#------------------------------------------------------------------------------ #$Date: 2011-07-04 21:24:21 +0300 (Mon, 04 Jul 2011) $ #$Revision: 22560 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230140.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230140_Fobs loop_ _publ_author_name 'Liu, Guang-Xiang' 'Xu, Xu-Yong' _publ_section_title ; trans-Tetraaquabis[1,3-bis(4-pyridyl)propane-\kN]cobalt(II) biphenyl-4,4'-disulfonate monohydrate ; _journal_coeditor_code RZ2587 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m651 _journal_page_last m652 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.959 _cell_angle_gamma 90.000 _cell_length_a 15.5546 _cell_length_b 18.9828 _cell_length_c 14.7254 _exptl_crystal_F_000 1796.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file rz2587Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dd in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 578.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 32.65 59.27 8.13 o 4 0 0 179.28 122.96 11.16 o 6 0 0 32140.31 34369.48 563.21 o 8 0 0 19070.49 18940.16 327.59 o 10 0 0 21343.21 21586.18 1032.71 o 12 0 0 430.27 358.20 73.05 o 14 0 0 443.38 398.25 84.55 o 16 0 0 905.47 641.87 112.36 o 1 1 0 30219.06 31866.79 885.13 o 3 1 0 4166.53 4014.00 59.79 o 5 1 0 19.02 17.32 6.73 o 7 1 0 24319.17 25339.62 300.85 o 9 1 0 12135.57 11609.58 191.40 o 11 1 0 1125.44 1191.59 60.85 o 13 1 0 2059.33 1586.57 98.96 o 15 1 0 814.86 787.46 85.66 o 17 1 0 149.14 183.24 74.16 o 0 2 0 4771.99 5471.35 111.53 o 2 2 0 4396.86 4855.60 76.69 o 4 2 0 25.78 21.41 7.58 o 6 2 0 252.84 297.07 19.75 o 8 2 0 1190.89 1144.15 38.69 o 10 2 0 496.30 423.33 38.35 o 12 2 0 63.32 55.19 23.79 o 14 2 0 436.45 395.60 69.53 o 16 2 0 134.60 121.93 41.90 o 1 3 0 6.09 64.55 5.85 o 3 3 0 1554.97 1697.06 37.25 o 5 3 0 426.08 515.43 23.72 o 7 3 0 4006.58 4001.12 101.51 o 9 3 0 458.37 440.71 29.23 o 11 3 0 184.77 194.28 31.61 o 13 3 0 3.89 0.32 22.11 o 15 3 0 180.38 184.71 56.92 o 17 3 0 27.53 60.31 43.20 o 0 4 0 334701.19 359943.22 5661.73 o 2 4 0 189.82 249.42 11.84 o 4 4 0 6280.50 6627.63 111.85 o 6 4 0 7794.00 8214.68 139.27 o 8 4 0 7730.74 7568.99 141.78 o 10 4 0 11.91 12.22 14.17 o 12 4 0 93.89 89.07 26.46 o 14 4 0 281.33 289.78 41.55 o 16 4 0 867.70 909.29 86.85 o 1 5 0 1320.88 1270.51 23.92 o 3 5 0 31393.33 33138.87 381.52 o 5 5 0 1271.21 1275.28 50.78 o 7 5 0 2857.05 2543.25 62.59 o 9 5 0 7518.67 7667.00 143.39 o 11 5 0 39.88 7.52 20.17 o 13 5 0 1151.88 1018.52 68.97 o 15 5 0 1188.03 1167.01 95.70 o 0 6 0 35371.08 38620.86 624.98 o 2 6 0 5078.10 5940.16 79.84 o 4 6 0 521.63 442.35 19.01 o 6 6 0 346.49 522.16 28.74 o 8 6 0 5667.04 5754.91 115.60 o 10 6 0 2654.06 2514.17 71.08 o 12 6 0 8.14 25.06 26.69 o 14 6 0 2107.02 1811.53 114.95 o 16 6 0 822.11 825.98 93.85 o 1 7 0 2971.95 3174.61 49.57 o 3 7 0 372.23 342.04 15.86 o 5 7 0 433.68 542.88 21.97 o 7 7 0 432.43 542.68 36.71 o 9 7 0 600.13 679.09 46.79 o 11 7 0 571.89 633.65 52.00 o 13 7 0 17.33 34.17 28.11 o 15 7 0 250.36 273.72 45.39 o 0 8 0 42.43 81.42 13.85 o 2 8 0 4644.68 4863.23 71.17 o 4 8 0 1209.16 1368.58 34.66 o 6 8 0 1415.36 1575.43 56.08 o 8 8 0 4651.58 4033.22 93.50 o 10 8 0 1990.42 1853.64 64.52 o 12 8 0 10.41 0.00 21.78 o 14 8 0 141.02 161.34 39.95 o 16 8 0 260.55 336.72 101.79 o 1 9 0 7756.46 7471.38 102.33 o 3 9 0 2321.65 2739.43 72.73 o 5 9 0 1099.12 1029.45 27.45 o 7 9 0 5520.55 5489.93 114.33 o 9 9 0 5856.97 5362.24 118.67 o 11 9 0 98.29 110.74 25.59 o 13 9 0 83.66 98.41 35.44 o 15 9 0 999.25 996.47 81.82 o 0 10 0 2359.77 2060.17 57.84 o 2 10 0 13758.41 14584.24 184.70 o 4 10 0 1312.42 1257.49 33.43 o 6 10 0 2270.06 1969.26 56.23 o 8 10 0 14431.37 12973.85 412.07 o 10 10 0 2340.69 2011.53 71.34 o 12 10 0 499.28 463.75 43.06 o 14 10 0 1232.36 1265.88 100.49 o 1 11 0 12102.01 12532.25 163.54 o 3 11 0 1097.84 983.65 28.60 o 5 11 0 884.40 834.21 33.76 o 7 11 0 7614.69 7140.37 141.86 o 9 11 0 2364.02 2176.63 71.18 o 11 11 0 1827.40 1681.76 71.28 o 13 11 0 58.88 87.64 35.40 o 15 11 0 1058.96 943.50 97.50 o 0 12 0 1679.94 1443.15 51.09 o 2 12 0 75.48 45.54 11.37 o 4 12 0 817.36 862.78 35.28 o 6 12 0 947.61 876.78 45.55 o 8 12 0 27.13 33.27 20.83 o 10 12 0 124.30 133.66 28.20 o 12 12 0 259.16 295.10 38.30 o 14 12 0 62.12 127.98 39.99 o 1 13 0 2387.73 2466.89 57.29 o 3 13 0 21.03 35.31 14.39 o 5 13 0 324.69 343.60 25.99 o 7 13 0 652.50 563.08 40.91 o 9 13 0 1194.85 1152.60 61.23 o 11 13 0 274.60 280.44 37.11 o 13 13 0 20.78 8.38 30.45 o 0 14 0 19969.71 19708.39 354.84 o 2 14 0 629.69 654.15 33.05 o 4 14 0 168.30 167.20 20.54 o 6 14 0 298.39 304.31 32.83 o 8 14 0 3499.52 3068.28 89.29 o 10 14 0 367.83 418.04 42.49 o 12 14 0 9.80 44.02 20.07 o 1 15 0 4826.32 4750.50 96.27 o 3 15 0 554.97 671.22 35.68 o 5 15 0 192.66 204.95 24.43 o 7 15 0 5160.28 4492.17 128.92 o 9 15 0 1246.99 1144.95 62.12 o 11 15 0 491.17 530.52 48.12 o 13 15 0 168.75 257.62 35.67 o 0 16 0 5979.51 6328.72 236.95 o 2 16 0 525.54 562.77 34.69 o 4 16 0 3.00 8.37 17.17 o 6 16 0 615.75 588.82 44.92 o 8 16 0 548.50 649.72 57.51 o 10 16 0 764.84 835.15 65.12 o 12 16 0 144.08 249.34 34.74 o 1 17 0 240.97 201.47 45.22 o 3 17 0 123.91 98.09 23.91 o 5 17 0 369.61 292.53 40.84 o 7 17 0 216.44 220.99 36.11 o 9 17 0 42.70 60.63 26.25 o 11 17 0 23.13 55.89 32.01 o 0 18 0 3463.64 3540.88 195.42 o 2 18 0 153.48 75.71 38.90 o 4 18 0 149.02 183.96 36.84 o 6 18 0 109.01 66.73 34.01 o 8 18 0 24.30 77.86 33.56 o 10 18 0 127.55 264.50 39.58 o 1 19 0 866.18 765.15 76.14 o 3 19 0 3.14 0.00 34.60 o 5 19 0 26.96 21.26 35.47 o 7 19 0 832.17 906.71 83.49 o 9 19 0 269.47 405.59 54.92 o 0 20 0 1847.94 2152.93 156.85 o 2 20 0 58.62 91.00 51.36 o 4 20 0 8.66 82.32 54.88 o 6 20 0 98.47 180.85 37.60 o 8 20 0 253.11 382.40 50.06 o 1 21 0 24.30 49.82 40.38 o 3 21 0 3.33 12.72 41.91 o 5 21 0 23.16 66.75 67.12 o 7 21 0 144.64 219.83 37.08 o 0 22 0 2.43 0.00 58.22 o 2 22 0 28.78 76.93 47.81 o 4 22 0 182.54 131.27 77.50 o -17 1 1 30.01 33.23 25.01 o -15 1 1 76.20 73.67 55.81 o -13 1 1 693.24 558.80 50.71 o -11 1 1 5222.98 5034.54 111.37 o -9 1 1 220.29 283.83 19.22 o -7 1 1 2062.79 2087.37 36.85 o -5 1 1 12879.19 14576.38 272.12 o -3 1 1 20281.07 24893.52 315.60 o -1 1 1 17997.49 19051.26 443.45 o 1 1 1 839.21 674.04 22.74 o 3 1 1 173.71 201.34 15.65 o 5 1 1 9103.93 9106.33 174.77 o 7 1 1 4041.39 3745.14 101.42 o 9 1 1 19.57 11.00 12.74 o 11 1 1 687.10 550.13 60.44 o 13 1 1 1951.64 1778.79 107.93 o 15 1 1 662.23 588.48 94.93 o -16 2 1 41.79 97.50 55.25 o -14 2 1 1126.06 858.30 106.42 o -12 2 1 13680.03 12431.66 261.65 o -10 2 1 4082.62 3957.86 113.20 o -8 2 1 1103.02 1334.79 37.22 o -6 2 1 5773.80 5998.63 92.33 o -4 2 1 71670.45 84264.23 1047.38 o -2 2 1 18758.53 22409.99 314.76 o 0 2 1 3666.17 3333.02 53.11 o 2 2 1 9884.62 11253.37 196.02 o 4 2 1 19243.47 20428.11 352.27 o 6 2 1 139862.14 158728.16 2184.24 o 8 2 1 2187.72 2049.14 54.75 o 10 2 1 7.93 3.38 22.44 o 12 2 1 1387.40 1345.67 90.39 o 14 2 1 4498.28 3765.36 188.93 o 16 2 1 4.94 28.07 38.32 o -17 3 1 634.86 629.28 115.14 o -15 3 1 96.18 73.90 25.86 o -13 3 1 1001.63 1041.14 66.41 o -11 3 1 2926.34 2791.54 155.21 o -9 3 1 3287.47 3281.26 74.51 o -7 3 1 31.46 37.81 11.87 o -5 3 1 19576.03 21159.97 277.43 o -3 3 1 49589.14 54489.71 667.93 o -1 3 1 77390.88 89696.84 1090.66 o 1 3 1 2537.22 2697.64 54.55 o 3 3 1 728.19 628.60 22.15 o 5 3 1 32631.19 33539.94 482.27 o 7 3 1 2925.55 2683.72 63.66 o 9 3 1 18.06 21.30 12.88 o 11 3 1 923.96 843.45 71.06 o 13 3 1 4483.56 4054.61 156.14 o 15 3 1 517.38 615.50 72.22 o -16 4 1 597.97 689.77 63.73 o -14 4 1 1507.01 1310.04 77.64 o -12 4 1 15.71 39.78 24.07 o -10 4 1 5277.02 4715.53 100.50 o -8 4 1 1053.19 983.93 37.85 o -6 4 1 3398.90 3499.36 94.95 o -4 4 1 7133.02 6783.25 96.36 o -2 4 1 7772.43 8248.52 111.64 o 0 4 1 8055.03 8015.37 98.49 o 2 4 1 5732.55 6157.43 80.18 o 4 4 1 1370.15 1163.37 34.07 o 6 4 1 2713.62 2524.30 60.01 o 8 4 1 17.43 19.45 12.72 o 10 4 1 552.58 587.70 37.34 o 12 4 1 1588.57 1641.04 99.51 o 14 4 1 478.82 506.77 69.90 o 16 4 1 119.40 243.99 77.50 o -17 5 1 69.67 150.33 57.66 o -15 5 1 104.11 135.49 32.21 o -13 5 1 1773.34 1667.99 83.07 o -11 5 1 358.82 330.84 38.92 o -9 5 1 300.50 256.01 24.08 o -7 5 1 683.68 793.90 34.19 o -5 5 1 472.35 571.88 28.12 o -3 5 1 137.86 164.96 11.72 o -1 5 1 22571.30 24662.00 285.30 o 1 5 1 20629.15 22718.51 264.69 o 3 5 1 194.63 261.11 17.50 o 5 5 1 119.23 136.17 15.59 o 7 5 1 777.55 857.84 38.67 o 9 5 1 1646.80 1665.62 61.33 o 11 5 1 1170.99 1051.42 64.28 o 13 5 1 222.90 245.48 74.53 o 15 5 1 138.53 149.44 48.50 o -16 6 1 130.95 173.07 35.16 o -14 6 1 132.95 195.34 38.13 o -12 6 1 5699.98 5283.41 145.56 o -10 6 1 2523.61 2272.71 65.40 o -8 6 1 300.83 356.60 26.81 o -6 6 1 735.53 741.87 34.62 o -4 6 1 19.51 87.60 10.73 o -2 6 1 6991.10 7367.13 95.32 o 0 6 1 684.39 763.94 19.03 o 2 6 1 4670.91 4815.30 68.07 o 4 6 1 2907.04 2796.42 63.36 o 6 6 1 9889.10 9879.27 172.45 o 8 6 1 131.62 142.46 20.93 o 10 6 1 165.43 112.25 23.60 o 12 6 1 248.95 263.45 41.41 o 14 6 1 2241.61 2081.31 120.08 o 16 6 1 176.28 240.30 60.17 o -15 7 1 83.37 106.79 49.73 o -13 7 1 3145.36 2892.88 130.90 o -11 7 1 740.06 763.98 50.96 o -9 7 1 5302.79 4959.63 202.42 o -7 7 1 2313.64 2627.29 66.07 o -5 7 1 11.65 35.30 11.19 o -3 7 1 16459.45 17646.77 233.18 o -1 7 1 133.62 136.77 11.43 o 1 7 1 2158.81 2083.67 55.34 o 3 7 1 3523.99 3635.24 57.15 o 5 7 1 13084.93 12729.89 183.22 o 7 7 1 166.79 161.83 21.27 o 9 7 1 9709.83 9352.89 174.74 o 11 7 1 2391.42 2158.13 71.48 o 13 7 1 4146.35 3940.30 132.56 o 15 7 1 190.91 262.50 58.07 o -16 8 1 175.13 136.33 43.52 o -14 8 1 116.85 158.30 36.58 o -12 8 1 68.82 73.78 28.86 o -10 8 1 5708.73 5399.48 119.16 o -8 8 1 1431.24 1412.69 49.48 o -6 8 1 50.60 87.15 12.79 o -4 8 1 2156.88 2743.71 53.76 o -2 8 1 3213.29 3019.18 49.37 o 0 8 1 2196.80 2253.34 40.42 o 2 8 1 153.88 133.94 11.33 o 4 8 1 1350.77 967.74 26.11 o 6 8 1 1109.16 1103.88 35.67 o 8 8 1 45.75 9.79 14.81 o 10 8 1 788.98 819.41 48.88 o 12 8 1 3389.08 3051.08 111.11 o 14 8 1 902.16 947.67 91.58 o -15 9 1 187.95 182.49 41.99 o -13 9 1 360.90 333.98 47.15 o -11 9 1 6.69 5.95 19.38 o -9 9 1 38.01 38.49 17.39 o -7 9 1 295.14 355.95 29.41 o -5 9 1 54.85 57.22 11.37 o -3 9 1 3211.82 3390.50 55.71 o -1 9 1 1228.97 1250.34 29.19 o 1 9 1 2068.85 2071.44 40.09 o 3 9 1 5969.35 5910.04 86.81 o 5 9 1 2440.68 2504.59 67.46 o 7 9 1 810.97 790.59 41.89 o 9 9 1 467.36 454.73 56.77 o 11 9 1 72.09 61.51 30.24 o 13 9 1 454.48 553.75 60.48 o 15 9 1 49.47 21.95 46.08 o -14 10 1 12.50 22.73 30.07 o -12 10 1 716.39 665.02 47.88 o -10 10 1 60.41 45.20 20.81 o -8 10 1 83.79 69.97 18.09 o -6 10 1 1.52 12.49 11.30 o -4 10 1 34.32 18.25 12.58 o -2 10 1 182.09 278.02 16.22 o 0 10 1 2932.58 2726.06 49.52 o 2 10 1 2651.38 2664.95 49.55 o 4 10 1 269.22 318.59 18.53 o 6 10 1 0.07 0.00 14.06 o 8 10 1 9.84 20.91 16.80 o 10 10 1 1172.27 1086.39 57.14 o 12 10 1 59.87 83.90 34.67 o 14 10 1 184.18 177.85 42.87 o -15 11 1 1.74 7.00 33.00 o -13 11 1 1364.26 1257.35 114.86 o -11 11 1 82.90 93.81 38.75 o -9 11 1 1684.46 1593.01 62.09 o -7 11 1 765.13 766.90 42.11 o -5 11 1 7.95 20.88 11.20 o -3 11 1 9781.32 10126.63 136.67 o -1 11 1 2853.11 2942.98 53.74 o 1 11 1 1831.05 1846.77 40.44 o 3 11 1 315.84 269.56 17.82 o 5 11 1 6556.04 6662.75 113.58 o 7 11 1 795.28 747.59 44.11 o 9 11 1 2080.32 1975.32 70.11 o 11 11 1 434.03 410.92 42.00 o 13 11 1 757.08 812.65 71.75 o -14 12 1 544.73 502.92 59.17 o -12 12 1 1248.87 1232.76 64.61 o -10 12 1 2142.68 1868.53 69.05 o -8 12 1 1605.19 1505.80 58.98 o -6 12 1 1188.33 1230.32 41.22 o -4 12 1 3943.16 3394.35 69.83 o -2 12 1 11462.23 10858.87 147.02 o 0 12 1 795.33 731.00 27.19 o 2 12 1 351.32 373.97 22.00 o 4 12 1 6812.87 6132.90 213.18 o 6 12 1 10250.52 9473.32 250.75 o 8 12 1 396.20 462.83 39.85 o 10 12 1 189.43 184.41 30.90 o 12 12 1 2819.51 2430.66 85.59 o 14 12 1 1024.58 977.45 134.68 o -13 13 1 162.36 168.76 39.73 o -11 13 1 3695.92 3454.28 99.65 o -9 13 1 1327.24 1340.94 68.94 o -7 13 1 291.33 359.68 44.37 o -5 13 1 4706.68 4464.33 104.84 o -3 13 1 10401.36 9793.04 264.53 o -1 13 1 12492.66 12452.76 167.31 o 1 13 1 1433.08 1377.34 37.15 o 3 13 1 4524.87 4244.70 83.28 o 5 13 1 9129.65 9025.56 147.40 o 7 13 1 4041.14 3865.83 98.74 o 9 13 1 22.00 0.00 21.02 o 11 13 1 871.17 957.25 59.90 o 13 13 1 676.02 728.83 71.82 o -14 14 1 26.60 48.45 33.63 o -12 14 1 484.59 577.10 48.59 o -10 14 1 491.41 420.42 41.69 o -8 14 1 1107.88 1043.58 55.18 o -6 14 1 1597.18 1339.19 92.91 o -4 14 1 756.39 785.44 36.65 o -2 14 1 3550.16 3719.37 76.15 o 0 14 1 197.39 147.78 17.52 o 2 14 1 496.88 462.49 28.72 o 4 14 1 2466.63 2264.18 67.12 o 6 14 1 1840.42 1719.03 63.05 o 8 14 1 217.48 163.64 30.62 o 10 14 1 251.06 210.53 33.39 o 12 14 1 484.06 508.70 53.30 o -13 15 1 0.10 37.49 19.22 o -11 15 1 32.83 75.21 24.72 o -9 15 1 187.52 160.59 30.20 o -7 15 1 50.91 33.11 21.18 o -5 15 1 12.34 19.77 15.47 o -3 15 1 605.87 558.42 32.53 o -1 15 1 497.29 599.44 32.97 o 1 15 1 3243.17 3052.44 75.71 o 3 15 1 52.39 51.99 17.36 o 5 15 1 629.89 554.37 49.39 o 7 15 1 157.18 133.36 33.82 o 9 15 1 0.45 10.46 24.65 o 11 15 1 124.17 134.73 29.74 o -12 16 1 90.71 165.69 29.75 o -10 16 1 64.94 76.89 26.45 o -8 16 1 127.82 152.82 29.51 o -6 16 1 40.69 30.77 22.89 o -4 16 1 1568.94 1587.82 61.29 o -2 16 1 1171.03 1122.29 51.23 o 0 16 1 131.84 202.39 33.45 o 2 16 1 388.97 404.70 36.34 o 4 16 1 1107.07 1179.94 55.56 o 6 16 1 4075.86 3794.45 118.54 o 8 16 1 9.20 39.71 26.00 o 10 16 1 22.00 70.97 25.80 o -11 17 1 1304.18 1451.15 101.68 o -9 17 1 223.55 258.50 39.79 o -7 17 1 229.64 199.05 36.42 o -5 17 1 984.25 899.68 61.08 o -3 17 1 570.62 629.04 43.75 o -1 17 1 4733.68 4659.81 126.37 o 1 17 1 29.72 30.26 25.64 o 3 17 1 36.15 65.81 24.02 o 5 17 1 2397.23 2569.66 94.47 o 7 17 1 414.47 386.54 47.32 o 9 17 1 90.76 73.63 26.90 o 11 17 1 87.00 148.44 26.54 o -10 18 1 160.84 220.85 37.79 o -8 18 1 159.91 116.45 49.32 o -6 18 1 315.93 294.82 50.71 o -4 18 1 230.31 239.02 39.64 o -2 18 1 976.96 1111.64 65.88 o 0 18 1 607.69 596.51 52.15 o 2 18 1 4.62 13.69 25.76 o 4 18 1 574.77 544.41 45.69 o 6 18 1 925.94 962.24 65.83 o 8 18 1 26.24 84.18 26.01 o 10 18 1 26.82 68.58 25.53 o -9 19 1 134.06 259.51 50.06 o -7 19 1 30.88 58.27 27.25 o -5 19 1 18.71 15.35 33.86 o -3 19 1 0.95 36.23 36.49 o -1 19 1 32.68 51.04 39.09 o 1 19 1 440.27 412.15 60.93 o 3 19 1 8.24 41.68 35.74 o 5 19 1 7.36 0.00 32.13 o 7 19 1 7.37 88.36 29.57 o 9 19 1 27.81 41.83 55.25 o -8 20 1 134.70 257.04 37.38 o -6 20 1 24.69 40.16 45.05 o -4 20 1 4.53 37.45 52.28 o 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