#------------------------------------------------------------------------------ #$Date: 2011-07-04 21:24:21 +0300 (Mon, 04 Jul 2011) $ #$Revision: 22560 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230001.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230001_Fobs loop_ _publ_author_name 'Kamaludin, Nurul Farahana' 'Baba, Ibrahim' 'Awang, Normah' 'Mohamed Tahir, Mohamed Ibrahim' 'Tiekink, Edward R. T.' _publ_section_title ; (N-Butyl-N-phenyldithiocarbamato-\kS)triphenyltin(IV) ; _journal_coeditor_code HB5836 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m555 _journal_page_last m556 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.442 _cell_angle_gamma 90.000 _cell_length_a 10.0488 _cell_length_b 18.0008 _cell_length_c 15.2054 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file hb5836Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in space group P 1 21/n 1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 351.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 123502.72 121464.52 1254.50 o 4 0 0 13384.27 13466.28 159.90 o 6 0 0 310.69 312.24 17.11 o 8 0 0 6794.13 7216.82 127.61 o 10 0 0 813.13 861.99 60.36 o 12 0 0 565.52 663.02 138.61 o 1 1 0 20219.82 20283.99 246.89 o 2 1 0 2279.81 2399.82 22.23 o 3 1 0 35291.76 36303.26 255.47 o 4 1 0 43.94 66.59 5.08 o 5 1 0 5259.30 5244.44 58.09 o 6 1 0 86.44 109.11 8.03 o 7 1 0 6458.54 6625.51 76.87 o 8 1 0 41.56 39.47 8.07 o 9 1 0 639.56 585.41 26.83 o 10 1 0 105.51 78.68 13.23 o 11 1 0 2110.68 2097.68 62.73 o 12 1 0 87.43 63.31 20.52 o 0 2 0 87287.27 79350.98 1298.36 o 1 2 0 321.09 324.49 7.67 o 2 2 0 5380.64 5517.46 57.19 o 3 2 0 12686.06 13370.95 107.85 o 4 2 0 15254.49 15269.87 139.90 o 5 2 0 2720.28 2941.91 38.34 o 6 2 0 227.75 257.83 11.46 o 7 2 0 11.40 16.38 6.04 o 8 2 0 6073.45 6371.29 88.63 o 9 2 0 326.42 367.27 19.71 o 10 2 0 1387.74 1353.11 43.85 o 11 2 0 303.91 315.77 28.86 o 12 2 0 598.32 623.89 48.62 o 1 3 0 36659.60 36312.64 324.84 o 2 3 0 21.92 25.55 2.54 o 3 3 0 26315.93 26514.98 275.93 o 4 3 0 3125.34 3226.63 38.83 o 5 3 0 669.32 640.29 14.64 o 6 3 0 8.67 17.72 4.37 o 7 3 0 5609.31 5656.99 71.47 o 8 3 0 495.09 467.42 20.51 o 9 3 0 6.24 11.12 8.90 o 10 3 0 263.93 302.24 28.67 o 11 3 0 1057.10 1122.29 50.51 o 12 3 0 517.93 490.63 39.71 o 0 4 0 18700.29 18745.91 466.66 o 1 4 0 1129.91 1149.16 15.14 o 2 4 0 774.15 687.85 11.12 o 3 4 0 1890.24 1919.45 23.49 o 4 4 0 22848.17 22692.54 201.14 o 5 4 0 21.64 31.12 5.29 o 6 4 0 6496.98 6693.36 101.22 o 7 4 0 199.84 172.69 12.70 o 8 4 0 663.95 652.38 24.37 o 9 4 0 1551.89 1566.06 43.28 o 10 4 0 1394.67 1480.38 47.59 o 11 4 0 266.09 321.87 29.25 o 12 4 0 292.53 247.42 38.22 o 1 5 0 3576.24 3465.55 55.64 o 2 5 0 463.45 419.48 8.83 o 3 5 0 9040.33 8922.43 75.17 o 4 5 0 988.31 1002.24 19.38 o 5 5 0 81.21 84.76 6.48 o 6 5 0 2205.26 2183.10 36.52 o 7 5 0 5785.69 5833.95 97.80 o 8 5 0 1572.30 1625.40 39.28 o 9 5 0 108.57 74.31 11.77 o 10 5 0 507.65 482.25 26.38 o 11 5 0 1728.19 1763.96 64.11 o 12 5 0 462.71 411.75 58.45 o 0 6 0 1698.87 1543.72 34.37 o 1 6 0 9126.92 9226.93 139.34 o 2 6 0 547.22 572.76 13.01 o 3 6 0 14.55 13.31 3.04 o 4 6 0 8266.05 8167.30 79.00 o 5 6 0 453.74 483.80 14.43 o 6 6 0 3608.17 3622.45 55.99 o 7 6 0 487.56 480.21 18.79 o 8 6 0 1128.88 1115.08 31.03 o 9 6 0 1693.97 1712.44 44.80 o 10 6 0 770.46 788.10 34.10 o 11 6 0 54.64 54.17 19.52 o 12 6 0 304.58 304.58 42.88 o 1 7 0 7085.96 7147.16 91.98 o 2 7 0 4753.78 4577.73 46.93 o 3 7 0 13564.90 13748.24 132.06 o 4 7 0 158.18 172.09 7.80 o 5 7 0 2.71 11.07 3.77 o 6 7 0 6868.49 6862.93 78.91 o 7 7 0 1782.58 1796.23 52.43 o 8 7 0 885.45 879.85 30.13 o 9 7 0 77.06 69.03 14.52 o 10 7 0 651.28 581.62 39.30 o 11 7 0 1863.88 2081.87 106.27 o 12 7 0 141.12 192.89 47.75 o 0 8 0 2869.41 2744.12 62.70 o 1 8 0 10575.94 10377.25 103.86 o 2 8 0 7.39 6.36 3.21 o 3 8 0 1141.91 985.42 20.76 o 4 8 0 6242.02 6047.02 77.99 o 5 8 0 7549.59 7373.90 78.46 o 6 8 0 5434.36 5588.88 72.03 o 7 8 0 139.50 148.27 12.23 o 8 8 0 285.59 297.75 18.28 o 9 8 0 1403.17 1335.77 46.16 o 10 8 0 155.49 158.08 22.62 o 11 8 0 46.65 75.95 27.06 o 1 9 0 2712.09 2715.09 39.43 o 2 9 0 18175.34 18659.66 210.06 o 3 9 0 2268.29 2216.81 35.25 o 4 9 0 232.18 268.18 11.00 o 5 9 0 860.35 858.78 22.93 o 6 9 0 4898.15 5077.35 90.43 o 7 9 0 1298.92 1261.62 34.88 o 8 9 0 390.87 389.30 24.55 o 9 9 0 101.90 71.19 15.98 o 10 9 0 1066.86 1097.26 55.65 o 11 9 0 851.58 876.75 60.45 o 0 10 0 9573.79 9768.37 165.25 o 1 10 0 5905.10 5853.96 85.21 o 2 10 0 897.48 999.01 20.79 o 3 10 0 6388.73 6201.41 61.05 o 4 10 0 4248.18 4255.46 93.72 o 5 10 0 10098.77 10381.51 156.25 o 6 10 0 927.22 876.98 29.60 o 7 10 0 307.05 331.51 19.75 o 8 10 0 158.30 136.45 18.66 o 9 10 0 1022.25 995.55 46.35 o 10 10 0 113.01 100.47 20.76 o 11 10 0 313.24 369.71 40.55 o 1 11 0 4085.09 3876.96 66.54 o 2 11 0 14064.26 13946.08 151.03 o 3 11 0 4913.28 4858.80 51.79 o 4 11 0 1143.28 1153.37 26.10 o 5 11 0 172.20 181.62 12.66 o 6 11 0 4975.96 5021.58 95.33 o 7 11 0 1251.51 1228.99 47.95 o 8 11 0 490.36 526.48 33.82 o 9 11 0 195.89 233.94 23.88 o 10 11 0 1880.40 1990.18 88.22 o 11 11 0 338.69 292.76 62.64 o 0 12 0 10432.60 9920.56 206.94 o 1 12 0 3372.96 3244.98 61.81 o 2 12 0 938.85 914.56 24.51 o 3 12 0 5010.31 4954.58 55.81 o 4 12 0 1239.67 1256.88 33.39 o 5 12 0 7996.03 8000.63 155.87 o 6 12 0 366.11 354.91 22.24 o 7 12 0 60.44 54.16 13.48 o 8 12 0 1401.39 1305.33 53.67 o 9 12 0 1525.22 1455.81 73.98 o 10 12 0 29.79 32.80 30.19 o 1 13 0 1825.45 1784.62 49.71 o 2 13 0 10898.90 10741.40 164.51 o 3 13 0 1503.92 1556.52 34.96 o 4 13 0 1573.98 1611.28 35.80 o 5 13 0 1423.58 1403.86 41.48 o 6 13 0 3473.36 3608.02 95.94 o 7 13 0 901.41 897.85 47.77 o 8 13 0 1060.52 1105.76 55.23 o 9 13 0 385.19 334.96 37.76 o 10 13 0 873.72 788.24 66.00 o 0 14 0 8305.50 8338.07 163.26 o 1 14 0 1286.36 1248.01 38.35 o 2 14 0 618.96 555.46 25.49 o 3 14 0 934.98 955.72 27.99 o 4 14 0 704.59 656.16 26.90 o 5 14 0 5248.81 5341.86 120.69 o 6 14 0 2.68 -1.05 15.29 o 7 14 0 51.96 35.84 16.09 o 8 14 0 355.84 389.26 38.27 o 9 14 0 1808.65 1676.38 96.08 o 10 14 0 11.56 -0.44 47.11 o 1 15 0 511.24 485.81 24.67 o 2 15 0 1709.01 1635.04 47.35 o 3 15 0 1319.38 1242.35 35.59 o 4 15 0 458.59 391.13 34.83 o 5 15 0 109.87 120.60 21.44 o 6 15 0 2103.55 2104.59 83.71 o 7 15 0 369.86 382.95 52.47 o 8 15 0 1276.07 1318.63 70.62 o 9 15 0 49.68 103.18 32.29 o 0 16 0 81.73 88.29 18.55 o 1 16 0 3796.74 3952.57 79.21 o 2 16 0 1.49 -2.69 10.26 o 3 16 0 195.99 176.65 14.09 o 4 16 0 209.77 136.23 22.17 o 5 16 0 2476.37 2586.26 93.81 o 6 16 0 180.92 186.28 27.32 o 7 16 0 8.45 -1.03 18.16 o 8 16 0 204.39 293.12 48.17 o 9 16 0 1514.60 1572.73 168.00 o 1 17 0 87.62 88.10 13.08 o 2 17 0 1355.43 1412.45 45.54 o 3 17 0 10.28 -5.22 11.34 o 4 17 0 719.10 714.12 48.00 o 5 17 0 248.37 290.24 45.32 o 6 17 0 1415.33 1301.47 69.22 o 7 17 0 0.39 4.15 26.00 o 8 17 0 1093.04 1124.85 84.74 o 0 18 0 127.36 106.35 23.35 o 1 18 0 5496.64 5592.46 115.17 o 2 18 0 483.18 518.86 28.67 o 3 18 0 62.08 57.08 15.10 o 4 18 0 594.28 658.43 48.14 o 5 18 0 1542.75 1581.55 75.80 o 6 18 0 20.20 6.15 20.23 o 7 18 0 150.02 148.03 26.79 o 1 19 0 508.71 478.17 30.97 o 2 19 0 3678.45 3831.43 93.20 o 3 19 0 192.80 181.62 29.75 o 4 19 0 211.44 176.40 25.96 o 5 19 0 779.54 817.93 56.43 o 6 19 0 1655.67 1668.55 82.92 o 0 20 0 1046.20 991.89 64.11 o 1 20 0 3676.63 3854.39 93.92 o 2 20 0 0.46 7.38 13.57 o 3 20 0 390.67 357.24 37.78 o 4 20 0 473.45 490.01 44.13 o 5 20 0 1181.12 1263.55 71.62 o 6 20 0 18.75 25.44 25.40 o 1 21 0 267.66 302.02 29.97 o 2 21 0 3075.94 3134.45 128.23 o 3 21 0 143.91 160.36 27.52 o 4 21 0 89.65 104.70 22.98 o 5 21 0 239.74 135.01 35.65 o 0 22 0 433.36 340.62 41.36 o 1 22 0 2752.88 2897.22 93.76 o 2 22 0 1.51 -36.58 24.39 o 3 22 0 496.67 519.36 47.76 o 4 22 0 280.93 270.45 49.50 o 1 23 0 138.64 260.98 38.59 o 2 23 0 2464.37 2643.21 155.60 o -11 0 1 225.55 204.55 36.91 o -9 0 1 5489.94 5322.84 126.57 o -7 0 1 1565.90 1535.80 45.52 o -5 0 1 14230.28 14267.06 192.47 o -3 0 1 11957.82 11812.24 193.13 o -1 0 1 40656.02 39393.83 863.72 o 1 0 1 22101.67 23301.91 606.99 o 3 0 1 18.37 32.01 4.84 o 5 0 1 4941.82 4979.92 77.03 o 7 0 1 7918.65 8145.36 137.20 o 9 0 1 7103.88 7381.73 158.83 o 11 0 1 417.18 391.02 47.77 o -12 1 1 1221.22 1143.70 73.88 o -11 1 1 51.96 55.88 16.62 o -10 1 1 1385.47 1340.14 43.19 o -9 1 1 0.31 10.06 9.47 o -8 1 1 1277.67 1289.08 30.90 o -7 1 1 0.18 9.48 5.54 o -6 1 1 2000.82 1708.79 41.38 o -5 1 1 242.67 200.88 10.21 o -4 1 1 17042.86 17769.89 207.62 o -3 1 1 1958.99 2083.49 23.31 o -2 1 1 44029.42 44209.19 441.30 o -1 1 1 686.43 636.60 16.71 o 1 1 1 60.04 59.29 4.57 o 2 1 1 33907.04 34072.52 314.35 o 3 1 1 212.05 218.27 7.17 o 4 1 1 311.86 304.12 9.09 o 5 1 1 282.12 280.46 9.81 o 6 1 1 13832.62 13705.94 125.37 o 7 1 1 8.52 9.05 6.32 o 8 1 1 16.49 26.11 7.31 o 9 1 1 2.63 28.34 13.17 o 10 1 1 5564.96 5637.01 98.94 o 11 1 1 3.27 14.56 13.40 o 12 1 1 260.76 233.02 31.14 o -12 2 1 1.89 34.14 24.76 o -11 2 1 202.94 192.66 25.39 o -10 2 1 779.46 766.17 32.72 o -9 2 1 5111.21 5389.87 83.71 o -8 2 1 925.51 911.20 30.53 o -7 2 1 777.20 745.86 22.13 o -6 2 1 10.67 14.10 4.87 o -5 2 1 7936.87 7722.98 82.16 o -4 2 1 484.08 512.14 11.44 o -3 2 1 1857.08 1838.24 20.49 o -2 2 1 18904.59 19547.57 149.47 o -1 2 1 12823.18 12925.86 131.81 o 0 2 1 171.75 180.70 6.50 o 1 2 1 8657.16 8653.48 124.68 o 2 2 1 4124.53 4127.24 42.82 o 3 2 1 5013.96 4843.39 58.15 o 4 2 1 4626.19 4671.43 58.43 o 5 2 1 3397.68 3202.21 39.45 o 6 2 1 402.78 391.34 13.21 o 7 2 1 5747.83 5952.47 75.06 o 8 2 1 111.00 103.78 10.15 o 9 2 1 6755.36 6907.46 105.64 o 10 2 1 586.02 505.01 27.85 o 11 2 1 113.92 115.49 15.32 o 12 2 1 2.00 14.53 21.21 o -12 3 1 999.16 972.32 67.97 o -11 3 1 669.06 664.80 45.55 o -10 3 1 1017.77 947.66 38.45 o -9 3 1 19.47 23.54 10.55 o -8 3 1 3701.43 3778.77 67.30 o -7 3 1 1153.29 1173.28 27.94 o -6 3 1 7012.69 6987.22 79.49 o -5 3 1 804.24 762.98 16.62 o -4 3 1 6837.30 7089.92 69.53 o -3 3 1 4653.32 4706.19 47.23 o -2 3 1 41079.14 41920.47 610.59 o -1 3 1 2407.05 2406.38 29.12 o 0 3 1 458.14 503.50 10.99 o 1 3 1 382.49 376.30 7.38 o 2 3 1 8140.56 7863.47 135.00 o 3 3 1 205.36 226.62 12.10 o 4 3 1 202.94 243.80 7.63 o 5 3 1 164.01 177.42 7.39 o 6 3 1 9535.70 9656.33 96.31 o 7 3 1 737.99 705.46 21.62 o 8 3 1 329.09 366.69 18.47 o 9 3 1 605.35 561.49 23.40 o 10 3 1 2899.34 2919.36 68.30 o 11 3 1 2.15 4.53 11.63 o 12 3 1 326.75 214.99 43.57 o -12 4 1 33.85 29.57 36.51 o -11 4 1 116.66 102.66 43.15 o -10 4 1 825.82 722.59 53.56 o -9 4 1 3482.32 3628.86 69.62 o -8 4 1 750.96 707.11 27.24 o -7 4 1 228.61 255.52 14.20 o -6 4 1 309.93 280.57 13.83 o -5 4 1 20572.12 20643.72 212.40 o -4 4 1 129.11 147.67 7.34 o -3 4 1 648.44 678.73 16.44 o -2 4 1 11314.66 12025.63 228.80 o -1 4 1 5944.71 5857.87 55.45 o 0 4 1 6888.94 6849.08 98.68 o 1 4 1 3708.80 3699.81 35.73 o 2 4 1 3706.01 3889.42 40.73 o 3 4 1 1447.66 1310.28 21.76 o 4 4 1 1089.86 1051.65 20.08 o 5 4 1 1577.47 1323.25 23.39 o 6 4 1 213.65 193.39 9.52 o 7 4 1 1296.39 1388.55 34.39 o 8 4 1 1193.15 1171.98 31.57 o 9 4 1 3436.42 3641.76 63.20 o 10 4 1 385.11 388.19 26.47 o 11 4 1 71.04 69.92 20.93 o 12 4 1 9.45 51.14 24.60 o -12 5 1 907.54 786.02 65.34 o -11 5 1 1050.04 974.28 83.06 o -10 5 1 644.68 664.03 36.08 o -9 5 1 0.96 25.18 10.07 o -8 5 1 6775.50 6960.88 101.60 o -7 5 1 762.88 706.57 23.56 o -6 5 1 6400.43 6610.11 83.52 o -5 5 1 917.05 930.75 23.02 o -4 5 1 9623.96 9654.72 142.97 o -3 5 1 7974.71 7955.75 148.95 o -2 5 1 20068.87 20055.04 160.17 o -1 5 1 1053.46 1132.66 23.62 o 0 5 1 2988.69 3101.97 48.92 o 1 5 1 8.83 6.65 2.64 o 2 5 1 7924.28 7832.13 89.06 o 3 5 1 505.64 571.23 12.40 o 4 5 1 538.34 626.93 14.72 o 5 5 1 4012.42 4092.72 51.26 o 6 5 1 9269.33 9465.89 105.92 o 7 5 1 753.48 749.29 28.24 o 8 5 1 2022.94 1992.01 58.20 o 9 5 1 32.36 30.19 9.76 o 10 5 1 1051.95 1168.72 44.78 o 11 5 1 144.58 142.39 23.96 o 12 5 1 779.55 885.67 58.83 o -12 6 1 25.88 44.72 21.85 o -11 6 1 29.68 42.31 17.40 o -10 6 1 1474.06 1392.72 53.40 o -9 6 1 3307.64 3573.22 97.55 o -8 6 1 2851.27 2849.45 56.85 o -7 6 1 1535.49 1488.33 35.70 o -6 6 1 332.55 322.56 15.09 o -5 6 1 23820.10 25213.18 331.66 o -4 6 1 2395.96 2522.78 51.13 o -3 6 1 6297.58 6562.40 65.64 o -2 6 1 4149.66 4038.71 46.71 o -1 6 1 3628.23 3243.57 39.78 o 0 6 1 9784.01 9967.87 166.10 o 1 6 1 46.01 40.02 3.43 o 2 6 1 2505.80 2753.42 46.14 o 3 6 1 7383.07 7243.53 71.02 o 4 6 1 4430.13 4438.32 50.41 o 5 6 1 2542.30 2524.67 39.36 o 6 6 1 55.29 59.72 7.63 o 7 6 1 1599.16 1534.72 38.30 o 8 6 1 2285.95 2376.26 51.25 o 9 6 1 2261.46 2331.46 53.42 o 10 6 1 305.70 245.07 21.56 o 11 6 1 18.72 30.42 18.36 o 12 6 1 85.41 46.02 20.32 o -12 7 1 609.89 518.32 68.42 o -11 7 1 309.73 360.28 37.51 o -10 7 1 358.11 416.51 32.54 o -9 7 1 66.70 63.42 13.43 o -8 7 1 5833.06 6077.22 112.47 o -7 7 1 16.46 27.27 7.87 o -6 7 1 9362.87 9484.72 111.20 o -5 7 1 54.44 55.40 7.43 o -4 7 1 9536.78 9787.57 106.91 o -3 7 1 5288.18 5168.01 74.51 o -2 7 1 10236.33 10049.65 109.35 o -1 7 1 5121.67 5219.02 77.23 o 0 7 1 2002.80 1815.14 32.14 o 1 7 1 6280.37 6412.10 69.56 o 2 7 1 1938.17 1588.31 26.53 o 3 7 1 4906.17 4922.22 69.96 o 4 7 1 31.95 33.96 6.14 o 5 7 1 2803.49 2791.60 42.73 o 6 7 1 1861.25 1850.02 39.95 o 7 7 1 1064.29 1031.83 30.96 o 8 7 1 994.87 953.31 31.85 o 9 7 1 541.75 475.46 26.41 o 10 7 1 970.34 1023.75 43.28 o 11 7 1 377.94 313.34 42.74 o 12 7 1 403.31 369.65 56.25 o -11 8 1 7.59 12.87 17.09 o -10 8 1 429.30 481.65 39.91 o -9 8 1 1912.80 2010.69 57.83 o -8 8 1 125.84 155.17 16.09 o -7 8 1 2384.45 2442.25 46.86 o -6 8 1 882.05 894.31 22.67 o -5 8 1 17715.76 18053.33 195.76 o -4 8 1 3170.69 3170.10 40.31 o -3 8 1 4969.79 5358.88 88.17 o -2 8 1 339.40 335.60 13.07 o -1 8 1 4579.71 4371.24 58.73 o 0 8 1 9581.28 9367.21 107.73 o 1 8 1 294.88 259.53 10.16 o 2 8 1 62.12 60.98 4.66 o 3 8 1 4986.71 4957.92 56.76 o 4 8 1 9592.59 9296.06 125.26 o 5 8 1 2596.68 2493.49 39.87 o 6 8 1 195.86 193.25 13.27 o 7 8 1 467.91 457.77 21.09 o 8 8 1 4042.72 4118.39 72.29 o 9 8 1 681.93 686.02 34.22 o 10 8 1 384.87 379.85 30.30 o 11 8 1 58.02 37.98 46.84 o -11 9 1 161.84 167.09 26.95 o -10 9 1 114.12 94.79 33.02 o -9 9 1 113.98 103.03 18.60 o -8 9 1 1049.88 1086.87 39.99 o -7 9 1 363.15 361.63 19.30 o -6 9 1 1506.88 1545.98 42.67 o -5 9 1 586.13 595.56 17.40 o -4 9 1 1734.37 1652.72 27.09 o -3 9 1 1524.59 1290.11 23.37 o -2 9 1 3246.53 3119.15 44.22 o -1 9 1 760.54 669.79 18.44 o 0 9 1 3295.74 3273.87 48.27 o 1 9 1 10915.87 11082.74 144.67 o 2 9 1 12455.44 12504.52 120.76 o 3 9 1 5443.26 5338.13 64.72 o 4 9 1 424.48 425.52 12.93 o 5 9 1 2929.53 2935.81 53.92 o 6 9 1 1689.94 1622.79 38.17 o 7 9 1 4011.25 3996.52 68.26 o 8 9 1 33.97 20.70 10.66 o 9 9 1 562.48 623.56 33.66 o 10 9 1 1263.19 1258.08 66.37 o 11 9 1 562.01 510.68 172.49 o -11 10 1 85.72 46.91 21.13 o -10 10 1 164.87 194.18 34.39 o -9 10 1 907.90 866.78 54.28 o -8 10 1 26.67 40.72 12.48 o -7 10 1 5.51 17.11 9.72 o -6 10 1 2000.36 1951.19 76.04 o -5 10 1 4654.34 4710.06 67.85 o -4 10 1 12986.38 13185.68 146.31 o -3 10 1 82.00 73.44 5.67 o -2 10 1 2597.37 2828.70 42.51 o -1 10 1 5662.45 5726.02 88.41 o 0 10 1 7795.39 7517.71 101.61 o 1 10 1 1777.04 1770.45 37.04 o 2 10 1 163.03 156.95 8.01 o 3 10 1 3812.39 3753.07 60.56 o 4 10 1 16024.00 16118.50 207.87 o 5 10 1 5083.07 5241.83 75.06 o 6 10 1 1.32 3.42 6.92 o 7 10 1 1.70 -1.62 9.87 o 8 10 1 3519.03 3527.77 95.47 o 9 10 1 829.19 900.44 44.43 o 10 10 1 11.52 27.55 22.12 o 11 10 1 102.35 106.44 31.99 o -11 11 1 595.85 756.49 146.87 o -10 11 1 7.70 -6.10 17.97 o -9 11 1 11.69 15.86 16.58 o -8 11 1 400.28 415.04 32.44 o -7 11 1 2412.92 2469.27 67.01 o -6 11 1 200.68 218.53 19.32 o -5 11 1 1037.13 1011.86 29.21 o -4 11 1 350.21 341.33 11.21 o -3 11 1 3798.10 3776.71 55.43 o -2 11 1 4109.44 4162.59 61.33 o -1 11 1 1867.06 1794.40 34.67 o 0 11 1 1.04 0.30 7.12 o 1 11 1 10238.42 10237.83 129.32 o 2 11 1 6010.28 6043.67 87.57 o 3 11 1 7141.95 7200.92 85.73 o 4 11 1 1543.54 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