#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/96/2229627.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229627_Fobs loop_ _publ_author_name 'Jasinski, Jerry P.' 'Miller, William M.' 'Samshuddin, S.' 'Narayana, B.' 'Yathirajan, H. S.' _publ_section_title ; (2E)-3-{4-[(1H-1,3-Benzimidazol-2-yl)methoxy]-3-ethoxyphenyl}-1-(4-bromophenyl)prop-2-en-1-one monohydrate ; _journal_coeditor_code EZ2232 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o834 _journal_page_last o835 _journal_volume 67 _journal_year 2011 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.8406 _cell_length_b 16.5192 _cell_length_c 19.4719 _exptl_crystal_F_000 2032.00 _reflns_d_resolution_high 0.8301 _[local]_cod_data_source_file ez2232Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hsy831mo' _shelx_refln_list_code 4 _shelx_f_calc_maximum 951.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 905694.19 661946.25 3170.72 o 6 0 0 2643.85 2859.61 105.91 o 8 0 0 116146.23 109898.23 1380.16 o 10 0 0 249.42 211.82 145.63 o 12 0 0 6504.29 6236.15 125.77 o 14 0 0 59.20 -15.36 171.30 o 16 0 0 505.12 781.63 203.27 o 5 1 0 1027.12 943.83 55.59 o 7 1 0 9933.29 9685.51 71.66 o 9 1 0 6.92 12.61 50.76 o 11 1 0 258.34 358.82 56.62 o 13 1 0 1.75 9.82 115.63 o 15 1 0 2.44 7.70 128.43 o 4 2 0 225.88 327.27 49.05 o 6 2 0 2374.97 2180.92 109.95 o 8 2 0 36.40 24.59 24.87 o 10 2 0 4.33 -8.49 31.47 o 12 2 0 2.49 -23.71 113.72 o 14 2 0 61.41 57.39 129.97 o 16 2 0 112.97 100.72 131.24 o 3 3 0 1948.17 1832.20 59.58 o 5 3 0 11979.88 11346.31 254.19 o 7 3 0 1529.09 1564.78 67.75 o 9 3 0 1016.13 951.31 74.39 o 11 3 0 1072.87 1052.47 104.46 o 13 3 0 3.12 -36.39 111.58 o 15 3 0 54.01 160.08 133.81 o 2 4 0 1300.78 1277.16 51.58 o 4 4 0 508.67 420.25 27.42 o 6 4 0 904.65 830.28 40.44 o 8 4 0 3053.91 2987.73 76.28 o 10 4 0 908.94 1059.18 71.60 o 12 4 0 103.23 74.87 101.80 o 14 4 0 24.42 98.66 125.85 o 16 4 0 21.34 114.00 227.43 o 1 5 0 1170.00 1076.69 47.83 o 3 5 0 1790.79 1700.02 43.34 o 5 5 0 19.02 39.27 28.83 o 7 5 0 4837.95 4785.87 99.29 o 9 5 0 1.73 22.23 59.70 o 11 5 0 1078.28 1097.04 81.21 o 13 5 0 35.74 108.64 158.94 o 15 5 0 71.93 196.32 191.74 o 0 6 0 19293.12 19163.84 185.78 o 2 6 0 91.66 103.92 20.42 o 4 6 0 18392.60 18237.25 90.90 o 6 6 0 3888.24 3951.82 59.58 o 8 6 0 2150.04 1926.26 79.43 o 10 6 0 1675.68 1458.92 88.81 o 12 6 0 151.24 171.55 166.76 o 14 6 0 263.24 401.65 217.31 o 1 7 0 773.10 826.93 31.19 o 3 7 0 10314.86 10340.93 245.27 o 5 7 0 207.41 264.78 86.05 o 7 7 0 5199.50 5421.34 145.63 o 9 7 0 0.47 11.09 56.72 o 11 7 0 1537.13 1477.14 92.97 o 13 7 0 53.33 6.62 291.26 o 15 7 0 150.50 132.39 324.35 o 0 8 0 22491.89 26094.79 486.99 o 2 8 0 2024.48 1876.03 77.39 o 4 8 0 7042.82 7102.68 125.77 o 6 8 0 1296.32 1165.03 112.53 o 8 8 0 1715.56 1595.29 211.82 o 10 8 0 566.28 337.59 231.68 o 12 8 0 111.57 -119.15 251.54 o 14 8 0 78.22 -191.96 337.59 o 1 9 0 28822.89 29642.88 387.16 o 3 9 0 35787.54 37044.95 582.51 o 5 9 0 4556.74 4112.68 105.20 o 7 9 0 13687.55 12993.04 160.26 o 9 9 0 74.37 -13.24 231.68 o 11 9 0 2622.50 2541.87 284.64 o 13 9 0 9.41 -59.58 278.02 o 0 10 0 29215.84 31080.66 330.23 o 2 10 0 1274.01 1404.80 51.16 o 4 10 0 11924.47 10493.84 225.76 o 6 10 0 1030.87 970.18 88.85 o 8 10 0 3842.62 3998.16 258.16 o 10 10 0 1209.52 1330.51 264.78 o 12 10 0 70.50 39.72 297.88 o 14 10 0 70.51 -13.24 304.50 o 1 11 0 53.86 92.69 52.94 o 3 11 0 665.63 544.93 40.61 o 5 11 0 138.18 196.47 84.95 o 7 11 0 414.64 418.03 154.25 o 9 11 0 114.05 46.34 271.40 o 11 11 0 39.41 -46.34 264.78 o 13 11 0 12.51 6.62 317.73 o 0 12 0 3070.38 3084.14 105.24 o 2 12 0 117.06 69.01 63.42 o 4 12 0 3800.78 3289.11 147.39 o 6 12 0 164.03 195.61 90.37 o 8 12 0 795.54 902.08 166.11 o 10 12 0 148.89 311.11 311.11 o 12 12 0 79.10 46.34 291.26 o 1 13 0 3366.50 3372.62 70.90 o 3 13 0 650.58 713.15 91.51 o 5 13 0 5574.25 5047.74 180.93 o 7 13 0 112.78 143.81 169.65 o 9 13 0 2248.12 2198.51 197.90 o 11 13 0 28.63 287.06 304.50 o 0 14 0 2290.56 2462.84 168.60 o 2 14 0 469.47 537.65 73.36 o 4 14 0 4352.68 4066.79 205.20 o 6 14 0 37.33 -10.73 172.43 o 8 14 0 106.27 112.09 210.47 o 10 14 0 123.62 83.17 219.39 o 1 15 0 3136.38 3056.17 94.92 o 3 15 0 6893.76 6986.25 155.50 o 5 15 0 33.91 1.53 179.68 o 7 15 0 2876.70 2619.95 193.87 o 9 15 0 24.26 -32.82 219.39 o 0 16 0 5033.09 4679.69 127.22 o 2 16 0 159.83 172.75 69.83 o 4 16 0 2910.47 2574.97 238.30 o 6 16 0 648.45 517.04 191.22 o 8 16 0 461.16 250.69 214.61 o 1 17 0 326.15 428.00 78.58 o 3 17 0 400.06 477.41 109.55 o 5 17 0 117.29 132.39 244.92 o 7 17 0 168.00 26.11 209.86 o 0 18 0 2506.24 2680.50 128.09 o 2 18 0 100.65 63.13 99.96 o 4 18 0 1516.54 1479.95 192.04 o 6 18 0 250.40 324.35 258.16 o 1 19 0 1427.71 1558.99 127.90 o 3 19 0 1443.35 1727.47 148.76 o 4 1 1 21676.93 20089.44 150.45 o 5 1 1 615.60 640.46 26.23 o 6 1 1 2178.55 2127.32 42.71 o 7 1 1 8924.77 7928.53 101.04 o 8 1 1 12126.30 11343.16 112.49 o 9 1 1 315.77 254.35 47.81 o 10 1 1 953.74 947.37 38.55 o 11 1 1 1662.33 1535.80 40.42 o 12 1 1 3277.42 2920.40 52.54 o 13 1 1 230.30 123.98 84.72 o 14 1 1 239.51 224.73 91.75 o 15 1 1 149.15 152.06 92.27 o 16 1 1 567.10 553.07 100.54 o 3 2 1 976.14 1036.07 59.58 o 4 2 1 146.36 217.53 14.20 o 5 2 1 109.35 102.37 25.41 o 6 2 1 96.03 102.91 19.94 o 7 2 1 703.00 639.85 25.50 o 8 2 1 903.55 799.35 41.20 o 9 2 1 55.20 38.40 31.38 o 10 2 1 1143.53 1122.83 42.61 o 11 2 1 209.98 140.73 38.97 o 12 2 1 126.75 56.35 62.95 o 13 2 1 19.87 66.86 86.30 o 14 2 1 2.36 39.50 92.16 o 15 2 1 106.73 134.16 94.48 o 16 2 1 2.59 -81.24 104.60 o 3 3 1 197.46 288.91 39.12 o 4 3 1 132.50 162.49 15.11 o 5 3 1 118.49 156.94 21.77 o 6 3 1 860.10 862.15 32.24 o 7 3 1 1083.41 1046.88 41.94 o 8 3 1 1.43 -4.49 47.10 o 9 3 1 3.70 6.60 47.87 o 10 3 1 180.65 195.19 61.54 o 11 3 1 775.71 666.41 71.61 o 12 3 1 6.23 27.84 73.68 o 13 3 1 22.07 35.60 82.94 o 14 3 1 56.76 56.57 88.81 o 15 3 1 40.36 128.28 111.38 o 16 3 1 2.52 72.42 113.66 o 1 4 1 12566.45 13025.67 460.05 o 2 4 1 417.52 380.39 20.12 o 3 4 1 3832.33 4019.89 49.17 o 4 4 1 29445.94 29550.79 220.28 o 5 4 1 5641.05 5582.60 44.47 o 6 4 1 2871.86 2649.23 35.70 o 7 4 1 1077.19 1090.14 45.86 o 8 4 1 2356.29 2288.65 61.90 o 9 4 1 2150.80 2247.15 57.56 o 10 4 1 381.56 419.67 49.38 o 11 4 1 62.83 106.50 68.48 o 12 4 1 516.11 471.08 90.96 o 13 4 1 228.23 341.16 101.76 o 14 4 1 268.18 308.57 105.31 o 15 4 1 3.91 68.35 111.08 o 16 4 1 12.56 32.07 119.91 o 1 5 1 8674.42 9473.00 56.98 o 2 5 1 45712.76 45934.73 228.59 o 3 5 1 18402.05 18722.27 140.00 o 4 5 1 24.86 10.72 24.06 o 5 5 1 580.23 468.41 16.69 o 6 5 1 15503.74 14481.33 309.41 o 7 5 1 5754.43 5345.45 92.78 o 8 5 1 397.21 398.26 45.01 o 9 5 1 182.71 261.01 46.53 o 10 5 1 1668.17 1644.72 56.51 o 11 5 1 1906.11 1812.07 63.40 o 12 5 1 111.00 167.47 83.94 o 13 5 1 34.32 67.10 92.90 o 14 5 1 68.22 175.61 108.91 o 15 5 1 108.43 213.07 137.63 o 16 5 1 10.71 161.46 168.03 o 0 6 1 12538.50 12974.91 247.49 o 1 6 1 389.52 396.31 18.17 o 2 6 1 45.64 38.69 17.76 o 3 6 1 916.94 859.18 30.42 o 4 6 1 3646.22 3782.46 53.53 o 5 6 1 1675.97 1612.77 84.77 o 6 6 1 51.88 91.95 22.95 o 7 6 1 0.34 -13.24 66.19 o 8 6 1 886.08 767.86 86.05 o 9 6 1 399.37 489.22 70.29 o 10 6 1 114.59 76.21 53.84 o 11 6 1 0.85 50.61 77.84 o 12 6 1 10.35 48.65 124.66 o 13 6 1 95.17 186.39 136.53 o 14 6 1 70.29 204.11 145.92 o 15 6 1 6.09 167.88 133.76 o 1 7 1 1370.40 1441.86 21.75 o 2 7 1 934.26 924.12 20.35 o 3 7 1 4333.01 4453.45 48.79 o 4 7 1 778.27 764.83 38.45 o 5 7 1 15.28 59.58 60.31 o 6 7 1 824.35 700.99 64.13 o 7 7 1 1374.81 1126.19 62.88 o 8 7 1 960.22 834.05 66.19 o 9 7 1 7.80 16.28 65.67 o 10 7 1 209.07 178.40 79.47 o 11 7 1 192.43 200.14 85.34 o 12 7 1 215.91 127.19 124.61 o 13 7 1 0.02 62.30 153.22 o 14 7 1 16.31 81.09 159.35 o 15 7 1 18.55 32.58 207.31 o 0 8 1 4281.41 4683.48 86.37 o 1 8 1 9495.94 9496.26 62.07 o 2 8 1 4249.34 4436.08 65.58 o 3 8 1 8458.58 8412.41 186.90 o 4 8 1 254.60 239.83 60.31 o 5 8 1 8623.53 8043.00 97.96 o 6 8 1 3006.89 3176.39 85.74 o 7 8 1 925.06 836.23 72.81 o 8 8 1 410.82 449.25 25.02 o 9 8 1 2046.14 2093.65 133.07 o 10 8 1 1567.18 1303.49 104.41 o 11 8 1 40.56 52.33 196.42 o 12 8 1 17.33 -65.86 184.49 o 13 8 1 371.96 432.47 201.64 o 14 8 1 88.33 79.43 203.25 o 15 8 1 3.30 -27.52 222.29 o 1 9 1 9.86 17.51 25.94 o 2 9 1 1874.20 2130.37 33.50 o 3 9 1 70.17 60.37 29.20 o 4 9 1 472.91 501.28 51.14 o 5 9 1 230.99 176.58 55.42 o 6 9 1 712.16 746.55 66.01 o 7 9 1 1.09 73.94 87.10 o 8 9 1 408.70 296.96 59.51 o 9 9 1 143.71 155.56 177.87 o 10 9 1 120.98 151.45 173.24 o 11 9 1 3.23 -120.49 184.84 o 12 9 1 104.63 17.77 215.16 o 13 9 1 38.11 -58.21 226.69 o 14 9 1 13.69 -3.79 224.53 o 0 10 1 9757.81 10359.34 214.46 o 1 10 1 2830.46 3073.22 48.30 o 2 10 1 582.52 535.12 31.81 o 3 10 1 1436.79 1608.98 46.74 o 4 10 1 3207.12 3185.99 80.06 o 5 10 1 4165.57 3963.47 68.22 o 6 10 1 187.50 131.67 61.03 o 7 10 1 69.01 162.36 88.36 o 8 10 1 1445.07 1162.04 57.80 o 9 10 1 1607.16 1376.17 143.70 o 10 10 1 240.41 100.34 177.13 o 11 10 1 1.62 -144.03 212.93 o 12 10 1 116.31 83.55 208.15 o 13 10 1 282.42 154.01 209.23 o 14 10 1 23.37 33.77 255.06 o 1 11 1 4388.07 4205.18 53.48 o 2 11 1 14820.21 14526.44 70.14 o 3 11 1 5428.84 5012.46 87.37 o 4 11 1 306.53 248.35 93.77 o 5 11 1 1217.16 1152.66 62.99 o 6 11 1 6399.31 6290.05 100.46 o 7 11 1 3292.79 3290.61 111.80 o 8 11 1 263.98 310.01 65.42 o 9 11 1 117.70 78.67 179.68 o 10 11 1 1373.79 1470.00 219.84 o 11 11 1 931.24 802.59 207.93 o 12 11 1 54.74 -7.63 213.94 o 13 11 1 2.45 79.43 248.08 o 0 12 1 1930.01 1886.15 56.98 o 1 12 1 13.70 15.42 42.51 o 2 12 1 116.93 74.80 42.92 o 3 12 1 42.74 -13.49 46.14 o 4 12 1 257.01 134.52 102.29 o 5 12 1 25.12 25.93 104.57 o 6 12 1 218.73 246.44 80.62 o 7 12 1 7.09 117.92 84.62 o 8 12 1 587.14 590.63 128.65 o 9 12 1 190.70 321.05 156.55 o 10 12 1 15.05 -142.32 219.99 o 11 12 1 13.24 -131.24 211.52 o 12 12 1 1.51 -28.96 243.26 o 13 12 1 98.69 106.49 215.16 o 1 13 1 2900.42 3267.35 49.78 o 2 13 1 354.95 328.65 47.97 o 3 13 1 2847.00 2601.45 56.97 o 4 13 1 324.85 262.24 108.47 o 5 13 1 1146.23 1146.61 116.79 o 6 13 1 139.76 64.88 119.72 o 7 13 1 1117.67 1000.86 126.94 o 8 13 1 326.32 407.16 129.16 o 9 13 1 261.46 343.25 145.57 o 10 13 1 27.80 160.93 148.44 o 11 13 1 323.77 369.77 180.71 o 12 13 1 69.83 -106.16 250.38 o 0 14 1 9100.02 9134.26 151.38 o 1 14 1 9349.89 9600.16 116.19 o 2 14 1 103.58 110.50 60.88 o 3 14 1 8077.61 8426.65 114.52 o 4 14 1 7520.15 6959.65 133.42 o 5 14 1 3504.15 3498.67 130.40 o 6 14 1 24.84 19.51 129.18 o 7 14 1 3588.57 3518.85 147.53 o 8 14 1 1210.88 1214.96 139.50 o 9 14 1 479.66 611.94 152.08 o 10 14 1 3.06 73.34 151.77 o 11 14 1 802.29 735.98 152.42 o 1 15 1 1687.89 1826.89 52.82 o 2 15 1 1940.45 1781.34 59.96 o 3 15 1 1728.40 1676.24 60.32 o 4 15 1 6.46 13.83 116.16 o 5 15 1 547.17 449.75 119.31 o 6 15 1 1005.32 981.02 136.97 o 7 15 1 392.15 401.91 142.42 o 8 15 1 40.63 85.31 138.10 o 9 15 1 202.52 113.79 155.35 o 10 15 1 194.69 274.55 155.50 o 0 16 1 506.35 610.29 77.02 o 1 16 1 199.70 223.46 52.24 o 2 16 1 6.03 44.14 56.07 o 3 16 1 40.30 100.78 114.14 o 4 16 1 608.58 682.04 156.75 o 5 16 1 110.64 14.96 130.05 o 6 16 1 39.79 7.10 136.71 o 7 16 1 1.95 -95.00 148.83 o 8 16 1 19.67 58.25 146.11 o 9 16 1 38.57 80.26 159.92 o 1 17 1 919.96 920.58 62.67 o 2 17 1 1654.85 1686.96 71.20 o 3 17 1 1087.51 1184.62 96.07 o 4 17 1 59.22 28.59 161.43 o 5 17 1 117.54 87.82 175.48 o 6 17 1 727.60 648.04 139.96 o 7 17 1 268.31 290.66 145.20 o 8 17 1 101.34 -51.26 160.06 o 0 18 1 9.12 51.02 82.22 o 1 18 1 16.60 27.66 70.32 o 2 18 1 0.24 -24.29 71.21 o 3 18 1 9.12 89.18 86.71 o 4 18 1 35.89 4.03 132.57 o 5 18 1 33.03 85.61 175.48 o 6 18 1 34.70 25.08 158.41 o 7 18 1 12.50 -94.60 148.28 o 1 19 1 159.34 196.08 80.75 o 2 19 1 769.94 774.50 82.83 o 3 19 1 257.00 378.93 103.61 o 4 19 1 41.13 132.97 108.09 o 4 0 2 107870.90 109315.31 745.43 o 5 0 2 78815.14 78757.26 690.92 o 6 0 2 4.15 69.69 39.22 o 7 0 2 19003.80 17839.20 205.84 o 8 0 2 17033.22 17064.45 362.11 o 9 0 2 13291.88 13498.86 105.89 o 10 0 2 1211.81 1075.57 68.63 o 11 0 2 2197.85 1945.32 94.82 o 12 0 2 4580.98 4253.66 133.55 o 13 0 2 1529.15 1572.88 122.07 o 14 0 2 16.84 -66.13 118.52 o 15 0 2 64.53 24.17 136.75 o 16 0 2 244.85 181.10 141.68 o 3 1 2 14582.90 14536.34 86.05 o 4 1 2 117.00 138.81 19.14 o 5 1 2 2509.68 2798.49 65.13 o 6 1 2 3520.06 3406.24 35.78 o 7 1 2 2838.14 2720.41 62.94 o 8 1 2 18.17 54.59 36.12 o 9 1 2 253.82 265.47 43.27 o 10 1 2 353.40 416.30 46.48 o 11 1 2 5.42 23.31 48.34 o 12 1 2 47.40 36.86 40.56 o 13 1 2 62.85 -15.88 85.19 o 14 1 2 10.67 53.39 87.01 o 15 1 2 2.63 13.14 95.19 o 16 1 2 2.06 49.59 111.74 o 3 2 2 37893.16 37536.14 536.05 o 4 2 2 1399.82 1585.19 24.40 o 5 2 2 2552.55 2642.08 53.78 o 6 2 2 88.14 99.61 24.84 o 7 2 2 4666.10 4334.47 76.97 o 8 2 2 562.30 550.74 36.03 o 9 2 2 676.25 741.28 38.99 o 10 2 2 344.90 402.49 43.91 o 11 2 2 66.99 52.50 41.84 o 12 2 2 484.27 555.22 79.60 o 13 2 2 33.06 46.30 86.01 o 14 2 2 3.71 -23.48 100.80 o 15 2 2 0.69 -27.30 108.04 o 16 2 2 55.11 82.01 110.77 o 2 3 2 29831.58 28622.56 112.53 o 3 3 2 1168.66 1159.65 18.80 o 4 3 2 5869.40 5942.41 70.83 o 5 3 2 776.05 760.19 26.98 o 6 3 2 10294.20 9720.96 89.00 o 7 3 2 631.45 554.57 47.04 o 8 3 2 2151.16 2026.01 62.35 o 9 3 2 4.22 20.54 55.25 o 10 3 2 1717.39 1854.60 81.89 o 11 3 2 9.92 -8.33 77.77 o 12 3 2 272.06 333.54 90.80 o 13 3 2 55.98 40.95 99.18 o 14 3 2 159.56 231.76 108.11 o 15 3 2 0.25 -6.73 103.95 o 16 3 2 31.17 42.15 110.74 o 0 4 2 215.86 421.89 31.77 o 1 4 2 24798.46 25281.65 222.66 o 2 4 2 88.54 160.25 16.67 o 3 4 2 9827.21 9457.28 102.41 o 4 4 2 28.99 33.27 15.89 o 5 4 2 8251.21 7602.11 45.88 o 6 4 2 851.50 916.93 30.09 o 7 4 2 650.74 697.90 55.59 o 8 4 2 674.83 665.35 65.03 o 9 4 2 1532.37 1404.64 58.91 o 10 4 2 69.17 93.86 51.09 o 11 4 2 176.36 199.38 81.41 o 12 4 2 2.86 106.30 89.52 o 13 4 2 453.30 547.78 95.49 o 14 4 2 57.95 54.57 106.49 o 15 4 2 8.29 117.11 106.13 o 16 4 2 0.03 49.00 120.13 o 1 5 2 973.71 939.34 46.40 o 2 5 2 13654.83 14784.88 142.02 o 3 5 2 12.02 26.60 21.90 o 4 5 2 234.61 290.64 25.70 o 5 5 2 91.00 88.15 17.43 o 6 5 2 1192.57 1098.56 35.82 o 7 5 2 169.03 161.31 27.19 o 8 5 2 187.58 99.82 57.26 o 9 5 2 0.10 24.18 53.91 o 10 5 2 99.78 101.07 61.87 o 11 5 2 15.18 62.80 84.23 o 12 5 2 67.30 116.13 88.04 o 13 5 2 7.53 29.05 91.50 o 14 5 2 19.26 138.32 105.15 o 15 5 2 3.83 85.46 110.99 o 16 5 2 21.67 182.03 154.41 o 0 6 2 1728.01 1786.33 47.75 o 1 6 2 9284.71 10313.72 212.11 o 2 6 2 28.26 73.64 19.66 o 3 6 2 1556.48 1382.73 28.27 o 4 6 2 220.32 170.80 27.84 o 5 6 2 8086.90 6931.73 110.50 o 6 6 2 1694.62 1601.99 46.79 o 7 6 2 85.31 91.56 27.86 o 8 6 2 399.87 418.01 52.47 o 9 6 2 2871.27 2876.64 100.99 o 10 6 2 433.47 328.25 61.25 o 11 6 2 19.66 91.99 67.01 o 12 6 2 0.79 15.51 83.19 o 13 6 2 399.50 602.48 93.92 o 14 6 2 77.02 111.99 101.39 o 15 6 2 35.24 150.07 176.35 o 1 7 2 561.74 532.26 21.90 o 2 7 2 32311.43 34069.90 309.30 o 3 7 2 113.06 156.34 29.39 o 4 7 2 45.44 89.95 35.93 o 5 7 2 453.01 482.48 53.22 o 6 7 2 11510.12 11310.13 219.03 o 7 7 2 559.11 622.23 66.19 o 8 7 2 316.90 272.86 39.72 o 9 7 2 9.02 55.74 80.64 o 10 7 2 1582.68 1765.57 95.07 o 11 7 2 124.46 202.05 86.71 o 12 7 2 107.61 234.87 128.93 o 13 7 2 0.60 17.61 145.85 o 14 7 2 158.38 248.65 154.16 o 15 7 2 55.23 204.00 193.54 o 0 8 2 460.39 598.05 37.08 o 1 8 2 2426.40 3052.67 44.96 o 2 8 2 765.28 798.07 24.33 o 3 8 2 2220.35 2226.01 38.82 o 4 8 2 34.56 40.38 51.52 o 5 8 2 1899.29 1624.47 128.86 o 6 8 2 50.70 56.72 30.00 o 7 8 2 362.67 364.60 31.30 o 8 8 2 1.77 12.97 35.56 o 9 8 2 854.20 794.14 72.00 o 10 8 2 9.49 15.59 72.53 o 11 8 2 2.39 64.99 179.80 o 12 8 2 54.68 99.95 188.49 o 13 8 2 183.46 9.93 219.99 o 14 8 2 5.40 -155.17 225.06 o 15 8 2 1.18 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379.91 371.75 43.19 o 2 7 8 4875.05 4462.63 64.23 o 3 7 8 175.78 117.51 55.17 o 4 7 8 8.61 22.63 83.46 o 5 7 8 122.24 174.31 88.81 o 6 7 8 1443.78 1475.47 77.56 o 7 7 8 242.60 275.20 69.78 o 8 7 8 8.95 56.50 68.63 o 9 7 8 60.71 49.93 71.47 o 10 7 8 115.29 121.83 88.86 o 11 7 8 114.63 156.32 75.17 o 12 7 8 2.09 123.90 104.94 o 13 7 8 94.51 212.33 114.45 o 14 7 8 6.40 188.73 197.22 o 0 8 8 1899.97 1801.37 41.81 o 1 8 8 768.39 908.23 43.04 o 2 8 8 139.16 148.21 50.32 o 3 8 8 376.90 391.40 56.39 o 4 8 8 205.95 182.80 75.23 o 5 8 8 97.32 52.68 81.03 o 6 8 8 3.97 44.79 76.36 o 7 8 8 389.13 376.75 69.58 o 8 8 8 297.23 287.40 70.06 o 9 8 8 21.40 9.73 76.08 o 10 8 8 135.51 94.24 74.91 o 11 8 8 60.39 76.84 76.26 o 12 8 8 0.65 96.18 190.85 o 13 8 8 0.28 303.13 203.25 o 14 8 8 3.85 137.41 203.25 o 1 9 8 1015.74 1009.95 47.55 o 2 9 8 4526.51 4545.23 77.32 o 3 9 8 2769.04 2414.37 63.03 o 4 9 8 34.03 121.70 67.36 o 5 9 8 98.82 184.71 88.87 o 6 9 8 2026.90 2028.82 95.67 o 7 9 8 2267.03 1903.57 97.49 o 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