#------------------------------------------------------------------------------ #$Date: 2011-04-13 11:12:47 +0300 (Wed, 13 Apr 2011) $ #$Revision: 17966 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2229454.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229454_Fobs loop_ _publ_author_name 'Karpoormath, Rajshekhar' 'Govender, Patrick' 'Govender, Thavendran' 'Kruger, Hendrik G.' 'Maguire, Glenn E. M.' _publ_section_title ; endo-11-(Dibenzylamino)tetracyclo[5.4.0.0^3,10^.0^5,9^]undecane-8-one ; _journal_coeditor_code LX2177 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o619 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.100 _cell_angle_gamma 90.000 _cell_length_a 6.6117 _cell_length_b 16.4344 _cell_length_c 17.2331 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.8246 _[local]_cod_data_source_file lx2177Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PCUDD IN P2(1)/N' _shelx_refln_list_code 4 _shelx_f_calc_maximum 214.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1341.51 925.47 10.86 o 4 0 0 1455.29 1773.90 20.92 o 6 0 0 14.30 12.38 0.43 o 1 1 0 419.65 345.36 2.52 o 2 1 0 850.10 775.20 5.30 o 3 1 0 144.14 144.23 0.90 o 4 1 0 625.75 697.78 3.64 o 5 1 0 13.85 9.38 0.36 o 6 1 0 5.73 5.02 0.21 o 7 1 0 18.99 17.92 0.96 o 1 2 0 2141.42 1874.18 15.72 o 2 2 0 272.82 416.28 2.21 o 3 2 0 122.69 107.07 0.76 o 4 2 0 438.51 484.60 2.88 o 5 2 0 89.64 107.73 0.68 o 6 2 0 91.31 84.96 0.92 o 7 2 0 43.12 45.56 1.07 o 1 3 0 5307.60 4570.06 56.77 o 2 3 0 359.07 364.19 2.02 o 3 3 0 41.98 48.44 0.46 o 4 3 0 124.09 108.03 0.95 o 5 3 0 411.31 386.55 1.70 o 6 3 0 27.47 20.71 0.37 o 7 3 0 18.24 11.29 0.72 o 0 4 0 2986.91 3032.06 36.65 o 1 4 0 7245.13 7010.91 109.52 o 2 4 0 1248.29 1278.57 6.44 o 3 4 0 314.17 356.53 1.82 o 4 4 0 255.62 281.11 1.83 o 5 4 0 360.86 314.03 1.71 o 6 4 0 346.47 381.91 2.53 o 7 4 0 15.45 15.09 0.32 o 1 5 0 138.53 136.28 1.75 o 2 5 0 602.30 570.97 4.61 o 3 5 0 796.27 895.40 4.68 o 4 5 0 24.16 20.92 0.45 o 5 5 0 3.45 3.98 0.15 o 6 5 0 7.49 7.48 0.23 o 7 5 0 2.76 4.16 0.17 o 0 6 0 66.25 119.76 1.67 o 1 6 0 3329.94 3124.50 16.39 o 2 6 0 1455.93 1332.21 7.74 o 3 6 0 21.66 33.02 0.44 o 4 6 0 820.53 819.71 7.94 o 5 6 0 1.00 4.32 0.24 o 6 6 0 193.72 217.34 1.65 o 7 6 0 13.14 17.12 0.49 o 1 7 0 1472.37 1769.06 9.76 o 2 7 0 44.19 62.02 0.73 o 3 7 0 88.44 110.07 1.11 o 4 7 0 19.78 16.57 0.59 o 5 7 0 1188.50 1118.67 4.41 o 6 7 0 135.68 132.64 2.40 o 7 7 0 14.64 17.25 0.34 o 0 8 0 3194.47 3464.87 25.13 o 1 8 0 122.82 184.68 1.60 o 2 8 0 632.15 625.57 7.52 o 3 8 0 128.78 121.08 1.60 o 4 8 0 135.09 141.73 2.48 o 5 8 0 3.78 4.76 0.24 o 6 8 0 49.23 49.73 0.64 o 7 8 0 35.61 43.36 0.98 o 1 9 0 1.56 20.63 4.44 o 2 9 0 1500.33 1518.30 10.62 o 3 9 0 17.07 13.02 0.68 o 4 9 0 1.04 0.83 0.12 o 5 9 0 45.50 45.03 0.54 o 6 9 0 77.95 77.49 0.81 o 7 9 0 9.33 10.48 0.24 o 0 10 0 2201.52 2007.53 21.86 o 1 10 0 0.37 3.00 0.16 o 2 10 0 466.72 437.71 3.16 o 4 10 0 121.03 100.64 0.58 o 5 10 0 308.41 310.32 1.64 o 6 10 0 5.32 5.68 0.16 o 1 11 0 3.94 8.60 1.07 o 2 11 0 15.38 20.30 0.51 o 3 11 0 611.97 586.91 3.41 o 4 11 0 3.45 2.74 0.20 o 5 11 0 142.09 144.15 0.75 o 6 11 0 29.05 28.54 0.42 o 0 12 0 217.57 251.28 2.59 o 1 12 0 55.86 49.82 1.56 o 2 12 0 65.75 44.05 0.68 o 3 12 0 32.89 38.08 0.44 o 4 12 0 278.93 287.21 1.67 o 5 12 0 90.85 98.82 0.80 o 6 12 0 40.65 44.49 0.68 o 1 13 0 1825.42 1810.42 12.06 o 2 13 0 202.11 197.65 1.38 o 3 13 0 766.27 776.54 4.51 o 4 13 0 52.13 60.75 0.60 o 5 13 0 1.67 3.13 0.18 o 0 14 0 496.36 507.11 2.81 o 1 14 0 840.18 793.46 3.71 o 2 14 0 40.12 42.70 0.53 o 3 14 0 32.59 32.94 0.42 o 4 14 0 280.10 277.34 1.55 o 5 14 0 18.55 18.39 0.35 o 1 15 0 32.88 39.47 0.41 o 2 15 0 34.30 37.12 0.55 o 3 15 0 14.00 14.79 0.32 o 4 15 0 2.29 4.61 0.21 o 5 15 0 91.15 103.52 1.44 o 0 16 0 23.49 19.96 0.36 o 1 16 0 14.91 14.02 0.30 o 2 16 0 2.86 2.82 0.28 o 3 16 0 139.67 133.18 0.85 o 4 16 0 18.81 22.07 0.33 o 1 17 0 57.56 62.18 0.65 o 2 17 0 9.45 11.05 0.28 o 3 17 0 62.72 62.98 0.73 o 0 18 0 71.66 67.31 0.70 o 1 18 0 1.36 1.54 0.15 o 2 18 0 0.00 0.19 0.19 o 3 18 0 5.41 8.84 0.39 o 1 19 0 39.01 42.10 0.42 o 2 19 0 15.41 22.66 0.72 o -7 0 1 202.90 203.38 3.35 o -5 0 1 18.93 28.81 0.43 o -3 0 1 329.99 343.34 3.03 o -1 0 1 9199.43 8806.33 56.52 o 1 0 1 45872.83 49535.47 602.46 o 3 0 1 2838.56 3100.37 27.73 o 5 0 1 32.54 37.89 0.76 o -7 1 1 7.67 4.27 0.35 o -6 1 1 21.91 24.66 0.42 o -5 1 1 43.17 38.15 0.38 o -4 1 1 6.94 8.37 0.24 o -3 1 1 1161.13 1315.84 6.44 o -2 1 1 66.48 40.71 0.85 o -1 1 1 2023.61 2074.43 10.49 o 1 1 1 6298.12 5913.93 36.91 o 2 1 1 7086.49 7338.51 38.77 o 3 1 1 177.41 174.90 1.17 o 4 1 1 190.24 205.08 1.30 o 5 1 1 36.29 56.36 0.50 o 6 1 1 64.24 53.84 1.27 o 7 1 1 69.46 67.99 1.67 o -7 2 1 9.34 5.78 0.26 o -6 2 1 140.82 121.73 0.80 o -5 2 1 45.98 58.27 0.85 o -4 2 1 429.65 499.87 3.00 o -3 2 1 235.90 238.10 1.61 o -2 2 1 408.93 574.23 2.35 o -1 2 1 2422.59 2088.52 10.81 o 1 2 1 24.33 12.63 0.20 o 2 2 1 1967.35 1685.36 10.87 o 3 2 1 318.44 394.66 2.13 o 4 2 1 119.45 133.36 1.07 o 5 2 1 66.23 52.14 0.44 o 6 2 1 47.42 51.15 0.75 o 7 2 1 9.08 12.76 0.57 o -7 3 1 5.98 4.17 0.68 o -6 3 1 46.28 50.17 0.64 o -5 3 1 16.21 18.01 0.27 o -4 3 1 43.17 38.08 0.46 o -3 3 1 961.13 1037.07 5.65 o -2 3 1 849.08 689.33 3.02 o -1 3 1 6532.79 6349.90 35.24 o 1 3 1 1488.72 1641.85 8.71 o 2 3 1 0.54 27.91 0.44 o 3 3 1 805.15 858.65 4.36 o 4 3 1 105.04 104.53 0.91 o 5 3 1 45.78 46.04 0.45 o 6 3 1 147.78 140.59 2.25 o 7 3 1 0.31 0.95 0.16 o -7 4 1 1.97 1.00 0.13 o -6 4 1 51.62 42.77 0.46 o -5 4 1 16.14 13.75 0.26 o -4 4 1 21.05 12.41 0.40 o -3 4 1 111.07 103.34 0.79 o -2 4 1 144.40 84.33 0.61 o -1 4 1 3079.09 3505.25 19.47 o 0 4 1 5443.81 5724.33 54.05 o 1 4 1 5614.60 4885.99 49.00 o 2 4 1 400.31 344.05 3.28 o 3 4 1 495.54 556.26 2.69 o 4 4 1 51.05 60.08 0.67 o 5 4 1 136.00 122.12 0.72 o 6 4 1 132.62 139.01 1.24 o 7 4 1 38.06 34.64 0.45 o -7 5 1 17.51 12.04 0.24 o -6 5 1 72.48 74.32 0.93 o -5 5 1 7.76 6.50 0.40 o -4 5 1 324.39 344.05 3.03 o -3 5 1 75.85 96.06 0.79 o -2 5 1 136.48 113.75 1.09 o -1 5 1 4044.97 4237.22 23.52 o 0 5 1 858.79 472.23 2.25 o 1 5 1 366.23 499.59 3.09 o 2 5 1 604.40 729.52 4.55 o 3 5 1 8.41 12.94 0.29 o 4 5 1 180.51 211.44 2.33 o 5 5 1 18.74 15.99 0.53 o 6 5 1 4.32 7.63 0.24 o 7 5 1 2.50 4.79 0.26 o -7 6 1 0.80 0.46 0.13 o -6 6 1 18.81 20.57 0.36 o -5 6 1 286.71 276.93 1.38 o -4 6 1 274.92 259.72 2.59 o -3 6 1 117.51 112.22 0.88 o -2 6 1 0.00 3.77 0.68 o -1 6 1 199.55 282.11 2.11 o 0 6 1 2786.58 2694.76 12.50 o 1 6 1 32.47 91.47 1.69 o 2 6 1 145.74 170.34 1.41 o 3 6 1 92.01 108.47 0.82 o 4 6 1 34.08 33.16 0.59 o 5 6 1 494.95 447.48 2.07 o 6 6 1 23.92 23.77 0.69 o 7 6 1 77.82 79.18 2.25 o -7 7 1 1.84 3.30 0.16 o -6 7 1 104.79 120.89 1.10 o -5 7 1 57.19 64.65 0.95 o -4 7 1 6.33 14.88 0.96 o -3 7 1 0.34 3.07 0.21 o -2 7 1 86.86 69.66 0.77 o -1 7 1 22.00 55.49 1.83 o 0 7 1 3714.64 4131.05 24.23 o 1 7 1 97.36 123.74 1.01 o 2 7 1 1996.80 2114.68 14.56 o 3 7 1 786.72 814.18 5.64 o 4 7 1 157.15 147.86 3.32 o 5 7 1 102.53 95.25 0.93 o 6 7 1 33.74 30.82 0.42 o 7 7 1 39.31 33.85 0.59 o -7 8 1 0.82 2.75 0.20 o -6 8 1 67.89 76.46 1.11 o -5 8 1 0.36 2.57 0.33 o -4 8 1 53.63 55.60 0.97 o -3 8 1 210.84 184.88 1.68 o -2 8 1 577.24 611.38 8.51 o -1 8 1 92.16 58.66 0.75 o 0 8 1 3083.34 3127.75 24.83 o 1 8 1 4361.90 4943.15 35.24 o 2 8 1 280.41 261.72 2.14 o 3 8 1 18.22 18.17 0.57 o 4 8 1 81.70 94.94 1.03 o 5 8 1 121.75 110.50 0.67 o 6 8 1 4.92 5.85 0.94 o 7 8 1 106.05 100.77 0.75 o -7 9 1 0.04 0.34 0.24 o -6 9 1 51.99 42.44 0.88 o -5 9 1 186.01 180.43 1.02 o -4 9 1 277.36 243.36 1.55 o -3 9 1 43.89 35.18 1.20 o -2 9 1 0.00 7.64 0.34 o -1 9 1 168.74 201.37 1.90 o 0 9 1 198.13 148.80 1.15 o 1 9 1 736.24 657.19 4.26 o 2 9 1 69.83 85.45 0.95 o 3 9 1 1.13 1.01 0.39 o 4 9 1 70.89 62.96 0.48 o 5 9 1 4.78 6.13 0.20 o 6 9 1 54.26 68.25 0.59 o -6 10 1 178.08 183.72 1.49 o -5 10 1 87.43 78.11 0.59 o -4 10 1 359.79 348.49 1.45 o -2 10 1 16.41 13.19 0.40 o -1 10 1 76.30 109.23 1.26 o 0 10 1 44.27 52.75 0.67 o 1 10 1 42.65 60.50 0.73 o 2 10 1 347.95 322.78 2.46 o 3 10 1 8.91 5.26 0.68 o 4 10 1 61.74 53.12 0.41 o 5 10 1 166.50 161.62 0.81 o 6 10 1 6.55 5.94 0.16 o -6 11 1 194.85 213.72 1.25 o -5 11 1 1.67 2.04 0.12 o -4 11 1 333.95 297.69 1.66 o -3 11 1 286.87 274.47 1.61 o -2 11 1 235.64 198.13 1.94 o -1 11 1 28.60 46.33 0.78 o 0 11 1 322.11 317.29 2.12 o 1 11 1 181.57 217.99 1.52 o 2 11 1 217.44 217.60 2.11 o 3 11 1 285.90 277.96 1.61 o 4 11 1 112.52 117.82 0.78 o 5 11 1 55.24 43.63 0.37 o 6 11 1 65.65 63.36 1.14 o -6 12 1 17.39 14.61 0.39 o -5 12 1 0.31 0.14 0.22 o -4 12 1 44.88 42.03 0.58 o -3 12 1 153.07 162.83 1.58 o -2 12 1 63.91 61.59 0.51 o -1 12 1 1.16 6.88 1.17 o 0 12 1 55.42 65.60 1.87 o 1 12 1 135.88 144.84 2.07 o 2 12 1 275.02 268.34 1.39 o 3 12 1 235.58 214.46 1.25 o 4 12 1 0.00 1.52 0.54 o 5 12 1 4.81 4.96 0.24 o 6 12 1 34.25 33.57 0.98 o -5 13 1 26.40 29.98 0.49 o -4 13 1 47.29 53.70 0.94 o -3 13 1 84.52 97.28 0.77 o -2 13 1 673.53 679.53 4.38 o -1 13 1 0.02 1.14 0.34 o 0 13 1 47.27 46.64 1.53 o 1 13 1 20.47 16.59 0.45 o 2 13 1 269.20 279.07 1.16 o 3 13 1 117.36 125.82 0.84 o 4 13 1 45.59 35.25 0.44 o 5 13 1 17.70 22.85 0.36 o -5 14 1 59.82 58.12 0.50 o -4 14 1 8.82 10.56 0.23 o -3 14 1 170.34 162.46 1.40 o -2 14 1 115.20 128.62 0.85 o -1 14 1 129.77 107.59 1.08 o 0 14 1 978.86 981.54 6.15 o 1 14 1 11.50 12.63 0.93 o 2 14 1 0.00 1.60 0.24 o 3 14 1 31.42 22.35 0.47 o 4 14 1 45.93 58.74 0.61 o 5 14 1 10.53 18.35 0.35 o -5 15 1 65.50 54.46 0.96 o -4 15 1 91.35 88.12 0.63 o -3 15 1 160.96 156.95 1.37 o -2 15 1 256.87 255.46 1.81 o -1 15 1 232.93 226.91 1.64 o 0 15 1 10.15 12.24 0.24 o 1 15 1 1.11 1.74 0.24 o 2 15 1 272.60 253.84 1.34 o 3 15 1 151.79 151.94 0.99 o 4 15 1 5.06 3.84 0.30 o -4 16 1 69.30 82.80 0.64 o -3 16 1 82.79 78.83 0.70 o -2 16 1 66.85 71.73 0.91 o -1 16 1 63.84 48.42 0.51 o 0 16 1 124.88 109.70 0.68 o 1 16 1 37.70 40.69 0.38 o 2 16 1 61.34 75.85 1.02 o 3 16 1 103.34 102.70 0.74 o 4 16 1 56.90 51.54 0.55 o -3 17 1 80.20 68.19 0.92 o -2 17 1 83.36 79.46 0.96 o -1 17 1 1.24 1.77 0.12 o 0 17 1 27.23 25.31 0.28 o 1 17 1 1.66 3.82 0.16 o 2 17 1 62.19 65.77 0.62 o 3 17 1 39.85 36.20 0.52 o -3 18 1 16.69 23.43 0.59 o -2 18 1 18.68 24.58 0.35 o -1 18 1 58.14 58.54 0.51 o 0 18 1 1.46 0.43 0.14 o 1 18 1 115.14 118.00 0.94 o 2 18 1 13.27 18.01 0.42 o 3 18 1 16.85 31.88 0.78 o -2 19 1 150.87 170.55 2.39 o -1 19 1 6.12 12.17 0.22 o 0 19 1 9.24 5.72 0.15 o 1 19 1 7.67 10.32 0.39 o 2 19 1 14.85 15.90 0.72 o -6 0 2 317.66 348.93 3.71 o -4 0 2 414.36 385.28 3.54 o -2 0 2 1656.69 1621.69 10.61 o 0 0 2 2178.05 1839.32 21.11 o 2 0 2 5523.03 4817.60 37.36 o 4 0 2 2590.97 2701.03 16.70 o 6 0 2 264.93 222.03 2.87 o -7 1 2 242.40 248.32 2.21 o -6 1 2 439.95 434.58 2.23 o -5 1 2 46.46 41.40 0.38 o -4 1 2 0.48 1.32 0.25 o -3 1 2 1496.81 1540.65 7.48 o -2 1 2 12.18 1.90 0.18 o -1 1 2 34.73 32.79 0.59 o 0 1 2 3795.99 4505.97 29.62 o 1 1 2 86.18 70.58 0.50 o 2 1 2 275.71 421.57 2.04 o 3 1 2 1877.49 2051.17 9.78 o 4 1 2 1.35 3.30 0.28 o 5 1 2 0.23 0.15 0.10 o 6 1 2 8.48 5.07 0.48 o 7 1 2 274.93 248.18 2.41 o -7 2 2 84.63 94.96 0.84 o -6 2 2 0.26 1.50 0.38 o -5 2 2 326.03 291.86 1.44 o -4 2 2 5.45 9.78 0.40 o -3 2 2 512.85 522.65 2.73 o -2 2 2 28.34 28.36 0.27 o -1 2 2 1184.05 1189.73 13.79 o 0 2 2 336.81 422.12 5.04 o 1 2 2 1441.83 1513.01 9.10 o 2 2 2 255.97 313.61 1.65 o 3 2 2 2008.00 2267.72 11.06 o 4 2 2 123.57 120.88 0.88 o 5 2 2 86.52 77.66 0.89 o 6 2 2 3.69 1.69 0.49 o 7 2 2 0.00 0.51 0.34 o -7 3 2 0.30 0.20 0.18 o -6 3 2 33.07 37.81 0.96 o -5 3 2 69.46 95.20 0.59 o -4 3 2 15.36 9.20 0.31 o -3 3 2 192.60 194.14 1.47 o -2 3 2 345.65 360.24 2.08 o -1 3 2 89.33 99.98 1.09 o 0 3 2 14993.56 15204.78 174.97 o 1 3 2 2624.83 2397.68 12.74 o 2 3 2 3762.26 4016.63 30.05 o 3 3 2 1357.78 1409.86 6.97 o 4 3 2 959.49 1049.76 5.88 o 5 3 2 91.27 82.81 0.67 o 6 3 2 0.67 1.50 0.26 o 7 3 2 0.16 0.51 0.16 o -7 4 2 9.65 11.31 0.27 o -6 4 2 0.74 2.44 0.17 o -5 4 2 39.75 37.26 0.33 o -4 4 2 284.23 252.74 2.35 o -3 4 2 35.86 41.16 0.45 o -2 4 2 1121.86 1122.33 5.66 o -1 4 2 782.15 649.61 3.73 o 0 4 2 157.91 72.11 0.50 o 1 4 2 417.61 372.17 2.89 o 2 4 2 177.92 213.32 1.23 o 3 4 2 201.56 234.30 1.29 o 4 4 2 0.29 1.16 0.26 o 5 4 2 5.69 4.62 0.14 o 6 4 2 89.63 87.67 0.61 o 7 4 2 20.92 17.91 0.35 o -7 5 2 9.29 7.82 0.32 o -6 5 2 17.50 13.31 0.61 o -5 5 2 30.21 43.66 0.39 o -4 5 2 164.99 154.54 1.60 o -3 5 2 105.32 102.27 0.87 o -2 5 2 3647.01 4036.51 19.77 o -1 5 2 47.14 53.30 1.22 o 0 5 2 9410.63 9452.78 81.46 o 1 5 2 1024.92 950.33 6.69 o 2 5 2 309.53 325.09 2.40 o 3 5 2 474.42 454.53 2.54 o 4 5 2 437.39 376.04 6.95 o 5 5 2 88.39 83.32 0.87 o 6 5 2 114.24 134.47 0.96 o 7 5 2 4.62 6.27 0.23 o -7 6 2 39.37 43.62 1.31 o -6 6 2 495.03 484.66 2.25 o -5 6 2 549.15 573.16 2.50 o -4 6 2 60.56 73.25 0.70 o -3 6 2 47.99 47.84 0.55 o -2 6 2 6.36 9.59 0.24 o -1 6 2 2205.72 2259.63 15.24 o 0 6 2 501.99 586.64 3.75 o 1 6 2 1058.05 1275.24 9.09 o 2 6 2 337.14 396.50 3.62 o 3 6 2 1055.39 1109.57 7.83 o 4 6 2 521.39 471.82 3.01 o 5 6 2 1.94 1.67 0.14 o 6 6 2 1.42 3.13 0.26 o 7 6 2 9.79 8.04 0.49 o -7 7 2 106.98 120.82 1.57 o -6 7 2 5.72 7.99 0.31 o -5 7 2 1333.32 1300.72 10.70 o -4 7 2 12.60 14.55 0.42 o -3 7 2 149.55 130.65 1.43 o -2 7 2 334.24 439.42 3.17 o -1 7 2 179.50 171.49 1.30 o 0 7 2 17.38 44.29 0.86 o 1 7 2 316.35 306.71 2.10 o 2 7 2 441.89 473.00 5.46 o 3 7 2 1237.29 1188.78 13.77 o 4 7 2 150.67 180.19 1.75 o 5 7 2 8.67 9.44 0.28 o 6 7 2 28.93 20.71 0.32 o 7 7 2 90.87 89.89 1.46 o -7 8 2 1.23 1.69 0.29 o -6 8 2 4.75 8.03 0.32 o -5 8 2 50.90 57.16 0.70 o -4 8 2 73.54 69.64 1.27 o -3 8 2 131.27 120.95 1.34 o -2 8 2 441.75 469.67 6.16 o -1 8 2 1442.68 1481.38 9.53 o 0 8 2 3.53 7.70 0.49 o 1 8 2 1001.94 825.53 7.26 o 2 8 2 176.82 173.44 4.03 o 3 8 2 29.39 25.10 0.70 o 4 8 2 9.98 11.99 0.48 o 5 8 2 25.39 28.93 0.49 o 6 8 2 35.14 28.55 0.34 o 7 8 2 23.81 36.53 0.48 o -7 9 2 11.36 19.61 0.48 o -6 9 2 73.80 72.68 1.51 o -5 9 2 7.79 6.47 0.23 o -4 9 2 273.79 252.56 1.33 o -3 9 2 298.96 294.12 2.65 o -2 9 2 7.17 7.36 0.78 o -1 9 2 163.34 116.82 2.05 o 0 9 2 1.92 9.92 0.28 o 1 9 2 38.55 34.68 0.68 o 2 9 2 103.43 78.82 0.74 o 3 9 2 639.59 608.03 8.63 o 4 9 2 128.63 144.62 0.74 o 5 9 2 31.64 32.72 0.54 o 6 9 2 2.39 1.82 0.14 o -6 10 2 0.86 1.05 0.25 o -5 10 2 0.06 0.15 0.15 o -4 10 2 172.57 161.63 0.82 o -2 10 2 320.84 361.86 3.90 o -1 10 2 245.39 276.07 2.52 o 0 10 2 29.08 45.58 0.54 o 1 10 2 496.33 529.85 5.31 o 2 10 2 234.98 214.32 1.57 o 3 10 2 9.07 11.60 0.57 o 4 10 2 1.82 4.50 0.26 o 5 10 2 22.57 24.80 0.32 o 6 10 2 59.57 64.08 0.47 o -6 11 2 21.67 26.32 0.28 o -5 11 2 58.72 56.50 0.43 o -4 11 2 236.78 235.24 1.03 o -3 11 2 565.93 535.04 3.90 o -2 11 2 362.38 335.28 2.96 o -1 11 2 18.27 41.93 3.03 o 0 11 2 1086.03 1003.48 6.77 o 1 11 2 1215.97 1033.08 6.76 o 2 11 2 0.87 3.38 0.48 o 3 11 2 14.40 13.94 0.59 o 4 11 2 327.63 290.81 1.44 o 5 11 2 97.34 112.57 1.07 o 6 11 2 0.84 1.92 0.16 o -6 12 2 165.96 163.79 1.91 o -5 12 2 41.96 48.34 0.63 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