#------------------------------------------------------------------------------ #$Date: 2016-04-03 05:04:48 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181220 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/99/2229986.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2229986_Fobs loop_ _publ_author_name 'Tafeenko, Viktor A.' 'Aslanov, Leonid A.' 'Puretskiy, Nikolay A.' 'Fedotov, Aleksander N.' 'Mochalov, Sergei S.' _publ_section_title ; rac-12,14-Dicyclopropyl-5,8,13,18,21-pentaoxapentacyclo[13.8.0.0^2,11^.0^4,9^.0^17,22^]tricosa-1(15),2(11),3,9(10),16,22(23)-hexaene ; _journal_coeditor_code GK2364 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1180 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.422 _cell_angle_gamma 90.000 _cell_length_a 14.3249 _cell_length_b 7.3927 _cell_length_c 19.7260 _exptl_crystal_F_000 832.00 _reflns_d_resolution_high 0.8211 _cod_data_source_file gk2364Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' molchan2a in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 321.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24651.05 22450.34 153.76 o 4 0 0 6813.19 6238.27 32.62 o 6 0 0 1371.66 1399.70 72.42 o 8 0 0 0.37 -3.70 15.10 o 10 0 0 195.30 177.34 16.88 o 12 0 0 109.04 84.73 17.98 o 14 0 0 3.68 6.55 17.75 o 16 0 0 8.66 -19.04 21.19 o 1 1 0 1989.41 1979.43 13.39 o 3 1 0 4982.89 4790.10 26.80 o 5 1 0 5928.25 5750.76 105.55 o 7 1 0 57.09 34.90 11.64 o 9 1 0 69.83 63.90 15.31 o 11 1 0 18.65 25.86 16.66 o 13 1 0 18.98 32.45 24.14 o 15 1 0 0.02 -19.07 19.07 o 0 2 0 1382.44 1619.12 25.38 o 2 2 0 5.64 10.28 10.31 o 4 2 0 9.20 -10.27 10.27 o 6 2 0 1977.67 1955.48 63.85 o 8 2 0 2175.28 1872.53 31.30 o 10 2 0 50.80 27.11 42.29 o 12 2 0 126.37 119.98 19.61 o 14 2 0 12.63 42.48 20.40 o 16 2 0 0.28 10.96 20.75 o 1 3 0 941.90 1080.50 18.65 o 3 3 0 1537.28 1617.71 34.51 o 5 3 0 1132.02 1210.72 30.35 o 7 3 0 2287.58 2264.10 56.24 o 9 3 0 189.55 210.93 19.03 o 11 3 0 272.83 297.97 22.32 o 13 3 0 3.36 21.91 18.35 o 15 3 0 10.01 40.55 21.17 o 0 4 0 60.11 62.91 19.15 o 2 4 0 0.07 7.38 13.56 o 4 4 0 455.78 456.38 19.56 o 6 4 0 15.32 -14.87 17.55 o 8 4 0 692.91 643.74 64.91 o 10 4 0 31.31 -9.18 19.18 o 12 4 0 0.01 15.20 18.92 o 14 4 0 14.32 20.84 20.82 o 1 5 0 195.31 168.23 20.03 o 3 5 0 903.21 870.02 26.52 o 5 5 0 1534.95 1559.72 43.89 o 7 5 0 108.14 127.88 51.89 o 9 5 0 18.76 30.18 18.49 o 11 5 0 0.39 -12.60 20.52 o 13 5 0 0.33 -8.20 20.32 o 0 6 0 2237.22 2373.75 57.86 o 2 6 0 25.43 51.15 28.84 o 4 6 0 294.32 264.91 23.53 o 6 6 0 9.27 26.33 19.22 o 8 6 0 12.75 3.22 19.98 o 10 6 0 10.99 27.77 20.39 o 12 6 0 11.63 37.64 39.07 o 1 7 0 3610.36 3546.43 90.58 o 3 7 0 111.14 105.93 22.93 o 5 7 0 13.08 14.41 24.12 o 7 7 0 12.20 -6.83 36.00 o 9 7 0 0.10 24.28 49.72 o 0 8 0 97.38 52.70 35.20 o 2 8 0 0.93 -23.31 23.31 o 4 8 0 37.90 19.28 23.68 o 6 8 0 200.01 183.13 27.44 o -15 1 1 0.00 -14.43 27.78 o -13 1 1 210.62 219.63 29.03 o -11 1 1 53.42 38.91 22.39 o -9 1 1 15.40 -14.56 20.67 o -7 1 1 477.70 428.76 22.35 o -5 1 1 5257.88 4843.41 47.12 o -3 1 1 25353.25 23389.51 164.83 o -1 1 1 2583.25 3039.05 22.91 o 1 1 1 760.68 761.86 14.49 o 3 1 1 6086.03 5613.86 42.58 o 5 1 1 1109.90 979.16 25.22 o 7 1 1 11.40 57.41 16.45 o 9 1 1 601.92 607.40 31.36 o 11 1 1 95.46 88.17 26.70 o 13 1 1 73.82 111.96 26.33 o 15 1 1 0.59 35.16 27.10 o -16 2 1 12.91 29.50 28.38 o -14 2 1 1.80 -13.65 26.60 o -12 2 1 437.75 511.43 35.62 o -10 2 1 454.79 523.60 32.90 o -8 2 1 1078.95 1085.22 33.73 o -6 2 1 161.26 158.04 18.65 o -4 2 1 1630.85 1744.30 30.09 o -2 2 1 1415.28 1364.15 24.95 o 0 2 1 2455.50 2559.13 30.44 o 2 2 1 981.24 1106.03 24.66 o 4 2 1 103.29 59.59 15.98 o 6 2 1 329.39 286.44 21.90 o 8 2 1 615.02 574.13 30.15 o 10 2 1 384.28 481.91 32.59 o 12 2 1 5.35 -25.52 25.52 o 14 2 1 37.03 47.57 27.58 o -15 3 1 1.47 69.85 24.54 o -13 3 1 0.28 8.83 26.09 o -11 3 1 63.57 92.24 25.45 o -9 3 1 538.09 526.46 33.85 o -7 3 1 510.05 479.44 28.35 o -5 3 1 362.83 320.38 22.37 o -3 3 1 1.42 36.27 15.14 o -1 3 1 200.10 203.29 18.18 o 1 3 1 3068.32 3174.61 41.55 o 3 3 1 586.49 694.00 26.99 o 5 3 1 1.71 16.89 19.99 o 7 3 1 164.69 171.08 24.75 o 9 3 1 1.81 11.19 24.10 o 11 3 1 302.77 333.50 32.48 o 13 3 1 39.84 36.85 29.23 o 15 3 1 0.23 10.79 29.93 o -14 4 1 13.18 21.68 27.41 o -12 4 1 0.21 20.87 26.80 o -10 4 1 555.78 554.60 37.76 o -8 4 1 1308.88 1242.81 43.60 o -6 4 1 513.02 508.90 29.83 o -4 4 1 66.70 88.54 21.24 o -2 4 1 552.66 628.68 27.21 o 0 4 1 483.45 535.41 26.16 o 2 4 1 108.53 126.52 22.90 o 4 4 1 12.02 -3.67 25.35 o 6 4 1 299.46 305.07 30.02 o 8 4 1 12.88 25.52 26.09 o 10 4 1 16.79 -0.98 27.31 o 12 4 1 148.87 207.09 33.99 o 14 4 1 77.73 123.39 33.55 o -13 5 1 80.48 70.83 30.95 o -11 5 1 349.00 330.00 37.51 o -9 5 1 1.33 -16.75 25.55 o -7 5 1 0.00 14.77 25.75 o -5 5 1 862.17 855.56 37.86 o -3 5 1 938.88 984.55 37.12 o -1 5 1 230.11 272.25 27.35 o 1 5 1 432.67 441.87 30.34 o 3 5 1 5.79 22.79 26.50 o 5 5 1 30.21 0.00 29.06 o 7 5 1 355.91 270.19 33.33 o 9 5 1 305.41 336.46 35.78 o 11 5 1 86.37 126.06 31.59 o 13 5 1 0.47 -34.11 34.11 o -12 6 1 9.51 -13.28 31.28 o -10 6 1 0.60 -16.55 27.88 o -8 6 1 0.38 -27.27 27.27 o -6 6 1 87.86 97.64 29.10 o -4 6 1 615.75 625.56 38.14 o -2 6 1 2742.98 2769.07 60.86 o 0 6 1 584.39 587.62 38.47 o 2 6 1 141.70 124.15 31.36 o 4 6 1 2.06 -9.78 28.96 o 6 6 1 90.19 53.14 31.86 o 8 6 1 9.90 50.26 31.42 o 10 6 1 5.40 -30.91 30.91 o 12 6 1 53.32 78.28 36.14 o -9 7 1 4.48 11.43 29.23 o -7 7 1 19.68 -10.42 29.26 o -5 7 1 9.13 3.24 30.14 o -3 7 1 3.12 -12.27 31.38 o -1 7 1 0.03 -1.01 32.40 o 1 7 1 122.04 136.28 34.90 o 3 7 1 584.60 564.37 40.93 o 5 7 1 53.68 50.74 32.47 o 7 7 1 96.23 111.90 35.43 o 9 7 1 2.10 33.20 32.56 o -6 8 1 308.00 304.94 41.65 o -4 8 1 507.96 433.93 43.08 o -2 8 1 16.22 13.01 31.59 o 0 8 1 2.83 37.55 31.92 o 2 8 1 2.61 3.54 33.85 o 4 8 1 21.81 39.00 35.09 o 6 8 1 68.30 99.25 35.57 o -16 0 2 144.12 170.81 33.95 o -14 0 2 62.04 46.12 26.16 o -12 0 2 108.29 85.14 26.70 o -10 0 2 1618.44 1464.19 42.96 o -8 0 2 847.32 753.18 28.65 o -6 0 2 192.65 218.76 16.90 o -4 0 2 103621.97 113366.52 432.08 o -2 0 2 17878.70 16591.30 106.98 o 0 0 2 40.87 33.29 6.31 o 2 0 2 6514.70 5698.51 36.23 o 4 0 2 1385.94 1256.82 25.57 o 6 0 2 1062.00 1007.35 28.24 o 8 0 2 952.81 794.30 32.67 o 10 0 2 48.33 95.91 22.59 o 12 0 2 235.82 279.70 29.88 o 14 0 2 9.22 36.31 27.10 o -15 1 2 5.47 -18.91 27.54 o -13 1 2 36.98 31.69 26.16 o -11 1 2 273.05 253.00 28.16 o -9 1 2 1313.45 1240.76 37.37 o -7 1 2 408.69 449.81 22.75 o -5 1 2 1309.84 1152.84 25.79 o -3 1 2 39700.45 38904.82 218.93 o -1 1 2 1810.10 1908.52 19.93 o 1 1 2 48658.38 53623.60 233.73 o 3 1 2 252.49 208.49 16.07 o 5 1 2 40.41 22.22 14.77 o 7 1 2 7.11 29.19 16.82 o 9 1 2 158.44 156.74 25.33 o 11 1 2 5.74 -13.48 23.90 o 13 1 2 30.05 37.96 24.61 o 15 1 2 3.35 19.28 29.63 o -16 2 2 13.74 -3.94 28.45 o -14 2 2 46.34 41.43 27.31 o -12 2 2 252.60 267.34 30.52 o -10 2 2 768.24 722.23 35.42 o -8 2 2 433.43 407.15 26.05 o -6 2 2 1838.08 1710.76 35.22 o -4 2 2 34.38 42.24 14.83 o -2 2 2 1112.77 1049.82 22.95 o 0 2 2 4100.16 4644.07 40.04 o 2 2 2 6362.63 6888.66 52.34 o 4 2 2 2601.00 2577.66 38.74 o 6 2 2 31.91 14.63 18.68 o 8 2 2 610.06 620.88 32.03 o 10 2 2 70.71 92.14 26.50 o 12 2 2 43.78 42.11 25.89 o 14 2 2 7.86 -1.21 29.19 o -15 3 2 4.99 -27.64 27.64 o -13 3 2 9.05 -3.27 25.72 o -11 3 2 168.43 156.02 26.54 o -9 3 2 0.25 26.83 22.52 o -7 3 2 611.62 540.03 27.85 o -5 3 2 65.86 58.06 16.93 o -3 3 2 1569.65 1636.26 32.09 o -1 3 2 725.98 794.64 23.80 o 1 3 2 1600.27 1493.90 30.85 o 3 3 2 8113.80 9186.78 73.41 o 5 3 2 6153.28 6183.66 68.41 o 7 3 2 127.93 130.09 24.51 o 9 3 2 189.51 195.29 28.23 o 11 3 2 19.14 25.01 26.63 o 13 3 2 22.62 4.72 29.53 o -14 4 2 17.47 15.10 28.92 o -12 4 2 1.15 -27.31 27.31 o -10 4 2 243.99 227.03 31.47 o -8 4 2 231.52 216.82 26.64 o -6 4 2 48.06 42.41 20.67 o -4 4 2 4.69 -3.61 18.95 o -2 4 2 242.99 284.27 23.31 o 0 4 2 457.45 481.02 26.56 o 2 4 2 6.72 2.80 21.47 o 4 4 2 3097.27 3454.26 56.48 o 6 4 2 64.86 42.04 26.90 o 8 4 2 179.95 106.46 31.80 o 10 4 2 88.98 103.57 28.22 o 12 4 2 0.30 -28.59 28.59 o 14 4 2 39.64 -17.60 34.93 o -13 5 2 3.12 -3.81 27.24 o -11 5 2 28.42 2.22 26.46 o -9 5 2 92.56 84.83 26.77 o -7 5 2 779.12 823.13 38.82 o -5 5 2 461.50 482.92 32.93 o -3 5 2 553.83 618.46 33.14 o -1 5 2 9.16 10.92 24.91 o 1 5 2 168.27 177.65 30.28 o 3 5 2 113.28 89.96 29.03 o 5 5 2 13.80 12.78 29.43 o 7 5 2 53.55 73.66 27.64 o 9 5 2 0.44 43.96 26.16 o 11 5 2 3.76 11.90 30.14 o 13 5 2 18.52 16.35 32.50 o -12 6 2 0.26 -9.20 29.83 o -10 6 2 10.46 -8.19 28.65 o -8 6 2 328.97 381.60 33.42 o -6 6 2 5.34 -1.89 26.02 o -4 6 2 2364.57 2407.97 59.08 o -2 6 2 1131.93 1129.09 43.65 o 0 6 2 576.96 556.87 36.21 o 2 6 2 694.90 683.08 39.05 o 4 6 2 28.65 -9.00 29.90 o 6 6 2 20.04 58.93 31.18 o 8 6 2 19.77 58.76 30.27 o 10 6 2 5.85 42.64 32.80 o -9 7 2 42.61 -30.21 30.68 o -7 7 2 55.64 -9.20 31.86 o -5 7 2 876.72 822.35 46.99 o -3 7 2 1415.84 1300.24 52.34 o -1 7 2 320.07 359.58 36.29 o 1 7 2 120.76 129.37 33.65 o 3 7 2 23.93 37.08 31.01 o 5 7 2 1.52 -31.45 31.45 o 7 7 2 2.11 4.72 33.24 o 9 7 2 4.93 14.26 34.32 o -6 8 2 0.32 0.00 32.46 o -4 8 2 0.56 -33.00 33.00 o -2 8 2 62.19 22.52 32.50 o 0 8 2 69.58 91.94 32.40 o 2 8 2 114.13 46.16 34.86 o 4 8 2 65.07 68.91 35.20 o 6 8 2 43.89 28.69 37.18 o -15 1 3 107.37 166.86 30.88 o -13 1 3 104.29 80.08 26.40 o -11 1 3 38.26 64.19 24.34 o -9 1 3 599.25 547.20 28.56 o -7 1 3 6265.85 6017.10 61.90 o -5 1 3 748.31 602.01 20.52 o -3 1 3 78.65 140.57 13.79 o -1 1 3 1891.64 1796.57 21.30 o 1 1 3 4285.20 4078.98 33.65 o 3 1 3 509.76 441.46 18.31 o 5 1 3 0.43 -12.57 14.70 o 7 1 3 3.15 24.81 17.60 o 9 1 3 2.53 -21.30 21.30 o 11 1 3 110.70 82.77 28.09 o 13 1 3 11.36 -12.27 26.53 o 15 1 3 1.05 -5.29 27.68 o -16 2 3 19.84 -31.05 31.05 o -14 2 3 0.76 9.94 25.01 o -12 2 3 355.82 318.66 31.71 o -10 2 3 192.86 222.10 26.20 o -8 2 3 3338.44 3184.24 53.54 o -6 2 3 2472.44 2311.33 39.27 o -4 2 3 39.58 63.99 15.17 o -2 2 3 1608.23 1641.25 27.11 o 0 2 3 4161.87 4815.34 42.19 o 2 2 3 4103.85 4220.92 43.30 o 4 2 3 607.57 701.36 25.10 o 6 2 3 991.91 988.95 32.48 o 8 2 3 12.20 46.12 21.74 o 10 2 3 187.97 147.40 28.90 o 12 2 3 4.95 47.60 26.97 o 14 2 3 1.96 81.28 26.83 o -15 3 3 0.08 7.55 27.24 o -13 3 3 0.36 11.80 24.37 o -11 3 3 98.85 88.91 26.33 o -9 3 3 602.79 586.96 33.65 o -7 3 3 96.11 92.15 22.05 o -5 3 3 176.23 171.44 20.64 o -3 3 3 524.80 545.64 22.66 o -1 3 3 269.45 304.66 20.28 o 1 3 3 166.41 188.51 20.07 o 3 3 3 0.66 -20.29 20.29 o 5 3 3 245.85 311.58 24.02 o 7 3 3 82.95 91.67 25.12 o 9 3 3 36.57 6.81 25.45 o 11 3 3 11.22 10.28 27.10 o 13 3 3 96.17 153.67 32.37 o -14 4 3 1.65 1.25 27.64 o -12 4 3 133.95 141.65 28.93 o -10 4 3 640.85 626.61 37.29 o -8 4 3 377.67 335.94 30.43 o -6 4 3 4.14 21.84 20.77 o -4 4 3 538.95 673.07 28.29 o -2 4 3 55.98 73.26 19.66 o 0 4 3 1900.29 2110.61 42.29 o 2 4 3 349.95 304.31 25.37 o 4 4 3 139.45 161.15 27.69 o 6 4 3 339.63 364.39 32.38 o 8 4 3 2.64 34.79 25.25 o 10 4 3 166.79 167.15 30.85 o 12 4 3 87.15 133.14 32.26 o -13 5 3 6.76 61.72 26.77 o -11 5 3 18.06 9.94 27.47 o -9 5 3 424.29 371.28 34.71 o -7 5 3 2282.38 2126.95 55.89 o -5 5 3 1164.71 1179.98 40.95 o -3 5 3 100.42 105.17 26.94 o -1 5 3 39.69 20.80 25.86 o 1 5 3 192.36 151.19 29.31 o 3 5 3 34.59 72.01 28.59 o 5 5 3 3.88 -4.92 27.64 o 7 5 3 294.48 297.55 34.74 o 9 5 3 10.91 24.07 28.18 o 11 5 3 21.11 7.32 31.45 o -12 6 3 14.12 -23.50 29.29 o -10 6 3 36.56 20.94 28.49 o -8 6 3 155.05 192.57 29.74 o -6 6 3 214.67 174.11 31.83 o -4 6 3 96.24 92.21 29.33 o -2 6 3 4.94 16.18 29.19 o 0 6 3 82.30 77.92 29.87 o 2 6 3 10.85 -23.29 29.46 o 4 6 3 204.20 154.35 33.01 o 6 6 3 37.60 106.23 29.53 o 8 6 3 103.53 148.85 33.48 o 10 6 3 3.99 36.04 32.19 o -9 7 3 8.28 25.05 29.80 o -7 7 3 22.96 -2.29 30.27 o -5 7 3 387.17 352.59 38.49 o -3 7 3 173.81 172.64 33.58 o -1 7 3 104.93 107.96 31.83 o 1 7 3 22.55 12.07 30.58 o 3 7 3 30.85 24.04 32.16 o 5 7 3 4.28 33.34 31.72 o 7 7 3 17.36 26.46 33.68 o 9 7 3 13.77 -36.71 36.71 o -6 8 3 56.03 56.37 31.29 o -4 8 3 25.29 3.67 34.22 o -2 8 3 3.49 -3.57 32.43 o 0 8 3 0.82 -32.29 32.29 o 2 8 3 61.18 49.02 34.25 o 4 8 3 27.49 11.23 34.72 o 6 8 3 10.23 15.88 37.89 o -16 0 4 118.84 179.06 29.70 o -14 0 4 66.81 104.65 24.68 o -12 0 4 77.26 97.91 25.29 o -10 0 4 140.71 116.40 21.99 o -8 0 4 4502.86 4157.55 56.11 o -6 0 4 4074.74 4168.11 46.25 o -4 0 4 2437.45 2138.18 29.11 o -2 0 4 18857.02 17040.11 129.17 o 0 0 4 4718.05 4692.61 33.22 o 2 0 4 8629.83 7981.93 52.06 o 4 0 4 45.36 69.08 13.22 o 6 0 4 45.00 40.15 17.70 o 8 0 4 136.78 121.87 23.64 o 10 0 4 160.72 208.12 26.77 o 12 0 4 37.59 38.60 27.44 o 14 0 4 25.15 49.62 27.78 o -17 1 4 4.73 8.16 28.65 o -15 1 4 82.83 106.20 29.70 o -13 1 4 77.31 84.12 26.53 o -11 1 4 95.32 114.60 24.65 o -9 1 4 248.79 224.44 23.78 o -7 1 4 5835.60 5520.02 59.65 o -5 1 4 3797.14 3710.88 41.71 o -3 1 4 1608.68 1520.13 24.07 o -1 1 4 6395.79 6194.85 41.17 o 1 1 4 4047.96 4221.94 37.13 o 3 1 4 4703.65 4123.67 43.48 o 5 1 4 575.98 491.38 23.37 o 7 1 4 548.04 528.34 27.95 o 9 1 4 17.96 46.62 21.88 o 11 1 4 8.38 40.49 23.83 o 13 1 4 0.05 -27.44 27.44 o 15 1 4 25.53 -17.63 31.69 o -16 2 4 1.00 -11.60 28.32 o -14 2 4 36.19 20.80 26.16 o -12 2 4 274.74 246.07 30.83 o -10 2 4 171.17 148.65 27.79 o -8 2 4 408.57 411.38 26.15 o -6 2 4 428.08 412.04 22.11 o -4 2 4 2326.67 2301.95 34.52 o -2 2 4 6171.13 6354.50 50.34 o 0 2 4 1160.88 1371.96 26.43 o 2 2 4 215.48 188.86 17.44 o 4 2 4 5206.72 5178.09 56.34 o 6 2 4 40.06 60.08 19.05 o 8 2 4 81.22 46.70 24.92 o 10 2 4 1.99 29.29 24.27 o 12 2 4 17.73 29.46 27.85 o 14 2 4 56.39 14.16 30.34 o -15 3 4 9.45 19.96 27.61 o -13 3 4 200.08 276.78 32.71 o -11 3 4 79.93 9.91 25.72 o -9 3 4 264.13 274.82 26.98 o -7 3 4 172.45 206.26 23.20 o -5 3 4 549.26 545.98 23.77 o -3 3 4 73.78 102.91 17.57 o -1 3 4 3116.79 3539.22 44.52 o 1 3 4 15565.92 18276.97 100.70 o 3 3 4 1740.62 1934.98 39.43 o 5 3 4 986.77 1063.23 34.84 o 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