#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/01/2230162.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230162_Fobs loop_ _publ_author_name 'Shakuntala, K.' 'Foro, Sabine' 'Gowda, B. Thimme' _publ_section_title ; N-(2-Chlorophenylsulfonyl)acetamide ; _journal_coeditor_code VM2086 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1097 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.610 _cell_angle_gamma 90.000 _cell_length_a 11.2150 _cell_length_b 9.3930 _cell_length_c 19.6550 _exptl_crystal_F_000 960.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file vm2086Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SA85 P21/N' _shelx_refln_list_code 4 _shelx_f_calc_maximum 259.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5145.43 5306.90 47.78 o 4 0 0 44232.71 44482.93 113.03 o 6 0 0 960.57 917.81 28.12 o 8 0 0 177.33 265.30 54.99 o 10 0 0 260.52 278.19 69.76 o 12 0 0 54.33 121.99 68.86 o 2 1 0 2065.44 2044.40 16.29 o 3 1 0 400.69 378.10 12.73 o 4 1 0 1367.89 1473.64 18.98 o 5 1 0 232.80 208.21 16.63 o 6 1 0 111.93 111.61 16.74 o 7 1 0 352.54 351.69 20.46 o 8 1 0 71.15 23.95 37.60 o 9 1 0 361.92 383.16 47.76 o 10 1 0 51.90 16.67 77.03 o 11 1 0 274.81 246.16 49.22 o 12 1 0 183.56 252.57 53.24 o 13 1 0 104.59 31.55 71.19 o 0 2 0 895.83 862.14 34.49 o 1 2 0 15237.96 14089.18 39.87 o 2 2 0 2836.71 2972.77 95.15 o 3 2 0 1977.27 2117.37 22.04 o 4 2 0 4471.06 4612.75 37.32 o 5 2 0 1812.08 1776.15 24.09 o 6 2 0 93.23 95.81 17.93 o 7 2 0 134.16 123.06 21.94 o 8 2 0 825.71 776.20 43.58 o 9 2 0 6.36 11.82 33.64 o 10 2 0 86.15 56.62 46.34 o 11 2 0 6.85 -2.63 47.57 o 12 2 0 2.36 -8.81 49.28 o 13 2 0 4.86 2.52 57.83 o 1 3 0 402.17 394.03 15.71 o 2 3 0 19.82 26.06 15.28 o 3 3 0 1694.47 1602.78 69.50 o 4 3 0 1031.27 972.70 22.14 o 5 3 0 15.38 16.03 17.79 o 6 3 0 10.53 6.97 18.41 o 7 3 0 1785.77 1787.09 32.09 o 8 3 0 311.56 342.43 26.84 o 9 3 0 414.82 445.29 54.83 o 10 3 0 337.85 299.07 37.47 o 11 3 0 77.93 19.57 48.23 o 12 3 0 60.49 32.89 54.20 o 13 3 0 4.63 6.09 56.01 o 0 4 0 8308.51 8696.37 107.46 o 1 4 0 771.10 816.22 23.98 o 2 4 0 350.16 337.23 19.32 o 3 4 0 1345.01 1325.99 24.63 o 4 4 0 679.49 718.62 30.51 o 5 4 0 205.74 234.20 22.03 o 6 4 0 789.08 885.95 31.80 o 7 4 0 908.75 917.00 29.73 o 8 4 0 13.34 22.66 27.80 o 9 4 0 137.83 157.48 45.07 o 10 4 0 0.59 -15.34 45.70 o 11 4 0 67.81 60.07 38.16 o 12 4 0 41.00 72.51 53.77 o 13 4 0 22.35 66.63 73.57 o 1 5 0 3626.97 3651.57 57.39 o 2 5 0 1472.55 1537.61 27.11 o 3 5 0 73.54 69.60 19.28 o 4 5 0 292.79 303.34 21.11 o 5 5 0 663.84 611.26 34.96 o 6 5 0 428.82 412.42 37.87 o 7 5 0 1122.29 1084.87 37.79 o 8 5 0 1504.05 1444.91 44.74 o 9 5 0 17.68 15.24 40.40 o 10 5 0 0.10 -15.51 67.17 o 11 5 0 231.92 260.07 49.09 o 12 5 0 78.31 51.28 53.67 o 0 6 0 2122.83 2269.60 66.08 o 1 6 0 5.86 -16.67 27.99 o 2 6 0 179.60 167.20 20.71 o 3 6 0 293.73 284.24 22.71 o 4 6 0 34.45 53.45 34.86 o 5 6 0 854.78 846.86 41.41 o 6 6 0 854.56 946.94 71.69 o 7 6 0 519.61 485.50 37.54 o 8 6 0 47.43 48.69 32.75 o 9 6 0 8.32 -6.26 41.67 o 10 6 0 452.73 475.32 66.55 o 11 6 0 16.46 54.20 77.64 o 1 7 0 625.13 600.46 38.73 o 2 7 0 59.94 63.75 32.93 o 3 7 0 336.85 386.58 36.91 o 4 7 0 901.64 896.90 67.36 o 5 7 0 124.10 227.01 65.17 o 6 7 0 245.13 204.58 37.76 o 7 7 0 299.71 290.69 42.89 o 8 7 0 29.10 46.60 34.64 o 9 7 0 356.14 346.83 51.06 o 10 7 0 21.17 -8.11 46.70 o 11 7 0 18.20 -20.73 68.94 o 0 8 0 58.01 57.07 52.20 o 1 8 0 1710.75 1608.00 51.97 o 2 8 0 1777.43 1774.45 50.80 o 3 8 0 1262.27 1248.78 77.65 o 4 8 0 47.26 95.86 64.94 o 5 8 0 205.71 254.29 64.83 o 6 8 0 237.62 180.78 61.54 o 7 8 0 33.52 -31.95 60.41 o 8 8 0 22.66 51.87 45.23 o 9 8 0 44.06 55.41 45.38 o 10 8 0 70.53 37.63 52.78 o 1 9 0 5.51 2.01 35.85 o 2 9 0 0.31 47.26 39.24 o 3 9 0 26.44 73.00 68.45 o 4 9 0 9.58 46.41 70.08 o 5 9 0 32.05 56.10 67.92 o 6 9 0 12.84 -9.36 79.58 o 7 9 0 22.09 -29.87 77.82 o 8 9 0 2.22 -1.98 52.63 o 0 10 0 405.93 399.48 69.66 o 1 10 0 3.27 110.72 46.02 o 2 10 0 150.46 92.34 66.73 o 3 10 0 26.48 89.08 75.63 o 4 10 0 143.90 110.17 82.09 o 5 10 0 69.55 88.58 80.53 o 6 10 0 0.09 -11.30 73.77 o 7 10 0 28.06 130.31 82.34 o 1 11 0 76.37 90.55 49.01 o 2 11 0 10.15 25.45 70.67 o 3 11 0 24.14 70.13 78.55 o 4 11 0 25.67 -34.80 87.55 o -13 0 1 116.15 170.26 68.55 o -11 0 1 138.37 174.85 72.43 o -9 0 1 1.54 -44.64 62.28 o -7 0 1 2611.16 2610.96 50.33 o -5 0 1 195.93 174.96 15.29 o -3 0 1 10148.84 9907.05 51.71 o 3 0 1 24519.68 24114.16 92.26 o 5 0 1 79.44 50.69 15.89 o 7 0 1 1981.32 1886.59 65.10 o 9 0 1 489.15 460.20 65.85 o 11 0 1 56.02 66.34 73.35 o 13 0 1 61.33 116.60 70.33 o -13 1 1 205.42 231.16 59.59 o -12 1 1 1.37 -49.64 49.64 o -11 1 1 35.07 45.13 47.51 o -10 1 1 51.08 7.96 68.30 o -9 1 1 2453.83 2429.72 61.34 o -8 1 1 171.53 176.19 31.18 o -7 1 1 411.58 408.11 22.83 o -6 1 1 2366.69 2377.56 28.13 o -5 1 1 941.36 913.82 18.35 o -4 1 1 654.01 709.04 15.31 o -3 1 1 8138.25 8259.30 31.33 o -2 1 1 4780.33 4866.33 34.34 o -1 1 1 1200.58 1038.31 361.92 o 1 1 1 1437.00 1478.26 31.38 o 2 1 1 2436.46 2532.46 30.87 o 3 1 1 21409.59 21188.41 102.78 o 4 1 1 1790.54 1921.85 18.73 o 5 1 1 1844.75 1826.74 19.52 o 6 1 1 140.63 118.41 16.55 o 7 1 1 1608.32 1611.55 27.36 o 8 1 1 6.31 -5.61 30.15 o 9 1 1 319.65 323.09 46.09 o 10 1 1 174.53 157.61 50.87 o 11 1 1 99.93 104.01 52.32 o 12 1 1 61.82 11.28 49.88 o 13 1 1 0.22 -13.38 56.32 o -13 2 1 30.85 32.38 57.32 o -12 2 1 17.68 -29.10 46.58 o -11 2 1 60.68 55.08 48.62 o -10 2 1 59.26 57.60 49.57 o -9 2 1 18.40 13.05 50.35 o -8 2 1 1403.21 1353.00 39.61 o -7 2 1 2.55 -1.84 20.74 o -6 2 1 3203.44 3100.37 29.45 o -5 2 1 53.55 42.28 16.73 o -4 2 1 3366.18 3357.18 39.18 o -3 2 1 95.43 86.36 13.78 o -2 2 1 12195.85 11827.16 104.18 o -1 2 1 68.92 101.16 14.61 o 0 2 1 382.88 422.09 22.46 o 1 2 1 5.94 20.90 13.02 o 2 2 1 20040.48 19586.50 43.56 o 3 2 1 2424.67 2482.43 18.34 o 4 2 1 2.26 -4.46 13.57 o 5 2 1 6524.70 6832.48 37.37 o 6 2 1 1102.87 1085.53 25.44 o 7 2 1 77.14 88.42 24.70 o 8 2 1 64.65 63.59 31.40 o 9 2 1 348.42 341.28 38.60 o 10 2 1 749.20 811.84 52.15 o 11 2 1 19.59 -22.68 45.47 o 12 2 1 27.58 36.37 49.80 o 13 2 1 52.14 38.33 113.43 o -13 3 1 29.59 -12.43 49.21 o -12 3 1 51.16 85.47 51.31 o -11 3 1 5.86 18.61 47.50 o -10 3 1 4.89 -43.87 43.87 o -9 3 1 989.44 967.94 45.28 o -8 3 1 0.59 -5.39 24.03 o -7 3 1 1063.38 1062.40 28.55 o -6 3 1 50.88 55.46 19.15 o -5 3 1 180.90 211.17 18.16 o -4 3 1 527.98 540.03 16.89 o -3 3 1 1619.53 1724.68 45.17 o -2 3 1 201.96 224.86 16.52 o -1 3 1 888.64 753.17 17.86 o 0 3 1 594.18 580.94 23.78 o 1 3 1 149.33 162.17 10.73 o 2 3 1 464.03 445.62 14.57 o 3 3 1 75.45 53.87 11.77 o 4 3 1 831.58 826.53 21.23 o 5 3 1 839.77 913.16 24.81 o 6 3 1 883.82 869.85 23.27 o 7 3 1 175.40 195.56 28.35 o 8 3 1 13.37 15.91 29.74 o 9 3 1 713.75 734.05 40.18 o 10 3 1 667.19 648.86 43.33 o 11 3 1 149.85 186.96 41.36 o 12 3 1 1.08 105.11 56.20 o 13 3 1 17.38 52.90 59.74 o -13 4 1 0.01 12.03 71.94 o -12 4 1 60.19 46.88 49.14 o -11 4 1 146.71 212.13 47.92 o -10 4 1 614.54 660.95 48.01 o -9 4 1 19.31 22.42 36.55 o -8 4 1 1751.99 1758.33 37.10 o -7 4 1 13.27 61.89 24.48 o -6 4 1 2890.15 2860.16 47.58 o -5 4 1 69.71 79.70 24.54 o -4 4 1 1671.14 1540.57 24.97 o -3 4 1 303.59 366.32 22.38 o -2 4 1 5024.99 4947.01 80.29 o -1 4 1 1883.14 1889.14 25.01 o 0 4 1 153.36 155.31 15.37 o 1 4 1 1447.25 1556.03 22.94 o 2 4 1 277.18 279.71 18.84 o 3 4 1 2500.76 2571.11 29.66 o 4 4 1 367.35 347.97 17.41 o 5 4 1 443.89 451.31 26.43 o 6 4 1 90.96 57.56 26.55 o 7 4 1 210.75 214.31 31.76 o 8 4 1 6.04 32.29 30.68 o 9 4 1 3.37 43.61 41.82 o 10 4 1 272.48 309.49 38.47 o 11 4 1 42.08 31.42 39.31 o 12 4 1 45.09 54.42 42.98 o -12 5 1 3.28 13.14 38.07 o -11 5 1 194.30 207.01 50.74 o -10 5 1 4.56 39.30 35.25 o -9 5 1 3.78 -13.99 33.91 o -8 5 1 35.39 30.36 32.10 o -7 5 1 561.91 572.97 33.36 o -6 5 1 217.12 214.48 30.23 o -5 5 1 834.48 811.23 37.90 o -4 5 1 722.90 743.74 24.30 o -3 5 1 0.26 -6.66 18.90 o -2 5 1 35.84 49.05 18.70 o -1 5 1 50.38 48.54 17.89 o 0 5 1 38.97 56.50 11.86 o 1 5 1 3224.53 3157.09 147.12 o 2 5 1 1292.95 1294.69 25.31 o 3 5 1 556.00 608.82 22.73 o 4 5 1 223.48 229.30 22.27 o 5 5 1 2319.94 2023.34 251.51 o 6 5 1 544.18 614.00 40.15 o 7 5 1 173.75 209.60 32.52 o 8 5 1 665.20 672.56 64.23 o 9 5 1 20.13 -8.84 40.58 o 10 5 1 1.49 -62.87 62.87 o 11 5 1 169.73 170.90 50.50 o 12 5 1 0.10 51.53 51.95 o -11 6 1 31.12 -50.54 58.06 o -10 6 1 141.74 138.36 47.27 o -9 6 1 19.79 -25.93 33.98 o -8 6 1 330.20 349.61 36.86 o -7 6 1 11.69 42.99 32.14 o -6 6 1 150.75 202.07 37.84 o -5 6 1 812.68 755.18 86.82 o -4 6 1 3251.21 3375.57 53.60 o -3 6 1 949.18 954.26 27.70 o -2 6 1 1887.60 1870.05 31.36 o -1 6 1 1960.27 1644.96 201.86 o 0 6 1 1651.65 1563.76 42.98 o 1 6 1 33.93 40.17 28.40 o 2 6 1 8.09 23.11 29.16 o 3 6 1 388.01 316.38 25.58 o 4 6 1 269.21 275.71 32.50 o 5 6 1 159.16 151.22 34.91 o 6 6 1 1262.03 1269.44 46.93 o 7 6 1 12.72 24.45 40.07 o 8 6 1 328.34 345.88 47.10 o 9 6 1 0.04 -26.79 46.46 o 10 6 1 232.68 245.51 78.55 o 11 6 1 1.72 -49.27 49.27 o -11 7 1 52.25 94.32 73.09 o -10 7 1 114.25 96.56 99.22 o -9 7 1 0.26 -14.36 44.80 o -8 7 1 3.75 52.41 36.25 o -7 7 1 0.73 10.97 34.10 o -6 7 1 387.23 350.81 42.48 o -5 7 1 10.98 36.08 61.10 o -4 7 1 144.14 125.89 61.80 o -3 7 1 424.05 437.30 37.25 o -2 7 1 42.76 31.46 37.25 o -1 7 1 975.45 1003.44 41.39 o 0 7 1 266.80 277.38 35.69 o 1 7 1 0.01 -1.54 34.26 o 2 7 1 472.89 562.44 38.24 o 3 7 1 2429.85 2323.17 50.64 o 4 7 1 543.52 458.89 68.18 o 5 7 1 340.12 275.90 65.35 o 6 7 1 356.26 390.08 68.44 o 7 7 1 179.83 182.75 71.19 o 8 7 1 64.48 74.62 47.55 o 9 7 1 234.70 256.40 49.59 o 10 7 1 107.98 136.98 79.13 o 11 7 1 3.29 -82.26 82.26 o -10 8 1 2.08 -33.16 78.99 o -9 8 1 0.96 -32.24 58.33 o -8 8 1 21.91 1.60 65.98 o -7 8 1 201.57 211.82 44.99 o -6 8 1 113.46 182.66 60.01 o -5 8 1 112.09 104.70 57.15 o -4 8 1 3.18 104.22 65.03 o -3 8 1 57.57 67.42 56.01 o -2 8 1 4.28 34.12 36.94 o -1 8 1 263.99 340.85 41.59 o 0 8 1 96.87 106.17 37.73 o 1 8 1 8.74 25.18 38.34 o 2 8 1 225.25 266.18 38.51 o 3 8 1 307.67 380.74 68.40 o 4 8 1 34.12 43.22 61.25 o 5 8 1 120.79 155.72 72.65 o 6 8 1 15.18 -45.00 59.40 o 7 8 1 205.12 256.28 64.13 o 8 8 1 9.91 5.03 48.52 o 9 8 1 6.15 -15.57 64.80 o 10 8 1 0.06 88.32 55.46 o -8 9 1 45.21 -10.95 46.12 o -7 9 1 271.65 529.46 88.04 o -6 9 1 2.25 18.99 71.96 o -5 9 1 5.12 79.29 60.03 o -4 9 1 4.37 -50.00 69.11 o -3 9 1 129.47 80.06 66.75 o -2 9 1 171.24 162.47 42.74 o -1 9 1 166.49 222.10 47.01 o 0 9 1 27.19 29.76 40.10 o 1 9 1 540.79 576.58 46.71 o 2 9 1 384.98 375.26 41.08 o 3 9 1 12.49 -11.14 71.28 o 4 9 1 2.14 9.51 74.20 o 5 9 1 248.39 183.78 76.38 o 6 9 1 299.55 262.07 76.29 o 7 9 1 70.21 -11.14 63.01 o 8 9 1 1.95 12.42 49.49 o -7 10 1 290.42 206.06 87.44 o -6 10 1 79.36 240.55 90.06 o -5 10 1 155.26 172.07 65.90 o -4 10 1 341.41 426.92 76.38 o -3 10 1 29.47 150.57 71.27 o -2 10 1 27.34 14.35 56.31 o -1 10 1 122.69 148.92 46.08 o 0 10 1 529.35 595.76 52.40 o 1 10 1 0.40 50.91 45.92 o 2 10 1 12.91 -7.11 75.08 o 3 10 1 19.16 17.95 71.79 o 4 10 1 75.50 60.66 69.81 o 5 10 1 46.42 47.95 80.92 o 6 10 1 59.72 15.41 86.95 o 7 10 1 5.63 -63.97 87.33 o -4 11 1 139.48 127.05 75.01 o -3 11 1 23.05 51.79 74.21 o -2 11 1 3.23 -16.66 74.35 o -1 11 1 52.30 110.63 45.31 o 0 11 1 69.80 117.83 49.32 o 1 11 1 18.80 47.71 45.78 o 2 11 1 31.23 50.85 71.26 o 3 11 1 25.10 33.14 82.01 o 4 11 1 44.65 109.28 71.54 o -12 0 2 1132.15 1192.43 88.39 o -10 0 2 21.13 -24.24 63.53 o -8 0 2 6993.35 6879.50 74.61 o -6 0 2 6306.67 6129.99 107.40 o -4 0 2 16211.63 15470.73 170.36 o -2 0 2 18424.54 18143.96 98.81 o 2 0 2 389.34 405.82 17.63 o 4 0 2 7543.17 7664.90 46.18 o 6 0 2 705.78 678.91 21.70 o 8 0 2 1092.18 1111.66 68.66 o 10 0 2 1.05 -69.72 69.72 o 12 0 2 310.94 435.54 84.60 o -13 1 2 0.33 -56.95 56.95 o -12 1 2 0.62 54.15 48.78 o -11 1 2 67.53 -5.33 49.51 o -10 1 2 146.80 117.95 53.55 o -9 1 2 0.17 -30.20 33.38 o -8 1 2 570.93 556.79 40.32 o -7 1 2 12.68 55.68 18.11 o -6 1 2 12.82 24.24 14.37 o -5 1 2 2848.89 2778.94 23.25 o -4 1 2 7642.54 7607.42 33.61 o -3 1 2 11367.02 11506.96 41.98 o -2 1 2 43.16 53.60 15.11 o -1 1 2 13134.63 13030.90 60.73 o 0 1 2 21952.42 21708.74 76.31 o 1 1 2 8624.25 9043.73 67.50 o 2 1 2 10342.60 10356.91 30.05 o 3 1 2 2084.67 2121.05 21.13 o 4 1 2 5976.60 6137.67 36.45 o 5 1 2 7978.63 8231.84 28.12 o 6 1 2 37.90 29.91 15.04 o 7 1 2 24.11 27.61 20.46 o 8 1 2 14.53 -1.74 30.30 o 9 1 2 446.76 371.59 47.03 o 10 1 2 25.02 -8.01 48.57 o 11 1 2 15.88 11.39 46.11 o 12 1 2 10.11 -0.64 47.59 o 13 1 2 221.09 218.57 56.34 o -13 2 2 0.66 -5.00 54.58 o -12 2 2 29.10 24.32 50.26 o -11 2 2 125.52 156.14 48.08 o -10 2 2 3.69 -25.69 56.22 o -9 2 2 2.23 19.65 40.86 o -8 2 2 610.56 606.98 41.77 o -7 2 2 308.78 327.08 22.38 o -6 2 2 92.43 107.13 17.88 o -5 2 2 29.37 28.32 15.88 o -4 2 2 2331.45 2465.31 31.32 o -3 2 2 1749.53 1718.56 17.18 o -2 2 2 342.84 348.49 12.04 o -1 2 2 3437.70 3193.46 27.95 o 0 2 2 1696.17 1666.44 42.70 o 1 2 2 1576.99 1549.01 38.45 o 2 2 2 2229.54 2168.07 33.63 o 3 2 2 821.64 847.47 17.61 o 4 2 2 3167.29 3468.04 29.44 o 5 2 2 4099.36 4063.71 32.90 o 6 2 2 193.36 193.94 15.97 o 7 2 2 938.39 951.76 27.39 o 8 2 2 0.06 -12.76 31.17 o 9 2 2 27.07 37.57 35.63 o 10 2 2 37.20 60.28 38.43 o 11 2 2 148.24 215.76 48.48 o 12 2 2 76.95 74.65 48.19 o 13 2 2 67.65 54.62 58.68 o -13 3 2 3.71 35.26 51.67 o -12 3 2 10.61 -10.30 44.29 o -11 3 2 61.51 50.93 66.51 o -10 3 2 46.90 82.26 44.49 o -9 3 2 122.53 114.81 35.90 o -8 3 2 153.08 190.87 26.00 o -7 3 2 418.92 425.12 24.07 o -6 3 2 621.48 617.01 23.71 o -5 3 2 1262.89 1246.23 22.69 o -4 3 2 240.77 310.29 13.05 o -3 3 2 2823.34 2774.37 47.99 o -2 3 2 1307.25 1381.07 21.93 o -1 3 2 1674.51 1494.12 33.85 o 0 3 2 1157.52 1221.55 27.95 o 1 3 2 345.05 326.58 13.61 o 2 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