#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/94/2229442.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229442_Fobs loop_ _publ_author_name 'Ge, Yu-Hua' 'Han, Pei' 'Wei, Ping' 'Ou-yang, Ping-Kai' _publ_section_title ; 6-(1H-Tetrazol-5-yl)-1H-indole monohydrate ; _journal_coeditor_code LH5195 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o692 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.594 _cell_angle_gamma 90.000 _cell_length_a 17.1754 _cell_length_b 4.0653 _cell_length_c 14.4212 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.8413 _[local]_cod_data_source_file lh5195Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 IN P2(1)/C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 126.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 514.46 477.12 23.02 o 4 0 0 6657.81 6410.12 136.84 o 5 0 0 401.56 388.91 17.31 o 6 0 0 1717.08 1739.57 53.60 o 7 0 0 281.32 288.69 18.56 o 8 0 0 341.02 361.00 30.51 o 9 0 0 49.98 61.20 11.75 o 10 0 0 512.95 566.39 38.75 o 11 0 0 103.58 75.47 20.62 o 12 0 0 50.37 50.18 17.56 o 13 0 0 2.35 27.71 14.13 o 14 0 0 626.53 583.27 58.02 o 15 0 0 572.55 519.06 50.52 o 16 0 0 1112.44 1088.93 78.24 o 17 0 0 186.34 180.84 32.53 o 18 0 0 14.25 43.63 29.30 o 19 0 0 53.36 48.98 37.72 o 1 1 0 467.17 411.48 15.29 o 2 1 0 75.72 73.32 5.05 o 3 1 0 14147.40 13352.79 118.82 o 4 1 0 42.23 41.58 1.87 o 5 1 0 193.01 197.81 6.06 o 6 1 0 71.70 68.49 3.28 o 7 1 0 205.72 222.25 12.86 o 8 1 0 1.65 5.79 2.49 o 9 1 0 437.61 437.36 18.84 o 10 1 0 9.31 26.20 7.87 o 11 1 0 149.56 143.74 9.24 o 12 1 0 122.16 109.08 10.75 o 13 1 0 119.79 96.08 11.85 o 14 1 0 27.59 18.75 8.24 o 15 1 0 3.03 4.39 7.18 o 16 1 0 13.77 26.40 15.01 o 17 1 0 14.88 0.00 15.24 o 18 1 0 11.52 2.98 12.77 o 19 1 0 120.81 126.78 54.69 o 0 2 0 65.40 100.37 25.45 o 1 2 0 248.08 231.94 14.83 o 2 2 0 65.32 61.87 7.08 o 3 2 0 32.28 36.52 4.41 o 4 2 0 154.47 149.21 7.23 o 5 2 0 4.87 4.49 2.76 o 6 2 0 733.75 686.37 32.17 o 7 2 0 90.39 110.03 16.29 o 8 2 0 199.37 195.92 18.80 o 9 2 0 15.66 1.61 7.61 o 10 2 0 268.06 279.43 25.37 o 11 2 0 0.95 0.00 10.46 o 12 2 0 189.67 192.62 24.61 o 13 2 0 0.01 43.61 23.46 o 14 2 0 2.43 1.89 12.14 o 15 2 0 12.44 13.86 14.85 o 16 2 0 36.85 32.00 16.68 o 17 2 0 7.97 48.76 32.58 o 1 3 0 41.79 43.04 8.82 o 2 3 0 21.77 16.91 6.27 o 3 3 0 0.02 0.00 5.60 o 4 3 0 134.76 137.59 9.96 o 5 3 0 5.18 5.92 4.16 o 6 3 0 1.54 1.12 6.51 o 7 3 0 66.78 89.28 18.61 o 8 3 0 3.37 3.05 9.54 o 9 3 0 107.35 85.52 17.85 o 10 3 0 0.57 4.79 11.36 o 11 3 0 1.74 21.37 14.25 o 12 3 0 53.50 50.65 17.23 o 13 3 0 0.63 7.11 12.24 o 14 3 0 0.67 10.62 14.54 o 15 3 0 26.22 41.05 19.61 o 0 4 0 0.97 2.48 9.69 o 1 4 0 6.15 0.00 8.98 o 2 4 0 1.04 1.10 5.48 o 3 4 0 29.02 28.18 11.21 o 4 4 0 2.08 11.57 13.82 o 5 4 0 0.43 19.64 21.30 o 6 4 0 24.69 26.35 12.83 o 7 4 0 16.32 21.50 13.62 o 8 4 0 0.51 0.00 12.70 o 9 4 0 2.18 0.00 10.58 o 10 4 0 3.70 13.55 14.69 o -19 1 1 38.60 24.04 16.35 o -18 1 1 256.99 250.43 32.23 o -17 1 1 57.27 51.46 17.82 o -16 1 1 45.10 55.60 17.84 o -15 1 1 24.99 31.95 9.11 o -14 1 1 152.08 138.78 13.48 o -13 1 1 128.02 129.79 9.83 o -12 1 1 256.66 239.95 12.48 o -11 1 1 162.73 149.90 9.13 o -10 1 1 302.41 308.18 12.01 o -9 1 1 324.99 322.52 15.07 o -8 1 1 47.64 56.07 4.17 o -7 1 1 294.63 280.48 13.28 o -6 1 1 246.58 224.45 14.12 o -5 1 1 322.26 331.55 23.32 o -4 1 1 190.25 180.46 8.06 o -3 1 1 15985.40 15685.71 126.08 o -2 1 1 6466.28 6419.54 71.41 o -1 1 1 4720.48 4924.39 67.72 o 0 1 1 82.56 101.30 5.88 o 1 1 1 941.31 890.26 24.71 o 2 1 1 1878.72 1798.55 21.38 o 3 1 1 399.50 367.19 11.64 o 4 1 1 97.08 85.82 6.88 o 5 1 1 378.99 373.75 11.60 o 6 1 1 358.32 369.78 13.35 o 7 1 1 64.61 69.91 6.91 o 8 1 1 142.74 134.47 6.90 o 9 1 1 160.34 153.97 11.36 o 10 1 1 7.70 15.85 6.10 o 11 1 1 32.85 30.90 8.63 o 12 1 1 13.89 25.41 12.66 o 13 1 1 1116.80 1050.26 42.57 o 14 1 1 7.14 21.93 8.97 o 15 1 1 148.90 114.59 13.92 o 16 1 1 9.33 14.36 12.57 o 17 1 1 59.83 86.50 20.97 o 18 1 1 0.75 0.00 14.22 o -18 2 1 6.17 45.39 19.44 o -17 2 1 44.69 56.70 21.61 o -16 2 1 1.71 0.00 16.75 o -15 2 1 0.41 0.00 15.92 o -14 2 1 0.80 2.05 11.37 o -13 2 1 2.29 33.04 13.15 o -12 2 1 29.28 55.81 14.77 o -11 2 1 63.11 73.42 17.24 o -10 2 1 51.66 64.55 14.19 o -9 2 1 0.52 4.31 8.67 o -8 2 1 16.21 9.81 5.11 o -7 2 1 6.68 16.73 4.87 o -6 2 1 3134.19 3124.79 72.35 o -5 2 1 0.96 0.62 3.67 o -4 2 1 1029.42 941.85 36.46 o -3 2 1 292.36 303.34 10.57 o -2 2 1 566.02 586.38 18.42 o -1 2 1 632.67 654.21 20.55 o 0 2 1 77.80 96.26 9.01 o 1 2 1 0.52 5.37 4.13 o 2 2 1 0.82 1.49 2.96 o 3 2 1 210.55 193.66 10.26 o 4 2 1 145.35 148.81 7.47 o 5 2 1 0.05 0.00 3.99 o 6 2 1 0.12 17.36 8.32 o 7 2 1 12.50 27.62 15.10 o 8 2 1 228.75 231.52 25.15 o 9 2 1 76.71 108.68 18.08 o 10 2 1 672.01 649.87 44.50 o 11 2 1 117.34 129.24 20.31 o 12 2 1 24.84 30.43 13.11 o 13 2 1 43.97 19.09 11.59 o 14 2 1 66.53 76.56 18.46 o 15 2 1 0.01 0.00 13.03 o 16 2 1 2.59 0.00 13.94 o 17 2 1 7.71 14.86 15.53 o -15 3 1 31.53 20.11 15.96 o -14 3 1 6.98 11.60 13.35 o -13 3 1 55.63 42.99 17.05 o -12 3 1 0.00 6.15 11.96 o -11 3 1 13.36 4.27 11.62 o -10 3 1 1.45 28.56 13.32 o -9 3 1 124.32 114.81 19.47 o -8 3 1 17.73 32.70 12.82 o -7 3 1 35.44 68.43 14.11 o -6 3 1 55.80 74.94 9.98 o -5 3 1 75.95 80.22 10.71 o -4 3 1 1.17 13.08 5.16 o -3 3 1 24.97 39.92 9.53 o -2 3 1 377.86 333.67 18.60 o -1 3 1 65.40 68.02 16.01 o 0 3 1 7.37 9.33 9.21 o 1 3 1 6.87 10.64 6.70 o 2 3 1 38.07 30.24 7.36 o 3 3 1 57.52 55.76 7.47 o 4 3 1 116.70 95.95 8.65 o 5 3 1 29.78 35.31 7.60 o 6 3 1 42.91 40.37 11.53 o 7 3 1 65.33 92.70 18.17 o 8 3 1 8.55 21.57 12.16 o 9 3 1 91.90 103.95 20.56 o 10 3 1 2.93 13.56 12.24 o 11 3 1 1.82 10.16 11.60 o 12 3 1 3.76 9.92 13.05 o 13 3 1 4.34 5.29 12.08 o 14 3 1 58.37 74.72 20.06 o -11 4 1 0.66 0.56 11.71 o -10 4 1 4.41 0.00 13.79 o -9 4 1 8.61 12.58 13.42 o -8 4 1 7.61 0.00 8.80 o -7 4 1 0.07 2.55 10.57 o -6 4 1 3.20 1.54 9.52 o -5 4 1 37.88 52.30 15.49 o -4 4 1 0.93 36.00 13.60 o -3 4 1 13.00 12.94 8.64 o -2 4 1 5.49 2.60 6.21 o -1 4 1 12.34 1.52 5.85 o 0 4 1 70.19 75.26 13.22 o 1 4 1 205.82 193.30 18.75 o 2 4 1 4.91 17.25 7.77 o 3 4 1 0.18 0.00 8.05 o 4 4 1 5.09 21.83 13.32 o 5 4 1 5.68 6.73 10.99 o 6 4 1 40.45 50.70 19.28 o 7 4 1 2.28 6.39 12.20 o 8 4 1 0.68 5.76 11.01 o 9 4 1 3.36 0.00 13.65 o 10 4 1 11.92 14.44 13.53 o -20 0 2 2.83 0.00 41.64 o -19 0 2 21.15 27.75 18.69 o -18 0 2 7.31 36.83 20.18 o -17 0 2 159.41 142.94 30.70 o -16 0 2 1.37 6.32 13.13 o -15 0 2 527.34 522.30 36.46 o -14 0 2 41.26 45.29 13.09 o -13 0 2 383.77 390.24 26.92 o -12 0 2 429.73 427.86 27.06 o -11 0 2 228.82 231.17 16.72 o -10 0 2 167.10 162.59 12.86 o -9 0 2 248.86 267.65 16.10 o -8 0 2 110.56 106.75 9.77 o -7 0 2 777.27 781.35 24.84 o -6 0 2 1266.99 1236.23 44.93 o -5 0 2 135.23 136.47 8.53 o -4 0 2 12.34 13.58 5.53 o -3 0 2 3705.75 3592.68 62.79 o -2 0 2 94.82 84.25 4.48 o 1 0 2 13616.67 12236.37 151.63 o 2 0 2 1029.92 979.92 29.63 o 3 0 2 2185.68 2165.64 44.53 o 4 0 2 2284.74 2475.46 57.31 o 5 0 2 538.95 584.92 31.57 o 6 0 2 2.67 0.00 6.12 o 7 0 2 2157.51 2468.32 169.89 o 8 0 2 152.24 180.60 20.33 o 9 0 2 245.08 287.58 30.67 o 10 0 2 219.07 250.41 58.94 o 11 0 2 414.61 451.55 46.60 o 12 0 2 45.91 62.54 20.26 o 13 0 2 112.12 83.96 31.53 o 14 0 2 0.64 35.64 60.15 o 15 0 2 52.69 85.53 26.33 o 16 0 2 86.98 85.10 17.28 o 17 0 2 81.52 120.27 25.35 o 18 0 2 33.28 25.63 20.99 o -19 1 2 30.18 24.21 15.52 o -18 1 2 81.26 73.63 24.49 o -17 1 2 0.12 11.02 17.28 o -16 1 2 78.30 80.06 19.48 o -15 1 2 9.41 12.48 7.01 o -14 1 2 203.39 198.72 12.98 o -13 1 2 1.54 0.47 4.48 o -12 1 2 1.03 9.61 8.34 o -11 1 2 140.69 153.48 21.74 o -10 1 2 3.24 0.00 3.22 o -9 1 2 337.27 366.44 12.42 o -8 1 2 227.19 254.66 8.17 o -7 1 2 816.04 830.46 26.25 o -6 1 2 82.11 70.41 3.70 o -5 1 2 62.17 56.69 5.37 o -4 1 2 1646.48 1660.93 28.49 o -3 1 2 0.42 2.04 5.45 o -2 1 2 11781.25 12137.68 170.63 o -1 1 2 1128.13 1123.93 26.43 o 0 1 2 11.05 2.79 6.07 o 1 1 2 145.20 151.35 5.87 o 2 1 2 127.90 123.23 8.72 o 3 1 2 60.17 62.64 6.10 o 4 1 2 789.88 781.85 36.06 o 5 1 2 7.09 10.44 4.59 o 6 1 2 30.67 45.45 6.38 o 7 1 2 552.36 545.41 10.71 o 8 1 2 6.00 4.30 2.49 o 9 1 2 129.62 130.50 7.09 o 10 1 2 217.14 256.51 17.56 o 11 1 2 4.62 18.77 9.07 o 12 1 2 145.67 138.41 16.54 o 13 1 2 217.33 210.80 18.59 o 14 1 2 31.48 9.01 9.81 o 15 1 2 95.50 86.77 14.03 o 16 1 2 10.91 25.49 17.63 o 17 1 2 37.63 39.02 22.47 o 18 1 2 0.47 9.42 14.76 o -18 2 2 0.01 34.69 18.77 o -17 2 2 6.03 9.43 14.10 o -16 2 2 6.86 2.86 11.31 o -15 2 2 59.03 55.23 17.63 o -14 2 2 0.18 12.27 11.31 o -13 2 2 4.15 22.71 13.98 o -12 2 2 0.59 0.00 11.20 o -11 2 2 234.75 213.46 23.54 o -10 2 2 6.23 10.02 13.31 o -9 2 2 188.05 196.90 12.93 o -8 2 2 43.04 44.09 9.58 o -7 2 2 31.10 31.26 6.49 o -6 2 2 79.65 78.21 13.56 o -5 2 2 5885.21 5853.45 129.28 o -4 2 2 2.03 0.00 4.82 o -3 2 2 191.57 182.53 7.86 o -2 2 2 0.07 5.31 3.64 o -1 2 2 269.19 276.93 13.50 o 0 2 2 55.79 62.49 8.66 o 1 2 2 581.98 590.88 18.83 o 2 2 2 32.61 34.77 5.05 o 3 2 2 121.27 121.45 9.72 o 4 2 2 26.99 28.20 4.06 o 5 2 2 104.03 100.51 10.17 o 6 2 2 25.53 43.98 10.64 o 7 2 2 0.80 16.23 11.67 o 8 2 2 5.07 19.96 6.79 o 9 2 2 27.63 37.64 15.01 o 10 2 2 359.86 299.63 25.57 o 11 2 2 460.85 472.15 49.13 o 12 2 2 95.57 85.98 18.24 o 13 2 2 50.90 59.15 19.94 o 14 2 2 69.45 80.14 19.13 o 15 2 2 1.01 0.00 14.00 o 16 2 2 5.97 12.49 14.19 o -15 3 2 0.95 0.00 14.40 o -14 3 2 10.54 6.39 12.94 o -13 3 2 3.30 5.62 11.39 o -12 3 2 8.96 5.36 9.68 o -11 3 2 3.56 24.52 16.09 o -10 3 2 27.33 50.69 19.04 o -9 3 2 17.10 20.28 11.47 o -8 3 2 710.10 654.42 37.72 o -7 3 2 142.56 123.78 12.50 o -6 3 2 1.44 7.00 7.22 o -5 3 2 51.71 54.30 9.39 o -4 3 2 192.84 214.97 14.35 o -3 3 2 53.32 70.50 8.16 o -2 3 2 142.58 193.33 21.86 o -1 3 2 74.35 81.80 11.12 o 0 3 2 1.01 1.48 4.99 o 1 3 2 0.13 8.55 5.43 o 2 3 2 16.42 21.77 10.42 o 3 3 2 0.39 6.30 5.14 o 4 3 2 33.15 41.63 8.00 o 5 3 2 40.98 44.61 10.29 o 6 3 2 11.16 5.10 9.15 o 7 3 2 337.11 313.50 28.20 o 8 3 2 71.14 72.82 17.29 o 9 3 2 125.52 146.18 23.61 o 10 3 2 5.94 12.61 12.99 o 11 3 2 20.53 13.51 13.52 o 12 3 2 12.89 32.27 15.20 o 13 3 2 7.83 0.00 11.15 o 14 3 2 45.05 35.42 16.86 o -11 4 2 39.07 42.36 23.32 o -10 4 2 66.84 58.74 19.74 o -9 4 2 8.85 2.69 11.36 o -8 4 2 16.02 19.23 14.25 o -7 4 2 8.05 8.83 12.27 o -6 4 2 34.00 29.94 14.76 o -5 4 2 0.92 1.29 7.24 o -4 4 2 0.10 0.00 8.17 o -3 4 2 2.43 0.00 7.48 o -2 4 2 14.59 15.06 10.14 o -1 4 2 0.44 7.87 11.28 o 0 4 2 0.02 0.00 6.97 o 1 4 2 8.04 2.37 6.41 o 2 4 2 2.43 21.83 11.24 o 3 4 2 10.28 18.28 14.01 o 4 4 2 59.66 40.70 14.81 o 5 4 2 19.94 30.79 21.49 o 6 4 2 108.21 83.69 26.57 o 7 4 2 0.18 7.74 12.20 o 8 4 2 9.57 28.17 23.31 o 9 4 2 6.65 32.72 25.44 o -19 1 3 3.12 12.87 15.28 o -18 1 3 101.77 88.67 20.42 o -17 1 3 17.55 28.28 17.87 o -16 1 3 66.56 63.29 12.00 o -15 1 3 11.98 36.90 11.22 o -14 1 3 21.97 26.98 12.81 o -13 1 3 0.01 0.00 7.47 o -12 1 3 3.74 1.73 5.29 o -11 1 3 275.81 278.53 12.54 o -10 1 3 108.78 104.71 6.92 o -9 1 3 86.95 84.34 6.12 o -8 1 3 53.16 47.87 5.26 o -7 1 3 1870.46 1945.25 39.04 o -6 1 3 98.27 96.68 10.11 o -5 1 3 256.50 263.69 8.34 o -4 1 3 0.64 0.00 2.52 o -3 1 3 1.14 2.71 2.62 o -2 1 3 992.13 925.23 22.93 o -1 1 3 406.08 449.21 12.73 o 0 1 3 821.72 881.73 20.30 o 1 1 3 2619.43 2565.88 41.71 o 2 1 3 72.75 64.19 5.10 o 3 1 3 526.63 547.03 11.92 o 4 1 3 964.82 898.79 50.23 o 5 1 3 10.17 27.15 6.71 o 6 1 3 914.16 901.09 23.97 o 7 1 3 15.70 13.08 6.66 o 8 1 3 670.89 665.13 26.05 o 9 1 3 274.17 298.78 20.73 o 10 1 3 269.44 262.02 17.82 o 11 1 3 53.61 58.76 11.02 o 12 1 3 12.20 31.11 10.75 o 13 1 3 0.20 0.00 8.70 o 14 1 3 6.65 1.23 7.21 o 15 1 3 0.25 9.90 8.87 o 16 1 3 28.32 23.13 11.17 o 17 1 3 58.63 84.44 22.02 o -18 2 3 0.00 8.12 14.54 o -17 2 3 19.28 20.76 14.99 o -16 2 3 0.03 0.00 13.85 o -15 2 3 0.01 14.58 13.48 o -14 2 3 2.37 27.95 21.72 o -13 2 3 0.68 9.06 11.95 o -12 2 3 5.20 0.00 10.13 o -11 2 3 0.31 28.05 16.62 o -10 2 3 65.40 61.33 9.52 o -9 2 3 50.85 66.45 9.75 o -8 2 3 153.96 150.28 25.06 o -7 2 3 13.67 14.90 6.41 o -6 2 3 113.24 128.13 16.05 o -5 2 3 1658.44 1551.41 58.65 o -4 2 3 426.10 434.46 15.13 o -3 2 3 695.14 684.17 19.09 o -2 2 3 23.80 19.28 4.45 o -1 2 3 26.36 27.79 6.80 o 0 2 3 14.06 19.36 5.85 o 1 2 3 60.39 60.43 6.02 o 2 2 3 11.12 6.80 6.92 o 3 2 3 59.34 52.78 5.85 o 4 2 3 125.17 118.60 6.53 o 5 2 3 236.94 256.73 16.07 o 6 2 3 7.16 0.00 5.73 o 7 2 3 0.53 0.61 6.51 o 8 2 3 25.18 41.42 8.95 o 9 2 3 222.63 233.91 16.89 o 10 2 3 37.00 46.90 11.94 o 11 2 3 75.66 83.19 12.20 o 12 2 3 210.67 226.51 25.87 o 13 2 3 7.34 13.36 11.61 o 14 2 3 12.36 0.00 10.01 o 15 2 3 0.84 0.00 10.76 o 16 2 3 9.14 0.00 14.72 o -15 3 3 6.67 0.00 12.10 o -14 3 3 19.75 22.68 13.93 o -13 3 3 0.21 4.25 10.33 o -12 3 3 66.26 87.94 17.90 o -11 3 3 25.06 40.29 15.29 o -10 3 3 1.14 0.00 9.35 o -9 3 3 1.61 21.43 13.19 o -8 3 3 1188.05 1104.66 43.87 o -7 3 3 16.89 17.45 8.45 o -6 3 3 358.60 358.13 21.25 o -5 3 3 0.32 1.19 7.94 o -4 3 3 72.00 81.98 9.66 o -3 3 3 15.03 22.47 8.85 o -2 3 3 5.22 4.43 6.64 o -1 3 3 48.89 50.13 9.88 o 0 3 3 2.54 0.00 6.22 o 1 3 3 16.99 37.49 7.79 o 2 3 3 62.93 44.81 7.63 o 3 3 3 70.41 66.98 8.29 o 4 3 3 12.85 29.18 8.18 o 5 3 3 44.41 27.11 11.09 o 6 3 3 79.63 79.88 12.49 o 7 3 3 64.43 65.90 14.96 o 8 3 3 314.87 307.71 28.80 o 9 3 3 105.78 119.11 18.96 o 10 3 3 28.55 14.83 16.55 o 11 3 3 29.13 28.65 15.73 o 12 3 3 10.47 2.97 11.89 o 13 3 3 0.67 6.52 14.31 o -11 4 3 170.11 154.11 26.32 o -10 4 3 1.54 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