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Information card for entry 2229903
Preview
| Coordinates | 2229903.cif |
|---|---|
| Structure factors | 2229903.hkl |
| Original IUCr paper | HTML |
| External links | PubChem |
| Chemical name | Bis[dicyclohexyl(phenyl)phosphane-κ<i>P</i>]silver(I) perchlorate dichloromethane monosolvate |
|---|---|
| Formula | C37 H56 Ag Cl3 O4 P2 |
| Calculated formula | C37 H56 Ag Cl3 O4 P2 |
| SMILES | [O-]Cl(=O)(=O)=O.c1(ccccc1)[P]([Ag][P](c1ccccc1)(C1CCCCC1)C1CCCCC1)(C1CCCCC1)C1CCCCC1.C(Cl)Cl |
| Title of publication | Bis[dicyclohexyl(phenyl)phosphane-κ<i>P</i>]silver(I) perchlorate dichloromethane monosolvate |
| Authors of publication | Munyaneza, Apollinaire; Meijboom, Reinout; Omondi, Bernard |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2011 |
| Journal volume | 67 |
| Journal issue | 4 |
| Pages of publication | m483 - m484 |
| a | 9.591 ± 0.0003 Å |
| b | 13.4369 ± 0.0004 Å |
| c | 15.129 ± 0.0005 Å |
| α | 90° |
| β | 94.706 ± 0.001° |
| γ | 90° |
| Cell volume | 1943.15 ± 0.11 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 7 |
| Hermann-Mauguin space group symbol | P 1 n 1 |
| Hall space group symbol | P -2yac |
| Residual factor for all reflections | 0.0178 |
| Residual factor for significantly intense reflections | 0.0174 |
| Weighted residual factors for significantly intense reflections | 0.0444 |
| Weighted residual factors for all reflections included in the refinement | 0.0446 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301805 (current) | 2025-08-19 | Add cross-references to PubChem compounds in COD range 2/22 Each referenced PubChem compound corresponds to the full crystal structure. |
2229903.cif 2229903.hkl |
| 181220 | 2016-04-03 | hkl/2/22/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22/99. |
2229903.cif 2229903.hkl |
| 176789 | 2016-02-20 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/22. |
2229903.cif 2229903.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2229903.cif 2229903.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2229903.cif 2229903.hkl |
| 26848 | 2011-09-28 | cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree. |
2229903.cif 2229903.hkl |
| 19531 | 2011-05-17 | hkl/2/ Adding Fobs data for the latest IUCr deposition. |
2229903.cif 2229903.hkl |
| 19382 | 2011-05-06 | ../uploads/cif-deposit/cod/cif Adding structures of 2229903 via cif-deposit CGI script. |
2229903.cif |
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Users of the data should acknowledge the original authors of the
structural data.