#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/95/2229582.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229582_Fobs loop_ _publ_author_name 'Rodrigues, Vinola Z.' 'Foro, Sabine' 'Gowda, B. Thimme' _publ_section_title ; N,N'-Bis(2-chlorophenylsulfonyl)adipamide ; _journal_coeditor_code BQ2284 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o837 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.560 _cell_angle_gamma 90.000 _cell_length_a 11.8990 _cell_length_b 5.5640 _cell_length_c 16.3330 _exptl_crystal_F_000 508.00 _reflns_d_resolution_high 0.8206 _[local]_cod_data_source_file bq2284Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AS4 P21/N' _shelx_refln_list_code 4 _shelx_f_calc_maximum 157.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14829.64 15077.51 38.29 o 4 0 0 939.37 916.28 18.26 o 6 0 0 0.23 11.33 16.86 o 8 0 0 291.89 293.67 23.24 o 10 0 0 218.46 184.73 25.35 o 12 0 0 205.90 123.01 28.05 o 14 0 0 51.92 73.64 30.06 o 1 1 0 7412.73 7669.79 37.32 o 2 1 0 0.38 4.29 8.56 o 3 1 0 798.28 785.59 33.86 o 4 1 0 1200.98 1085.32 34.13 o 5 1 0 135.72 146.92 12.79 o 6 1 0 1583.77 1542.46 49.92 o 7 1 0 213.83 247.29 31.40 o 8 1 0 925.27 954.81 21.49 o 9 1 0 62.47 70.56 21.62 o 10 1 0 726.24 714.42 22.79 o 11 1 0 188.44 168.89 19.91 o 12 1 0 61.54 28.17 49.05 o 13 1 0 27.22 61.21 41.95 o 14 1 0 18.09 70.92 91.75 o 0 2 0 2954.22 3032.66 42.03 o 1 2 0 38.94 43.65 16.68 o 2 2 0 859.60 893.15 19.71 o 3 2 0 0.67 12.96 11.99 o 4 2 0 2896.89 2863.79 24.72 o 5 2 0 65.85 60.17 12.48 o 6 2 0 28.66 29.51 21.21 o 7 2 0 707.04 676.58 28.86 o 8 2 0 271.54 275.18 27.21 o 9 2 0 878.05 907.55 33.44 o 10 2 0 97.91 123.83 27.99 o 11 2 0 236.31 220.08 28.48 o 12 2 0 45.35 131.27 28.36 o 13 2 0 23.45 -15.97 26.09 o 1 3 0 178.84 158.01 19.49 o 2 3 0 24.36 43.91 18.18 o 3 3 0 146.86 116.68 18.17 o 4 3 0 54.81 61.41 13.79 o 5 3 0 2.90 11.13 14.73 o 6 3 0 353.00 365.85 26.89 o 7 3 0 1.67 2.94 22.37 o 8 3 0 293.92 251.07 28.64 o 9 3 0 49.79 25.31 26.88 o 10 3 0 87.49 117.15 28.76 o 11 3 0 6.93 87.83 28.83 o 12 3 0 72.22 63.02 28.17 o 0 4 0 1050.91 965.71 40.65 o 1 4 0 71.67 111.80 30.79 o 2 4 0 38.37 35.85 26.65 o 3 4 0 493.19 502.99 25.08 o 4 4 0 1192.54 1131.27 26.23 o 5 4 0 821.91 744.29 24.84 o 6 4 0 445.01 363.12 27.83 o 7 4 0 31.67 -3.86 23.68 o 8 4 0 189.15 128.50 24.84 o 9 4 0 10.82 29.33 26.78 o 10 4 0 5.24 4.72 27.97 o 11 4 0 39.26 146.09 30.20 o 1 5 0 583.20 532.58 40.55 o 2 5 0 1.66 53.85 22.61 o 3 5 0 47.91 25.71 22.43 o 4 5 0 11.85 10.03 19.48 o 5 5 0 261.69 305.11 29.23 o 6 5 0 26.24 23.33 24.74 o 7 5 0 176.91 220.68 27.56 o 8 5 0 39.37 41.68 24.04 o 0 6 0 312.30 391.89 39.26 o 1 6 0 17.12 22.12 93.10 o 2 6 0 98.72 150.30 35.89 o 3 6 0 168.88 160.19 31.90 o 4 6 0 76.78 25.26 27.93 o 5 6 0 110.93 185.31 31.23 o 6 6 0 117.40 208.34 28.40 o -13 0 1 91.58 21.44 26.63 o -11 0 1 12.54 37.93 23.56 o -9 0 1 113.71 132.73 22.84 o -7 0 1 339.86 333.18 19.90 o -5 0 1 502.30 574.16 17.96 o -3 0 1 23022.67 22344.21 54.98 o 3 0 1 139.21 226.94 11.75 o 5 0 1 874.54 963.67 22.49 o 7 0 1 795.86 871.59 26.03 o 9 0 1 136.03 149.90 24.81 o 11 0 1 31.82 34.25 27.98 o 13 0 1 84.20 113.56 30.01 o -14 1 1 16.85 38.89 68.95 o -13 1 1 3.84 20.52 47.05 o -12 1 1 46.07 1.38 18.13 o -11 1 1 133.22 133.28 28.96 o -10 1 1 8.60 30.39 16.96 o -9 1 1 276.41 287.68 18.13 o -8 1 1 84.81 112.93 15.97 o -7 1 1 932.08 859.60 18.59 o -6 1 1 1764.63 1858.32 33.32 o -5 1 1 482.77 468.92 14.11 o -4 1 1 364.31 384.46 16.38 o -3 1 1 34.92 26.03 13.88 o -2 1 1 7.45 -7.54 14.73 o -1 1 1 456.21 488.49 17.90 o 0 1 1 1750.49 1804.13 18.07 o 1 1 1 1622.66 1693.39 13.47 o 2 1 1 27.22 38.03 9.56 o 3 1 1 1.11 1.65 9.43 o 4 1 1 647.74 700.60 19.71 o 5 1 1 1509.91 1442.95 33.27 o 6 1 1 85.51 98.63 22.19 o 7 1 1 1200.44 1178.22 21.20 o 8 1 1 11.58 14.59 16.28 o 9 1 1 489.34 510.10 20.48 o 10 1 1 1.46 -4.93 31.91 o 11 1 1 387.37 384.48 21.91 o 12 1 1 5.16 0.21 22.22 o 13 1 1 2.87 24.87 20.49 o 14 1 1 11.21 -17.89 26.81 o -13 2 1 13.41 8.74 26.27 o -12 2 1 13.70 80.12 27.32 o -11 2 1 229.09 277.02 29.23 o -10 2 1 71.14 77.81 25.28 o -9 2 1 363.36 380.85 27.44 o -8 2 1 0.65 6.88 23.36 o -7 2 1 4.48 -9.97 22.14 o -6 2 1 233.03 228.06 14.05 o -5 2 1 195.69 199.25 13.70 o -4 2 1 112.90 91.93 8.77 o -3 2 1 2272.29 2268.60 24.48 o -2 2 1 103.84 100.52 16.56 o -1 2 1 5.83 -8.51 17.53 o 0 2 1 0.13 5.28 9.27 o 1 2 1 9252.45 9469.78 42.23 o 2 2 1 309.61 300.65 12.27 o 3 2 1 0.42 -0.56 10.95 o 4 2 1 1018.85 1042.22 38.24 o 5 2 1 37.91 44.27 10.58 o 6 2 1 1091.30 1065.85 29.68 o 7 2 1 261.49 271.15 25.81 o 8 2 1 28.79 42.05 24.75 o 9 2 1 600.92 560.47 31.39 o 10 2 1 20.99 48.13 26.83 o 11 2 1 247.86 293.92 29.73 o 12 2 1 7.81 16.71 26.53 o 13 2 1 3.15 66.95 26.50 o -12 3 1 85.69 49.12 28.76 o -11 3 1 240.49 225.95 30.52 o -10 3 1 207.63 227.40 30.29 o -9 3 1 120.46 97.21 28.71 o -8 3 1 6.11 -9.83 26.57 o -7 3 1 219.02 220.53 24.91 o -6 3 1 169.02 204.98 24.84 o -5 3 1 440.23 394.19 18.01 o -4 3 1 367.98 434.17 19.35 o -3 3 1 9.22 -0.55 24.67 o -2 3 1 34.71 27.93 18.84 o -1 3 1 7.58 8.94 6.34 o 0 3 1 1288.50 1261.32 18.15 o 1 3 1 24.37 9.54 18.98 o 2 3 1 306.34 312.49 21.83 o 3 3 1 79.99 95.64 15.24 o 4 3 1 5.14 -1.17 12.52 o 5 3 1 1094.78 1015.06 18.76 o 6 3 1 161.86 158.03 23.32 o 7 3 1 727.75 596.88 30.61 o 8 3 1 90.75 82.17 26.48 o 9 3 1 25.16 11.20 26.84 o 10 3 1 187.30 142.99 27.81 o 11 3 1 95.41 139.36 28.36 o 12 3 1 0.40 125.66 29.21 o -11 4 1 3.29 1.48 28.72 o -10 4 1 6.03 25.75 27.43 o -9 4 1 54.60 85.55 27.40 o -8 4 1 242.79 277.16 27.50 o -7 4 1 250.17 270.22 27.73 o -6 4 1 296.81 311.14 26.76 o -5 4 1 186.06 150.66 33.43 o -4 4 1 1.73 17.11 18.51 o -3 4 1 501.70 443.50 32.32 o -2 4 1 258.46 262.43 27.49 o -1 4 1 522.63 530.24 25.03 o 0 4 1 614.21 566.38 24.95 o 1 4 1 530.23 524.10 25.02 o 2 4 1 379.67 404.66 32.85 o 3 4 1 3.19 12.29 20.14 o 4 4 1 67.59 73.19 15.78 o 5 4 1 41.76 19.87 19.57 o 6 4 1 220.20 228.86 25.47 o 7 4 1 42.74 51.77 24.05 o 8 4 1 26.85 -13.32 26.10 o 9 4 1 40.57 -11.86 25.53 o 10 4 1 56.64 -5.28 25.74 o 11 4 1 36.03 7.97 25.75 o -9 5 1 21.97 5.25 24.36 o -7 5 1 13.89 -24.07 24.07 o -6 5 1 0.89 -20.82 24.46 o -5 5 1 157.78 192.95 29.57 o -4 5 1 189.69 230.93 23.14 o -3 5 1 7.48 48.75 32.11 o -2 5 1 665.58 631.33 39.23 o -1 5 1 2.62 -9.05 21.57 o 0 5 1 7.09 3.45 22.03 o 1 5 1 41.22 74.56 22.47 o 2 5 1 90.30 97.18 22.96 o 3 5 1 40.20 20.96 22.96 o 4 5 1 1.59 -16.57 16.57 o 5 5 1 0.47 -20.84 24.91 o 6 5 1 6.58 1.12 24.57 o 7 5 1 60.41 88.19 25.80 o 8 5 1 87.44 147.94 26.38 o 9 5 1 19.60 120.27 25.91 o -6 6 1 51.83 68.06 24.36 o -5 6 1 12.49 108.19 29.14 o -4 6 1 8.20 195.10 22.62 o -3 6 1 115.51 268.73 35.09 o -2 6 1 40.31 109.75 34.23 o -1 6 1 26.04 -20.43 32.04 o 0 6 1 143.15 21.90 33.28 o 1 6 1 25.36 70.65 35.67 o 2 6 1 91.09 183.28 40.84 o 3 6 1 4.91 41.73 31.52 o 4 6 1 20.61 -8.75 28.12 o 5 6 1 3.91 -26.23 26.23 o 6 6 1 96.36 144.85 27.28 o -14 0 2 4.72 101.15 29.33 o -12 0 2 0.69 28.43 24.30 o -10 0 2 38.48 16.84 22.43 o -8 0 2 0.32 1.13 17.83 o -6 0 2 1391.64 1459.26 24.03 o -4 0 2 1340.88 1365.86 18.90 o -2 0 2 806.78 897.88 20.52 o 2 0 2 164.84 134.88 10.65 o 4 0 2 47.64 55.84 12.70 o 6 0 2 3.38 16.32 17.74 o 8 0 2 228.98 213.90 24.31 o 10 0 2 1041.48 977.47 35.52 o 12 0 2 377.22 414.75 33.40 o -14 1 2 23.27 63.47 38.09 o -13 1 2 14.68 -18.50 18.50 o -12 1 2 1.94 -13.50 38.22 o -11 1 2 102.66 118.67 18.46 o -10 1 2 1209.71 1293.48 24.52 o -9 1 2 4.99 0.51 15.51 o -8 1 2 8.96 14.78 15.58 o -7 1 2 62.05 78.95 13.69 o -6 1 2 938.68 921.85 17.93 o -5 1 2 93.87 71.27 11.29 o -4 1 2 6.93 19.60 10.50 o -3 1 2 108.10 104.95 18.28 o -2 1 2 1675.92 1753.79 20.65 o -1 1 2 55.84 65.77 12.77 o 0 1 2 222.37 211.92 10.95 o 1 1 2 3552.31 3374.55 22.13 o 2 1 2 2944.57 2843.37 13.40 o 3 1 2 172.88 163.30 8.28 o 4 1 2 2069.99 2065.42 14.57 o 5 1 2 466.84 457.22 12.69 o 6 1 2 45.20 37.51 13.78 o 7 1 2 10.25 2.22 15.40 o 8 1 2 917.31 869.09 45.47 o 9 1 2 245.11 214.18 19.08 o 10 1 2 94.36 104.90 18.92 o 11 1 2 396.69 405.39 57.80 o 12 1 2 14.17 39.10 22.88 o 13 1 2 22.04 57.69 34.00 o 14 1 2 1.74 93.94 26.80 o -13 2 2 19.58 13.81 25.47 o -12 2 2 211.55 230.67 28.61 o -11 2 2 14.75 42.15 25.66 o -10 2 2 231.69 249.47 27.38 o -9 2 2 428.32 453.78 28.65 o -8 2 2 17.43 7.52 14.39 o -7 2 2 11.11 12.08 13.53 o -6 2 2 519.98 504.81 20.11 o -5 2 2 68.99 52.64 9.57 o -4 2 2 2772.45 2761.70 20.32 o -3 2 2 0.02 3.31 10.11 o -2 2 2 453.56 416.89 11.71 o -1 2 2 51.01 71.32 10.87 o 0 2 2 62.75 50.64 9.04 o 1 2 2 85.11 96.06 10.93 o 2 2 2 1370.51 1398.01 14.11 o 3 2 2 566.08 595.50 11.62 o 4 2 2 1416.64 1435.05 14.37 o 5 2 2 12.24 10.84 9.02 o 6 2 2 0.13 -1.74 20.42 o 7 2 2 130.65 143.27 24.40 o 8 2 2 820.84 846.07 31.83 o 9 2 2 15.69 10.98 25.95 o 10 2 2 18.35 12.34 26.14 o 11 2 2 36.74 122.03 26.77 o 12 2 2 0.35 -24.89 24.89 o 13 2 2 0.22 76.50 26.88 o -13 3 2 58.07 205.82 31.75 o -12 3 2 3.81 27.77 29.01 o -11 3 2 35.43 9.33 27.14 o -10 3 2 236.69 220.67 28.99 o -9 3 2 0.81 -27.12 27.12 o -8 3 2 72.08 17.97 27.70 o -7 3 2 44.02 18.71 23.07 o -6 3 2 313.02 285.26 18.44 o -5 3 2 290.91 240.11 21.86 o -4 3 2 23.26 3.38 17.02 o -3 3 2 22.53 28.13 28.42 o -2 3 2 928.68 708.79 159.67 o -1 3 2 176.36 184.14 11.74 o 0 3 2 470.46 461.58 9.23 o 1 3 2 26.96 30.38 13.95 o 2 3 2 810.14 720.74 16.44 o 3 3 2 89.02 73.01 11.00 o 4 3 2 282.03 262.30 16.49 o 5 3 2 3.26 2.78 16.58 o 6 3 2 9.01 27.46 17.03 o 7 3 2 241.77 228.92 26.86 o 8 3 2 371.50 359.96 29.82 o 9 3 2 6.50 24.62 26.00 o 10 3 2 17.56 77.35 27.25 o 11 3 2 0.52 -24.06 27.07 o 12 3 2 8.56 -27.95 27.95 o -11 4 2 10.28 -39.01 39.01 o -9 4 2 179.09 115.11 29.49 o -8 4 2 0.31 -7.19 24.62 o -7 4 2 29.02 -9.53 24.92 o -6 4 2 137.01 113.37 26.60 o -5 4 2 386.96 319.97 37.90 o -4 4 2 262.82 239.65 31.74 o -3 4 2 288.24 331.02 34.77 o -2 4 2 361.46 372.39 34.19 o -1 4 2 518.65 459.62 38.38 o 0 4 2 139.13 121.07 35.13 o 1 4 2 0.88 -0.05 20.43 o 2 4 2 442.99 515.52 37.03 o 3 4 2 189.82 207.78 16.81 o 4 4 2 12.94 20.94 15.02 o 5 4 2 0.35 -0.86 17.70 o 6 4 2 11.37 12.53 18.25 o 7 4 2 36.45 73.37 24.41 o 8 4 2 171.22 212.82 28.62 o 9 4 2 33.74 83.46 27.27 o 10 4 2 49.09 110.32 27.65 o 11 4 2 21.99 -25.61 25.61 o -9 5 2 0.10 93.04 26.65 o -8 5 2 17.03 58.73 25.55 o -7 5 2 20.53 -10.90 24.83 o -6 5 2 0.12 -25.25 25.25 o -5 5 2 197.19 221.08 77.52 o -4 5 2 97.96 167.55 34.20 o -3 5 2 0.18 41.59 34.19 o -2 5 2 17.45 -18.72 33.93 o -1 5 2 465.90 420.34 40.98 o 0 5 2 4.75 46.08 33.17 o 1 5 2 54.29 55.04 32.88 o 2 5 2 269.21 245.26 36.42 o 3 5 2 1.19 28.05 23.84 o 4 5 2 250.13 287.46 51.83 o 5 5 2 160.68 150.55 21.94 o 6 5 2 0.72 -20.67 23.14 o 7 5 2 384.91 297.54 28.08 o 8 5 2 73.90 -0.37 25.02 o 9 5 2 2.05 -25.68 25.68 o -6 6 2 20.72 -25.48 25.48 o -4 6 2 1.93 -27.86 27.86 o -1 6 2 17.57 -12.37 32.12 o 0 6 2 0.55 92.62 36.03 o 1 6 2 98.22 76.96 35.92 o 2 6 2 9.56 -36.75 36.75 o 3 6 2 242.07 343.59 25.82 o 4 6 2 119.35 242.98 127.40 o 5 6 2 25.47 13.62 26.02 o 6 6 2 130.94 35.67 25.29 o -13 0 3 71.74 21.53 25.78 o -11 0 3 32.48 -1.14 22.70 o -9 0 3 2030.39 2000.40 34.54 o -7 0 3 228.28 286.13 17.68 o -5 0 3 441.08 469.76 16.41 o -3 0 3 6535.81 6427.13 23.84 o -1 0 3 57.77 58.27 15.40 o 1 0 3 6213.05 5814.25 25.91 o 3 0 3 6.25 17.48 18.62 o 5 0 3 8479.90 9167.12 42.68 o 7 0 3 114.93 120.17 22.47 o 9 0 3 1512.10 1531.59 37.63 o 11 0 3 12.31 -20.41 27.69 o 13 0 3 35.07 3.26 28.80 o -14 1 3 32.77 105.37 19.98 o -13 1 3 263.90 304.43 23.95 o -12 1 3 1.27 26.98 22.28 o -11 1 3 66.49 50.84 26.00 o -10 1 3 340.77 358.94 18.11 o -9 1 3 780.23 745.00 19.71 o -8 1 3 955.64 902.28 19.16 o -7 1 3 0.07 -1.05 12.36 o -6 1 3 1059.72 1128.61 18.66 o -5 1 3 56.53 51.92 9.17 o -4 1 3 615.39 664.50 25.74 o -3 1 3 1579.28 1515.39 59.43 o -2 1 3 2147.99 2134.39 35.29 o -1 1 3 18443.43 18839.90 42.95 o 0 1 3 1.61 1.37 9.61 o 1 1 3 24715.43 23531.58 31.35 o 2 1 3 71.99 81.02 7.40 o 3 1 3 46.97 36.66 8.25 o 4 1 3 431.37 455.25 12.76 o 5 1 3 948.67 957.08 21.81 o 6 1 3 108.94 114.27 13.68 o 7 1 3 330.03 361.67 36.00 o 8 1 3 472.86 512.69 20.80 o 9 1 3 24.95 5.55 28.19 o 10 1 3 226.37 206.70 20.38 o 11 1 3 53.87 46.68 20.01 o 12 1 3 44.26 45.68 20.25 o 13 1 3 37.25 13.36 27.45 o -13 2 3 34.47 155.32 26.40 o -12 2 3 58.05 66.82 26.46 o -11 2 3 52.21 69.81 25.49 o -10 2 3 3.73 36.12 24.58 o -9 2 3 258.21 328.57 27.11 o -8 2 3 88.37 97.09 16.69 o -7 2 3 6.39 -11.32 13.64 o -6 2 3 3.73 9.01 12.83 o -5 2 3 2084.36 2069.25 21.95 o -4 2 3 211.29 209.37 10.89 o -3 2 3 665.08 653.07 15.03 o -2 2 3 124.21 156.00 12.33 o -1 2 3 4757.89 4964.71 22.40 o 0 2 3 1450.73 1433.09 13.25 o 1 2 3 765.54 776.81 17.84 o 2 2 3 205.54 209.75 11.51 o 3 2 3 1504.61 1672.07 12.74 o 4 2 3 242.63 230.09 15.47 o 5 2 3 7.42 -5.77 12.46 o 6 2 3 63.66 51.69 13.56 o 7 2 3 90.71 85.90 23.13 o 8 2 3 8.12 13.70 23.76 o 9 2 3 495.72 542.94 30.48 o 10 2 3 64.98 91.55 27.17 o 11 2 3 24.44 30.21 25.75 o 12 2 3 102.80 213.00 29.42 o 13 2 3 32.01 11.12 26.49 o -12 3 3 9.77 87.30 28.89 o -11 3 3 11.53 -6.31 26.61 o -10 3 3 115.19 49.75 28.40 o -9 3 3 524.28 432.15 31.64 o -8 3 3 75.63 70.77 24.69 o -7 3 3 191.70 217.63 25.45 o -6 3 3 140.22 123.38 17.91 o -5 3 3 520.82 511.61 20.95 o -4 3 3 799.03 834.03 35.50 o -3 3 3 1706.73 1869.38 45.07 o -2 3 3 15.16 -2.13 12.04 o -1 3 3 538.62 554.64 23.44 o 0 3 3 1290.10 1367.82 34.27 o 1 3 3 72.82 88.06 23.19 o 2 3 3 122.21 145.99 13.23 o 3 3 3 1078.69 1035.12 18.17 o 4 3 3 0.09 -3.04 12.76 o 5 3 3 1372.33 1318.14 20.88 o 6 3 3 22.45 5.78 17.43 o 7 3 3 346.18 278.31 28.06 o 8 3 3 142.96 140.68 25.18 o 9 3 3 1.79 -25.46 25.46 o 10 3 3 1.13 34.42 26.85 o 11 3 3 0.20 90.32 27.01 o -11 4 3 5.64 -22.69 28.63 o -10 4 3 1.02 -28.80 28.80 o -9 4 3 46.30 29.79 26.37 o -8 4 3 238.00 200.42 28.04 o -7 4 3 35.66 26.43 24.31 o -6 4 3 17.66 -8.24 18.21 o -5 4 3 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