#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/99/2229973.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229973_Fobs loop_ _publ_author_name 'Muller, Fabian M. A.' 'Muller, Theunis J.' 'Steyl, Gideon' _publ_section_title ; (2-Methyl-4-oxo-4H-pyran-3-olato-\k^2^O^3^,O^4^)bis(triphenylphosphane-\kP)copper(I)--triphenylphosphane--methanol (1/1/1) ; _journal_coeditor_code FI2105 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m581 _journal_page_last m582 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 119.205 _cell_angle_gamma 90.000 _cell_length_a 20.5253 _cell_length_b 13.5716 _cell_length_c 20.3129 _exptl_crystal_F_000 2104.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file fi2105Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 7Llk7_tx in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 336.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4719.84 4502.58 151.81 o 3 0 0 242.19 156.65 18.34 o 4 0 0 762.28 630.26 29.03 o 5 0 0 19748.75 18862.86 332.39 o 7 0 0 55803.80 56096.89 945.53 o 8 0 0 8663.49 7220.52 156.11 o 9 0 0 24589.74 25015.13 451.97 o 10 0 0 14363.50 15348.89 299.07 o 11 0 0 1554.68 1446.89 67.40 o 12 0 0 2309.61 2500.49 114.86 o 13 0 0 1097.16 1246.89 71.01 o 14 0 0 3183.83 3077.11 110.06 o 15 0 0 1314.70 1353.83 92.69 o 16 0 0 15.08 60.19 45.54 o 17 0 0 417.83 277.50 60.48 o 18 0 0 438.13 384.07 71.06 o 19 0 0 282.58 204.18 63.70 o 20 0 0 621.30 593.13 85.80 o 21 0 0 21.71 37.86 60.77 o 22 0 0 5.68 28.44 64.69 o 1 1 0 25.84 32.63 7.87 o 2 1 0 436.81 625.08 29.70 o 3 1 0 11332.08 12409.91 144.60 o 4 1 0 90575.88 98943.29 1442.18 o 5 1 0 544.36 534.72 26.69 o 6 1 0 14393.98 15540.55 199.90 o 7 1 0 0.68 13.27 14.67 o 8 1 0 1477.98 1667.37 60.19 o 9 1 0 295.59 279.45 23.81 o 10 1 0 1560.08 1605.83 47.71 o 11 1 0 584.39 598.93 33.75 o 12 1 0 565.32 644.99 36.62 o 13 1 0 184.40 222.36 29.25 o 14 1 0 477.82 497.20 37.58 o 15 1 0 910.61 927.18 52.01 o 16 1 0 9.41 28.01 31.21 o 17 1 0 289.92 281.01 44.10 o 18 1 0 736.98 945.57 69.45 o 19 1 0 756.86 653.11 59.27 o 20 1 0 149.67 153.21 44.45 o 21 1 0 114.62 144.25 47.35 o 22 1 0 117.60 172.53 50.15 o 0 2 0 22294.28 20664.77 314.30 o 1 2 0 2517.36 2333.90 33.05 o 2 2 0 42.39 144.05 9.44 o 3 2 0 24402.37 24036.80 306.70 o 4 2 0 1206.36 1178.18 33.23 o 5 2 0 4213.08 4359.04 61.97 o 6 2 0 3732.46 3356.99 54.01 o 7 2 0 2891.45 2994.39 71.07 o 8 2 0 5256.99 5895.05 95.22 o 9 2 0 160.91 83.84 18.90 o 10 2 0 6514.97 6149.54 104.17 o 11 2 0 16.25 73.94 20.90 o 12 2 0 3016.84 2566.47 65.37 o 13 2 0 933.75 912.96 44.32 o 14 2 0 2596.32 2691.93 86.47 o 15 2 0 401.22 388.16 39.40 o 16 2 0 3499.31 3007.08 96.62 o 17 2 0 110.70 131.90 52.58 o 18 2 0 1302.39 1118.01 69.60 o 19 2 0 2819.31 3004.42 137.63 o 20 2 0 334.69 444.01 55.37 o 21 2 0 1100.25 1131.52 78.10 o 22 2 0 1850.72 2089.83 101.53 o 1 3 0 112901.20 115237.34 1206.65 o 2 3 0 592.67 712.88 18.52 o 3 3 0 15078.73 19203.02 233.29 o 4 3 0 1205.20 1111.38 26.45 o 5 3 0 2745.64 2438.48 40.66 o 6 3 0 3153.80 3022.87 48.64 o 7 3 0 15.58 7.06 14.15 o 8 3 0 13654.31 14475.87 195.97 o 9 3 0 1848.16 1793.24 48.57 o 10 3 0 307.54 511.19 30.45 o 11 3 0 11.12 45.03 19.79 o 12 3 0 448.60 524.75 34.84 o 13 3 0 41.33 66.06 23.68 o 14 3 0 955.40 821.73 48.29 o 15 3 0 826.17 892.89 52.50 o 16 3 0 1855.87 1841.04 89.98 o 17 3 0 196.58 201.27 40.46 o 18 3 0 1559.65 1572.31 81.68 o 19 3 0 43.02 24.08 41.95 o 20 3 0 49.87 36.57 41.73 o 21 3 0 607.18 606.83 64.38 o 22 3 0 0.99 72.34 53.76 o 0 4 0 7167.48 6445.52 107.82 o 1 4 0 1621.70 1973.83 32.33 o 2 4 0 8041.10 9017.86 107.91 o 3 4 0 39.97 51.13 11.18 o 4 4 0 79.93 63.42 13.08 o 5 4 0 13773.33 13412.12 157.35 o 6 4 0 468.93 343.71 21.18 o 7 4 0 2661.04 2342.60 46.61 o 8 4 0 355.57 357.74 22.01 o 9 4 0 32.38 0.89 14.89 o 10 4 0 3331.95 3479.76 85.21 o 11 4 0 144.58 172.43 27.00 o 12 4 0 16034.68 15933.74 227.54 o 13 4 0 675.14 669.69 47.39 o 14 4 0 254.58 243.35 34.47 o 15 4 0 1498.59 1495.33 64.03 o 16 4 0 4229.13 4441.15 131.30 o 17 4 0 4596.70 4627.68 126.33 o 18 4 0 5.19 -21.44 32.94 o 19 4 0 44.60 12.37 37.89 o 20 4 0 23.23 -1.82 39.96 o 21 4 0 2232.57 2172.31 138.61 o 22 4 0 794.72 777.17 91.36 o 1 5 0 24332.65 26852.06 281.16 o 2 5 0 37.87 87.63 12.95 o 3 5 0 3079.18 2739.30 43.81 o 4 5 0 14.11 5.36 10.86 o 5 5 0 0.20 6.09 12.86 o 6 5 0 786.63 1049.76 32.60 o 7 5 0 4505.59 4512.87 75.98 o 8 5 0 784.53 787.15 32.48 o 9 5 0 312.69 324.74 28.51 o 10 5 0 258.34 180.49 23.87 o 11 5 0 81.31 70.91 20.63 o 12 5 0 0.39 -21.04 21.81 o 13 5 0 113.78 128.51 30.11 o 14 5 0 989.56 1158.44 55.92 o 15 5 0 26.98 15.54 27.94 o 16 5 0 3160.87 3169.82 102.13 o 17 5 0 426.37 474.53 51.36 o 18 5 0 118.44 144.86 41.41 o 19 5 0 139.89 95.94 39.59 o 20 5 0 60.92 97.43 42.16 o 21 5 0 10.15 -42.40 51.27 o 0 6 0 2068.50 1564.39 48.84 o 1 6 0 1127.68 1002.24 25.90 o 2 6 0 27030.79 27985.53 295.97 o 3 6 0 1867.39 2222.62 42.47 o 4 6 0 3788.60 4039.99 60.41 o 5 6 0 23942.52 23489.63 255.18 o 6 6 0 1314.45 1395.16 38.42 o 7 6 0 16673.93 16451.10 200.41 o 8 6 0 31.02 11.50 16.75 o 9 6 0 1042.22 1093.21 43.00 o 10 6 0 5.98 15.43 18.20 o 11 6 0 6874.92 6434.97 117.22 o 12 6 0 5963.99 5913.11 113.14 o 13 6 0 5417.52 5113.43 118.01 o 14 6 0 78.06 50.92 28.11 o 15 6 0 30.93 2.78 28.90 o 16 6 0 1139.79 1165.55 76.10 o 17 6 0 549.59 510.45 54.14 o 18 6 0 1520.36 1704.42 85.03 o 19 6 0 88.62 87.96 45.53 o 20 6 0 1529.10 1349.53 105.78 o 21 6 0 1573.92 1417.33 111.16 o 1 7 0 1224.53 1394.12 36.66 o 2 7 0 117.18 170.51 16.88 o 3 7 0 143.94 163.67 17.10 o 4 7 0 4119.84 4469.53 66.94 o 5 7 0 1976.62 2269.96 44.85 o 6 7 0 163.57 280.07 20.53 o 7 7 0 225.53 350.39 22.78 o 8 7 0 469.54 529.69 29.56 o 9 7 0 870.24 773.49 37.91 o 10 7 0 3815.68 4012.50 82.92 o 11 7 0 1476.69 1381.76 60.84 o 12 7 0 559.83 547.75 39.19 o 13 7 0 225.07 207.55 31.01 o 14 7 0 370.15 317.66 38.07 o 15 7 0 677.47 676.84 51.47 o 16 7 0 473.17 588.37 54.08 o 17 7 0 1.10 -26.12 34.79 o 18 7 0 25.57 -37.70 44.01 o 19 7 0 682.15 587.92 80.48 o 20 7 0 268.23 360.63 70.32 o 0 8 0 2777.83 2129.25 64.52 o 1 8 0 90.43 290.40 20.71 o 2 8 0 670.72 920.40 28.70 o 3 8 0 582.43 630.78 26.82 o 4 8 0 3498.54 3464.87 58.98 o 5 8 0 16997.81 16129.61 187.84 o 6 8 0 69.16 98.26 17.77 o 7 8 0 7227.78 6784.31 102.84 o 8 8 0 5.54 21.96 20.34 o 9 8 0 199.85 248.58 28.86 o 10 8 0 747.61 812.82 43.50 o 11 8 0 1127.65 1236.92 50.82 o 12 8 0 3984.50 4080.23 89.71 o 13 8 0 688.96 681.09 43.39 o 14 8 0 844.95 835.81 52.14 o 15 8 0 1053.88 1194.02 64.40 o 16 8 0 295.25 305.70 50.03 o 17 8 0 3679.45 3788.95 149.70 o 18 8 0 478.03 493.55 71.76 o 19 8 0 131.08 226.56 63.39 o 20 8 0 395.77 352.58 72.38 o 1 9 0 2255.45 2454.52 52.04 o 2 9 0 129.62 177.41 20.19 o 3 9 0 1656.95 1693.96 70.97 o 4 9 0 8.43 51.32 17.52 o 5 9 0 249.72 304.17 26.07 o 6 9 0 3314.96 3287.74 70.34 o 7 9 0 1938.20 1745.51 62.30 o 8 9 0 1700.25 1665.90 53.79 o 9 9 0 691.38 720.60 40.28 o 10 9 0 1.12 28.04 24.03 o 11 9 0 2.93 -11.14 24.42 o 12 9 0 713.60 701.00 45.13 o 13 9 0 201.88 262.02 44.67 o 14 9 0 224.09 315.67 42.72 o 15 9 0 32.72 18.76 36.25 o 16 9 0 891.85 996.20 88.31 o 17 9 0 411.95 414.57 66.49 o 18 9 0 66.82 67.04 54.64 o 19 9 0 119.53 217.57 66.61 o 0 10 0 7677.59 7502.05 155.18 o 1 10 0 387.83 446.20 28.97 o 2 10 0 145.97 164.03 23.32 o 3 10 0 1966.51 2019.00 57.71 o 4 10 0 271.83 374.78 29.56 o 5 10 0 6021.35 5878.50 102.56 o 6 10 0 196.96 298.71 29.08 o 7 10 0 311.85 240.14 31.19 o 8 10 0 195.79 156.30 40.73 o 9 10 0 2607.02 2737.00 76.54 o 10 10 0 2698.65 2611.63 94.97 o 11 10 0 1330.27 1483.84 62.46 o 12 10 0 11.27 5.69 29.87 o 13 10 0 5.66 -29.24 29.80 o 14 10 0 1788.03 1687.32 84.85 o 15 10 0 3669.65 3876.09 136.96 o 16 10 0 135.00 80.04 78.11 o 17 10 0 914.82 988.84 97.76 o 18 10 0 397.40 369.51 74.10 o 1 11 0 654.12 726.44 46.61 o 2 11 0 149.72 183.20 28.80 o 3 11 0 1153.83 1023.80 48.67 o 4 11 0 2921.65 2874.25 80.25 o 5 11 0 2489.92 2580.31 70.41 o 6 11 0 1642.15 1464.26 55.81 o 7 11 0 1659.08 1671.30 60.80 o 8 11 0 604.56 537.97 41.25 o 9 11 0 171.66 133.80 32.40 o 10 11 0 28.90 24.69 28.43 o 11 11 0 423.33 488.34 44.60 o 12 11 0 6717.60 6786.26 162.93 o 13 11 0 537.88 466.57 73.52 o 14 11 0 483.63 441.65 55.58 o 15 11 0 22.01 65.46 46.84 o 16 11 0 143.44 80.34 47.85 o 17 11 0 105.66 22.04 53.83 o 0 12 0 18119.80 17732.93 410.21 o 1 12 0 73.21 34.14 26.87 o 2 12 0 1292.83 1278.95 55.47 o 3 12 0 5.63 2.34 25.67 o 4 12 0 1144.16 1190.08 52.16 o 5 12 0 7813.90 8002.32 142.38 o 6 12 0 401.53 467.44 39.76 o 7 12 0 1647.41 1431.66 60.02 o 8 12 0 1706.20 1561.05 64.04 o 9 12 0 5844.90 5593.92 120.56 o 10 12 0 135.83 140.59 34.81 o 11 12 0 555.35 505.20 55.79 o 12 12 0 835.27 925.62 72.59 o 13 12 0 468.07 603.14 66.85 o 14 12 0 283.72 213.58 54.07 o 15 12 0 391.51 483.78 68.04 o 16 12 0 1025.48 1325.62 97.93 o 1 13 0 17.35 115.93 31.61 o 2 13 0 0.55 79.12 32.68 o 3 13 0 205.02 225.77 35.94 o 4 13 0 445.11 483.47 47.60 o 5 13 0 339.22 268.21 36.76 o 6 13 0 40.91 117.08 31.26 o 7 13 0 60.13 124.34 33.56 o 8 13 0 695.12 779.64 52.79 o 9 13 0 0.17 42.43 34.64 o 10 13 0 331.66 392.25 55.65 o 11 13 0 42.77 29.20 40.80 o 12 13 0 646.42 690.14 71.46 o 13 13 0 7.31 -48.10 41.28 o 14 13 0 778.02 617.16 83.93 o 15 13 0 14.78 35.80 50.64 o 0 14 0 2415.97 2181.00 117.13 o 1 14 0 108.44 110.22 34.08 o 2 14 0 894.61 864.88 58.69 o 3 14 0 234.33 166.68 36.03 o 4 14 0 600.02 717.64 52.74 o 5 14 0 19.37 -26.00 28.72 o 6 14 0 54.44 38.05 35.67 o 7 14 0 1645.49 1513.95 79.45 o 8 14 0 761.36 722.08 98.48 o 9 14 0 412.13 442.67 71.28 o 10 14 0 868.69 1026.46 88.12 o 11 14 0 28.57 27.00 43.66 o 12 14 0 1117.57 1184.43 100.92 o 13 14 0 88.85 106.74 59.03 o 1 15 0 151.10 102.67 38.44 o 2 15 0 429.61 404.49 49.17 o 3 15 0 246.99 218.59 43.75 o 4 15 0 108.76 38.19 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12973.13 13037.42 182.68 o -9 1 1 8792.83 10074.65 144.92 o -8 1 1 3976.69 3425.51 63.78 o -7 1 1 318.22 349.51 22.34 o -6 1 1 16162.42 15888.14 215.83 o -5 1 1 39391.49 39617.94 467.88 o -4 1 1 650.99 1059.96 25.90 o -3 1 1 1892.86 1638.93 28.81 o -2 1 1 17018.06 19732.33 293.00 o -1 1 1 21580.86 22244.21 379.34 o 0 1 1 102.75 185.15 14.01 o 1 1 1 18162.46 19952.02 269.55 o 2 1 1 6110.24 4947.69 63.23 o 3 1 1 2502.72 2110.08 37.89 o 4 1 1 13720.95 12675.62 205.50 o 5 1 1 10514.59 9692.87 131.71 o 6 1 1 1114.86 756.11 28.47 o 7 1 1 1216.95 988.12 33.31 o 8 1 1 21602.89 20538.70 308.31 o 9 1 1 10.46 57.66 18.62 o 10 1 1 10369.24 9457.62 145.03 o 11 1 1 1382.54 1471.25 50.43 o 12 1 1 359.10 458.62 33.76 o 13 1 1 7148.93 6549.12 119.32 o 14 1 1 4609.17 4147.41 102.94 o 15 1 1 6075.23 6050.70 141.56 o 16 1 1 690.30 778.37 57.62 o 17 1 1 196.45 303.17 45.93 o 18 1 1 1326.18 1327.77 131.63 o 19 1 1 11.28 2.72 36.95 o 20 1 1 784.39 841.75 70.00 o 21 1 1 4.32 48.54 43.75 o 22 1 1 66.70 38.35 55.36 o -23 2 1 464.93 570.29 72.72 o -22 2 1 104.42 149.48 57.16 o -21 2 1 1.08 26.05 40.49 o -20 2 1 555.29 636.37 61.01 o -19 2 1 1473.81 1561.97 80.15 o -18 2 1 41.50 21.40 34.31 o -17 2 1 2520.90 2416.89 88.34 o -16 2 1 642.65 598.58 50.00 o -15 2 1 314.15 301.55 35.52 o -14 2 1 32.75 -34.81 21.96 o -13 2 1 1572.11 1566.25 52.90 o -12 2 1 88.92 58.94 21.27 o -11 2 1 4775.61 5064.19 91.98 o -10 2 1 4606.65 5172.77 101.50 o -9 2 1 740.26 752.43 31.33 o -8 2 1 5007.68 4953.09 81.77 o -7 2 1 31843.93 34530.95 394.01 o -6 2 1 6363.28 6159.84 86.34 o -5 2 1 11446.48 11431.78 139.77 o -4 2 1 2856.27 3306.18 49.45 o -3 2 1 749.31 524.78 15.07 o -2 2 1 0.43 88.58 7.84 o -1 2 1 5715.17 7270.94 87.51 o 0 2 1 319.55 585.60 21.36 o 1 2 1 9406.84 9135.84 121.34 o 2 2 1 15086.39 15937.02 173.08 o 3 2 1 42421.21 40134.79 421.75 o 4 2 1 4546.75 4836.31 65.83 o 5 2 1 1805.27 1601.71 34.75 o 6 2 1 709.70 524.59 23.47 o 7 2 1 288.62 537.17 34.70 o 8 2 1 9534.41 10435.77 150.20 o 9 2 1 1107.61 1470.16 45.05 o 10 2 1 4685.82 4654.73 87.89 o 11 2 1 3618.90 3693.56 79.01 o 12 2 1 304.41 422.69 33.45 o 13 2 1 1555.32 1475.07 54.41 o 14 2 1 772.10 663.55 46.23 o 15 2 1 803.08 737.42 65.77 o 16 2 1 38.01 91.85 35.39 o 17 2 1 34.94 47.32 34.95 o 18 2 1 77.04 36.92 43.78 o 19 2 1 4.96 -18.90 36.52 o 20 2 1 174.81 77.66 42.85 o 21 2 1 26.64 11.93 46.11 o 22 2 1 73.00 44.59 52.81 o -23 3 1 344.76 336.58 64.96 o -22 3 1 3068.09 2891.56 128.52 o -21 3 1 85.92 15.93 39.74 o -20 3 1 4058.95 3737.15 120.54 o -19 3 1 241.04 264.40 44.33 o -18 3 1 219.91 200.39 40.09 o -17 3 1 3013.00 2889.35 133.84 o -16 3 1 210.55 265.20 39.80 o -15 3 1 9472.17 8565.28 158.31 o -14 3 1 1506.75 1858.64 64.54 o -13 3 1 1450.13 1136.26 50.54 o -12 3 1 36.02 -0.03 19.07 o -11 3 1 1072.96 971.28 39.11 o -10 3 1 12676.44 12591.31 177.90 o -9 3 1 5088.12 4883.15 80.41 o -8 3 1 283.83 149.73 21.30 o -7 3 1 15506.94 15785.79 220.18 o -6 3 1 257.33 243.68 18.01 o -5 3 1 117.50 169.83 15.86 o -4 3 1 12963.91 13087.86 149.26 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