#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/96/2229670.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229670_Fobs loop_ _publ_author_name 'Yousuf, S.' 'Kamdem, R. S. T.' 'Ngadjui, B. T.' 'Wafo, P.' 'Fun, Hoong-Kun' _publ_section_title ; 3\a-Hydroxytirucalla-8,24-dien-21-oic acid ; _journal_coeditor_code HB5815 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o937 _journal_page_last o938 _journal_volume 67 _journal_year 2011 _space_group_IT_number 152 _symmetry_space_group_name_Hall 'P 31 2"' _symmetry_space_group_name_H-M 'P 31 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 11.2794 _cell_length_b 11.2794 _cell_length_c 36.6986 _exptl_crystal_F_000 1512.00 _reflns_d_resolution_high 0.8113 _[local]_cod_data_source_file hb5815Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rasa6m in P3(1)21 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 169.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z+1/3' '-x+y, -x, z+2/3' 'y, x, -z' 'x-y, -y, -z+2/3' '-x, -x+y, -z+1/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 4887.38 4251.55 156.95 o 1 1 0 20631.90 22090.90 837.25 o -1 2 0 20567.55 20328.58 775.55 o 0 2 0 9636.81 9898.47 268.25 o 1 2 0 5560.59 5603.44 108.79 o 2 2 0 11265.74 11754.93 466.40 o -1 3 0 5563.72 5658.20 125.80 o 0 3 0 532.61 669.77 19.04 o 1 3 0 1498.71 1529.21 34.53 o 2 3 0 3349.46 3521.91 79.08 o -1 4 0 1509.99 1519.72 51.29 o 0 4 0 1.65 7.18 1.66 o 1 4 0 4255.79 4831.13 130.46 o 2 4 0 679.21 583.30 17.55 o 3 4 0 1400.47 1396.44 26.82 o 4 4 0 843.74 786.77 22.45 o -1 5 0 4280.58 4763.15 177.53 o 0 5 0 387.27 375.38 16.31 o 1 5 0 56.47 35.24 2.16 o 2 5 0 526.14 524.72 11.40 o 3 5 0 76.86 75.42 3.79 o 4 5 0 169.22 143.25 15.02 o 5 5 0 281.97 263.84 13.95 o -3 6 0 1371.83 1579.22 60.35 o -2 6 0 686.53 580.78 14.60 o -1 6 0 56.25 35.91 3.07 o 0 6 0 619.31 628.63 13.25 o 1 6 0 1062.58 1020.89 20.33 o 2 6 0 2273.74 2243.70 48.13 o 3 6 0 307.52 297.17 21.03 o 4 6 0 144.00 151.47 3.89 o 5 6 0 241.56 236.26 6.63 o 6 6 0 71.30 70.50 3.96 o -3 7 0 1407.14 1383.88 35.58 o -2 7 0 530.46 521.59 16.90 o -1 7 0 1065.94 993.89 35.11 o 0 7 0 79.57 84.76 4.94 o 1 7 0 360.04 403.08 14.87 o 2 7 0 911.28 861.30 14.62 o 3 7 0 1372.20 1239.63 19.77 o 4 7 0 242.38 254.44 5.21 o 5 7 0 154.76 164.46 5.16 o 6 7 0 127.66 133.99 3.56 o -4 8 0 845.42 787.58 35.33 o -3 8 0 77.91 72.48 5.77 o -2 8 0 2276.02 2235.66 60.53 o -1 8 0 361.58 377.65 14.35 o 0 8 0 50.99 45.77 6.31 o 1 8 0 1939.40 1866.81 28.96 o 2 8 0 337.26 352.79 7.14 o 3 8 0 123.22 117.58 4.10 o 4 8 0 189.47 184.88 5.46 o 5 8 0 36.01 39.35 2.39 o -4 9 0 169.67 162.46 12.38 o -3 9 0 307.27 297.60 19.35 o -2 9 0 910.03 890.39 18.93 o -1 9 0 1941.73 1863.14 26.68 o 0 9 0 544.58 541.41 9.46 o 1 9 0 389.67 399.02 12.07 o 2 9 0 121.88 110.71 3.70 o 3 9 0 211.84 218.31 12.73 o 4 9 0 139.72 139.16 4.96 o -5 10 0 283.35 241.69 14.01 o -4 10 0 143.03 138.53 3.59 o -3 10 0 1372.23 1241.73 16.74 o -2 10 0 337.12 349.66 6.76 o -1 10 0 387.81 384.37 9.65 o 0 10 0 20.59 26.12 2.00 o 1 10 0 308.82 309.84 6.14 o 2 10 0 9.03 15.04 2.66 o 3 10 0 13.86 9.82 2.04 o -5 11 0 240.58 238.86 6.69 o -4 11 0 242.16 238.86 5.96 o -3 11 0 122.69 125.84 3.54 o -2 11 0 120.04 113.18 3.13 o -1 11 0 307.08 302.52 5.63 o 0 11 0 531.12 588.80 8.96 o 1 11 0 44.10 43.66 3.82 o -6 12 0 70.69 67.96 7.12 o -5 12 0 152.45 153.91 5.62 o -4 12 0 186.92 176.80 5.44 o -3 12 0 211.51 211.59 5.06 o -2 12 0 9.10 12.78 1.35 o -1 12 0 44.29 43.34 3.43 o -6 13 0 128.66 132.36 7.74 o -5 13 0 35.78 37.65 2.17 o -4 13 0 138.79 137.31 4.59 o -3 13 0 13.87 16.07 1.74 o -1 1 1 6085.57 5939.22 225.51 o 0 1 1 112.20 88.45 3.76 o 1 1 1 2927.10 3006.87 138.20 o -3 2 1 7709.61 7361.36 143.72 o -2 2 1 5398.69 5161.27 139.64 o -1 2 1 2947.99 2981.93 113.59 o 0 2 1 7570.65 7233.78 257.40 o 1 2 1 3491.50 3695.22 80.56 o 2 2 1 349.42 419.56 66.07 o -5 3 1 2684.38 2884.78 65.08 o -4 3 1 4610.04 5226.70 116.52 o -3 3 1 495.74 509.28 14.77 o -2 3 1 7701.76 7406.67 163.95 o -1 3 1 3480.62 3765.55 83.41 o 0 3 1 2423.29 2432.37 66.09 o 1 3 1 1086.40 1067.27 27.79 o 2 3 1 778.21 818.31 36.94 o -7 4 1 272.96 269.22 9.44 o -6 4 1 1023.02 1129.21 26.02 o -5 4 1 2642.86 2405.17 105.00 o -4 4 1 1228.73 1361.00 38.01 o -3 4 1 4631.75 5205.67 140.02 o -1 4 1 1079.61 1092.38 45.89 o 0 4 1 1187.63 1276.47 35.65 o 1 4 1 5087.17 5244.66 142.41 o 2 4 1 350.87 411.12 13.44 o 3 4 1 299.33 306.45 9.92 o 4 4 1 235.58 214.61 11.02 o -9 5 1 337.58 306.34 7.73 o -8 5 1 3.79 3.97 1.25 o -7 5 1 147.24 161.20 5.80 o -6 5 1 271.66 312.82 7.26 o -5 5 1 369.71 469.94 19.84 o -4 5 1 2647.69 2622.28 95.83 o -1 5 1 5092.50 5220.42 191.50 o 0 5 1 4.73 9.69 2.45 o 1 5 1 650.41 656.98 12.02 o 2 5 1 455.49 503.63 10.91 o 3 5 1 1.00 3.02 1.57 o 4 5 1 954.05 947.06 18.89 o 5 5 1 886.17 818.18 12.57 o -11 6 1 291.81 293.04 4.88 o -10 6 1 300.14 300.63 5.99 o -9 6 1 134.46 134.03 7.83 o -8 6 1 302.60 307.50 28.02 o -7 6 1 557.73 521.86 11.43 o -6 6 1 3.24 11.60 1.70 o -5 6 1 268.32 301.88 8.41 o -4 6 1 1022.47 1048.89 29.22 o -3 6 1 2181.68 2327.88 61.05 o -2 6 1 346.75 401.20 16.73 o -1 6 1 647.80 664.97 13.92 o 0 6 1 1420.96 1370.33 26.34 o 1 6 1 175.24 168.28 11.75 o 2 6 1 640.84 677.94 16.83 o 3 6 1 774.54 779.16 18.52 o 4 6 1 114.91 114.10 6.07 o 5 6 1 137.56 117.26 5.32 o 6 6 1 64.31 56.31 2.56 o -13 7 1 19.45 23.25 1.75 o -12 7 1 14.93 16.45 1.74 o -11 7 1 807.07 794.19 11.53 o -10 7 1 169.85 155.00 7.62 o -9 7 1 2607.58 2511.26 41.51 o -8 7 1 1340.10 1258.08 36.33 o -7 7 1 29.34 29.37 2.82 o -6 7 1 560.15 534.27 23.77 o -5 7 1 148.48 157.75 10.67 o -4 7 1 277.55 303.89 14.94 o -3 7 1 298.45 305.72 10.55 o -2 7 1 456.09 508.52 21.75 o -1 7 1 174.65 187.40 11.62 o 0 7 1 1220.26 1111.23 25.84 o 1 7 1 226.84 193.55 10.99 o 2 7 1 105.21 108.38 7.96 o 3 7 1 69.71 60.66 2.94 o 4 7 1 175.95 191.19 5.20 o 5 7 1 226.18 237.82 5.12 o 6 7 1 42.31 35.04 1.99 o -13 8 1 23.13 23.44 1.95 o -12 8 1 0.01 2.59 1.63 o -11 8 1 55.70 46.55 2.79 o -10 8 1 211.90 206.15 4.93 o -9 8 1 529.20 517.08 13.71 o -8 8 1 950.88 964.68 24.09 o -7 8 1 1336.28 1308.02 37.67 o -6 8 1 302.57 352.52 22.19 o -5 8 1 3.80 4.99 2.69 o -4 8 1 234.34 223.13 10.40 o -3 8 1 1.06 6.95 4.89 o -2 8 1 646.76 716.83 22.87 o -1 8 1 225.87 245.88 23.34 o 0 8 1 531.12 548.57 19.22 o 1 8 1 63.69 79.01 3.49 o 2 8 1 57.93 60.58 2.89 o 3 8 1 488.38 475.81 18.03 o 4 8 1 75.02 82.31 4.74 o 5 8 1 54.25 47.17 2.54 o -13 9 1 157.11 149.77 4.14 o -12 9 1 71.89 97.08 5.93 o -11 9 1 181.22 175.52 5.30 o -10 9 1 14.33 24.84 1.98 o -9 9 1 404.49 409.04 7.69 o -8 9 1 530.70 533.68 8.73 o -7 9 1 2618.22 2604.68 51.29 o -6 9 1 135.69 133.36 8.18 o -5 9 1 338.20 303.76 9.35 o -4 9 1 951.87 909.88 26.72 o -3 9 1 780.98 771.40 19.51 o -2 9 1 105.56 102.42 4.72 o -1 9 1 63.04 84.00 4.61 o 0 9 1 159.19 139.13 4.06 o 1 9 1 269.03 239.51 9.45 o 2 9 1 148.14 150.37 10.69 o 3 9 1 135.16 125.71 9.70 o 4 9 1 37.61 33.42 2.10 o -13 10 1 23.43 23.93 2.50 o -12 10 1 2.22 3.87 1.73 o -11 10 1 106.54 108.45 3.78 o -10 10 1 390.39 371.12 6.39 o -9 10 1 13.52 21.77 1.55 o -8 10 1 208.72 199.57 4.54 o -7 10 1 170.15 159.72 6.30 o -6 10 1 299.53 314.03 5.81 o -5 10 1 880.79 813.50 16.01 o -4 10 1 115.83 112.65 4.62 o -3 10 1 68.65 70.76 4.11 o -2 10 1 58.29 58.93 2.58 o -1 10 1 269.58 253.41 5.95 o 0 10 1 184.80 190.73 4.40 o 1 10 1 66.36 74.90 2.80 o 2 10 1 10.30 15.13 3.00 o 3 10 1 16.04 19.90 2.47 o -12 11 1 93.96 86.83 3.18 o -11 11 1 65.61 77.24 2.38 o -10 11 1 105.29 120.20 3.74 o -9 11 1 182.12 186.06 4.09 o -8 11 1 55.95 41.52 2.22 o -7 11 1 806.11 783.71 12.65 o -6 11 1 294.25 305.59 11.87 o -5 11 1 136.68 116.83 6.40 o -4 11 1 177.63 173.70 4.72 o -3 11 1 489.73 489.31 12.30 o -2 11 1 149.09 157.22 3.79 o -1 11 1 65.52 73.28 2.54 o 0 11 1 9.15 12.48 1.29 o 1 11 1 27.99 35.13 1.81 o -11 12 1 94.93 92.94 2.75 o -10 12 1 1.96 4.30 1.42 o -9 12 1 71.62 83.92 7.95 o -8 12 1 0.01 1.60 1.31 o -7 12 1 14.62 15.71 3.08 o -6 12 1 63.48 55.15 4.61 o -5 12 1 226.88 227.44 7.03 o -4 12 1 76.14 79.10 3.48 o -3 12 1 134.51 126.57 4.42 o -2 12 1 10.17 13.34 1.35 o -1 12 1 28.11 35.25 1.91 o -10 13 1 23.26 22.31 1.90 o -9 13 1 159.33 150.77 5.30 o -8 13 1 23.04 24.52 1.83 o -7 13 1 19.78 23.25 3.95 o -6 13 1 41.72 38.42 4.56 o -5 13 1 55.34 48.69 2.34 o -4 13 1 38.59 33.06 2.35 o -3 13 1 15.55 20.73 1.99 o -1 1 2 3195.09 3220.02 142.43 o 0 1 2 643.28 818.76 32.70 o 1 1 2 23310.73 22723.17 896.82 o -3 2 2 676.09 622.23 18.72 o -2 2 2 9575.82 10254.88 277.40 o 0 2 2 17362.71 17763.82 675.64 o 1 2 2 1445.20 1544.60 32.54 o 2 2 2 1994.09 2078.75 54.79 o -5 3 2 3469.97 3743.59 84.09 o -4 3 2 4376.63 4455.95 99.54 o -3 3 2 15048.27 16426.48 444.30 o -2 3 2 675.36 625.74 18.21 o -1 3 2 1442.99 1603.00 69.55 o 0 3 2 7372.10 7475.53 201.34 o 1 3 2 542.12 538.83 12.95 o 2 3 2 1537.45 1725.54 39.46 o -7 4 2 1588.03 1551.37 34.25 o -6 4 2 515.00 529.89 13.28 o -5 4 2 978.67 842.82 32.69 o -4 4 2 2901.00 2767.09 75.57 o -3 4 2 4352.14 4419.67 161.91 o -1 4 2 537.81 542.89 15.42 o 0 4 2 783.33 966.23 27.32 o 1 4 2 680.31 757.14 71.02 o 2 4 2 64.25 106.19 6.78 o 3 4 2 196.70 170.19 11.89 o 4 4 2 182.51 177.79 6.74 o -9 5 2 197.60 173.40 11.53 o -8 5 2 12.52 9.28 1.49 o -7 5 2 336.73 292.69 7.25 o -6 5 2 261.98 234.39 6.25 o -5 5 2 56.20 74.15 5.16 o -4 5 2 967.44 903.82 33.33 o -1 5 2 675.40 753.39 28.13 o 0 5 2 308.69 335.06 14.92 o 1 5 2 13.24 14.80 1.41 o 2 5 2 769.12 802.85 16.17 o 3 5 2 199.72 191.77 7.78 o 4 5 2 40.37 37.55 2.74 o 5 5 2 73.95 70.90 3.48 o -11 6 2 122.42 105.33 2.74 o -10 6 2 9.07 14.89 1.68 o -9 6 2 182.82 167.94 7.13 o -8 6 2 439.60 442.50 12.02 o -7 6 2 273.94 261.12 18.70 o -6 6 2 13.22 15.06 2.90 o -5 6 2 262.39 234.35 6.99 o -4 6 2 510.32 523.07 16.28 o -3 6 2 1787.59 1740.87 46.67 o -2 6 2 64.26 108.75 6.64 o -1 6 2 13.35 13.56 2.00 o 0 6 2 650.09 691.00 12.81 o 1 6 2 93.39 68.03 5.03 o 2 6 2 306.13 285.68 10.11 o 3 6 2 223.91 223.45 8.91 o 4 6 2 1676.00 1505.66 21.69 o 5 6 2 439.82 420.71 6.52 o 6 6 2 176.26 180.92 4.40 o -13 7 2 78.51 80.85 2.76 o -12 7 2 103.80 104.65 3.25 o -11 7 2 115.81 108.96 3.49 o -10 7 2 208.61 208.47 6.38 o -9 7 2 516.21 503.05 10.29 o -8 7 2 262.54 280.74 11.91 o -7 7 2 68.70 71.61 3.95 o -6 7 2 274.87 286.65 11.45 o -5 7 2 333.75 296.49 11.35 o -4 7 2 1592.11 1653.94 45.05 o -3 7 2 195.67 164.25 11.38 o -2 7 2 766.43 793.65 19.17 o -1 7 2 90.60 75.91 5.51 o 0 7 2 265.41 218.83 7.24 o 1 7 2 579.22 632.59 48.37 o 2 7 2 743.54 689.81 32.47 o 3 7 2 211.26 213.65 5.18 o 4 7 2 52.89 40.49 2.30 o 5 7 2 52.58 54.31 2.73 o 6 7 2 3.49 3.58 1.23 o -13 8 2 82.68 88.89 3.21 o -12 8 2 33.84 30.25 2.52 o -11 8 2 19.29 19.77 2.05 o -10 8 2 96.03 96.26 3.95 o -9 8 2 199.71 211.21 9.97 o -8 8 2 262.73 261.78 9.11 o -7 8 2 263.52 278.69 11.94 o -6 8 2 434.23 438.37 15.76 o -5 8 2 11.99 10.74 3.93 o -4 8 2 183.71 176.26 8.47 o -3 8 2 199.81 186.76 8.93 o -2 8 2 309.23 293.29 11.76 o -1 8 2 576.04 614.76 20.22 o 0 8 2 305.68 322.34 18.32 o 1 8 2 673.18 654.10 12.78 o 2 8 2 44.49 47.18 2.88 o 3 8 2 238.10 233.68 7.44 o 4 8 2 10.40 13.40 2.16 o 5 8 2 2.20 2.04 1.33 o -13 9 2 79.80 81.23 2.93 o -12 9 2 221.60 212.20 17.52 o -11 9 2 109.10 131.98 9.41 o -10 9 2 236.92 229.30 5.18 o -9 9 2 151.71 153.22 3.88 o -8 9 2 201.01 211.33 5.01 o -7 9 2 515.52 508.44 12.26 o -6 9 2 179.54 166.50 5.79 o -5 9 2 192.48 186.43 8.07 o -4 9 2 41.80 36.60 3.44 o -3 9 2 226.26 224.23 22.16 o -2 9 2 737.81 760.93 48.12 o -1 9 2 666.61 636.36 10.12 o 0 9 2 4.99 6.76 1.59 o 1 9 2 147.76 148.80 8.07 o 2 9 2 83.84 83.17 6.42 o 3 9 2 14.81 24.08 5.09 o 4 9 2 92.12 102.57 4.32 o -13 10 2 12.78 15.41 3.01 o -12 10 2 73.61 85.90 4.89 o -11 10 2 2.27 3.03 1.21 o -10 10 2 71.79 65.58 2.34 o -9 10 2 236.70 230.52 4.50 o -8 10 2 96.68 100.30 3.12 o -7 10 2 205.43 206.57 6.08 o -6 10 2 8.90 12.98 1.85 o -5 10 2 74.60 72.64 4.87 o -4 10 2 1676.02 1480.16 21.62 o -3 10 2 211.96 208.72 4.71 o -2 10 2 43.71 40.98 2.22 o -1 10 2 147.63 137.24 5.07 o 0 10 2 237.59 299.15 5.85 o 1 10 2 11.08 17.36 1.67 o 2 10 2 15.85 14.51 2.15 o 3 10 2 15.60 13.88 2.23 o -12 11 2 6.29 9.77 1.22 o -11 11 2 6.26 11.46 1.33 o -10 11 2 2.30 3.35 1.11 o -9 11 2 110.36 124.02 3.71 o -8 11 2 18.99 18.26 1.65 o -7 11 2 117.17 118.48 3.45 o -6 11 2 121.39 103.26 5.05 o -5 11 2 442.03 416.19 8.46 o -4 11 2 53.13 43.25 3.67 o -3 11 2 238.88 240.44 7.24 o -2 11 2 83.28 83.28 5.41 o -1 11 2 11.07 14.81 1.48 o 0 11 2 89.67 95.05 2.65 o 1 11 2 148.82 164.02 3.99 o -11 12 2 6.15 7.17 1.08 o -10 12 2 73.26 86.94 2.49 o -9 12 2 219.71 213.60 6.49 o -8 12 2 32.46 28.05 2.14 o -7 12 2 103.46 101.66 6.72 o -6 12 2 176.90 183.20 8.97 o -5 12 2 52.07 56.27 3.54 o -4 12 2 10.45 13.02 1.69 o -3 12 2 14.69 23.38 3.45 o -2 12 2 15.74 12.22 1.30 o -1 12 2 148.56 157.52 4.08 o -10 13 2 12.78 15.88 2.88 o -9 13 2 79.26 81.41 3.04 o -8 13 2 81.16 83.39 3.50 o -7 13 2 77.70 81.95 6.23 o -5 13 2 2.15 3.70 1.22 o -4 13 2 91.24 104.44 4.08 o -3 13 2 14.91 14.93 1.69 o 0 0 3 7634.91 7275.60 288.30 o -1 1 3 12168.27 12988.95 497.07 o 0 1 3 15991.01 17758.63 700.97 o 1 1 3 7589.77 7704.35 269.76 o -3 2 3 6736.49 6933.14 153.06 o -2 2 3 838.10 757.36 21.11 o -1 2 3 7604.23 7892.84 187.28 o 0 2 3 90.96 172.37 5.41 o 1 2 3 4201.08 4147.77 94.49 o 2 2 3 333.42 404.24 16.64 o -5 3 3 1110.35 1244.94 61.33 o -4 3 3 1907.13 1978.92 45.14 o -3 3 3 261.67 267.71 8.43 o -2 3 3 6741.49 6805.47 153.50 o -1 3 3 4193.24 4135.69 111.58 o 0 3 3 3931.56 3772.93 102.01 o 1 3 3 171.77 140.50 14.16 o 2 3 3 3731.05 4113.03 92.17 o 3 3 3 1088.60 1036.47 40.75 o -7 4 3 614.15 576.66 20.32 o -6 4 3 1785.85 1619.53 36.47 o -5 4 3 75.41 61.07 15.46 o -4 4 3 1012.73 1245.80 34.91 o -3 4 3 1912.30 2065.51 74.54 o -1 4 3 167.71 126.80 14.77 o 0 4 3 4203.34 4460.40 120.78 o 1 4 3 263.09 380.61 26.80 o 2 4 3 299.79 301.82 10.21 o 3 4 3 249.45 217.79 5.79 o 4 4 3 357.94 376.79 7.97 o -9 5 3 146.96 146.11 4.51 o -8 5 3 807.31 759.46 14.27 o -7 5 3 469.69 436.52 12.57 o -6 5 3 166.08 171.12 5.73 o -5 5 3 1070.18 1176.20 26.26 o -4 5 3 77.20 50.64 3.73 o -1 5 3 262.32 377.92 14.86 o 0 5 3 11426.88 12235.58 449.26 o 1 5 3 153.10 167.15 4.91 o 2 5 3 477.72 415.53 9.41 o 3 5 3 807.05 783.71 17.13 o 4 5 3 681.85 668.37 14.05 o 5 5 3 75.24 77.64 2.78 o -11 6 3 41.24 37.31 1.85 o -10 6 3 747.21 743.75 13.88 o -9 6 3 642.55 580.30 20.19 o -8 6 3 2732.01 2722.65 58.07 o -7 6 3 15.94 19.90 1.85 o -6 6 3 243.49 267.06 8.06 o -5 6 3 165.62 169.37 5.58 o -4 6 3 1772.93 1595.41 42.62 o -3 6 3 1094.95 1035.27 23.64 o -2 6 3 302.94 304.57 11.33 o -1 6 3 150.42 155.11 5.02 o 0 6 3 2955.45 2920.75 53.60 o 1 6 3 25.26 33.69 3.18 o 2 6 3 854.87 851.26 48.81 o 3 6 3 881.26 798.81 23.10 o 4 6 3 36.87 58.20 4.98 o 5 6 3 0.96 1.09 1.15 o 6 6 3 68.91 72.18 2.97 o -13 7 3 97.43 105.12 3.44 o -12 7 3 283.45 285.53 5.71 o -11 7 3 57.30 62.15 3.31 o -10 7 3 821.66 798.04 12.77 o -9 7 3 102.46 89.91 7.19 o -8 7 3 778.38 826.87 25.79 o -7 7 3 10.99 12.71 2.02 o -6 7 3 15.71 20.52 3.50 o -5 7 3 470.57 431.37 14.60 o -4 7 3 620.39 580.77 18.02 o -3 7 3 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