#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/98/2229887.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229887_Fobs loop_ _publ_author_name 'Rizzoli, Corrado' 'Karami, Kazem' 'Borzooie, Farzaneh' _publ_section_title ; [1,2-Bis(diphenylphosphanyl)ethane-\k^2^P,P']{2-[(4-nitrobenzoylmethyl)diphenylphosphanyl]phenyl-\k^2^C,C'}palladium(II) trifluoromethanesulfonate--dichloromethane--n-hexane (1/1/0.5) ; _journal_coeditor_code ZJ2004 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m416 _journal_page_last m417 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.668 _cell_angle_gamma 90.000 _cell_length_a 12.4063 _cell_length_b 14.2445 _cell_length_c 31.3633 _exptl_crystal_F_000 2468.00 _reflns_d_resolution_high 0.8192 _[local]_cod_data_source_file zj2004Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' KK5 (KB5) - P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 355.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 206.94 350.67 21.17 o 4 0 0 1049.67 908.30 32.22 o 6 0 0 9451.64 9200.01 217.98 o 8 0 0 5171.20 5099.11 122.79 o 10 0 0 1328.71 1260.50 58.81 o 12 0 0 5059.13 5078.35 166.95 o 14 0 0 464.90 419.44 61.17 o 1 1 0 913.23 793.15 18.83 o 2 1 0 4127.39 4629.30 75.82 o 3 1 0 5499.94 5900.12 95.04 o 4 1 0 5201.33 5524.77 92.05 o 5 1 0 14674.02 15021.50 234.27 o 6 1 0 141.84 115.88 11.37 o 7 1 0 223.15 229.63 26.99 o 8 1 0 29.68 10.24 7.38 o 9 1 0 987.06 942.74 34.17 o 10 1 0 96.49 59.45 15.76 o 11 1 0 1713.63 1600.90 50.77 o 12 1 0 43.51 38.62 20.97 o 13 1 0 1.86 0.00 17.67 o 14 1 0 153.58 174.56 36.91 o 15 1 0 112.33 107.32 44.15 o 0 2 0 5652.68 4949.35 117.41 o 1 2 0 54490.59 61604.46 1081.51 o 2 2 0 3269.76 3676.36 62.42 o 3 2 0 16.44 67.41 7.19 o 4 2 0 184.67 174.24 10.41 o 5 2 0 20058.17 20727.82 318.72 o 6 2 0 7039.18 6890.01 117.49 o 7 2 0 6427.25 6200.36 109.61 o 8 2 0 412.97 398.91 21.88 o 9 2 0 724.61 693.34 29.73 o 10 2 0 669.95 648.81 31.05 o 11 2 0 6583.76 6485.95 125.18 o 12 2 0 425.89 408.01 33.45 o 13 2 0 1080.88 1219.92 66.36 o 14 2 0 42.22 22.33 24.16 o 15 2 0 121.29 130.83 60.43 o 1 3 0 70674.75 72859.29 1080.16 o 2 3 0 18814.48 17922.91 313.78 o 3 3 0 8098.20 6908.99 113.64 o 4 3 0 4409.33 4711.02 83.15 o 5 3 0 1530.76 1622.60 35.50 o 6 3 0 2723.86 2760.35 56.58 o 7 3 0 571.41 536.32 22.65 o 8 3 0 283.52 311.54 19.82 o 9 3 0 1273.09 1277.09 39.60 o 10 3 0 239.17 259.43 22.53 o 11 3 0 91.17 64.60 18.38 o 12 3 0 515.31 488.32 39.96 o 13 3 0 13.04 0.00 24.42 o 14 3 0 22.24 0.00 30.47 o 0 4 0 91490.48 98627.66 2063.64 o 1 4 0 850.87 945.45 24.22 o 2 4 0 5006.38 5564.41 98.15 o 3 4 0 2826.19 2666.64 52.57 o 4 4 0 18141.31 15797.75 243.97 o 5 4 0 807.56 813.39 24.73 o 6 4 0 2393.76 2246.54 48.96 o 7 4 0 1213.91 1230.53 34.97 o 8 4 0 451.50 467.99 23.69 o 9 4 0 54.12 44.78 12.26 o 10 4 0 1667.51 1568.06 51.19 o 11 4 0 3028.03 2861.18 84.53 o 12 4 0 2200.52 2228.90 85.84 o 13 4 0 857.58 842.75 59.67 o 14 4 0 303.20 293.63 56.87 o 1 5 0 4054.39 4230.53 80.64 o 2 5 0 254.99 294.54 13.76 o 3 5 0 3885.03 3455.60 66.27 o 4 5 0 11424.27 12753.97 221.33 o 5 5 0 1.93 3.18 9.71 o 6 5 0 1.13 0.00 8.92 o 7 5 0 1807.58 1971.06 47.89 o 8 5 0 929.45 985.88 33.84 o 9 5 0 86.08 74.54 18.70 o 10 5 0 156.95 151.22 23.20 o 11 5 0 128.23 142.13 34.83 o 12 5 0 350.36 357.40 42.26 o 13 5 0 12.68 0.00 22.51 o 14 5 0 207.50 250.37 47.29 o 0 6 0 30840.77 30699.37 657.95 o 1 6 0 6139.85 6515.34 109.71 o 2 6 0 1632.32 1695.50 36.72 o 3 6 0 2376.43 2095.21 46.28 o 4 6 0 2118.68 2171.30 50.81 o 5 6 0 1973.29 1815.50 46.51 o 6 6 0 11101.11 11334.87 199.44 o 7 6 0 856.85 922.15 35.44 o 8 6 0 56.58 25.92 15.72 o 9 6 0 74.68 61.75 19.27 o 10 6 0 676.70 662.14 41.04 o 11 6 0 1785.25 1810.82 91.92 o 12 6 0 2738.01 2732.15 100.24 o 13 6 0 461.87 510.49 52.01 o 14 6 0 676.48 594.78 68.10 o 1 7 0 4109.68 4463.16 147.35 o 2 7 0 337.83 388.93 20.94 o 3 7 0 255.29 236.85 16.70 o 4 7 0 324.90 282.20 18.53 o 5 7 0 1850.34 1882.03 57.97 o 6 7 0 21.49 41.32 13.73 o 7 7 0 2185.05 2163.18 61.57 o 8 7 0 13.37 0.00 16.79 o 9 7 0 324.98 352.07 32.06 o 10 7 0 266.51 232.14 35.00 o 11 7 0 109.25 122.62 36.59 o 12 7 0 15.49 13.01 26.32 o 13 7 0 201.92 199.66 44.46 o 0 8 0 11869.28 12549.61 292.70 o 1 8 0 15532.46 14542.71 232.99 o 2 8 0 250.07 262.85 15.99 o 3 8 0 1290.26 1262.39 37.81 o 4 8 0 143.65 164.50 16.16 o 5 8 0 4010.81 3681.00 79.85 o 6 8 0 2154.70 2219.30 85.99 o 7 8 0 924.32 879.56 43.29 o 8 8 0 1159.01 1134.48 52.10 o 9 8 0 403.66 436.50 36.96 o 10 8 0 4.10 6.44 17.10 o 11 8 0 3941.14 3745.53 122.78 o 12 8 0 451.01 463.54 51.14 o 13 8 0 943.07 1026.11 70.64 o 1 9 0 209.64 226.05 17.32 o 2 9 0 139.55 141.68 16.66 o 3 9 0 189.25 231.79 17.03 o 4 9 0 625.78 657.33 29.05 o 5 9 0 13.16 0.00 15.85 o 6 9 0 150.42 138.81 24.38 o 7 9 0 1705.19 1777.52 62.81 o 8 9 0 92.46 100.13 25.78 o 9 9 0 49.95 84.52 24.73 o 10 9 0 52.57 51.41 28.69 o 11 9 0 31.00 23.35 26.78 o 12 9 0 4.16 0.00 22.08 o 0 10 0 17605.97 18122.76 411.83 o 1 10 0 77.56 85.14 20.55 o 2 10 0 4162.66 4159.57 83.27 o 3 10 0 16.33 13.39 13.09 o 4 10 0 4277.48 4055.25 101.19 o 5 10 0 47.77 21.06 23.58 o 6 10 0 1180.78 1118.07 51.06 o 7 10 0 85.49 73.15 28.97 o 8 10 0 1066.54 1047.92 55.38 o 9 10 0 8.35 4.59 19.53 o 10 10 0 696.57 693.59 56.82 o 11 10 0 382.34 397.63 51.58 o 12 10 0 1322.05 1231.47 77.55 o 1 11 0 572.84 490.79 27.62 o 2 11 0 301.07 303.19 24.89 o 3 11 0 0.14 17.18 18.51 o 4 11 0 948.57 945.57 46.80 o 5 11 0 30.65 9.23 18.63 o 6 11 0 143.92 159.84 29.27 o 7 11 0 58.95 33.05 22.07 o 8 11 0 266.06 275.88 33.54 o 9 11 0 136.00 127.74 38.41 o 10 11 0 224.13 216.43 43.15 o 11 11 0 3.10 37.85 35.38 o 0 12 0 3.85 0.00 23.90 o 1 12 0 5372.88 4856.86 105.91 o 2 12 0 432.65 479.26 38.05 o 3 12 0 3476.79 3352.25 93.96 o 4 12 0 1.83 0.37 20.34 o 5 12 0 1766.49 1657.62 63.92 o 6 12 0 101.95 116.22 31.31 o 7 12 0 952.23 940.42 53.40 o 8 12 0 16.63 4.46 20.03 o 9 12 0 475.73 561.30 54.61 o 10 12 0 28.21 27.71 30.37 o 1 13 0 105.51 96.12 27.66 o 2 13 0 0.55 0.00 21.01 o 3 13 0 381.31 400.97 38.19 o 4 13 0 318.73 319.54 36.47 o 5 13 0 344.14 380.32 39.10 o 6 13 0 47.27 38.56 31.77 o 7 13 0 143.34 166.46 36.20 o 8 13 0 36.58 28.35 25.84 o 9 13 0 211.23 204.22 53.83 o 10 13 0 35.91 1.39 40.21 o 0 14 0 4603.43 5139.71 236.34 o 1 14 0 647.52 625.46 49.38 o 2 14 0 1967.72 1813.94 69.54 o 3 14 0 267.41 274.15 34.18 o 4 14 0 1568.73 1615.05 67.86 o 5 14 0 261.51 254.03 38.04 o 6 14 0 1405.67 1381.50 67.31 o 7 14 0 173.99 202.98 38.04 o 8 14 0 79.40 82.62 41.65 o 1 15 0 21.27 14.88 30.02 o 2 15 0 84.50 54.16 44.77 o 3 15 0 60.17 42.77 29.31 o 4 15 0 696.01 742.70 51.54 o 5 15 0 109.50 110.37 30.74 o 6 15 0 107.34 84.65 33.79 o 7 15 0 40.71 26.46 28.96 o 0 16 0 81.30 112.28 72.14 o 1 16 0 1543.27 1707.12 97.36 o 2 16 0 614.71 603.01 66.28 o 3 16 0 456.22 445.68 58.33 o 4 16 0 412.51 389.07 46.90 o 5 16 0 685.88 709.35 56.64 o 1 17 0 10.19 6.61 30.49 o 2 17 0 134.55 79.56 48.33 o 3 17 0 86.06 87.14 97.19 o -15 0 1 76.55 66.15 96.78 o -13 0 1 210.35 229.69 49.33 o -11 0 1 2485.30 2641.75 94.23 o -9 0 1 63.76 37.33 43.20 o -7 0 1 5.83 115.28 17.81 o -5 0 1 4171.35 4810.39 119.34 o -3 0 1 38740.61 34201.40 722.42 o -1 0 1 64974.79 73498.70 2240.28 o 1 0 1 63455.76 69466.53 1456.29 o 3 0 1 3588.59 4093.41 98.99 o 5 0 1 17412.30 15625.48 343.55 o 7 0 1 10889.32 12252.38 288.69 o 9 0 1 1092.25 1101.22 51.81 o 11 0 1 6307.98 5879.70 164.31 o 13 0 1 310.89 347.67 57.91 o 15 0 1 393.32 392.64 81.43 o -15 1 1 510.84 473.91 53.66 o -14 1 1 330.58 309.85 45.27 o -13 1 1 783.97 791.44 49.96 o -12 1 1 1211.73 1166.40 50.13 o -11 1 1 6287.85 6134.93 119.99 o -10 1 1 2992.07 2980.79 68.77 o -9 1 1 1089.61 1165.25 37.69 o -8 1 1 588.18 600.80 25.46 o -7 1 1 8476.47 8010.83 135.94 o -6 1 1 4792.60 5045.06 89.59 o -5 1 1 11820.18 10936.89 174.01 o -4 1 1 18356.49 20046.53 307.55 o -3 1 1 7543.71 7422.37 198.45 o -2 1 1 36160.22 40978.14 647.91 o -1 1 1 30402.03 35045.76 573.39 o 0 1 1 6487.89 7813.79 151.44 o 1 1 1 38469.25 44420.18 674.86 o 2 1 1 39156.77 41252.63 613.73 o 3 1 1 812.89 966.77 22.45 o 4 1 1 1047.07 1070.26 26.00 o 5 1 1 993.98 943.97 26.53 o 6 1 1 709.63 848.39 38.28 o 7 1 1 1664.43 1699.95 42.03 o 8 1 1 7.56 0.00 11.47 o 9 1 1 273.37 278.42 22.64 o 10 1 1 56.50 63.53 15.38 o 11 1 1 743.25 778.68 36.66 o 12 1 1 48.29 48.55 21.06 o 13 1 1 454.55 453.80 40.57 o 14 1 1 10.30 0.00 27.92 o 15 1 1 5.57 0.00 29.49 o -15 2 1 1.71 0.00 30.64 o -14 2 1 104.71 83.82 33.49 o -13 2 1 146.43 149.95 40.56 o -12 2 1 1142.32 1229.15 50.83 o -11 2 1 275.70 322.86 30.37 o -10 2 1 659.81 639.65 29.38 o -9 2 1 912.73 989.31 34.61 o -8 2 1 548.59 546.61 24.71 o -7 2 1 6206.34 6480.98 113.57 o -6 2 1 13986.98 14805.82 235.59 o -5 2 1 14.45 38.55 11.11 o -4 2 1 6.33 17.90 6.33 o -3 2 1 3020.47 3490.50 65.67 o -2 2 1 29936.53 28050.88 419.54 o -1 2 1 13.99 56.20 4.96 o 0 2 1 58085.63 53132.81 931.31 o 1 2 1 3351.35 3728.52 77.11 o 2 2 1 60186.53 52499.94 775.55 o 3 2 1 156.63 164.14 9.29 o 4 2 1 19745.28 17186.01 261.91 o 5 2 1 7457.49 7431.40 132.14 o 6 2 1 20600.99 18670.77 291.08 o 7 2 1 86.34 80.70 12.52 o 8 2 1 6656.66 6779.39 121.28 o 9 2 1 34.25 47.38 14.90 o 10 2 1 847.92 904.59 35.98 o 11 2 1 841.76 849.45 37.59 o 12 2 1 1706.91 1657.15 59.04 o 13 2 1 19.77 16.71 22.01 o 14 2 1 306.48 303.88 38.62 o 15 2 1 172.03 201.99 44.86 o -14 3 1 749.23 771.74 70.13 o -13 3 1 341.04 323.32 42.09 o -12 3 1 1936.60 1884.42 64.91 o -11 3 1 859.55 850.27 39.38 o -10 3 1 4145.77 4268.79 89.29 o -9 3 1 408.33 435.82 24.25 o -8 3 1 23.19 18.64 8.27 o -7 3 1 527.64 541.58 23.59 o -6 3 1 10032.79 10495.49 178.67 o -5 3 1 12149.56 11246.78 179.01 o -4 3 1 3088.21 3414.98 69.03 o -3 3 1 8566.33 7816.01 123.61 o -2 3 1 5156.40 5653.14 113.52 o -1 3 1 28.01 37.82 6.62 o 0 3 1 51589.65 55910.43 830.37 o 1 3 1 842.37 796.81 18.55 o 2 3 1 2645.96 2667.29 48.96 o 3 3 1 1173.28 1066.31 24.55 o 4 3 1 392.36 427.78 16.94 o 5 3 1 569.93 536.93 19.87 o 6 3 1 11043.32 10409.34 162.98 o 7 3 1 2.90 11.72 10.16 o 8 3 1 1103.72 1242.35 38.07 o 9 3 1 1508.12 1449.00 40.77 o 10 3 1 88.34 131.00 29.93 o 11 3 1 18.20 0.00 16.98 o 12 3 1 1203.42 1150.80 54.52 o 13 3 1 164.91 170.45 45.23 o 14 3 1 24.65 20.90 31.86 o -14 4 1 171.10 177.39 48.53 o -13 4 1 837.21 827.12 69.72 o -12 4 1 1146.84 1178.21 56.15 o -11 4 1 767.43 711.83 43.92 o -10 4 1 1266.22 1229.26 46.41 o -9 4 1 40.12 56.00 15.40 o -8 4 1 1285.90 1217.75 36.93 o -7 4 1 1931.45 1975.10 46.79 o -6 4 1 645.74 648.56 23.88 o -5 4 1 1107.89 1143.40 30.01 o -4 4 1 916.32 909.07 27.50 o -3 4 1 10164.77 9191.39 156.35 o -2 4 1 5556.14 5239.38 88.19 o -1 4 1 1162.60 1040.21 24.05 o 0 4 1 7506.23 7943.19 126.54 o 1 4 1 18600.35 19292.36 293.62 o 2 4 1 1909.91 1931.05 38.72 o 3 4 1 18893.29 20065.54 354.76 o 4 4 1 4283.84 3658.83 65.02 o 5 4 1 17260.89 17965.12 279.50 o 6 4 1 3266.52 3087.65 61.76 o 7 4 1 3298.19 3587.51 72.65 o 8 4 1 4.76 1.59 8.57 o 9 4 1 94.81 107.19 15.93 o 10 4 1 1977.07 1894.35 56.91 o 11 4 1 4518.38 4424.47 101.80 o 12 4 1 558.31 599.29 49.05 o 13 4 1 316.16 329.49 40.79 o 14 4 1 237.82 247.79 48.20 o -14 5 1 61.20 47.64 35.94 o -13 5 1 1158.94 1094.35 67.05 o -12 5 1 1.60 0.00 24.41 o -11 5 1 2617.26 2780.34 129.18 o -10 5 1 357.64 325.79 28.04 o -9 5 1 580.84 646.67 33.66 o -8 5 1 897.38 855.19 31.30 o -7 5 1 213.32 195.95 16.89 o -6 5 1 2332.82 2571.60 54.74 o -5 5 1 9776.81 9253.55 163.00 o -4 5 1 34.36 64.17 10.26 o -3 5 1 2375.04 2623.78 55.35 o -2 5 1 71.37 100.02 8.50 o -1 5 1 40703.46 39692.71 595.84 o 0 5 1 3064.25 2693.50 50.72 o 1 5 1 3246.10 3102.29 55.01 o 2 5 1 0.05 16.23 4.83 o 3 5 1 3153.01 2981.01 60.44 o 4 5 1 3468.70 3373.21 68.66 o 5 5 1 5359.81 5478.69 96.76 o 6 5 1 560.78 572.38 23.00 o 7 5 1 7787.92 8005.97 138.55 o 8 5 1 304.75 333.72 21.07 o 9 5 1 49.60 3.19 15.40 o 10 5 1 12.50 0.00 14.82 o 11 5 1 340.17 342.11 41.14 o 12 5 1 85.59 75.36 31.45 o 13 5 1 631.93 637.65 55.48 o 14 5 1 0.49 0.00 28.04 o -14 6 1 2.32 0.00 28.90 o -13 6 1 247.25 270.47 41.39 o -12 6 1 584.74 637.97 53.62 o -11 6 1 403.04 475.97 46.61 o -10 6 1 2115.71 2129.94 105.35 o -9 6 1 781.61 797.36 38.32 o -8 6 1 287.14 282.79 23.10 o -7 6 1 4833.47 4616.22 95.22 o -6 6 1 68.05 99.41 17.77 o -5 6 1 3001.56 3092.14 67.79 o -4 6 1 711.61 755.77 27.89 o -3 6 1 4273.16 4182.61 81.80 o -2 6 1 393.91 451.58 18.30 o -1 6 1 4739.63 4655.06 82.22 o 0 6 1 8387.76 9174.65 149.34 o 1 6 1 1745.77 1770.65 42.68 o 2 6 1 8349.10 9168.19 156.72 o 3 6 1 103.48 60.50 12.31 o 4 6 1 1952.75 1977.99 45.41 o 5 6 1 5407.83 5070.40 98.66 o 6 6 1 4914.64 5308.97 104.92 o 7 6 1 554.97 637.37 25.75 o 8 6 1 21.25 28.76 17.17 o 9 6 1 2022.18 1902.03 63.88 o 10 6 1 295.89 274.90 30.92 o 11 6 1 1842.58 1916.26 83.10 o 12 6 1 751.61 757.61 57.65 o 13 6 1 1351.29 1268.05 72.68 o 14 6 1 187.05 126.10 38.73 o -13 7 1 24.77 7.36 35.58 o -12 7 1 1477.33 1486.85 77.19 o -11 7 1 226.03 251.99 39.19 o -10 7 1 1702.46 1649.17 73.24 o -9 7 1 22.48 12.00 17.78 o -8 7 1 180.73 163.33 24.69 o -7 7 1 439.98 538.42 30.75 o -6 7 1 1124.07 1111.07 38.80 o -5 7 1 303.22 342.78 22.54 o -4 7 1 5304.32 4948.50 97.50 o -3 7 1 2282.64 2291.85 52.28 o -2 7 1 4616.05 4965.24 89.04 o -1 7 1 2033.82 2025.88 44.59 o 0 7 1 11687.64 11044.80 178.92 o 1 7 1 3232.29 3473.21 67.86 o 2 7 1 10320.88 10787.82 182.37 o 3 7 1 832.60 830.74 28.58 o 4 7 1 664.41 626.05 25.50 o 5 7 1 104.24 148.49 21.74 o 6 7 1 2085.03 2063.71 53.69 o 7 7 1 76.24 64.87 15.87 o 8 7 1 189.38 213.17 26.75 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