 0.98 o -9 9 1 12.86 10.48 0.82 o -8 9 1 29.14 29.31 1.07 o -7 9 1 206.08 204.31 3.74 o -6 9 1 31.19 29.09 1.26 o -5 9 1 6.16 6.47 0.95 o -4 9 1 46.12 43.07 1.39 o -3 9 1 56.78 55.53 1.43 o -2 9 1 114.60 101.69 2.08 o -1 9 1 143.67 128.87 2.53 o 0 9 1 115.18 110.83 2.32 o 1 9 1 22.63 22.48 1.25 o 2 9 1 103.87 93.24 1.85 o 3 9 1 42.05 37.44 1.40 o 4 9 1 90.49 99.31 1.94 o 5 9 1 4.15 3.12 1.47 o 6 9 1 4.17 4.12 1.37 o 7 9 1 58.45 54.06 1.42 o 8 9 1 10.28 11.57 0.85 o -4 10 1 1.49 -0.25 0.99 o -3 10 1 4.42 5.59 0.78 o -2 10 1 68.42 73.98 1.48 o -1 10 1 1.64 0.68 1.10 o 0 10 1 34.71 33.88 1.10 o 1 10 1 16.15 14.90 0.95 o 2 10 1 53.72 56.94 1.32 o 3 10 1 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