#------------------------------------------------------------------------------ #$Date: 2016-04-03 05:04:48 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181220 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/99/2229963.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229963_Fobs loop_ _publ_author_name 'McLauchlan, Craig C.' 'Smith, Brigette L.' 'Pippins, Reyhana S.' 'Nelson, Brandon M.' _publ_section_title ; 2,2,2-Tris(pyrazol-1-yl)ethanol ; _journal_coeditor_code DN2673 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1133 _journal_page_last o1134 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 125.740 _cell_angle_gamma 90.000 _cell_length_a 19.6589 _cell_length_b 11.5155 _cell_length_c 12.4185 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.8001 _cod_data_source_file dn2673Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' c2c in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 40080.62 39451.23 613.90 o 6 0 0 13598.75 13717.99 138.07 o 8 0 0 428.47 444.26 7.90 o 10 0 0 1731.80 1766.87 20.79 o 12 0 0 207.27 173.69 4.64 o 14 0 0 1435.89 1315.76 17.73 o 16 0 0 538.47 577.04 26.82 o 18 0 0 64.53 37.10 6.70 o 1 1 0 4316.37 4114.47 39.81 o 3 1 0 6310.84 6159.89 48.91 o 5 1 0 11757.85 11570.80 153.54 o 7 1 0 1826.63 1681.65 13.41 o 9 1 0 12060.36 13015.94 93.25 o 11 1 0 127.06 79.94 2.15 o 13 1 0 2285.51 2309.93 19.40 o 15 1 0 3060.20 3032.49 27.78 o 17 1 0 299.32 358.04 10.82 o 19 1 0 60.73 70.67 5.98 o 0 2 0 17660.44 16368.94 281.58 o 2 2 0 11395.50 10593.83 85.84 o 4 2 0 8379.66 8155.09 72.68 o 6 2 0 1430.19 1494.88 11.96 o 8 2 0 888.92 842.92 7.71 o 10 2 0 0.77 0.19 0.62 o 12 2 0 374.07 370.10 5.03 o 14 2 0 1646.29 1584.80 16.18 o 16 2 0 0.38 -0.06 1.42 o 18 2 0 32.15 45.65 3.99 o 1 3 0 6191.04 6726.43 48.27 o 3 3 0 2169.97 2163.70 25.39 o 5 3 0 2315.17 2474.00 23.86 o 7 3 0 1910.43 1881.52 19.28 o 9 3 0 1917.16 1873.70 15.31 o 11 3 0 903.44 830.15 9.35 o 13 3 0 12.70 15.93 1.71 o 15 3 0 35.60 32.29 2.67 o 17 3 0 478.10 481.72 9.12 o 19 3 0 220.87 262.90 8.29 o 0 4 0 3399.05 3170.31 33.36 o 2 4 0 13.41 15.13 1.16 o 4 4 0 1285.64 1293.57 11.78 o 6 4 0 4374.43 4627.73 38.04 o 8 4 0 2064.35 2095.55 21.75 o 10 4 0 692.78 632.71 9.14 o 12 4 0 128.82 120.10 3.90 o 14 4 0 3620.26 3474.07 35.99 o 16 4 0 324.38 272.28 6.61 o 18 4 0 18.12 30.46 3.01 o 1 5 0 23.54 19.97 1.26 o 3 5 0 578.47 497.25 4.95 o 5 5 0 0.04 0.76 0.58 o 7 5 0 840.37 917.99 9.49 o 9 5 0 478.01 475.97 7.59 o 11 5 0 10.93 13.26 2.39 o 13 5 0 144.96 126.97 4.29 o 15 5 0 341.65 288.95 6.75 o 17 5 0 113.77 99.45 4.57 o 0 6 0 129.48 179.30 3.82 o 2 6 0 53.64 57.27 1.55 o 4 6 0 3114.67 3342.42 30.65 o 6 6 0 99.76 110.10 2.46 o 8 6 0 280.39 278.69 5.52 o 10 6 0 143.42 133.81 4.08 o 12 6 0 1041.06 961.65 13.75 o 14 6 0 0.54 2.43 1.59 o 16 6 0 7.24 5.34 2.01 o 18 6 0 0.18 -0.09 1.66 o 1 7 0 1808.06 1982.67 16.20 o 3 7 0 4785.96 4881.85 39.21 o 5 7 0 1535.11 1606.22 19.24 o 7 7 0 1854.10 1848.54 20.46 o 9 7 0 637.21 592.95 9.32 o 11 7 0 447.26 453.93 8.26 o 13 7 0 1668.68 1509.28 20.90 o 15 7 0 11.65 8.93 1.96 o 17 7 0 80.31 73.43 4.29 o 0 8 0 195.62 202.70 4.70 o 2 8 0 627.34 672.75 7.10 o 4 8 0 122.42 138.49 4.59 o 6 8 0 0.06 1.58 1.80 o 8 8 0 1.63 8.12 2.92 o 10 8 0 2774.43 2508.02 27.38 o 12 8 0 1716.86 1546.57 19.42 o 14 8 0 250.07 271.55 6.92 o 16 8 0 251.89 260.48 7.21 o 1 9 0 446.24 473.27 5.81 o 3 9 0 62.38 75.64 2.26 o 5 9 0 2.69 0.03 1.35 o 7 9 0 768.74 712.84 10.70 o 9 9 0 46.65 57.93 3.29 o 11 9 0 1455.62 1313.95 17.40 o 13 9 0 14.32 10.88 2.08 o 15 9 0 43.66 45.62 4.00 o 0 10 0 118.86 108.30 4.02 o 2 10 0 685.23 688.08 7.72 o 4 10 0 399.22 371.95 7.14 o 6 10 0 448.53 426.68 8.54 o 8 10 0 112.43 131.26 5.10 o 10 10 0 311.21 269.18 6.70 o 12 10 0 1053.16 1025.82 15.18 o 14 10 0 0.05 1.76 1.68 o 1 11 0 477.66 516.67 6.75 o 3 11 0 208.85 244.94 5.71 o 5 11 0 4.55 5.63 1.77 o 7 11 0 7.95 8.11 1.85 o 9 11 0 124.79 98.17 5.89 o 11 11 0 0.47 1.33 1.70 o 0 12 0 2652.39 2764.11 41.68 o 2 12 0 320.45 336.81 7.04 o 4 12 0 99.90 118.35 4.29 o 6 12 0 142.31 157.68 5.19 o 8 12 0 79.92 107.28 4.57 o 10 12 0 43.23 48.05 3.62 o 1 13 0 628.38 650.35 16.75 o 3 13 0 24.78 14.70 2.25 o 5 13 0 99.37 117.68 4.62 o 7 13 0 6.22 14.17 2.35 o 0 14 0 3.34 1.34 2.68 o 2 14 0 311.11 328.20 11.69 o 4 14 0 756.92 783.17 12.94 o -19 1 1 45.13 61.62 4.30 o -17 1 1 673.89 711.13 9.55 o -15 1 1 335.44 348.61 6.45 o -13 1 1 10.63 14.22 1.29 o -11 1 1 489.93 492.42 7.05 o -9 1 1 249.34 282.42 4.10 o -7 1 1 2575.18 2546.99 19.40 o -5 1 1 219.12 215.13 2.43 o -3 1 1 2247.74 2091.35 21.91 o -1 1 1 42.66 47.61 0.69 o 1 1 1 1526.13 1569.00 11.86 o 3 1 1 23805.45 22492.77 226.50 o 5 1 1 3628.77 3614.36 26.80 o 7 1 1 68.75 66.85 1.69 o 9 1 1 159.62 173.06 2.92 o 11 1 1 14.74 12.40 1.20 o 13 1 1 520.73 499.12 6.41 o 15 1 1 35.05 39.67 2.86 o 17 1 1 30.49 26.82 4.11 o -20 2 1 10.46 5.08 2.16 o -18 2 1 135.03 123.08 4.62 o -16 2 1 1256.76 1226.64 13.68 o -14 2 1 1525.80 1566.33 15.90 o -12 2 1 1289.59 1357.66 13.63 o -10 2 1 810.56 898.51 9.12 o -8 2 1 1921.76 1819.53 14.59 o -6 2 1 2643.87 2617.25 19.73 o -4 2 1 203.85 260.04 2.98 o -2 2 1 1773.26 1693.80 12.68 o 0 2 1 145.83 124.78 1.49 o 2 2 1 34565.63 33280.65 559.86 o 4 2 1 1045.32 845.79 7.14 o 6 2 1 1433.80 1558.57 13.53 o 8 2 1 4.04 8.37 0.91 o 10 2 1 430.53 504.46 7.40 o 12 2 1 311.18 288.93 5.55 o 14 2 1 99.74 98.40 3.84 o 16 2 1 4.86 7.73 1.85 o 18 2 1 0.06 1.06 1.51 o -19 3 1 13.07 6.70 1.89 o -17 3 1 112.65 116.30 4.30 o -15 3 1 2184.92 2179.74 24.23 o -13 3 1 30.25 29.97 1.93 o -11 3 1 1651.70 1599.27 13.67 o -9 3 1 640.35 804.91 9.26 o -7 3 1 2618.17 2659.57 25.83 o -5 3 1 8466.36 8659.76 69.06 o -3 3 1 437.88 420.71 4.25 o -1 3 1 27293.08 25610.18 259.67 o 1 3 1 2264.33 2199.42 16.54 o 3 3 1 1055.81 1031.52 10.62 o 5 3 1 3154.30 3321.61 30.58 o 7 3 1 9437.14 10213.87 78.39 o 9 3 1 27.89 30.45 1.28 o 11 3 1 2145.89 2106.42 19.77 o 13 3 1 374.98 348.48 7.10 o 15 3 1 41.18 22.16 2.38 o 17 3 1 23.14 12.49 2.10 o -20 4 1 198.33 241.18 6.92 o -18 4 1 11.87 9.65 2.03 o -16 4 1 232.93 246.40 6.84 o -14 4 1 3297.13 2935.99 30.88 o -12 4 1 199.25 196.39 4.74 o -10 4 1 19.70 19.33 2.06 o -8 4 1 2063.56 2237.83 22.82 o -6 4 1 1941.44 1993.13 19.19 o -4 4 1 3312.17 3161.00 25.60 o -2 4 1 1461.43 1449.10 11.52 o 0 4 1 1902.94 1952.09 15.03 o 2 4 1 0.00 1.94 0.64 o 4 4 1 146.62 97.26 2.85 o 6 4 1 1464.63 1498.46 25.22 o 8 4 1 4596.59 4579.71 43.92 o 10 4 1 289.87 258.18 8.39 o 12 4 1 19.31 12.96 1.93 o 14 4 1 5.55 6.09 1.59 o 16 4 1 371.82 403.13 8.39 o 18 4 1 2.28 7.57 2.00 o -19 5 1 1.81 3.76 1.66 o -17 5 1 267.96 274.97 12.26 o -15 5 1 1816.11 1788.77 21.87 o -13 5 1 1031.09 976.28 13.16 o -11 5 1 284.29 358.21 6.58 o -9 5 1 1849.19 2068.77 18.99 o -7 5 1 1767.72 1784.27 16.34 o -5 5 1 2500.18 2364.29 18.39 o -3 5 1 28.40 41.71 2.35 o -1 5 1 1766.87 1627.61 13.03 o 1 5 1 1788.46 1807.98 15.04 o 3 5 1 2913.78 2988.00 25.58 o 5 5 1 1926.14 2200.39 26.35 o 7 5 1 5179.66 4905.68 46.65 o 9 5 1 258.74 224.06 6.64 o 11 5 1 2026.79 1910.89 21.67 o 13 5 1 943.89 925.25 13.24 o 15 5 1 107.61 121.87 4.68 o 17 5 1 105.16 94.66 5.42 o -18 6 1 79.35 78.93 5.61 o -16 6 1 7.44 3.66 1.47 o -14 6 1 38.10 40.95 2.96 o -12 6 1 160.82 168.04 4.69 o -10 6 1 942.74 887.36 11.89 o -8 6 1 82.16 111.70 2.74 o -6 6 1 18.58 28.48 1.73 o -4 6 1 11627.90 12107.20 86.82 o -2 6 1 848.94 755.49 7.16 o 0 6 1 2033.95 2112.95 18.09 o 2 6 1 1284.71 1237.50 11.81 o 4 6 1 374.77 395.65 4.35 o 6 6 1 458.86 451.44 7.19 o 8 6 1 4227.49 4156.78 40.86 o 10 6 1 75.87 82.13 6.52 o 12 6 1 518.71 498.05 8.98 o 14 6 1 1.47 9.67 2.18 o 16 6 1 2177.24 2252.35 26.91 o -17 7 1 1.85 -0.86 1.49 o -15 7 1 135.34 152.95 5.02 o -13 7 1 437.93 373.19 7.59 o -11 7 1 46.52 46.99 2.84 o -9 7 1 7315.15 7271.32 79.83 o -7 7 1 1910.58 2111.99 19.48 o -5 7 1 88.54 67.10 1.76 o -3 7 1 971.77 1064.04 9.69 o -1 7 1 3237.76 3213.38 24.84 o 1 7 1 103.34 139.85 2.93 o 3 7 1 229.61 283.26 3.73 o 5 7 1 0.00 4.56 1.21 o 7 7 1 422.91 426.36 7.42 o 9 7 1 1573.61 1490.93 17.95 o 11 7 1 2256.33 2305.36 25.99 o 13 7 1 276.39 294.97 10.12 o 15 7 1 61.24 63.48 3.90 o -16 8 1 145.63 136.02 5.48 o -14 8 1 192.79 225.19 6.14 o -12 8 1 8.54 17.42 2.64 o -10 8 1 34.42 22.46 2.27 o -8 8 1 349.77 327.86 6.42 o -6 8 1 108.94 130.61 4.28 o -4 8 1 378.71 378.65 4.81 o -2 8 1 402.50 410.00 5.12 o 0 8 1 50.16 53.05 1.78 o 2 8 1 150.24 160.63 2.95 o 4 8 1 270.87 258.47 5.41 o 6 8 1 4053.68 3948.14 39.35 o 8 8 1 659.86 607.87 10.38 o 10 8 1 102.34 98.26 4.02 o 12 8 1 132.90 154.82 5.08 o 14 8 1 0.32 0.98 2.13 o -15 9 1 201.04 188.19 6.01 o -13 9 1 671.20 655.29 11.11 o -11 9 1 24.83 37.16 2.84 o -9 9 1 10.54 11.76 1.85 o -7 9 1 0.42 0.35 1.48 o -5 9 1 850.99 767.00 9.23 o -3 9 1 1104.14 1188.17 11.19 o -1 9 1 7.15 8.12 1.17 o 1 9 1 37.86 69.79 3.25 o 3 9 1 2157.50 2078.25 22.62 o 5 9 1 2527.54 2411.73 25.96 o 7 9 1 830.01 793.87 11.71 o 9 9 1 64.97 48.98 3.62 o 11 9 1 16.21 19.23 2.40 o 13 9 1 4.17 2.37 2.30 o -14 10 1 0.01 -0.62 1.49 o -12 10 1 504.35 511.35 9.71 o -10 10 1 1560.56 1490.46 18.96 o -8 10 1 348.04 337.40 7.07 o -6 10 1 3653.56 3436.91 35.36 o -4 10 1 1616.66 1569.18 15.97 o -2 10 1 6.02 8.90 1.23 o 0 10 1 4046.86 3951.63 31.18 o 2 10 1 4790.47 4597.51 45.06 o 4 10 1 6.64 5.68 1.54 o 6 10 1 945.95 893.66 12.88 o 8 10 1 80.87 101.06 4.13 o 10 10 1 296.84 285.99 7.04 o 12 10 1 5.69 3.18 1.92 o -13 11 1 227.57 250.95 8.83 o -11 11 1 1421.75 1380.50 18.56 o -9 11 1 62.43 66.61 5.29 o -7 11 1 24.00 25.25 2.56 o -5 11 1 13.55 15.23 2.16 o -3 11 1 986.45 939.47 12.82 o -1 11 1 1256.04 1192.47 11.88 o 1 11 1 680.53 675.26 10.35 o 3 11 1 1718.98 1625.98 19.54 o 5 11 1 3199.94 3125.58 33.30 o 7 11 1 82.54 79.83 3.91 o 9 11 1 125.83 95.67 4.46 o 11 11 1 221.51 219.47 6.59 o -10 12 1 0.18 1.56 1.58 o -8 12 1 3.53 1.03 1.58 o -6 12 1 0.00 1.85 1.59 o -4 12 1 1103.02 1091.59 14.84 o -2 12 1 226.83 238.21 5.87 o 0 12 1 313.11 302.35 6.61 o 2 12 1 39.89 41.44 3.00 o 4 12 1 1560.88 1575.73 19.75 o 6 12 1 1264.90 1334.63 17.86 o 8 12 1 35.66 40.37 3.28 o 10 12 1 297.90 333.92 8.21 o -9 13 1 623.57 676.46 12.04 o -7 13 1 1185.24 1148.24 16.30 o -5 13 1 71.40 83.22 4.17 o -3 13 1 701.31 702.22 13.39 o -1 13 1 37.79 39.18 6.03 o 1 13 1 33.96 38.94 3.04 o 3 13 1 186.12 169.06 5.51 o 5 13 1 212.79 196.78 6.03 o 7 13 1 733.06 773.67 13.10 o -4 14 1 33.88 40.55 3.85 o -2 14 1 19.61 18.25 3.43 o 0 14 1 22.77 25.50 4.07 o 2 14 1 39.73 38.05 3.85 o -20 0 2 52.23 54.13 5.59 o -18 0 2 1734.70 1818.95 51.62 o -16 0 2 686.60 592.46 10.18 o -14 0 2 1936.78 1737.39 21.49 o -12 0 2 3483.24 3563.93 39.03 o -10 0 2 1860.04 2201.54 24.80 o -8 0 2 74.58 77.47 2.29 o -6 0 2 3328.27 3461.32 36.06 o -4 0 2 1158.25 1130.14 15.63 o -2 0 2 8320.55 8135.15 105.51 o 0 0 2 5051.33 4670.75 48.31 o 2 0 2 818.99 796.56 9.43 o 4 0 2 434.60 524.48 7.27 o 6 0 2 3979.12 4211.24 52.94 o 8 0 2 59.91 48.29 2.63 o 10 0 2 630.91 723.67 26.37 o 12 0 2 78.46 99.71 7.59 o 14 0 2 1224.32 1178.10 42.24 o 16 0 2 6.83 21.01 5.81 o -21 1 2 24.12 51.28 4.30 o -19 1 2 356.18 335.15 7.35 o -17 1 2 266.94 243.54 5.13 o -15 1 2 1027.81 1017.41 10.24 o -13 1 2 468.12 427.24 6.62 o -11 1 2 466.29 488.38 5.85 o -9 1 2 72.83 77.64 1.69 o -7 1 2 1351.02 1366.31 11.01 o -5 1 2 1197.49 1221.66 12.05 o -3 1 2 46401.91 42756.18 949.91 o -1 1 2 13468.23 12946.91 187.08 o 1 1 2 8880.51 8279.65 76.92 o 3 1 2 1.47 0.72 0.43 o 5 1 2 4028.51 4152.15 30.86 o 7 1 2 3972.42 3996.17 32.61 o 9 1 2 2421.22 2521.10 20.41 o 11 1 2 3512.47 3526.91 28.02 o 13 1 2 1212.15 1164.37 12.96 o 15 1 2 861.62 846.59 29.16 o 17 1 2 129.84 161.35 12.07 o -20 2 2 45.61 40.35 3.78 o -18 2 2 118.08 124.31 3.87 o -16 2 2 27.95 21.53 1.91 o -14 2 2 1735.98 1829.70 15.86 o -12 2 2 552.68 671.33 7.02 o -10 2 2 1955.83 2286.29 18.21 o -8 2 2 225.73 242.68 3.08 o -6 2 2 2795.95 2665.49 25.29 o -4 2 2 41490.40 38136.20 443.40 o -2 2 2 4790.46 4638.31 33.51 o 0 2 2 7453.62 7634.81 60.27 o 2 2 2 3651.55 3675.06 27.18 o 4 2 2 1638.91 1562.66 14.70 o 6 2 2 5205.75 5280.01 43.34 o 8 2 2 357.81 340.19 4.31 o 10 2 2 2002.13 1906.97 16.21 o 12 2 2 2398.47 2420.03 29.64 o 14 2 2 521.11 542.83 9.35 o 16 2 2 52.09 50.50 3.42 o -21 3 2 0.25 3.47 1.72 o -19 3 2 399.99 442.79 10.97 o -17 3 2 216.64 180.87 5.19 o -15 3 2 2422.81 2331.77 23.07 o -13 3 2 219.86 254.55 5.09 o -11 3 2 111.76 77.96 2.15 o -9 3 2 7748.72 8354.59 66.76 o -7 3 2 3214.26 3121.20 32.69 o -5 3 2 3560.12 3584.47 30.44 o -3 3 2 2501.06 2394.97 17.96 o -1 3 2 3034.30 3141.09 23.24 o 1 3 2 393.93 392.85 4.43 o 3 3 2 66.15 53.76 1.42 o 5 3 2 301.34 265.17 3.38 o 7 3 2 147.67 217.68 3.10 o 9 3 2 549.62 540.47 5.99 o 11 3 2 6323.30 6179.98 58.86 o 13 3 2 426.74 389.90 7.71 o 15 3 2 30.76 40.74 3.01 o 17 3 2 0.12 0.26 1.65 o -20 4 2 6.65 6.69 2.20 o -18 4 2 113.25 101.04 4.18 o -16 4 2 1.69 7.11 1.72 o -14 4 2 62.80 55.81 2.84 o -12 4 2 390.63 391.52 6.81 o -10 4 2 1184.58 1248.09 12.11 o -8 4 2 985.14 1095.94 11.78 o -6 4 2 351.35 348.91 3.87 o -4 4 2 7975.44 8028.58 57.78 o -2 4 2 14219.40 14060.88 137.48 o 0 4 2 1109.74 1311.15 10.64 o 2 4 2 2600.04 2512.70 24.02 o 4 4 2 173.03 212.53 3.16 o 6 4 2 59.06 75.40 1.90 o 8 4 2 370.31 435.12 7.24 o 10 4 2 253.82 237.77 5.46 o 12 4 2 0.52 -0.55 2.52 o 14 4 2 10.22 20.39 2.49 o 16 4 2 544.73 562.69 10.55 o -19 5 2 160.69 136.70 7.34 o -17 5 2 15.28 22.14 2.48 o -15 5 2 347.69 334.80 7.37 o -13 5 2 148.44 120.76 3.85 o -11 5 2 599.43 600.15 8.93 o -9 5 2 188.73 232.10 3.88 o -7 5 2 1456.92 1713.62 21.19 o -5 5 2 32.79 70.46 1.65 o -3 5 2 43.34 57.69 1.51 o -1 5 2 37.04 23.27 1.02 o 1 5 2 41.56 52.65 1.30 o 3 5 2 312.27 299.86 4.05 o 5 5 2 366.93 375.30 6.19 o 7 5 2 803.57 784.61 10.58 o 9 5 2 1516.53 1442.02 17.17 o 11 5 2 562.48 552.23 9.37 o 13 5 2 4101.81 3732.48 46.90 o 15 5 2 801.93 785.07 12.80 o -18 6 2 83.46 75.40 4.07 o -16 6 2 244.74 216.57 7.42 o -14 6 2 1.23 1.14 1.29 o -12 6 2 5.73 1.36 1.35 o -10 6 2 52.42 41.71 2.43 o -8 6 2 2683.74 2842.39 22.91 o -6 6 2 5.09 14.76 1.87 o -4 6 2 1594.58 1821.46 14.89 o -2 6 2 1778.27 2009.55 17.48 o 0 6 2 4.84 3.89 0.67 o 2 6 2 44.91 36.19 1.29 o 4 6 2 44.65 54.45 2.14 o 6 6 2 0.10 6.99 2.15 o 8 6 2 13.61 12.87 1.79 o 10 6 2 1745.57 1596.65 19.23 o 12 6 2 116.94 112.93 4.41 o 14 6 2 196.87 166.39 5.47 o 16 6 2 13.93 15.91 3.88 o -19 7 2 44.39 52.07 4.06 o -17 7 2 35.95 48.70 3.40 o -15 7 2 480.68 398.68 9.23 o -13 7 2 818.64 781.98 16.92 o -11 7 2 1657.83 1691.74 19.59 o -9 7 2 0.09 -0.54 0.88 o -7 7 2 81.26 88.63 2.08 o -5 7 2 115.23 88.58 2.16 o -3 7 2 484.16 474.81 5.39 o -1 7 2 3309.78 3452.29 26.61 o 1 7 2 2495.50 2731.90 21.50 o 3 7 2 604.20 627.39 7.85 o 5 7 2 541.76 547.24 8.47 o 7 7 2 25.05 16.90 1.81 o 9 7 2 2421.85 2197.48 28.06 o 11 7 2 133.40 157.30 5.07 o 13 7 2 401.38 375.05 8.21 o 15 7 2 58.49 44.38 3.66 o -18 8 2 194.63 205.19 6.37 o -16 8 2 1080.26 1085.93 15.74 o -14 8 2 24.11 30.50 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