#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/99/2229924.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229924_Fobs loop_ _publ_author_name 'Arderne, Charmaine' 'Kruger, Gert J.' _publ_section_title ; Butane-1,4-diammonium bis(perchlorate) ; _journal_coeditor_code BT5503 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1060 _journal_volume 67 _journal_year 2011 _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.222 _cell_angle_gamma 90.000 _cell_length_a 19.4755 _cell_length_b 5.6210 _cell_length_c 5.3470 _exptl_crystal_F_000 300.00 _reflns_d_resolution_high 0.7487 _[local]_cod_data_source_file bt5503Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 8cvb50_a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 107.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 7082.09 6096.82 177.52 o 6 0 0 4668.40 3602.99 158.58 o 8 0 0 2745.57 2134.05 118.85 o 10 0 0 639.97 513.82 10.79 o 12 0 0 774.04 750.20 21.74 o 14 0 0 70.41 64.16 2.49 o 16 0 0 750.85 732.90 15.42 o 18 0 0 3.03 0.93 1.97 o 20 0 0 123.90 122.49 5.78 o 22 0 0 72.49 82.35 5.32 o 24 0 0 14.59 31.34 3.93 o 1 1 0 214.68 276.76 7.84 o 3 1 0 7146.53 6375.20 112.70 o 5 1 0 17.28 20.86 0.82 o 7 1 0 959.98 817.67 13.02 o 9 1 0 29.56 14.32 0.65 o 11 1 0 99.53 96.82 1.83 o 13 1 0 376.55 311.46 4.80 o 15 1 0 101.14 97.16 2.47 o 17 1 0 39.27 41.29 3.35 o 19 1 0 166.47 183.83 5.07 o 21 1 0 1.75 -1.85 1.85 o 23 1 0 18.12 23.14 2.58 o 25 1 0 1.81 4.74 3.47 o 0 2 0 9272.52 7695.02 224.79 o 2 2 0 371.92 399.58 7.23 o 4 2 0 4786.33 4320.45 74.60 o 6 2 0 634.17 484.59 8.83 o 8 2 0 107.05 97.70 1.94 o 10 2 0 2356.44 2164.33 25.72 o 12 2 0 1273.62 1192.00 13.80 o 14 2 0 68.21 67.39 1.75 o 16 2 0 995.97 894.02 15.27 o 18 2 0 37.24 43.95 3.82 o 20 2 0 26.82 29.15 3.47 o 22 2 0 42.79 48.58 4.40 o 24 2 0 16.13 18.62 3.70 o 1 3 0 216.95 138.51 2.68 o 3 3 0 752.24 679.33 11.62 o 5 3 0 236.55 262.22 3.57 o 7 3 0 940.58 1001.12 11.34 o 9 3 0 301.56 241.36 6.61 o 11 3 0 3.20 2.94 1.23 o 13 3 0 423.87 434.64 5.96 o 15 3 0 178.64 196.69 3.38 o 17 3 0 0.05 0.01 1.68 o 19 3 0 83.65 73.45 4.97 o 21 3 0 3.89 6.48 3.12 o 23 3 0 5.09 2.08 3.24 o 0 4 0 3498.43 3240.75 66.94 o 2 4 0 137.30 94.75 8.10 o 4 4 0 816.08 770.37 11.72 o 6 4 0 673.16 601.69 10.67 o 8 4 0 74.19 69.71 1.84 o 10 4 0 255.12 286.30 4.13 o 12 4 0 291.41 289.30 4.22 o 14 4 0 6.65 10.16 1.29 o 16 4 0 214.83 222.17 3.87 o 18 4 0 0.46 1.51 2.19 o 20 4 0 25.28 23.60 3.59 o 1 5 0 106.46 120.58 4.74 o 3 5 0 611.10 608.39 9.63 o 5 5 0 59.49 58.20 2.18 o 7 5 0 64.11 63.06 2.67 o 9 5 0 56.01 52.83 2.28 o 11 5 0 8.77 5.96 1.50 o 13 5 0 40.27 44.09 2.34 o 15 5 0 10.39 8.18 1.81 o 17 5 0 8.40 12.63 2.10 o 19 5 0 34.57 37.94 5.78 o 0 6 0 480.63 458.35 10.95 o 2 6 0 12.76 9.97 2.06 o 4 6 0 131.85 137.77 3.63 o 6 6 0 100.49 97.11 3.11 o 8 6 0 2.05 0.98 1.79 o 10 6 0 102.41 109.24 3.44 o 12 6 0 58.50 64.00 2.97 o 14 6 0 11.89 16.14 2.29 o 1 7 0 7.84 12.97 2.01 o 3 7 0 48.20 42.16 2.61 o 5 7 0 0.04 -0.92 1.97 o 7 7 0 44.91 53.26 4.16 o 9 7 0 18.61 26.61 2.40 o -24 0 1 24.54 38.86 4.16 o -22 0 1 16.53 7.40 3.01 o -20 0 1 19.40 23.25 3.24 o -18 0 1 167.51 178.59 6.94 o -16 0 1 13.64 16.98 1.99 o -14 0 1 14.62 14.07 1.91 o -12 0 1 322.75 298.04 7.31 o -10 0 1 635.51 670.90 12.17 o -8 0 1 4.05 6.61 0.69 o -6 0 1 138.62 148.62 7.69 o -4 0 1 4161.17 4832.44 107.29 o -2 0 1 2015.26 2604.51 58.04 o 0 0 1 800.68 1283.30 37.62 o 2 0 1 3415.78 4320.86 120.44 o 4 0 1 4397.11 4377.85 104.02 o 6 0 1 3162.76 2958.41 86.24 o 8 0 1 66.32 64.32 1.95 o 10 0 1 1752.32 1596.94 26.29 o 12 0 1 32.26 40.93 1.96 o 14 0 1 15.00 14.36 2.83 o 16 0 1 56.22 62.53 7.58 o 18 0 1 83.75 89.23 3.60 o 20 0 1 30.55 45.37 3.70 o 22 0 1 3.45 2.54 3.01 o 24 0 1 2.35 4.28 3.35 o -25 1 1 1.67 0.00 3.24 o -23 1 1 20.04 26.23 2.61 o -21 1 1 117.04 124.16 4.50 o -19 1 1 23.16 25.32 3.35 o -17 1 1 233.65 215.58 5.48 o -15 1 1 352.77 350.08 5.44 o -13 1 1 1.46 2.84 0.69 o -11 1 1 1013.12 873.23 13.90 o -9 1 1 46.39 38.49 1.12 o -7 1 1 14.65 21.18 0.81 o -5 1 1 2969.95 2700.18 52.02 o -3 1 1 5393.46 4924.18 77.05 o -1 1 1 11622.28 11014.07 200.26 o 1 1 1 5884.25 5671.11 91.73 o 3 1 1 3.25 5.23 0.56 o 5 1 1 1432.64 1315.88 25.23 o 7 1 1 2375.24 2249.62 29.38 o 9 1 1 161.10 180.89 2.37 o 11 1 1 1532.53 1378.96 18.96 o 13 1 1 582.11 597.06 8.97 o 15 1 1 766.06 697.01 10.46 o 17 1 1 113.25 115.24 2.97 o 19 1 1 0.50 0.79 1.27 o 21 1 1 35.77 37.05 2.01 o 23 1 1 93.16 121.13 6.94 o -24 2 1 5.91 1.73 3.12 o -22 2 1 0.42 -1.16 3.01 o -20 2 1 43.39 30.88 3.59 o -18 2 1 70.81 80.16 4.63 o -16 2 1 42.13 43.26 2.05 o -14 2 1 423.36 391.02 6.17 o -12 2 1 35.64 51.12 2.59 o -10 2 1 275.01 269.89 4.06 o -8 2 1 547.68 486.75 5.96 o -6 2 1 3096.60 2917.53 43.30 o -4 2 1 122.00 166.33 3.32 o -2 2 1 54.64 54.07 2.09 o 0 2 1 649.29 622.78 9.48 o 2 2 1 10.40 16.78 0.73 o 4 2 1 60.49 73.77 2.29 o 6 2 1 4.06 3.19 0.75 o 8 2 1 365.61 292.74 4.14 o 10 2 1 423.24 376.29 4.62 o 12 2 1 243.72 203.66 3.28 o 14 2 1 394.89 371.98 7.01 o 16 2 1 151.88 150.28 3.83 o 18 2 1 68.50 60.85 2.60 o 20 2 1 67.62 73.26 2.94 o 22 2 1 2.34 5.90 3.47 o 24 2 1 0.01 -2.08 3.47 o -23 3 1 6.72 12.49 3.59 o -21 3 1 37.05 38.86 4.28 o -19 3 1 2.29 -0.23 2.66 o -17 3 1 170.81 166.42 6.94 o -15 3 1 153.88 161.54 3.82 o -13 3 1 40.21 41.80 1.95 o -11 3 1 936.01 952.26 12.14 o -9 3 1 381.86 389.72 5.64 o -7 3 1 25.62 34.53 1.09 o -5 3 1 1447.92 1354.80 16.37 o -3 3 1 2544.97 2313.38 27.82 o -1 3 1 729.07 696.23 7.96 o 1 3 1 547.52 462.31 5.94 o 3 3 1 38.95 50.20 1.30 o 5 3 1 321.68 328.76 4.63 o 7 3 1 333.42 281.86 4.58 o 9 3 1 38.03 49.61 1.60 o 11 3 1 1116.52 1054.59 15.57 o 13 3 1 322.52 309.51 4.74 o 15 3 1 375.77 363.64 6.05 o 17 3 1 126.24 138.94 3.77 o 19 3 1 4.21 5.21 1.80 o 21 3 1 12.74 9.73 3.05 o -20 4 1 7.84 2.91 2.54 o -18 4 1 27.37 34.08 4.80 o -16 4 1 0.81 -0.09 1.62 o -14 4 1 39.95 45.52 2.22 o -12 4 1 6.32 4.04 0.99 o -10 4 1 0.42 0.03 1.38 o -8 4 1 131.89 146.39 3.21 o -6 4 1 114.96 118.47 2.19 o -4 4 1 304.98 281.34 4.01 o -2 4 1 447.72 421.00 6.49 o 0 4 1 73.07 105.97 4.41 o 2 4 1 321.53 302.92 7.06 o 4 4 1 388.73 362.50 6.81 o 6 4 1 76.53 71.03 2.20 o 8 4 1 149.52 139.23 3.73 o 10 4 1 302.16 277.59 4.80 o 12 4 1 2.67 7.33 1.26 o 14 4 1 55.90 58.29 2.03 o 16 4 1 36.33 39.45 2.49 o 18 4 1 19.63 25.07 1.92 o 20 4 1 14.52 19.79 2.37 o -19 5 1 9.17 5.20 5.09 o -17 5 1 33.50 34.35 5.44 o -15 5 1 67.09 70.20 3.25 o -13 5 1 0.78 0.79 1.71 o -11 5 1 99.84 98.91 2.52 o -9 5 1 5.60 2.98 1.25 o -7 5 1 26.70 25.05 1.92 o -5 5 1 266.52 266.77 4.84 o -3 5 1 107.37 130.22 10.33 o -1 5 1 675.68 674.21 12.05 o 1 5 1 549.98 550.79 8.82 o 3 5 1 1.56 4.74 2.05 o 5 5 1 221.24 214.53 5.38 o 7 5 1 291.06 271.29 8.33 o 9 5 1 8.79 8.69 1.54 o 11 5 1 159.81 153.45 4.01 o 13 5 1 58.01 58.22 3.34 o 15 5 1 84.72 91.32 2.97 o 17 5 1 21.75 28.10 2.17 o -14 6 1 29.57 28.86 5.60 o -12 6 1 10.43 13.69 3.25 o -10 6 1 5.66 6.08 1.68 o -8 6 1 40.74 39.96 2.24 o -6 6 1 41.38 42.64 2.36 o -4 6 1 29.80 23.00 1.78 o -2 6 1 53.51 56.03 2.29 o 0 6 1 10.09 11.52 1.59 o 2 6 1 52.31 47.63 2.38 o 4 6 1 59.60 52.02 2.48 o 6 6 1 1.61 -0.22 1.94 o 8 6 1 45.09 43.78 2.44 o 10 6 1 34.08 35.34 3.26 o 12 6 1 9.26 9.19 2.30 o 14 6 1 23.57 31.76 2.48 o -7 7 1 1.72 -0.24 2.46 o -5 7 1 63.76 71.65 3.17 o -3 7 1 41.61 43.76 2.38 o -1 7 1 44.86 44.11 2.82 o 1 7 1 46.97 51.31 2.78 o 3 7 1 1.14 3.13 2.10 o 5 7 1 41.74 46.06 2.73 o 7 7 1 23.23 24.92 2.40 o -24 0 2 0.14 1.97 3.35 o -22 0 2 138.84 151.29 6.94 o -20 0 2 80.96 78.01 4.03 o -18 0 2 18.67 26.44 2.57 o -16 0 2 190.39 203.50 5.95 o -14 0 2 151.65 188.96 7.23 o -12 0 2 263.18 265.39 4.62 o -10 0 2 1.39 2.23 0.92 o -8 0 2 156.72 180.56 3.77 o -6 0 2 1385.94 1320.60 23.40 o -4 0 2 632.21 867.44 19.78 o -2 0 2 4863.73 7031.51 184.84 o 0 0 2 6129.52 8674.91 323.79 o 2 0 2 882.97 1000.96 19.98 o 4 0 2 1041.55 1166.05 21.49 o 6 0 2 1066.97 1091.85 20.10 o 8 0 2 1864.52 1772.87 35.41 o 10 0 2 25.03 25.47 1.69 o 12 0 2 1102.05 1118.43 22.89 o 14 0 2 147.70 129.37 3.90 o 16 0 2 46.08 52.36 3.00 o 18 0 2 2.62 2.74 1.83 o 20 0 2 1.67 1.04 2.95 o 22 0 2 82.25 83.88 5.73 o -25 1 2 12.98 17.23 4.16 o -23 1 2 9.30 5.44 3.24 o -21 1 2 0.24 -1.23 2.00 o -19 1 2 154.02 163.26 3.87 o -17 1 2 16.55 23.10 1.56 o -15 1 2 190.42 179.23 3.29 o -13 1 2 22.40 20.34 1.00 o -11 1 2 86.58 96.20 1.50 o -9 1 2 1.55 -0.05 0.47 o -7 1 2 237.20 232.43 3.25 o -5 1 2 244.65 298.51 4.50 o -3 1 2 539.62 466.07 6.72 o -1 1 2 44.60 81.30 2.38 o 1 1 2 352.16 363.39 6.07 o 3 1 2 127.61 179.63 2.74 o 5 1 2 1175.88 1169.59 16.00 o 7 1 2 9.30 11.03 0.68 o 9 1 2 594.51 578.62 8.15 o 11 1 2 1.94 3.43 1.05 o 13 1 2 0.30 0.50 1.37 o 15 1 2 111.41 114.05 2.66 o 17 1 2 0.12 0.48 1.32 o 19 1 2 22.25 21.04 1.57 o 21 1 2 16.19 15.88 2.90 o 23 1 2 1.20 5.24 3.61 o -24 2 2 0.05 -0.69 3.24 o -22 2 2 74.41 77.38 5.32 o -20 2 2 14.23 14.91 2.69 o -18 2 2 86.64 81.27 2.50 o -16 2 2 265.71 245.16 4.89 o -14 2 2 75.65 72.14 2.11 o -12 2 2 868.06 788.67 11.59 o -10 2 2 685.68 690.81 7.18 o -8 2 2 249.97 266.57 3.21 o -6 2 2 358.35 345.19 4.70 o -4 2 2 2346.53 2109.25 28.86 o -2 2 2 17.78 12.07 0.75 o 0 2 2 99.76 77.78 1.97 o 2 2 2 19.11 19.69 1.44 o 4 2 2 142.04 147.45 1.76 o 6 2 2 18.36 15.29 0.87 o 8 2 2 25.40 29.77 1.04 o 10 2 2 536.80 477.33 6.05 o 12 2 2 908.31 854.14 12.60 o 14 2 2 171.80 160.63 3.80 o 16 2 2 183.73 168.11 5.87 o 18 2 2 52.32 50.58 2.48 o 20 2 2 0.64 2.02 1.81 o 22 2 2 61.37 71.94 3.30 o -23 3 2 3.54 0.69 3.47 o -21 3 2 0.03 0.93 3.01 o -19 3 2 54.65 56.09 2.81 o -17 3 2 0.24 -0.48 1.38 o -15 3 2 218.33 214.81 4.13 o -13 3 2 1.69 6.90 1.48 o -11 3 2 20.09 21.23 1.36 o -9 3 2 182.18 180.97 3.03 o -7 3 2 695.02 682.98 7.67 o -5 3 2 0.61 3.84 0.65 o -3 3 2 73.40 75.87 1.31 o -1 3 2 30.95 35.36 1.02 o 1 3 2 1.02 3.64 0.56 o 3 3 2 98.26 109.87 1.83 o 5 3 2 35.20 48.53 1.46 o 7 3 2 26.31 27.02 1.28 o 9 3 2 254.60 239.95 4.87 o 11 3 2 6.16 8.56 1.03 o 13 3 2 54.10 51.77 1.99 o 15 3 2 131.85 140.51 3.75 o 17 3 2 2.00 4.56 1.81 o 19 3 2 18.88 18.43 2.19 o 21 3 2 18.12 15.02 2.87 o -20 4 2 23.46 17.35 3.06 o -18 4 2 4.50 6.53 2.08 o -16 4 2 54.75 63.26 2.95 o -14 4 2 30.19 30.01 2.07 o -12 4 2 172.32 171.29 4.01 o -10 4 2 52.52 58.77 2.34 o -8 4 2 8.66 7.13 1.36 o -6 4 2 309.42 328.73 5.13 o -4 4 2 483.60 460.59 6.18 o -2 4 2 239.73 237.80 5.44 o 0 4 2 639.76 649.17 8.43 o 2 4 2 115.00 142.15 3.36 o 4 4 2 67.57 77.46 2.41 o 6 4 2 247.61 223.71 4.72 o 8 4 2 171.00 158.28 3.79 o 10 4 2 68.66 64.45 2.08 o 12 4 2 298.07 276.12 4.48 o 14 4 2 18.60 23.27 1.94 o 16 4 2 36.59 38.04 2.05 o 18 4 2 9.05 7.65 2.02 o -17 5 2 13.32 13.94 2.97 o -15 5 2 13.36 13.83 2.88 o -13 5 2 0.15 -1.35 2.32 o -11 5 2 12.39 13.00 2.05 o -9 5 2 9.30 11.40 1.67 o -7 5 2 31.14 34.87 1.54 o -5 5 2 63.95 55.02 1.85 o -3 5 2 142.09 161.36 2.90 o -1 5 2 16.11 27.44 2.05 o 1 5 2 57.87 56.17 2.36 o 3 5 2 86.06 79.85 2.60 o 5 5 2 146.03 155.38 3.83 o 7 5 2 3.63 2.45 1.50 o 9 5 2 115.15 105.38 3.32 o 11 5 2 7.37 8.97 1.75 o 13 5 2 0.57 1.68 1.60 o 15 5 2 20.66 17.98 2.29 o -14 6 2 23.52 16.89 5.55 o -12 6 2 37.31 31.92 5.44 o -10 6 2 52.31 56.47 3.71 o -8 6 2 5.74 5.29 1.64 o -6 6 2 40.00 46.36 2.90 o -4 6 2 80.21 81.98 3.32 o -2 6 2 19.22 21.47 3.82 o 0 6 2 106.24 100.01 3.28 o 2 6 2 19.93 22.37 1.97 o 4 6 2 36.71 37.62 2.29 o 6 6 2 58.11 52.98 2.70 o 8 6 2 17.86 16.84 2.05 o 10 6 2 30.72 36.15 2.48 o 12 6 2 71.91 69.34 3.29 o -5 7 2 0.58 0.35 2.06 o -3 7 2 14.61 15.77 2.09 o -1 7 2 9.73 8.68 2.97 o 1 7 2 0.69 0.06 1.90 o 3 7 2 4.83 3.78 2.71 o -24 0 3 11.48 7.06 4.16 o -22 0 3 37.96 32.51 3.22 o -20 0 3 56.49 60.68 6.94 o -18 0 3 191.05 211.52 6.47 o -16 0 3 2.39 4.68 1.54 o -14 0 3 3.44 2.90 1.06 o -12 0 3 182.45 183.21 5.03 o -10 0 3 0.95 2.36 1.03 o -8 0 3 345.07 398.51 9.64 o -6 0 3 4.05 1.07 0.84 o -4 0 3 2432.11 2931.81 51.71 o -2 0 3 817.01 1037.57 17.32 o 0 0 3 702.91 1052.89 49.13 o 2 0 3 218.61 236.42 7.52 o 4 0 3 2462.65 2468.93 48.99 o 6 0 3 176.83 155.70 4.40 o 8 0 3 840.91 850.72 17.62 o 10 0 3 128.82 151.29 4.31 o 12 0 3 22.52 16.42 1.79 o 14 0 3 17.83 30.19 3.07 o 16 0 3 10.51 14.99 2.00 o 18 0 3 1.98 4.70 2.72 o 20 0 3 29.07 29.58 3.00 o 22 0 3 3.97 8.33 3.70 o -23 1 3 43.91 57.37 5.09 o -21 1 3 86.63 85.14 3.21 o -19 1 3 7.65 5.74 1.42 o -17 1 3 102.48 109.67 2.79 o -15 1 3 530.09 548.45 6.93 o -13 1 3 12.91 15.82 0.90 o -11 1 3 578.84 558.49 7.52 o -9 1 3 568.96 526.62 7.08 o -7 1 3 485.48 419.90 5.72 o -5 1 3 1772.73 1977.36 23.83 o -3 1 3 2.06 3.46 0.92 o -1 1 3 1566.06 1826.97 29.08 o 1 1 3 1715.74 1802.48 24.84 o 3 1 3 257.75 246.88 3.64 o 5 1 3 706.96 684.81 9.14 o 7 1 3 783.47 744.22 13.42 o 9 1 3 14.84 19.38 1.40 o 11 1 3 1026.50 973.78 14.34 o 13 1 3 0.62 0.07 1.10 o 15 1 3 76.32 75.64 2.38 o 17 1 3 62.50 63.97 2.34 o 19 1 3 4.97 6.26 1.63 o 21 1 3 23.65 24.50 2.26 o -22 2 3 15.43 16.88 2.84 o -20 2 3 45.77 46.74 2.24 o -18 2 3 86.72 87.36 2.75 o -16 2 3 70.69 66.68 2.55 o -14 2 3 101.74 101.50 2.51 o -12 2 3 318.85 309.97 4.18 o -10 2 3 8.10 6.70 0.83 o -8 2 3 1127.15 1111.08 14.25 o -6 2 3 603.24 571.23 7.30 o -4 2 3 224.89 194.44 2.86 o -2 2 3 295.33 271.10 3.72 o 0 2 3 15.50 15.71 1.30 o 2 2 3 125.76 116.81 1.90 o 4 2 3 189.52 176.98 2.62 o 6 2 3 7.75 6.93 0.77 o 8 2 3 505.14 461.91 6.51 o 10 2 3 0.09 1.20 0.98 o 12 2 3 48.47 45.03 1.77 o 14 2 3 117.97 121.67 3.46 o 16 2 3 22.69 23.57 2.21 o 18 2 3 0.44 1.45 1.80 o 20 2 3 49.59 51.43 3.26 o -21 3 3 32.49 36.33 2.43 o -19 3 3 1.44 -1.31 1.68 o -17 3 3 49.25 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