#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/99/2229901.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229901_Fobs loop_ _publ_author_name 'Hyun, Min Young' 'Kim, Pan-Gi' 'Kim, Cheal' 'Kim, Youngmee' _publ_section_title ; catena-Poly[[tetraaqua[trans-1,2-bis(4-pyridyl)ethene-\k^2^N:N']nickel(II)] dinitrate] ; _journal_coeditor_code ZS2096 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m390 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.307 _cell_angle_gamma 90.000 _cell_length_a 7.4145 _cell_length_b 11.4256 _cell_length_c 10.9498 _exptl_crystal_F_000 452.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file zs2096Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yk864P21n in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 133.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4825.34 5407.50 85.53 o 4 0 0 446.77 338.14 13.16 o 6 0 0 364.46 380.84 38.56 o 8 0 0 226.39 248.23 45.49 o 1 1 0 3788.29 3955.36 80.91 o 2 1 0 7.19 5.21 2.21 o 3 1 0 225.14 277.08 6.90 o 4 1 0 868.33 945.46 13.81 o 5 1 0 73.13 72.31 7.51 o 6 1 0 335.76 308.13 19.70 o 7 1 0 86.80 85.13 20.17 o 8 1 0 9.19 1.61 17.88 o 9 1 0 154.15 182.39 31.72 o 0 2 0 108.45 77.39 6.59 o 1 2 0 374.27 401.69 6.42 o 2 2 0 2111.45 2269.68 26.78 o 3 2 0 134.14 115.52 5.93 o 4 2 0 2700.64 2745.82 36.27 o 5 2 0 8.16 3.51 6.47 o 6 2 0 298.73 324.34 17.19 o 7 2 0 50.93 44.64 17.75 o 8 2 0 296.99 319.27 34.30 o 1 3 0 9082.85 9444.86 269.90 o 2 3 0 90.76 86.44 3.87 o 3 3 0 1240.45 1195.34 24.55 o 4 3 0 232.26 260.77 12.89 o 5 3 0 1022.92 972.10 25.67 o 6 3 0 150.43 155.84 13.92 o 7 3 0 74.28 65.62 15.16 o 8 3 0 0.01 -1.32 17.63 o 0 4 0 5443.42 5147.14 326.70 o 1 4 0 3128.82 3169.61 92.55 o 2 4 0 6902.15 7855.67 136.90 o 3 4 0 224.97 226.00 13.59 o 4 4 0 299.26 300.47 16.21 o 5 4 0 43.92 27.92 8.55 o 6 4 0 5.46 3.06 8.48 o 7 4 0 30.20 14.17 13.20 o 8 4 0 72.16 69.78 23.58 o 1 5 0 4028.15 4115.80 142.61 o 2 5 0 12.37 23.14 4.28 o 3 5 0 2386.41 2281.73 55.31 o 4 5 0 9.48 16.94 8.82 o 5 5 0 34.66 29.16 9.10 o 6 5 0 236.61 267.75 18.05 o 7 5 0 476.85 462.18 24.05 o 8 5 0 0.67 -0.03 20.20 o 0 6 0 1791.91 1623.45 101.77 o 1 6 0 251.19 288.08 13.00 o 2 6 0 1094.94 834.41 17.33 o 3 6 0 296.30 335.81 17.76 o 4 6 0 90.74 91.70 12.66 o 5 6 0 147.98 136.89 13.44 o 6 6 0 565.24 516.42 23.61 o 7 6 0 82.61 81.44 15.70 o 8 6 0 142.66 126.05 23.20 o 1 7 0 3399.13 3197.52 105.06 o 2 7 0 280.63 261.74 12.32 o 3 7 0 995.09 890.53 56.45 o 4 7 0 224.18 228.63 18.72 o 5 7 0 625.24 519.03 26.17 o 6 7 0 171.33 155.50 16.76 o 7 7 0 191.77 202.27 20.21 o 0 8 0 1030.66 924.25 62.23 o 1 8 0 193.21 185.99 11.97 o 2 8 0 1317.90 1234.60 41.49 o 3 8 0 0.12 6.57 11.80 o 4 8 0 10.83 18.75 13.32 o 5 8 0 8.81 10.60 12.66 o 6 8 0 86.09 79.26 15.59 o 7 8 0 20.31 19.56 15.00 o 1 9 0 1804.81 1615.30 56.45 o 2 9 0 114.76 109.04 17.17 o 3 9 0 886.00 813.38 65.43 o 4 9 0 35.87 24.65 15.73 o 5 9 0 526.56 432.79 43.63 o 6 9 0 2.50 -4.73 19.46 o 0 10 0 746.06 644.56 31.60 o 1 10 0 423.54 438.84 23.02 o 2 10 0 166.81 152.30 20.95 o 3 10 0 459.32 401.00 31.34 o 4 10 0 348.38 296.12 29.68 o 5 10 0 5.07 2.61 19.12 o 6 10 0 112.80 95.44 25.85 o 1 11 0 720.03 647.22 62.28 o 2 11 0 346.38 325.83 30.79 o 3 11 0 334.97 286.96 30.34 o 4 11 0 11.08 7.75 18.81 o 5 11 0 22.98 26.10 22.59 o 0 12 0 991.64 1081.20 66.26 o 1 12 0 33.16 27.84 17.91 o 2 12 0 606.12 483.60 36.88 o 3 12 0 1.93 0.45 18.91 o 4 12 0 429.33 326.29 36.00 o 1 13 0 284.67 274.30 49.52 o 2 13 0 1.17 0.63 19.69 o 3 13 0 78.67 55.64 23.60 o 1 14 0 0.53 4.78 31.02 o -9 0 1 12.92 20.01 28.91 o -7 0 1 225.39 174.64 34.59 o -5 0 1 421.83 359.80 15.83 o -3 0 1 4938.31 5014.11 148.75 o -1 0 1 1607.66 1241.15 443.26 o 1 0 1 3321.21 3486.50 37.20 o 3 0 1 194.48 265.87 10.49 o 5 0 1 464.55 432.21 24.90 o 7 0 1 1566.69 1342.55 73.04 o -9 1 1 0.00 -1.17 19.02 o -8 1 1 434.74 428.86 36.56 o -7 1 1 3.87 2.68 13.84 o -6 1 1 500.40 552.90 24.27 o -5 1 1 294.99 308.89 12.25 o -4 1 1 4833.56 4759.45 63.73 o -3 1 1 831.36 770.46 84.38 o -2 1 1 3762.44 3809.22 425.99 o -1 1 1 34.75 32.32 5.93 o 0 1 1 3998.28 3385.29 858.66 o 1 1 1 7931.90 8179.26 208.48 o 2 1 1 7.29 8.25 2.14 o 3 1 1 1026.49 976.62 13.01 o 4 1 1 1728.58 1623.87 24.69 o 5 1 1 6.37 5.31 6.38 o 6 1 1 306.15 306.11 26.11 o 7 1 1 9.29 10.75 15.46 o 8 1 1 291.32 333.15 35.09 o -9 2 1 292.50 239.77 34.00 o -8 2 1 0.29 3.93 17.95 o -7 2 1 542.64 551.60 35.41 o -6 2 1 2.05 -0.02 7.90 o -5 2 1 1003.65 966.92 23.27 o -4 2 1 103.31 102.04 7.29 o -3 2 1 1202.97 1008.39 176.86 o -2 2 1 1670.19 1953.47 25.78 o -1 2 1 1631.29 1667.16 31.67 o 0 2 1 1460.51 1805.74 43.90 o 1 2 1 497.83 556.51 16.01 o 2 2 1 689.31 582.58 14.53 o 3 2 1 941.72 1081.45 14.32 o 4 2 1 117.12 119.77 6.34 o 5 2 1 861.49 885.31 22.80 o 6 2 1 183.16 194.19 14.49 o 7 2 1 54.41 53.21 18.86 o 8 2 1 0.53 -1.30 17.33 o -8 3 1 78.09 65.09 22.68 o -7 3 1 11.45 21.62 12.92 o -6 3 1 545.19 502.57 20.80 o -5 3 1 850.05 757.96 21.85 o -4 3 1 1705.53 1370.91 244.56 o -3 3 1 295.14 299.81 60.06 o -2 3 1 2102.87 2051.51 35.96 o -1 3 1 227.73 168.70 6.52 o 0 3 1 1856.81 1771.67 50.38 o 1 3 1 240.92 231.28 6.74 o 2 3 1 2240.23 2493.73 64.68 o 3 3 1 1177.09 1093.70 31.00 o 4 3 1 779.83 828.35 23.60 o 5 3 1 40.36 43.54 8.95 o 6 3 1 878.82 813.98 25.40 o 7 3 1 38.80 34.46 17.59 o 8 3 1 355.43 375.79 36.87 o -8 4 1 0.29 -0.22 18.29 o -7 4 1 54.79 41.62 14.67 o -6 4 1 134.12 143.56 13.98 o -5 4 1 2334.25 2455.23 38.91 o -4 4 1 1.60 3.56 5.88 o -3 4 1 5163.16 5114.96 129.19 o -2 4 1 21.36 18.85 3.65 o -1 4 1 3001.30 2923.91 54.80 o 0 4 1 243.62 190.48 7.94 o 1 4 1 147.06 148.40 6.33 o 2 4 1 1085.10 1155.42 29.64 o 3 4 1 533.97 514.12 18.28 o 4 4 1 84.45 102.63 11.51 o 5 4 1 1422.62 1282.75 29.05 o 6 4 1 92.97 82.90 12.20 o 7 4 1 325.62 304.92 24.30 o 8 4 1 0.34 1.89 18.98 o -8 5 1 119.09 108.58 21.30 o -7 5 1 2.67 5.61 11.58 o -6 5 1 1360.20 1287.39 32.76 o -5 5 1 165.78 161.90 13.52 o -4 5 1 565.00 579.55 19.39 o -3 5 1 127.38 129.93 8.88 o -2 5 1 2259.27 2021.71 23.62 o -1 5 1 1819.59 1916.02 34.55 o 0 5 1 1093.28 1047.78 42.87 o 1 5 1 649.11 718.07 14.88 o 2 5 1 90.16 70.04 5.32 o 3 5 1 4.27 10.33 7.08 o 4 5 1 363.76 402.24 19.83 o 5 5 1 121.83 126.96 14.93 o 6 5 1 706.61 626.43 24.46 o 7 5 1 12.05 14.36 12.03 o 8 5 1 74.50 69.36 24.52 o -8 6 1 3.05 3.91 17.16 o -7 6 1 656.37 607.21 27.82 o -6 6 1 116.47 108.04 14.22 o -5 6 1 280.71 251.34 16.50 o -4 6 1 3.74 1.98 7.90 o -3 6 1 301.64 238.77 15.65 o -2 6 1 121.81 141.56 9.29 o -1 6 1 1392.13 1351.94 35.93 o 0 6 1 1203.33 1266.85 52.23 o 1 6 1 1577.23 1674.12 65.35 o 2 6 1 2.19 3.32 4.63 o 3 6 1 1074.65 947.08 48.64 o 4 6 1 126.86 128.64 14.17 o 5 6 1 239.49 233.04 19.31 o 6 6 1 305.50 263.72 19.21 o 7 6 1 718.27 718.71 42.06 o 8 6 1 23.71 30.40 19.01 o -7 7 1 98.20 108.15 17.79 o -6 7 1 269.67 253.07 19.49 o -5 7 1 64.02 60.04 11.65 o -4 7 1 509.25 505.48 23.82 o -3 7 1 117.63 97.29 15.72 o -2 7 1 2067.15 2007.77 38.40 o -1 7 1 11.96 10.28 5.72 o 0 7 1 524.11 526.82 18.40 o 1 7 1 77.79 83.93 8.40 o 2 7 1 1587.19 1567.39 76.35 o 3 7 1 11.99 14.58 8.69 o 4 7 1 169.13 153.91 15.97 o 5 7 1 40.10 30.81 12.45 o 6 7 1 339.42 321.23 21.54 o 7 7 1 16.22 14.02 14.16 o -7 8 1 211.37 184.06 24.75 o -6 8 1 7.50 14.69 14.43 o -5 8 1 814.19 762.14 31.99 o -4 8 1 53.24 48.93 15.24 o -3 8 1 1672.12 1556.52 48.01 o -2 8 1 10.05 7.48 6.50 o -1 8 1 1654.52 1532.65 58.27 o 0 8 1 0.00 0.51 6.19 o 1 8 1 523.34 514.13 22.94 o 2 8 1 44.61 44.36 10.03 o 3 8 1 627.13 496.06 29.54 o 4 8 1 24.50 23.12 11.74 o 5 8 1 329.56 292.78 22.72 o 6 8 1 5.92 9.72 15.11 o 7 8 1 191.83 170.05 23.74 o -7 9 1 2.34 9.32 18.67 o -6 9 1 192.97 173.49 27.75 o -5 9 1 22.42 35.20 18.09 o -4 9 1 703.93 593.67 35.56 o -3 9 1 0.39 1.91 12.03 o -2 9 1 761.02 707.15 61.48 o -1 9 1 348.87 301.37 16.06 o 0 9 1 50.95 58.43 9.69 o 1 9 1 0.63 0.28 7.30 o 2 9 1 507.71 478.82 44.74 o 3 9 1 8.31 8.64 13.43 o 4 9 1 1026.19 832.85 41.80 o 5 9 1 21.53 19.10 18.55 o 6 9 1 320.62 298.08 34.07 o -6 10 1 1.20 2.22 20.15 o -5 10 1 451.35 436.32 36.42 o -4 10 1 188.54 185.82 25.31 o -3 10 1 824.26 702.41 38.06 o -2 10 1 58.62 59.05 16.12 o -1 10 1 125.86 116.61 12.56 o 0 10 1 10.22 9.49 8.58 o 1 10 1 189.86 181.62 17.06 o 2 10 1 143.95 101.80 18.45 o 3 10 1 539.28 448.79 32.43 o 4 10 1 0.02 -7.15 15.14 o 5 10 1 307.34 230.64 29.96 o 6 10 1 119.97 144.66 28.06 o -5 11 1 1.99 2.67 18.89 o -4 11 1 308.37 322.16 33.15 o -3 11 1 2.71 1.66 16.63 o -2 11 1 183.74 180.47 24.37 o -1 11 1 259.53 204.92 23.87 o 0 11 1 1735.20 1623.48 86.07 o 1 11 1 22.70 24.14 15.41 o 2 11 1 231.30 185.52 25.11 o 3 11 1 100.81 91.11 21.89 o 4 11 1 174.70 144.06 26.10 o 5 11 1 0.02 11.67 20.66 o -4 12 1 1.76 -5.04 20.43 o -3 12 1 171.56 158.44 26.94 o -2 12 1 0.05 -2.66 16.85 o -1 12 1 547.99 503.06 44.61 o 0 12 1 0.56 -0.35 13.07 o 1 12 1 414.79 380.36 41.95 o 2 12 1 4.07 -0.69 17.53 o 3 12 1 150.55 114.02 25.74 o 4 12 1 8.43 6.66 20.30 o -3 13 1 0.49 3.76 21.27 o -2 13 1 94.56 50.75 23.18 o -1 13 1 3.43 7.84 28.00 o 1 13 1 0.04 1.78 18.72 o 2 13 1 79.46 58.80 22.80 o 3 13 1 0.29 -0.92 19.81 o -8 0 2 334.94 388.13 51.43 o -6 0 2 273.53 282.38 22.70 o -4 0 2 779.30 697.20 22.73 o -2 0 2 2321.03 2403.27 843.20 o 0 0 2 7537.66 7517.12 66.66 o 2 0 2 293.55 400.71 13.20 o 4 0 2 14.25 4.00 5.42 o 6 0 2 222.55 262.71 36.19 o 8 0 2 249.77 209.42 43.78 o -9 1 2 114.73 112.62 27.43 o -8 1 2 131.01 125.07 25.55 o -7 1 2 418.43 448.19 32.21 o -6 1 2 1.84 1.97 9.34 o -5 1 2 906.87 980.40 22.73 o -4 1 2 0.06 -0.52 3.64 o -3 1 2 3771.43 3736.67 547.36 o -2 1 2 1876.87 1492.27 652.00 o -1 1 2 9627.50 9605.06 2068.81 o 0 1 2 26.71 37.05 12.51 o 1 1 2 4794.05 5023.57 75.21 o 2 1 2 806.84 746.57 25.92 o 3 1 2 460.44 433.57 10.13 o 4 1 2 21.30 15.14 4.62 o 5 1 2 1867.52 1730.20 30.06 o 6 1 2 2.51 1.21 11.93 o 7 1 2 355.52 318.21 31.24 o 8 1 2 111.41 98.05 25.46 o -9 2 2 9.24 19.08 21.04 o -8 2 2 105.53 89.79 23.67 o -7 2 2 103.81 127.21 17.50 o -6 2 2 418.34 473.67 19.58 o -5 2 2 48.91 56.00 7.63 o -4 2 2 1766.99 1713.63 278.05 o -3 2 2 12.94 10.45 3.84 o -2 2 2 4349.51 5186.18 44.20 o -1 2 2 3016.64 3130.40 976.85 o 0 2 2 2077.60 2019.94 470.15 o 1 2 2 164.78 130.32 24.78 o 2 2 2 485.01 447.20 9.45 o 3 2 2 299.32 274.72 9.05 o 4 2 2 626.59 621.91 15.81 o 5 2 2 120.88 122.88 11.59 o 6 2 2 374.50 401.39 19.35 o 7 2 2 2.85 2.94 15.08 o 8 2 2 226.74 225.10 31.56 o -8 3 2 7.71 9.39 18.59 o -7 3 2 55.17 72.95 15.55 o -6 3 2 23.76 23.64 9.57 o -5 3 2 1231.96 1331.64 28.35 o -4 3 2 67.77 60.17 14.80 o -3 3 2 3805.73 3892.85 325.41 o -2 3 2 368.64 395.53 9.15 o -1 3 2 9.57 12.24 2.68 o 0 3 2 35.97 48.78 12.21 o 1 3 2 446.48 594.66 88.53 o 2 3 2 2.24 0.43 2.64 o 3 3 2 999.48 1027.01 23.77 o 4 3 2 352.07 273.98 15.89 o 5 3 2 404.68 406.02 20.45 o 6 3 2 389.85 380.83 19.44 o 7 3 2 330.91 327.32 45.82 o 8 3 2 42.23 17.94 20.01 o -8 4 2 128.68 147.52 22.26 o -7 4 2 50.21 48.73 15.02 o -6 4 2 165.59 203.53 15.96 o -5 4 2 166.10 210.58 14.51 o -4 4 2 1411.92 1231.75 209.61 o -3 4 2 269.75 226.56 7.70 o -2 4 2 5020.41 5455.13 48.16 o -1 4 2 263.45 256.66 9.61 o 0 4 2 23.24 25.38 4.44 o 1 4 2 114.45 119.32 6.14 o 2 4 2 3439.69 3737.56 129.99 o 3 4 2 73.38 60.40 9.03 o 4 4 2 2136.19 2170.73 39.33 o 5 4 2 172.06 152.10 15.34 o 6 4 2 335.70 301.87 18.66 o 7 4 2 21.49 18.78 14.29 o 8 4 2 162.71 141.05 28.03 o -8 5 2 11.65 10.52 16.87 o -7 5 2 544.89 555.79 25.79 o -6 5 2 72.77 54.30 13.77 o -5 5 2 183.83 242.08 15.94 o -4 5 2 32.05 44.67 8.60 o -3 5 2 372.18 403.45 12.47 o -2 5 2 20.46 19.12 5.09 o -1 5 2 4464.25 4768.66 111.02 o 0 5 2 221.28 230.51 15.91 o 1 5 2 1243.67 1415.83 33.86 o 2 5 2 1163.35 1301.56 21.57 o 3 5 2 832.24 737.67 26.75 o 4 5 2 219.50 218.83 16.18 o 5 5 2 14.24 14.46 10.45 o 6 5 2 105.35 82.34 13.19 o 7 5 2 366.62 386.59 23.74 o 8 5 2 29.48 23.44 21.70 o -8 6 2 196.80 181.58 25.10 o -7 6 2 0.26 1.52 12.56 o -6 6 2 469.24 535.84 24.02 o -5 6 2 36.68 39.88 10.33 o -4 6 2 400.10 519.51 19.38 o -3 6 2 250.33 322.94 13.51 o -2 6 2 2228.92 2476.74 53.34 o -1 6 2 2.23 4.84 5.06 o 0 6 2 1605.73 1813.77 36.80 o 1 6 2 62.35 85.23 7.77 o 2 6 2 709.13 718.69 28.48 o 3 6 2 25.36 17.88 8.64 o 4 6 2 34.67 31.35 10.61 o 5 6 2 66.54 57.76 13.21 o 6 6 2 449.01 458.22 26.94 o 7 6 2 0.09 1.02 12.90 o -7 7 2 48.60 63.88 18.57 o -6 7 2 31.88 24.66 14.60 o -5 7 2 412.29 404.50 24.32 o -4 7 2 1.98 1.55 11.80 o -3 7 2 1093.99 1138.17 78.14 o -2 7 2 406.52 399.51 15.07 o -1 7 2 994.11 993.25 27.30 o 0 7 2 106.30 141.99 10.28 o 1 7 2 120.89 154.27 10.55 o 2 7 2 202.27 205.59 14.69 o 3 7 2 542.03 575.28 24.93 o 4 7 2 1.36 0.63 9.80 o 5 7 2 360.36 343.24 23.42 o 6 7 2 0.44 4.15 13.61 o 7 7 2 301.71 325.97 24.59 o -7 8 2 54.82 67.56 20.10 o -6 8 2 674.63 684.70 34.12 o -5 8 2 31.33 53.55 18.31 o -4 8 2 333.84 420.09 29.35 o -3 8 2 0.98 -2.32 10.50 o -2 8 2 1440.42 1448.70 31.33 o -1 8 2 704.70 667.43 20.31 o 0 8 2 1742.00 1691.30 60.21 o 1 8 2 51.95 43.97 8.25 o 2 8 2 1435.03 1458.22 61.89 o 3 8 2 18.62 27.54 13.75 o 4 8 2 1021.56 878.91 40.49 o 5 8 2 2.51 4.98 15.47 o 6 8 2 453.54 439.84 36.24 o 7 8 2 3.28 -1.03 16.57 o -7 9 2 48.96 29.94 23.72 o -6 9 2 13.78 25.97 20.39 o -5 9 2 314.64 339.38 31.95 o -4 9 2 42.26 50.03 17.27 o -3 9 2 186.59 195.91 25.26 o -2 9 2 38.00 18.62 12.29 o -1 9 2 391.28 400.56 18.28 o 0 9 2 343.46 356.64 17.23 o 1 9 2 256.69 259.75 18.27 o 2 9 2 27.70 22.68 13.48 o 3 9 2 24.51 32.92 15.75 o 4 9 2 7.52 3.35 15.48 o 5 9 2 184.75 192.64 28.03 o 6 9 2 4.64 8.55 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