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Information card for entry 2230103
Preview
| Coordinates | 2230103.cif |
|---|---|
| Structure factors | 2230103.hkl |
| Original IUCr paper | HTML |
| Chemical name | Poly[[μ-aqua-bis(μ-4,4'-bipyridine-κ^2^<i>N</i>:<i>N</i>')bis(μ-3- hydroxyadamantane-1-carboxylato-κ^2^<i>O</i>:<i>O</i>')bis(3- hydroxyadamantane-1-carboxylato-κ<i>O</i>)dicobalt(II)] heptahydrate] |
|---|---|
| Formula | C64 H92 Co2 N4 O20 |
| Calculated formula | C64 H92 Co2 N4 O20 |
| Title of publication | Poly[[μ-aqua-bis(μ-4,4'-bipyridine-κ^2^<i>N</i>:<i>N</i>')bis(μ-3-hydroxyadamantane-1-carboxylato-κ^2^<i>O</i>:<i>O</i>')bis(3-hydroxyadamantane-1-carboxylato-κ<i>O</i>)dicobalt(II)] heptahydrate] |
| Authors of publication | Shen, Jin-Bei; Wu, Xiao-Yong; Chen, Xiao-Ju; Zhao, Guo-Liang |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2011 |
| Journal volume | 67 |
| Journal issue | 5 |
| Pages of publication | m558 - m559 |
| a | 12.0201 ± 0.0003 Å |
| b | 20.7463 ± 0.0005 Å |
| c | 17.6353 ± 0.0003 Å |
| α | 90° |
| β | 132.806 ± 0.001° |
| γ | 90° |
| Cell volume | 3226.46 ± 0.14 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 7 |
| Hermann-Mauguin space group symbol | P 1 c 1 |
| Hall space group symbol | P -2yc |
| Residual factor for all reflections | 0.0426 |
| Residual factor for significantly intense reflections | 0.0345 |
| Weighted residual factors for significantly intense reflections | 0.0779 |
| Weighted residual factors for all reflections included in the refinement | 0.0825 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.025 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181223 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/01. |
2230103.cif 2230103.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2230103.cif 2230103.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2230103.cif 2230103.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2230103.cif 2230103.hkl |
| 26848 | 2011-09-28 | cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree. |
2230103.cif 2230103.hkl |
| 22560 | 2011-07-04 | hkl/ Adding Fobs files for the recent IUCr data deposition. |
2230103.cif 2230103.hkl |
| 20173 | 2011-06-03 | ../uploads/cif-deposit/cod/cif Adding structures of 2230103 via cif-deposit CGI script. |
2230103.cif |
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Users of the data should acknowledge the original authors of the
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