#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/96/2229668.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229668_Fobs loop_ _publ_author_name 'Tamizh, M. Muthu' 'Karvembu, R.' 'Varghese, B.' 'Tiekink, Edward R. T.' _publ_section_title ; {4-Bromo-2-[(2-sulfidophenyl)iminomethyl]phenolato-\k^3^S,N,O}(triphenylphosphane-\kP)nickel(II) ; _journal_coeditor_code HB5813 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m441 _journal_volume 67 _journal_year 2011 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.7197 _cell_length_b 18.7729 _cell_length_c 29.8372 _exptl_crystal_F_000 2544.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file hb5813Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NIBRL in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 587.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 46706.01 48898.55 1161.45 o 4 0 0 1458.07 1135.07 80.51 o 6 0 0 1065.07 1076.90 68.64 o 8 0 0 5963.03 6235.75 178.95 o 10 0 0 7979.74 8021.57 383.04 o 12 0 0 2704.99 2949.20 297.73 o 2 1 0 151214.80 154289.52 1845.14 o 4 1 0 7.38 18.72 23.78 o 6 1 0 2351.79 2539.80 68.38 o 8 1 0 6887.87 6767.93 131.48 o 10 1 0 60.80 34.91 113.61 o 12 1 0 0.72 201.80 208.99 o 2 2 0 62188.20 66077.62 655.38 o 4 2 0 128.55 152.49 20.72 o 6 2 0 54.25 123.14 46.80 o 8 2 0 3249.55 3244.04 92.21 o 10 2 0 850.04 914.46 156.43 o 12 2 0 926.98 975.07 239.14 o 2 3 0 345297.28 336986.63 3638.28 o 4 3 0 136.21 177.13 18.37 o 6 3 0 1074.94 1065.06 43.64 o 8 3 0 4816.28 4865.19 113.01 o 10 3 0 7.13 -50.49 92.98 o 12 3 0 62.33 -136.70 186.38 o 0 4 0 149647.80 147471.00 3616.61 o 2 4 0 480.52 416.34 18.85 o 4 4 0 4487.24 5138.79 154.04 o 6 4 0 2197.16 2178.39 66.64 o 8 4 0 903.89 925.28 66.49 o 10 4 0 2359.76 2459.57 145.89 o 12 4 0 1336.89 1238.88 229.55 o 2 5 0 2976.18 3257.17 66.94 o 4 5 0 8055.68 9363.01 105.58 o 6 5 0 172.45 194.82 36.89 o 8 5 0 16.41 15.65 55.42 o 10 5 0 211.52 58.44 104.93 o 12 5 0 188.57 -6.17 187.07 o 0 6 0 108298.20 108361.88 2676.14 o 2 6 0 12413.22 12623.66 248.53 o 4 6 0 3641.76 4092.24 71.31 o 6 6 0 876.91 947.95 39.36 o 8 6 0 1273.36 1387.46 86.95 o 10 6 0 6273.75 6415.27 450.36 o 12 6 0 2718.70 2466.46 284.71 o 2 7 0 4063.59 4436.19 476.92 o 4 7 0 38165.19 38393.91 481.60 o 6 7 0 3721.13 3744.46 117.89 o 8 7 0 2638.31 2821.33 128.14 o 10 7 0 1895.19 1868.67 150.35 o 12 7 0 3.19 -106.93 142.31 o 0 8 0 89747.76 89293.15 2224.92 o 2 8 0 4920.11 5466.52 171.99 o 4 8 0 1430.84 1540.21 76.11 o 6 8 0 3433.07 3480.89 97.91 o 8 8 0 2926.06 2990.05 130.27 o 10 8 0 984.11 868.48 130.44 o 2 9 0 64363.63 66501.88 1188.05 o 4 9 0 2806.64 2784.87 91.04 o 6 9 0 349.51 374.51 70.64 o 8 9 0 6929.89 6729.99 197.73 o 10 9 0 1.03 -123.94 104.35 o 0 10 0 23772.85 24444.31 666.72 o 2 10 0 1979.18 1882.53 89.03 o 4 10 0 287.09 300.70 50.92 o 6 10 0 1590.26 1538.38 182.44 o 8 10 0 52.89 100.89 84.98 o 10 10 0 2245.67 2640.92 298.93 o 2 11 0 3166.29 3028.02 118.56 o 4 11 0 16127.69 15739.96 273.43 o 6 11 0 69.44 189.97 112.38 o 8 11 0 1376.96 1285.97 115.90 o 10 11 0 1944.37 1885.47 137.42 o 0 12 0 78323.13 80094.37 2034.09 o 2 12 0 1488.82 1743.54 187.75 o 4 12 0 24.57 -36.96 53.06 o 6 12 0 3497.01 3592.75 199.74 o 8 12 0 3150.22 3540.66 208.31 o 10 12 0 2022.16 1937.57 145.94 o 2 13 0 17131.61 16821.63 361.11 o 4 13 0 9673.06 9630.00 200.98 o 6 13 0 12109.12 11420.46 585.52 o 8 13 0 7106.92 7291.98 241.37 o 10 13 0 71.82 -100.09 107.58 o 0 14 0 2849.32 2772.07 184.67 o 2 14 0 41.87 119.93 82.61 o 4 14 0 227.74 172.77 71.23 o 6 14 0 239.37 344.98 99.63 o 8 14 0 46.67 236.75 113.58 o 10 14 0 1.79 -117.50 119.77 o 2 15 0 2406.78 2409.96 131.70 o 4 15 0 233.40 215.85 217.39 o 6 15 0 1797.93 1885.56 169.76 o 8 15 0 1609.78 1254.81 160.51 o 0 16 0 11316.63 11263.70 414.56 o 2 16 0 3646.79 3407.37 162.90 o 4 16 0 783.47 336.79 162.74 o 6 16 0 70.19 124.62 110.38 o 8 16 0 939.32 793.40 135.57 o 2 17 0 2117.37 2084.07 158.29 o 4 17 0 2400.33 2851.21 241.20 o 6 17 0 1899.93 2018.37 156.31 o 8 17 0 653.28 605.68 200.60 o 0 18 0 616.13 618.41 172.68 o 2 18 0 794.84 966.63 125.37 o 4 18 0 86.40 91.13 180.21 o 6 18 0 2.19 128.13 124.37 o 8 18 0 0.46 -118.01 155.37 o 2 19 0 1129.45 1263.55 139.27 o 4 19 0 9767.34 9678.09 444.37 o 6 19 0 2460.06 2714.23 184.57 o 0 20 0 72.39 -152.80 156.92 o 2 20 0 1155.02 1175.04 167.19 o 4 20 0 393.35 440.94 226.12 o 6 20 0 200.66 281.57 144.73 o 2 21 0 2945.39 3136.31 191.73 o 4 21 0 30.44 79.05 132.58 o 6 21 0 251.70 147.69 149.07 o 0 22 0 592.05 717.09 225.44 o 2 22 0 468.69 444.71 233.66 o 4 22 0 83.04 105.81 141.76 o 2 23 0 1.24 126.08 236.74 o 4 23 0 1501.52 1710.53 261.07 o 0 24 0 962.77 894.90 263.81 o 2 24 0 741.26 656.44 269.64 o 1 1 1 10384.83 9295.49 105.68 o 2 1 1 31191.71 32968.04 284.46 o 3 1 1 7728.38 8118.21 105.92 o 4 1 1 4237.90 3946.22 57.79 o 5 1 1 10172.80 10066.07 111.79 o 6 1 1 2180.70 1952.72 64.65 o 7 1 1 843.50 979.48 48.23 o 8 1 1 1049.69 982.83 43.06 o 9 1 1 243.37 268.90 40.64 o 10 1 1 48.35 -38.07 55.41 o 11 1 1 261.38 250.36 98.48 o 12 1 1 66.42 112.28 117.33 o 0 2 1 95021.05 61839.32 1081.10 o 1 2 1 42612.14 45524.25 419.76 o 2 2 1 18586.35 19351.79 145.56 o 3 2 1 13226.00 13281.03 114.74 o 4 2 1 24200.73 25079.61 223.41 o 5 2 1 11990.00 13057.05 126.87 o 6 2 1 1715.48 1793.77 51.20 o 7 2 1 12.47 16.72 35.27 o 8 2 1 2652.39 2580.78 58.81 o 9 2 1 2376.11 2494.36 69.64 o 10 2 1 2090.33 2063.37 116.92 o 11 2 1 1167.37 1284.70 158.86 o 12 2 1 1181.53 1335.12 368.99 o 1 3 1 5537.18 6020.96 74.65 o 2 3 1 60450.78 64874.73 555.83 o 3 3 1 33.95 16.87 9.28 o 4 3 1 3446.75 3972.84 48.13 o 5 3 1 47.48 83.75 19.16 o 6 3 1 1149.29 1210.62 33.04 o 7 3 1 2348.51 2286.72 56.62 o 8 3 1 852.23 892.58 47.67 o 9 3 1 196.67 142.98 56.47 o 10 3 1 2.68 17.68 67.05 o 11 3 1 285.04 97.25 91.98 o 12 3 1 122.47 133.59 136.32 o 0 4 1 9715.84 9583.85 185.33 o 1 4 1 16002.51 16396.66 214.04 o 2 4 1 169487.84 175996.59 1687.01 o 3 4 1 55.02 74.90 11.20 o 4 4 1 3692.58 3599.61 44.43 o 5 4 1 734.06 702.51 23.62 o 6 4 1 6606.73 6085.06 82.35 o 7 4 1 147.83 174.79 27.73 o 8 4 1 2349.42 2027.14 78.11 o 9 4 1 364.93 248.99 67.11 o 10 4 1 778.77 779.50 82.39 o 11 4 1 1791.14 1878.13 103.82 o 12 4 1 569.38 566.82 154.39 o 1 5 1 20364.25 20297.33 264.58 o 2 5 1 141.84 186.57 15.60 o 3 5 1 7912.97 8207.81 82.20 o 4 5 1 54328.18 56971.14 671.53 o 5 5 1 238.78 263.85 18.94 o 6 5 1 11797.23 11421.53 133.80 o 7 5 1 66.64 46.46 27.31 o 8 5 1 68.50 25.98 46.14 o 9 5 1 590.19 604.89 84.78 o 10 5 1 280.53 314.94 77.55 o 11 5 1 48.75 12.09 85.77 o 12 5 1 2.55 199.38 145.90 o 0 6 1 340.15 313.62 36.43 o 1 6 1 662.67 808.74 32.87 o 2 6 1 1549.98 1621.83 50.89 o 3 6 1 12.56 -33.32 22.22 o 4 6 1 1222.61 1374.17 46.87 o 5 6 1 142.62 201.28 22.68 o 6 6 1 5.07 8.72 23.93 o 7 6 1 117.49 115.59 38.98 o 8 6 1 312.75 342.98 57.02 o 9 6 1 3.05 -53.06 76.37 o 10 6 1 1.28 81.51 79.00 o 11 6 1 14.41 57.11 86.59 o 12 6 1 248.90 318.97 156.25 o 1 7 1 5055.90 4699.23 83.28 o 2 7 1 569.24 478.61 31.28 o 3 7 1 867.05 944.86 32.43 o 4 7 1 24810.45 23993.71 236.64 o 5 7 1 1029.69 1027.08 58.20 o 6 7 1 378.97 404.86 26.97 o 7 7 1 204.05 222.13 40.28 o 8 7 1 26.32 26.13 49.14 o 9 7 1 162.15 169.20 49.79 o 10 7 1 280.55 238.29 81.26 o 11 7 1 64.99 64.84 113.81 o 12 7 1 22.95 4.89 98.03 o 0 8 1 299.61 238.71 43.73 o 1 8 1 24514.55 25812.16 342.44 o 2 8 1 14713.48 14131.07 201.78 o 3 8 1 135.58 118.13 28.20 o 4 8 1 8858.78 8913.65 104.17 o 5 8 1 156.68 144.50 24.08 o 6 8 1 3601.56 3627.85 70.46 o 7 8 1 64.65 8.14 37.90 o 8 8 1 1653.59 1471.50 69.35 o 9 8 1 668.29 761.72 67.58 o 10 8 1 2069.33 2068.02 172.00 o 11 8 1 900.89 711.92 98.19 o 1 9 1 1.37 52.13 31.87 o 2 9 1 6599.56 7208.69 123.04 o 3 9 1 6573.47 6484.00 115.19 o 4 9 1 13094.46 13348.62 162.35 o 5 9 1 14635.85 14546.71 175.93 o 6 9 1 1811.31 1700.13 70.29 o 7 9 1 313.16 302.48 70.32 o 8 9 1 806.17 900.53 67.09 o 9 9 1 1876.59 2080.20 86.76 o 10 9 1 421.81 443.72 65.20 o 11 9 1 77.74 73.16 89.53 o 0 10 1 949.10 999.49 92.51 o 1 10 1 15229.75 15307.38 223.49 o 2 10 1 403.32 243.66 40.64 o 3 10 1 5064.41 4769.42 101.31 o 4 10 1 3307.17 3318.83 98.72 o 5 10 1 1615.56 1640.08 61.75 o 6 10 1 107.96 26.12 51.23 o 7 10 1 80.28 35.34 54.20 o 8 10 1 2407.38 2360.87 91.87 o 9 10 1 1727.61 1726.61 85.77 o 10 10 1 838.64 1011.88 91.73 o 11 10 1 268.17 154.99 92.66 o 1 11 1 13632.86 13245.17 203.77 o 2 11 1 528.16 561.36 48.57 o 3 11 1 9667.06 9679.23 163.29 o 4 11 1 9691.35 9332.09 131.80 o 5 11 1 6.54 33.67 49.23 o 6 11 1 9160.25 9134.32 167.55 o 7 11 1 3893.88 3788.61 112.12 o 8 11 1 1589.05 1609.24 83.77 o 9 11 1 406.32 404.80 73.52 o 10 11 1 25.90 44.64 70.09 o 11 11 1 138.82 89.32 67.04 o 0 12 1 28252.58 29398.66 673.57 o 1 12 1 471.71 529.80 53.34 o 2 12 1 323.71 266.43 48.66 o 3 12 1 81.90 133.21 46.33 o 4 12 1 148.43 150.77 40.33 o 5 12 1 4.58 48.42 54.36 o 6 12 1 213.14 376.73 94.02 o 7 12 1 47.70 92.42 64.15 o 8 12 1 317.09 301.41 72.12 o 9 12 1 2.62 -64.44 72.95 o 10 12 1 42.18 91.41 73.78 o 1 13 1 2875.52 2700.97 88.57 o 2 13 1 575.85 492.63 57.60 o 3 13 1 8.28 -1.03 50.07 o 4 13 1 143.17 125.95 45.17 o 5 13 1 4277.19 4168.61 142.06 o 6 13 1 687.78 708.89 75.13 o 7 13 1 27.98 149.53 70.53 o 8 13 1 253.06 383.50 88.02 o 9 13 1 601.20 643.99 86.93 o 10 13 1 168.07 27.32 79.73 o 0 14 1 1181.00 1279.63 100.68 o 1 14 1 4545.28 4658.46 118.63 o 2 14 1 4653.72 4492.07 120.66 o 3 14 1 5029.58 4856.26 137.67 o 4 14 1 3277.95 3248.19 84.91 o 5 14 1 176.72 159.34 74.82 o 6 14 1 448.07 545.74 80.41 o 7 14 1 59.93 52.34 74.64 o 8 14 1 1702.21 1648.12 128.62 o 9 14 1 178.96 198.30 84.70 o 10 14 1 56.47 14.16 82.70 o 1 15 1 890.40 874.20 71.13 o 2 15 1 2955.54 2890.39 100.48 o 3 15 1 2344.72 2386.10 94.36 o 4 15 1 1072.68 1008.64 91.48 o 5 15 1 446.42 261.91 73.31 o 6 15 1 7348.26 7247.96 175.95 o 7 15 1 2758.12 2768.86 155.03 o 8 15 1 1555.54 1725.18 104.51 o 9 15 1 390.84 433.84 93.07 o 0 16 1 1398.34 1274.16 111.53 o 1 16 1 36.46 16.20 64.30 o 2 16 1 735.73 825.68 75.54 o 3 16 1 95.59 24.13 64.46 o 4 16 1 22.28 -96.78 80.68 o 5 16 1 306.75 244.02 75.20 o 6 16 1 837.90 788.36 88.42 o 7 16 1 22.87 34.57 108.30 o 8 16 1 7.50 55.55 119.08 o 9 16 1 2.52 -75.20 91.09 o 1 17 1 1051.95 994.04 85.07 o 2 17 1 532.16 448.24 74.10 o 3 17 1 771.70 769.76 83.04 o 4 17 1 7030.79 6760.08 193.08 o 5 17 1 148.13 264.75 81.79 o 6 17 1 1988.31 2234.48 112.81 o 7 17 1 131.86 111.43 87.78 o 8 17 1 150.21 160.37 94.00 o 9 17 1 156.33 165.19 95.57 o 0 18 1 493.17 463.15 118.88 o 1 18 1 96.46 20.65 72.10 o 2 18 1 756.87 700.18 85.13 o 3 18 1 134.26 230.44 79.61 o 4 18 1 1766.15 1964.85 126.26 o 5 18 1 14.56 -78.54 80.12 o 6 18 1 15.90 -124.90 83.26 o 7 18 1 47.80 19.00 90.19 o 8 18 1 147.72 -56.10 95.31 o 1 19 1 320.90 214.79 86.69 o 2 19 1 182.03 38.25 82.04 o 3 19 1 0.08 -108.88 130.43 o 4 19 1 37.88 152.30 107.30 o 5 19 1 633.17 773.08 97.90 o 6 19 1 212.16 105.17 91.87 o 7 19 1 2.15 -4.13 96.04 o 0 20 1 395.11 568.93 140.39 o 1 20 1 89.22 72.47 87.84 o 2 20 1 1192.39 1175.02 107.11 o 3 20 1 364.79 198.68 144.86 o 4 20 1 336.36 302.28 111.17 o 5 20 1 145.77 74.61 96.05 o 6 20 1 339.91 406.61 121.06 o 7 20 1 83.19 -3.26 99.78 o 1 21 1 0.43 -97.35 93.25 o 2 21 1 4.41 -18.65 94.71 o 3 21 1 1416.43 1574.20 177.46 o 4 21 1 2500.82 2971.61 162.37 o 5 21 1 1449.77 1724.87 123.95 o 6 21 1 1388.50 1428.96 123.88 o 0 22 1 261.68 19.25 141.72 o 1 22 1 104.32 182.80 101.29 o 2 22 1 436.46 274.43 444.37 o 3 22 1 1325.27 1335.53 179.34 o 4 22 1 29.47 -119.91 136.80 o 5 22 1 2.99 -140.20 98.81 o 1 23 1 526.14 510.20 107.40 o 2 23 1 104.62 162.72 169.27 o 3 23 1 482.56 755.66 182.52 o 4 23 1 434.03 488.24 115.07 o 0 24 1 814.69 1263.34 485.48 o 1 24 1 269.51 262.22 124.96 o 2 24 1 163.95 342.55 250.79 o 1 0 2 61983.38 59608.89 1536.04 o 2 0 2 1327.36 1406.15 43.18 o 3 0 2 78085.66 80606.79 1355.92 o 4 0 2 1091.45 1146.03 45.11 o 5 0 2 2189.78 2234.89 70.14 o 6 0 2 2525.79 2728.57 85.11 o 7 0 2 23268.42 22680.46 307.68 o 8 0 2 5.71 -71.00 47.33 o 9 0 2 3474.64 3107.04 99.63 o 10 0 2 246.36 383.24 82.09 o 11 0 2 1928.52 1949.89 349.64 o 12 0 2 179.06 109.29 195.29 o 1 1 2 180.73 182.20 5.98 o 2 1 2 18058.81 18554.33 139.76 o 3 1 2 3546.69 3730.11 45.83 o 4 1 2 3.50 29.69 17.68 o 5 1 2 4793.94 4942.20 74.92 o 6 1 2 1289.11 1317.40 40.81 o 7 1 2 1886.79 1736.46 49.97 o 8 1 2 345.77 310.91 47.07 o 9 1 2 161.49 157.53 41.08 o 10 1 2 151.11 143.81 68.04 o 11 1 2 267.76 356.10 101.59 o 12 1 2 35.10 -174.16 116.10 o 0 2 2 2121.13 2159.13 63.55 o 1 2 2 11945.05 12837.72 97.73 o 2 2 2 20899.16 22408.34 176.11 o 3 2 2 40240.44 41155.01 380.66 o 4 2 2 348.92 357.65 17.11 o 5 2 2 1713.36 1865.08 41.15 o 6 2 2 63.70 23.17 25.65 o 7 2 2 3356.51 3167.46 64.40 o 8 2 2 70.48 73.52 34.85 o 9 2 2 369.32 304.46 59.80 o 10 2 2 110.13 -35.46 63.66 o 11 2 2 872.72 1091.94 126.96 o 12 2 2 12.45 28.76 140.82 o 1 3 2 58864.00 61070.42 609.07 o 2 3 2 20428.95 21454.76 190.22 o 3 3 2 2922.24 3278.21 41.50 o 4 3 2 2134.60 2014.32 31.21 o 5 3 2 32895.84 32514.03 308.82 o 6 3 2 1972.84 1879.99 38.03 o 7 3 2 698.52 618.02 40.31 o 8 3 2 142.98 92.70 39.13 o 9 3 2 6.11 -80.69 53.80 o 10 3 2 383.42 383.00 65.29 o 11 3 2 43.77 68.14 95.23 o 12 3 2 17.77 46.14 138.33 o 0 4 2 65224.56 68044.89 1191.57 o 1 4 2 19211.16 19939.27 257.30 o 2 4 2 53.87 51.47 10.99 o 3 4 2 6497.99 6138.02 64.97 o 4 4 2 14.84 1.81 16.77 o 5 4 2 3825.41 3866.59 57.86 o 6 4 2 15.04 15.17 24.91 o 7 4 2 1297.91 1280.62 50.50 o 8 4 2 584.52 676.67 60.40 o 9 4 2 845.52 789.58 88.35 o 10 4 2 368.60 246.28 74.40 o 11 4 2 742.39 890.08 92.61 o 12 4 2 253.08 256.56 144.95 o 1 5 2 26586.31 27236.80 349.03 o 2 5 2 3450.50 3746.03 81.10 o 3 5 2 5204.21 5312.91 72.64 o 4 5 2 712.57 848.35 28.31 o 5 5 2 7167.67 7472.44 102.41 o 6 5 2 1978.65 1971.36 54.16 o 7 5 2 1701.43 1726.51 45.14 o 8 5 2 138.85 58.89 97.54 o 9 5 2 12.07 -41.49 75.03 o 10 5 2 0.07 -32.10 72.54 o 11 5 2 0.28 -31.12 82.07 o 12 5 2 7.03 122.20 146.00 o 0 6 2 10182.47 10271.47 209.31 o 1 6 2 888.89 935.15 33.87 o 2 6 2 7962.80 8113.47 122.03 o 3 6 2 137780.61 137488.08 1178.41 o 4 6 2 966.23 1184.34 29.22 o 5 6 2 656.39 755.28 26.55 o 6 6 2 43.00 45.62 26.42 o 7 6 2 5181.64 5188.24 129.86 o 8 6 2 163.08 174.63 43.57 o 9 6 2 402.23 265.95 83.25 o 10 6 2 107.25 143.82 77.45 o 11 6 2 2889.81 3270.52 172.69 o 12 6 2 119.21 41.92 126.51 o 1 7 2 4418.51 4507.57 124.37 o 2 7 2 5547.34 5839.19 99.06 o 3 7 2 6154.42 6416.25 78.11 o 4 7 2 11807.35 12245.42 134.24 o 5 7 2 18928.88 18487.60 166.84 o 6 7 2 1420.65 1454.83 45.26 o 7 7 2 991.97 1046.29 38.80 o 8 7 2 58.16 -58.31 48.33 o 9 7 2 1507.35 1569.67 65.89 o 10 7 2 18.90 -14.31 89.30 o 11 7 2 171.24 179.65 92.05 o 12 7 2 20.38 -95.23 119.04 o 0 8 2 1767.76 1564.39 72.43 o 1 8 2 1479.75 1552.93 52.94 o 2 8 2 12152.71 12810.78 186.40 o 3 8 2 6298.13 6660.08 101.77 o 4 8 2 5343.30 5898.97 81.49 o 5 8 2 1166.29 1203.69 38.38 o 6 8 2 4.08 -10.04 31.16 o 7 8 2 537.84 604.38 81.44 o 8 8 2 3.44 2.45 52.00 o 9 8 2 688.58 726.43 62.08 o 10 8 2 89.78 55.30 151.53 o 11 8 2 113.07 139.57 95.35 o 1 9 2 10829.95 11207.16 170.20 o 2 9 2 7118.74 7298.17 124.19 o 3 9 2 120.03 59.65 31.18 o 4 9 2 6253.32 6493.23 98.03 o 5 9 2 13867.78 13701.19 154.86 o 6 9 2 1103.62 1198.48 66.26 o 7 9 2 222.54 269.60 56.13 o 8 9 2 26.84 -39.00 54.61 o 9 9 2 1.05 69.45 55.64 o 10 9 2 22.96 21.41 64.67 o 11 9 2 6.40 78.28 91.39 o 0 10 2 9022.19 8806.00 268.95 o 1 10 2 1.88 -46.38 33.97 o 2 10 2 5363.72 5103.21 103.40 o 3 10 2 6084.24 5755.97 112.87 o 4 10 2 877.54 883.37 61.47 o 5 10 2 1316.12 1275.35 50.59 o 6 10 2 544.81 629.43 64.73 o 7 10 2 682.04 689.18 71.31 o 8 10 2 561.80 651.26 68.74 o 9 10 2 293.62 275.93 69.92 o 10 10 2 106.01 138.41 64.53 o 11 10 2 379.41 322.80 99.97 o 1 11 2 1154.98 1089.14 71.26 o 2 11 2 65.72 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54.76 o 3 4 28 1487.07 1446.43 77.60 o 4 4 28 74.58 103.47 65.45 o 5 4 28 118.19 98.89 68.29 o 6 4 28 205.71 229.94 78.00 o 7 4 28 357.15 445.97 89.69 o 8 4 28 28.06 89.84 86.40 o 1 5 28 5.01 50.22 60.67 o 2 5 28 2046.70 2152.55 78.89 o 3 5 28 30.27 19.55 59.88 o 4 5 28 13.98 13.25 62.47 o 5 5 28 50.30 -50.27 71.48 o 6 5 28 196.80 311.72 116.14 o 7 5 28 202.84 184.57 82.14 o 8 5 28 513.76 608.05 92.69 o 0 6 28 5380.24 5092.22 175.43 o 1 6 28 2931.81 2751.08 95.33 o 2 6 28 5.24 -16.80 77.74 o 3 6 28 2924.78 2903.01 97.02 o 4 6 28 1020.24 1181.48 79.77 o 5 6 28 8.64 -88.32 79.00 o 6 6 28 290.82 249.57 114.98 o 7 6 28 559.62 466.44 91.20 o 8 6 28 37.70 64.40 87.33 o 1 7 28 2321.45 2224.36 95.71 o 2 7 28 2996.44 2724.82 105.33 o 3 7 28 390.70 492.84 67.58 o 4 7 28 279.32 342.94 77.58 o 5 7 28 4475.67 4510.40 151.25 o 6 7 28 44.86 41.28 90.95 o 7 7 28 534.67 615.59 90.39 o 0 8 28 11.56 -141.57 94.38 o 1 8 28 1887.12 1949.35 100.40 o 2 8 28 657.64 537.13 81.39 o 3 8 28 271.46 220.28 67.92 o 4 8 28 163.29 203.88 85.28 o 5 8 28 34.06 8.31 90.43 o 6 8 28 185.45 205.04 93.21 o 7 8 28 65.39 -143.75 95.84 o 1 9 28 14.44 44.01 74.00 o 2 9 28 4110.65 4187.01 130.12 o 3 9 28 1497.68 1573.71 102.75 o 4 9 28 834.19 790.67 99.00 o 5 9 28 104.66 140.20 94.45 o 6 9 28 92.78 21.87 100.45 o 7 9 28 230.67 181.58 105.26 o 0 10 28 3527.08 3086.44 244.62 o 1 10 28 319.05 348.23 82.20 o 2 10 28 1183.75 1174.64 93.95 o 3 10 28 1756.11 1504.21 96.89 o 4 10 28 77.79 -33.07 86.56 o 5 10 28 5.37 26.62 91.20 o 6 10 28 39.52 -146.25 97.50 o 7 10 28 456.35 467.68 106.36 o 1 11 28 589.81 572.26 78.45 o 2 11 28 641.11 718.58 81.53 o 3 11 28 1025.79 1002.74 113.98 o 4 11 28 113.11 50.77 91.44 o 5 11 28 1177.51 1154.77 110.81 o 6 11 28 2.29 61.23 98.18 o 0 12 28 3193.97 3176.58 158.71 o 1 12 28 2545.90 2518.32 128.95 o 2 12 28 80.49 7.73 78.85 o 3 12 28 262.65 227.24 93.19 o 4 12 28 590.19 779.57 108.09 o 5 12 28 57.13 -25.52 95.45 o 6 12 28 3.63 -98.18 98.93 o 1 13 28 52.38 169.47 81.14 o 2 13 28 578.03 590.08 112.13 o 3 13 28 1697.70 1628.17 126.28 o 4 13 28 337.20 184.52 102.87 o 5 13 28 1990.90 1952.74 131.91 o 0 14 28 2.53 172.52 186.10 o 1 14 28 120.48 79.57 87.43 o 2 14 28 960.60 943.25 114.86 o 3 14 28 95.69 -32.26 103.65 o 4 14 28 421.41 569.15 112.14 o 1 15 28 3.68 -20.42 90.91 o 2 15 28 1231.79 1286.07 132.17 o 3 15 28 282.51 279.78 138.77 o 0 16 28 2384.91 2605.25 161.53 o 1 16 28 4.26 -163.40 127.54 o 2 16 28 897.22 812.59 127.99 o 1 1 29 1049.73 1135.11 72.49 o 2 1 29 223.10 319.25 52.92 o 3 1 29 41.79 98.06 53.91 o 4 1 29 2636.86 2656.30 79.38 o 5 1 29 237.74 299.70 65.79 o 6 1 29 505.30 535.26 81.93 o 7 1 29 112.17 37.07 70.44 o 8 1 29 0.22 -36.50 75.55 o 0 2 29 2258.64 2468.16 224.01 o 1 2 29 124.52 227.53 62.92 o 2 2 29 7826.53 7554.45 152.61 o 3 2 29 2060.67 2071.90 74.26 o 4 2 29 2291.79 2257.10 83.68 o 5 2 29 2308.53 2175.44 103.70 o 6 2 29 231.43 268.56 83.34 o 7 2 29 320.80 351.16 77.89 o 8 2 29 671.04 648.26 81.85 o 1 3 29 1.38 -62.60 59.43 o 2 3 29 17.88 29.57 55.08 o 3 3 29 101.11 100.00 70.65 o 4 3 29 423.99 392.37 63.11 o 5 3 29 230.36 201.84 75.77 o 6 3 29 595.30 452.05 86.33 o 7 3 29 1226.86 1110.39 97.54 o 8 3 29 104.22 144.93 102.13 o 0 4 29 552.48 485.77 99.13 o 1 4 29 713.51 605.42 68.08 o 2 4 29 2328.87 2432.85 82.74 o 3 4 29 8179.64 8106.03 149.70 o 4 4 29 1173.17 1001.36 76.55 o 5 4 29 197.29 126.63 76.53 o 6 4 29 907.68 846.89 90.51 o 7 4 29 728.82 752.51 156.13 o 8 4 29 17.43 52.71 87.07 o 1 5 29 1292.58 1297.01 82.17 o 2 5 29 45.10 34.00 56.58 o 3 5 29 611.93 518.30 69.00 o 4 5 29 4292.77 3868.38 111.34 o 5 5 29 2161.75 2175.04 122.40 o 6 5 29 1266.93 1468.62 100.82 o 7 5 29 330.68 424.06 114.27 o 0 6 29 271.15 200.60 94.22 o 1 6 29 148.68 91.45 67.56 o 2 6 29 11.27 45.96 72.20 o 3 6 29 91.44 154.78 64.25 o 4 6 29 411.36 400.96 106.36 o 5 6 29 14.26 102.75 85.41 o 6 6 29 11.84 6.65 90.27 o 7 6 29 21.94 163.24 85.58 o 1 7 29 1186.30 1211.22 107.59 o 2 7 29 137.45 117.52 73.75 o 3 7 29 33.88 81.67 86.41 o 4 7 29 1675.64 1779.64 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31 252.99 246.06 67.43 o 5 3 31 8.10 101.96 80.36 o 6 3 31 190.24 277.84 86.56 o 7 3 31 91.11 133.19 89.10 o 0 4 31 6739.21 7238.91 251.18 o 1 4 31 4785.88 4613.72 122.75 o 2 4 31 3891.39 3925.25 101.83 o 3 4 31 7.69 44.38 65.41 o 4 4 31 658.86 688.29 79.44 o 5 4 31 176.31 128.10 81.77 o 6 4 31 96.81 46.18 83.83 o 7 4 31 210.16 172.26 100.82 o 1 5 31 716.91 872.21 80.62 o 2 5 31 967.44 1048.46 77.75 o 3 5 31 1366.01 1337.07 88.36 o 4 5 31 1001.61 1138.46 84.34 o 5 5 31 72.39 95.41 89.30 o 6 5 31 210.37 273.46 88.03 o 7 5 31 5.07 -62.98 88.58 o 0 6 31 293.79 232.31 103.60 o 1 6 31 64.20 16.69 67.74 o 2 6 31 115.82 140.05 65.87 o 3 6 31 105.89 204.63 71.28 o 4 6 31 110.55 129.96 77.45 o 5 6 31 5.04 65.16 96.12 o 6 6 31 355.00 312.21 92.73 o 1 7 31 574.76 590.55 80.44 o 2 7 31 754.21 875.23 90.52 o 3 7 31 52.79 52.54 72.29 o 4 7 31 2.76 35.95 95.15 o 5 7 31 377.34 467.87 100.37 o 6 7 31 371.12 425.21 109.07 o 0 8 31 3912.54 4000.57 171.86 o 1 8 31 1838.04 1805.88 103.56 o 2 8 31 1986.49 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