#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/01/2230193.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230193_Fobs loop_ _publ_author_name 'Zhang, Yan-Ling' 'Zhang, Xiao-Wei' 'Zhang, Fu-Juan' _publ_section_title ; 3-[(Cyclohexylidene)amino]-1-(4-methylphenyl)thiourea ; _journal_coeditor_code XU5197 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1268 _journal_volume 67 _journal_year 2011 _space_group_IT_number 73 _symmetry_space_group_name_Hall '-I 2b 2c' _symmetry_space_group_name_H-M 'I b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.9151 _cell_length_b 22.5593 _cell_length_c 17.1642 _exptl_crystal_F_000 2240.00 _reflns_d_resolution_high 0.8371 _[local]_cod_data_source_file xu5197Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 20110333 in Ibca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 415.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z' 'x, -y, -z+1/2' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1, z+1/2' 'x+1/2, -y+1/2, -z+1' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z' '-x, y, z-1/2' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, y, -z+1/2' '-x+1/2, y+1/2, z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 796.56 792.20 98.15 o 4 0 0 123720.30 122124.80 1734.05 o 6 0 0 6863.41 7728.05 829.09 o 8 0 0 5837.51 5885.70 320.14 o 10 0 0 331.46 178.38 65.47 o 12 0 0 276.80 272.78 29.67 o 14 0 0 705.70 861.36 52.67 o 16 0 0 101.96 134.61 35.39 o 0 2 0 165643.27 158262.03 1342.12 o 2 2 0 22534.02 22228.96 549.18 o 4 2 0 108.46 53.40 21.47 o 6 2 0 949.16 1049.32 76.41 o 8 2 0 1836.17 2250.18 142.58 o 10 2 0 1343.88 1294.06 175.30 o 12 2 0 202.69 211.86 17.04 o 14 2 0 237.60 223.52 26.68 o 16 2 0 179.75 263.19 31.40 o 0 4 0 28740.59 29475.19 818.25 o 2 4 0 35664.38 33463.32 459.11 o 4 4 0 1206.18 1198.53 67.06 o 6 4 0 652.80 849.74 47.44 o 8 4 0 1818.00 1430.13 164.52 o 10 4 0 3848.58 3739.70 302.96 o 12 4 0 8.91 -4.46 9.09 o 14 4 0 417.04 431.08 31.80 o 16 4 0 717.79 902.32 62.43 o 0 6 0 85.90 139.09 83.68 o 2 6 0 45.13 11.36 19.46 o 4 6 0 6827.35 7086.44 231.48 o 6 6 0 6307.75 5518.92 134.72 o 8 6 0 22508.52 20798.61 640.15 o 10 6 0 11616.86 11731.84 545.89 o 12 6 0 187.17 123.23 32.62 o 14 6 0 2232.84 2413.70 72.95 o 16 6 0 264.04 286.70 30.13 o 0 8 0 42759.92 42585.13 1387.03 o 2 8 0 5160.27 4804.29 129.22 o 4 8 0 464.46 607.68 76.00 o 6 8 0 19840.34 19333.91 349.82 o 8 8 0 2854.09 2533.61 231.14 o 10 8 0 493.34 480.70 109.31 o 12 8 0 131.39 127.46 19.14 o 14 8 0 1592.94 1960.44 80.57 o 16 8 0 134.11 166.03 23.07 o 0 10 0 1971.58 2705.10 150.04 o 2 10 0 12783.69 12834.95 193.65 o 4 10 0 1582.22 1646.58 137.51 o 6 10 0 10931.62 10363.69 368.40 o 8 10 0 1657.66 1412.88 113.33 o 10 10 0 21.92 -19.44 19.44 o 12 10 0 82.19 70.24 30.16 o 14 10 0 24.10 44.14 17.64 o 16 10 0 9.24 15.01 15.89 o 0 12 0 441.63 718.54 88.64 o 2 12 0 722.63 762.24 115.47 o 4 12 0 515.72 432.09 80.84 o 6 12 0 160.55 155.25 55.20 o 8 12 0 208.17 184.65 59.41 o 10 12 0 478.23 413.29 61.19 o 12 12 0 241.93 166.77 41.19 o 14 12 0 90.35 94.63 28.89 o 0 14 0 8765.06 8327.33 323.67 o 2 14 0 3838.35 4060.23 160.05 o 4 14 0 3309.92 2754.24 209.17 o 6 14 0 1951.20 1782.31 178.76 o 8 14 0 17675.63 17261.37 334.81 o 10 14 0 3430.41 3462.35 171.78 o 12 14 0 101.72 90.88 32.40 o 14 14 0 119.12 80.13 26.58 o 0 16 0 1642.55 1285.45 139.61 o 2 16 0 689.06 595.85 67.59 o 4 16 0 523.01 531.30 100.99 o 6 16 0 4334.02 4013.03 117.58 o 8 16 0 6914.96 7101.74 211.30 o 10 16 0 2502.96 2825.25 155.20 o 12 16 0 0.51 9.30 22.90 o 14 16 0 681.92 810.00 59.93 o 0 18 0 796.55 680.71 48.81 o 2 18 0 14.71 24.70 18.64 o 4 18 0 278.74 244.67 23.46 o 6 18 0 4204.23 4280.09 114.88 o 8 18 0 446.68 464.79 63.29 o 10 18 0 9.17 43.01 26.15 o 12 18 0 6.14 22.90 23.11 o 0 20 0 7152.88 6146.34 154.66 o 2 20 0 298.76 280.77 28.96 o 4 20 0 2084.82 1982.95 84.30 o 6 20 0 85.75 95.53 24.25 o 8 20 0 1036.74 1019.57 84.37 o 10 20 0 344.10 340.64 46.58 o 0 22 0 5088.44 5045.94 162.02 o 2 22 0 117.15 140.19 21.78 o 4 22 0 2149.77 2283.98 106.37 o 6 22 0 135.14 179.58 23.81 o 8 22 0 218.11 219.40 35.71 o 10 22 0 38.60 161.72 28.66 o 0 24 0 484.81 567.27 54.31 o 2 24 0 1158.85 1307.96 56.47 o 4 24 0 23.57 29.21 19.07 o 6 24 0 23.12 24.32 9.44 o 8 24 0 48.41 68.75 19.42 o 0 26 0 496.52 614.41 48.37 o 2 26 0 640.55 674.48 34.23 o 4 26 0 50.75 38.00 13.12 o 2 1 1 7256.35 7892.57 130.31 o 4 1 1 3260.61 3191.95 122.10 o 6 1 1 9071.13 9573.49 321.48 o 8 1 1 6482.25 6479.53 167.61 o 10 1 1 2277.30 2510.89 142.45 o 12 1 1 219.60 167.15 10.54 o 14 1 1 7.32 18.57 8.60 o 16 1 1 142.06 183.72 19.32 o 1 2 1 4117.79 3649.50 134.29 o 3 2 1 69101.27 71451.38 583.26 o 5 2 1 1399.33 1326.76 57.99 o 7 2 1 3581.88 3675.13 117.21 o 9 2 1 82.72 51.33 26.61 o 11 2 1 1839.60 1665.25 148.12 o 13 2 1 233.47 219.62 15.45 o 15 2 1 51.06 57.67 10.30 o 17 2 1 202.55 318.78 37.98 o 2 3 1 93186.50 89038.11 567.77 o 4 3 1 62154.76 59166.96 483.52 o 6 3 1 833.10 870.75 40.11 o 8 3 1 371.50 427.53 51.88 o 10 3 1 1.96 -61.02 83.16 o 12 3 1 201.71 181.02 13.68 o 14 3 1 179.68 159.81 14.50 o 16 3 1 19.19 35.06 13.04 o 1 4 1 24661.72 23484.15 204.08 o 3 4 1 96784.80 94999.28 709.32 o 5 4 1 24052.38 24035.71 160.30 o 7 4 1 810.05 601.01 45.27 o 9 4 1 217.03 240.06 87.61 o 11 4 1 363.30 322.03 67.32 o 13 4 1 100.67 87.80 10.52 o 15 4 1 0.40 14.90 8.18 o 17 4 1 223.17 281.89 29.10 o 2 5 1 1244.35 1217.93 62.87 o 4 5 1 11642.83 10886.02 131.69 o 6 5 1 21206.78 20631.23 221.67 o 8 5 1 998.51 1065.21 102.15 o 10 5 1 989.30 869.40 107.68 o 12 5 1 262.39 257.25 15.76 o 14 5 1 382.55 399.79 22.11 o 16 5 1 71.63 110.28 20.39 o 1 6 1 185.16 179.56 18.37 o 3 6 1 13620.45 13541.91 267.34 o 5 6 1 7862.38 8593.30 129.08 o 7 6 1 3607.95 3857.98 94.06 o 9 6 1 139.83 245.84 121.12 o 11 6 1 504.51 452.08 21.07 o 13 6 1 4.32 9.72 8.51 o 15 6 1 0.04 13.52 10.03 o 17 6 1 58.12 66.65 23.15 o 2 7 1 1162.17 1118.60 42.65 o 4 7 1 11649.03 11005.58 173.28 o 6 7 1 9453.49 9033.04 154.97 o 8 7 1 1141.59 1051.37 106.72 o 10 7 1 176.87 206.68 55.31 o 12 7 1 1437.93 1419.06 35.68 o 14 7 1 166.38 157.20 16.31 o 16 7 1 161.02 230.29 18.67 o 1 8 1 11662.50 11733.55 172.59 o 3 8 1 6626.91 6749.68 208.71 o 5 8 1 2440.96 2379.16 92.01 o 7 8 1 7550.94 7901.94 148.14 o 9 8 1 3.17 33.56 26.94 o 11 8 1 2579.01 2590.42 54.81 o 13 8 1 5.36 -5.92 10.89 o 15 8 1 2.09 5.63 9.38 o 2 9 1 19252.40 18726.49 204.06 o 4 9 1 1892.90 1790.33 123.46 o 6 9 1 5086.60 5108.17 129.04 o 8 9 1 213.38 201.34 36.60 o 10 9 1 13.52 -8.73 8.73 o 12 9 1 902.05 888.60 43.04 o 14 9 1 120.18 135.53 19.70 o 16 9 1 56.21 82.58 13.27 o 1 10 1 19.98 12.61 13.08 o 3 10 1 889.11 747.69 42.72 o 5 10 1 9.39 40.23 22.94 o 7 10 1 2960.64 2851.79 87.98 o 9 10 1 126.53 36.81 101.53 o 11 10 1 3546.01 3516.54 86.58 o 13 10 1 79.42 84.91 16.92 o 15 10 1 23.13 28.08 11.07 o 2 11 1 233.75 202.97 23.81 o 4 11 1 4249.35 4548.67 150.15 o 6 11 1 315.75 292.07 42.34 o 8 11 1 36.03 74.85 21.34 o 10 11 1 1197.86 1143.96 62.15 o 12 11 1 491.05 502.84 53.24 o 14 11 1 70.36 74.84 15.72 o 16 11 1 2.73 5.44 10.76 o 1 12 1 61.01 68.81 19.41 o 3 12 1 4024.59 4364.28 136.63 o 5 12 1 1261.35 1203.26 95.44 o 7 12 1 532.37 485.24 47.99 o 9 12 1 2171.79 1855.75 78.52 o 11 12 1 3694.51 3737.16 122.24 o 13 12 1 1.92 -10.70 18.45 o 15 12 1 97.12 106.23 19.10 o 2 13 1 8422.97 8001.00 151.99 o 4 13 1 83.35 92.04 30.05 o 6 13 1 2649.07 2286.41 115.98 o 8 13 1 897.02 853.03 45.87 o 10 13 1 167.42 207.60 37.21 o 12 13 1 259.32 248.09 33.36 o 14 13 1 119.28 78.38 21.81 o 1 14 1 937.42 877.87 53.49 o 3 14 1 182.74 217.61 42.87 o 5 14 1 525.57 671.97 76.99 o 7 14 1 816.13 698.97 32.23 o 9 14 1 2182.71 1912.61 121.94 o 11 14 1 2192.77 2026.03 92.28 o 13 14 1 12.73 28.86 16.74 o 15 14 1 37.06 36.35 12.87 o 2 15 1 2783.71 2086.21 85.24 o 4 15 1 165.54 132.47 36.93 o 6 15 1 970.91 923.29 57.18 o 8 15 1 1025.45 1009.07 41.20 o 10 15 1 13.90 45.18 30.15 o 12 15 1 686.81 714.86 53.39 o 14 15 1 75.05 80.72 17.07 o 1 16 1 242.95 211.39 30.43 o 3 16 1 69.89 124.17 38.97 o 5 16 1 196.92 159.82 16.08 o 7 16 1 28.92 12.50 11.12 o 9 16 1 58.97 40.52 17.92 o 11 16 1 25.23 26.03 16.88 o 13 16 1 346.28 364.17 45.82 o 2 17 1 257.58 201.27 35.70 o 4 17 1 2536.33 2322.34 52.27 o 6 17 1 138.17 128.59 16.69 o 8 17 1 158.97 161.13 20.43 o 10 17 1 5.95 26.48 17.78 o 12 17 1 56.90 61.52 19.16 o 1 18 1 1277.84 1092.16 31.00 o 3 18 1 871.59 699.22 24.40 o 5 18 1 3595.52 3326.02 64.17 o 7 18 1 738.26 701.03 39.92 o 9 18 1 0.01 5.13 14.45 o 11 18 1 695.88 846.25 65.96 o 13 18 1 550.23 693.46 37.96 o 2 19 1 3706.69 3412.69 79.95 o 4 19 1 393.04 413.03 21.80 o 6 19 1 184.58 171.46 26.17 o 8 19 1 10.57 28.16 17.39 o 10 19 1 48.39 80.70 19.84 o 12 19 1 8.66 -5.76 11.21 o 1 20 1 12.91 0.47 7.48 o 3 20 1 1234.91 1107.09 37.68 o 5 20 1 503.08 423.17 32.83 o 7 20 1 79.39 94.73 15.72 o 9 20 1 9.14 -14.62 14.62 o 11 20 1 133.44 159.76 21.31 o 2 21 1 2575.45 2529.82 57.11 o 4 21 1 17.70 30.28 10.38 o 6 21 1 131.51 124.37 14.51 o 8 21 1 256.22 296.85 31.98 o 10 21 1 47.06 35.34 19.69 o 1 22 1 757.74 752.86 33.40 o 3 22 1 15.82 39.20 10.14 o 5 22 1 28.68 32.51 32.21 o 7 22 1 1.31 5.38 8.95 o 9 22 1 39.26 46.16 14.96 o 2 23 1 927.55 995.08 43.57 o 4 23 1 24.20 33.89 16.19 o 6 23 1 128.35 157.73 12.71 o 8 23 1 143.95 119.30 17.61 o 1 24 1 951.16 1018.02 41.40 o 3 24 1 303.94 322.72 23.19 o 5 24 1 12.72 11.74 7.94 o 7 24 1 2.33 -11.23 11.23 o 2 25 1 18.01 35.59 11.31 o 4 25 1 66.55 106.87 12.05 o 6 25 1 112.15 116.11 10.31 o 1 26 1 69.41 84.14 10.83 o 3 26 1 8.48 27.08 6.09 o 0 0 2 11295.97 14479.01 322.79 o 2 0 2 18767.58 19260.79 1634.29 o 4 0 2 556.55 469.14 47.27 o 6 0 2 878.58 952.47 50.37 o 8 0 2 97.59 146.41 37.41 o 10 0 2 3401.03 3134.87 275.19 o 12 0 2 216.51 178.87 15.42 o 14 0 2 341.61 389.77 25.89 o 16 0 2 5.37 3.82 13.72 o 1 1 2 93.83 134.27 14.59 o 3 1 2 172422.09 178091.73 1141.13 o 5 1 2 6309.83 6392.01 137.58 o 7 1 2 3972.70 3566.77 136.67 o 9 1 2 134.66 85.15 28.59 o 11 1 2 67.85 56.02 27.80 o 13 1 2 351.52 348.67 16.05 o 15 1 2 232.28 259.37 22.72 o 17 1 2 5.40 30.25 15.72 o 0 2 2 20757.69 23315.26 536.77 o 2 2 2 313.96 293.18 32.99 o 4 2 2 889.46 784.82 43.08 o 6 2 2 1928.29 1558.15 61.68 o 8 2 2 309.04 269.12 42.30 o 10 2 2 1682.87 1844.10 120.55 o 12 2 2 444.15 385.11 15.51 o 14 2 2 0.74 -8.37 8.37 o 16 2 2 2.16 7.35 20.19 o 1 3 2 52.25 24.79 24.45 o 3 3 2 69044.36 70454.04 372.28 o 5 3 2 12972.84 12168.21 228.07 o 7 3 2 778.67 823.76 65.82 o 9 3 2 34.15 36.44 20.93 o 11 3 2 34.80 21.78 39.07 o 13 3 2 1016.72 1060.47 31.62 o 15 3 2 747.18 902.65 31.20 o 17 3 2 28.04 34.11 22.35 o 0 4 2 113.12 106.64 42.62 o 2 4 2 6463.30 5899.88 334.36 o 4 4 2 129.04 92.60 12.44 o 6 4 2 5157.22 5254.59 124.62 o 8 4 2 2613.38 2516.38 125.04 o 10 4 2 974.24 1192.59 123.32 o 12 4 2 675.03 646.65 22.74 o 14 4 2 50.72 47.55 11.59 o 16 4 2 13.31 13.86 11.57 o 1 5 2 21101.32 20935.63 548.81 o 3 5 2 3069.38 3303.61 122.53 o 5 5 2 6672.82 6265.61 96.98 o 7 5 2 655.00 740.80 52.71 o 9 5 2 626.47 447.01 72.89 o 11 5 2 103.04 99.12 12.44 o 13 5 2 8.89 13.14 7.88 o 15 5 2 404.46 466.04 24.76 o 17 5 2 141.79 130.53 29.00 o 0 6 2 17540.57 17084.74 636.31 o 2 6 2 2791.15 2994.64 131.53 o 4 6 2 13168.22 13418.91 160.38 o 6 6 2 266.96 374.91 27.73 o 8 6 2 338.67 261.51 39.87 o 10 6 2 290.40 132.96 43.41 o 12 6 2 26.68 30.59 9.34 o 14 6 2 7.87 -3.33 8.81 o 16 6 2 3.06 23.26 9.80 o 1 7 2 8621.95 8732.46 144.26 o 3 7 2 347.16 229.69 23.64 o 5 7 2 41.83 12.68 15.85 o 7 7 2 11500.55 12010.81 316.96 o 9 7 2 165.79 200.14 85.76 o 11 7 2 337.77 334.36 27.15 o 13 7 2 868.46 875.36 31.92 o 15 7 2 482.25 535.76 29.57 o 17 7 2 9.64 19.84 19.28 o 0 8 2 23010.75 22734.66 339.78 o 2 8 2 804.01 843.62 50.21 o 4 8 2 11879.26 12916.82 208.38 o 6 8 2 83.73 189.54 25.67 o 8 8 2 1120.49 1021.40 79.54 o 10 8 2 691.85 618.09 89.32 o 12 8 2 95.27 60.66 12.62 o 14 8 2 68.25 89.96 17.54 o 16 8 2 0.61 14.46 9.92 o 1 9 2 5499.31 5514.12 143.28 o 3 9 2 1674.48 1339.21 88.18 o 5 9 2 285.73 222.91 28.57 o 7 9 2 3775.95 3687.91 115.19 o 9 9 2 4735.86 4460.79 249.87 o 11 9 2 2.03 -8.60 10.86 o 13 9 2 999.19 948.57 48.08 o 15 9 2 94.65 80.42 15.49 o 0 10 2 13437.35 13943.46 341.20 o 2 10 2 20.14 12.08 12.18 o 4 10 2 12.47 -1.84 13.97 o 6 10 2 89.83 74.59 22.81 o 8 10 2 20.63 -4.34 112.21 o 10 10 2 247.14 296.06 35.26 o 12 10 2 0.03 -9.75 15.96 o 14 10 2 0.41 -7.94 12.61 o 16 10 2 28.26 41.31 10.72 o 1 11 2 2734.79 3675.10 131.26 o 3 11 2 22.27 52.17 18.88 o 5 11 2 4171.41 4017.53 140.03 o 7 11 2 4788.15 4689.79 159.65 o 9 11 2 7844.70 7208.34 148.26 o 11 11 2 152.99 127.42 23.81 o 13 11 2 583.35 524.76 36.07 o 15 11 2 23.69 42.20 11.29 o 0 12 2 14740.15 15677.92 402.17 o 2 12 2 54.68 30.35 16.06 o 4 12 2 4190.43 4009.76 138.69 o 6 12 2 44.64 92.31 27.61 o 8 12 2 622.63 593.65 64.61 o 10 12 2 39.66 55.30 19.35 o 12 12 2 16.21 6.48 16.30 o 14 12 2 53.07 61.61 15.53 o 1 13 2 783.19 484.66 53.47 o 3 13 2 613.03 765.42 62.43 o 5 13 2 4615.58 4645.74 191.89 o 7 13 2 3261.80 3223.64 126.31 o 9 13 2 1628.47 1581.97 79.32 o 11 13 2 1518.53 1589.72 80.46 o 13 13 2 49.35 81.80 23.64 o 15 13 2 12.88 -2.90 11.34 o 0 14 2 19.15 46.39 21.70 o 2 14 2 803.08 712.07 58.03 o 4 14 2 1441.09 1431.22 108.48 o 6 14 2 1406.45 1339.58 92.63 o 8 14 2 598.07 586.90 32.76 o 10 14 2 45.48 19.51 17.72 o 12 14 2 297.61 244.31 33.57 o 14 14 2 2.69 1.02 13.82 o 1 15 2 860.13 675.22 49.46 o 3 15 2 2138.63 2059.09 131.70 o 5 15 2 2615.36 2641.50 129.57 o 7 15 2 1230.52 1152.06 43.99 o 9 15 2 1029.99 970.01 64.27 o 11 15 2 33.19 8.70 15.55 o 13 15 2 141.40 163.88 24.94 o 0 16 2 85.61 63.57 27.36 o 2 16 2 304.66 223.91 36.29 o 4 16 2 42.09 49.55 29.85 o 6 16 2 48.62 32.42 24.95 o 8 16 2 1084.92 1152.60 46.29 o 10 16 2 187.33 177.53 28.52 o 12 16 2 38.34 32.99 17.40 o 14 16 2 6.79 11.57 22.30 o 1 17 2 1030.66 1062.23 66.92 o 3 17 2 1386.90 1115.78 32.99 o 5 17 2 8482.90 8129.80 116.33 o 7 17 2 3.87 -11.59 11.59 o 9 17 2 395.37 383.22 29.83 o 11 17 2 274.70 349.69 36.50 o 13 17 2 148.54 281.78 38.48 o 0 18 2 299.13 298.41 40.16 o 2 18 2 17.58 21.83 6.69 o 4 18 2 260.21 240.91 18.06 o 6 18 2 1461.48 1465.72 96.06 o 8 18 2 117.66 87.05 18.18 o 10 18 2 175.68 210.81 45.36 o 12 18 2 314.23 374.16 32.06 o 1 19 2 377.17 308.90 18.50 o 3 19 2 1.28 11.12 7.11 o 5 19 2 1561.65 1450.34 52.40 o 7 19 2 36.97 34.35 10.50 o 9 19 2 185.04 197.95 28.52 o 11 19 2 61.91 68.74 17.37 o 0 20 2 279.50 324.49 26.37 o 2 20 2 0.33 8.09 8.30 o 4 20 2 10.70 -3.68 8.84 o 6 20 2 147.39 148.69 15.71 o 8 20 2 6.34 -9.72 12.37 o 10 20 2 5.36 2.55 13.08 o 1 21 2 648.03 583.18 28.20 o 3 21 2 187.55 163.15 18.26 o 5 21 2 94.03 88.43 17.81 o 7 21 2 0.30 2.36 10.38 o 9 21 2 0.95 -9.33 11.93 o 11 21 2 110.42 88.00 13.99 o 0 22 2 22.53 33.23 15.72 o 2 22 2 6.24 1.95 8.32 o 4 22 2 39.20 47.36 11.66 o 6 22 2 101.87 120.09 11.92 o 8 22 2 89.53 111.87 20.06 o 10 22 2 192.45 279.20 23.22 o 1 23 2 6.74 4.47 10.72 o 3 23 2 179.09 185.17 14.91 o 5 23 2 378.99 405.30 20.41 o 7 23 2 218.95 229.81 18.91 o 9 23 2 164.26 182.90 20.24 o 0 24 2 44.50 67.70 16.60 o 2 24 2 105.19 110.61 16.88 o 4 24 2 6.70 -2.95 10.52 o 6 24 2 122.53 140.01 11.23 o 1 25 2 224.54 256.52 17.92 o 3 25 2 36.58 63.76 11.67 o 5 25 2 185.87 242.09 13.78 o 0 26 2 22.49 57.99 15.28 o 2 26 2 65.23 78.17 11.39 o 4 26 2 102.42 153.08 13.11 o 2 1 3 1565.44 1828.36 135.69 o 4 1 3 39338.75 42704.43 308.91 o 6 1 3 1559.20 1771.67 52.41 o 8 1 3 2543.74 2515.30 152.28 o 10 1 3 1985.81 2010.44 157.04 o 12 1 3 21.61 9.50 5.72 o 14 1 3 515.50 556.13 23.58 o 16 1 3 11.84 9.99 27.52 o 1 2 3 40435.82 46063.67 286.76 o 3 2 3 1457.59 1638.19 54.13 o 5 2 3 2995.59 3132.35 66.63 o 7 2 3 5143.18 5556.87 134.27 o 9 2 3 923.30 942.84 103.95 o 11 2 3 1000.27 905.18 112.60 o 13 2 3 61.88 72.11 10.24 o 15 2 3 93.67 108.67 15.80 o 17 2 3 13.23 2.39 11.87 o 2 3 3 10516.30 10662.39 318.34 o 4 3 3 5068.18 5019.57 72.34 o 6 3 3 1908.67 1736.80 77.76 o 8 3 3 3709.63 3838.01 153.25 o 10 3 3 133.37 64.65 35.92 o 12 3 3 442.10 391.58 18.34 o 14 3 3 142.03 128.32 12.56 o 16 3 3 100.87 130.66 24.47 o 1 4 3 3184.81 3612.88 283.01 o 3 4 3 66432.16 67562.13 457.32 o 5 4 3 75.14 92.44 15.22 o 7 4 3 2891.53 2518.38 102.17 o 9 4 3 198.92 362.85 51.58 o 11 4 3 856.87 851.80 31.02 o 13 4 3 11.40 -5.21 8.01 o 15 4 3 251.73 292.41 20.07 o 17 4 3 2.81 25.64 19.98 o 2 5 3 6479.09 6503.68 155.49 o 4 5 3 6212.81 6562.70 175.36 o 6 5 3 6.25 1.49 9.20 o 8 5 3 0.14 -26.10 26.10 o 10 5 3 107.95 188.29 83.17 o 12 5 3 289.98 263.23 17.72 o 14 5 3 30.01 43.70 12.93 o 16 5 3 5.51 16.78 10.67 o 1 6 3 2142.15 2216.23 69.91 o 3 6 3 2943.79 2604.57 85.15 o 5 6 3 2090.27 2156.81 89.54 o 7 6 3 795.01 678.75 53.34 o 9 6 3 941.82 1030.32 110.08 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8 2.61 -26.67 26.67 o 10 4 8 1101.08 919.93 77.25 o 12 4 8 23.04 15.35 29.58 o 14 4 8 12.39 2.89 15.62 o 16 4 8 118.51 107.51 25.11 o 1 5 8 6258.64 6806.87 137.57 o 3 5 8 988.13 1371.61 98.72 o 5 5 8 4211.04 4666.45 161.30 o 7 5 8 85.20 160.12 41.65 o 9 5 8 2519.05 1981.00 107.04 o 11 5 8 10.89 17.38 29.87 o 13 5 8 174.99 101.81 33.42 o 15 5 8 10.10 -6.37 14.97 o 0 6 8 334.57 189.84 35.93 o 2 6 8 962.05 1084.41 68.62 o 4 6 8 8134.96 8226.72 356.77 o 6 6 8 716.40 508.63 72.03 o 8 6 8 1069.59 1071.38 145.02 o 10 6 8 253.84 281.55 46.24 o 12 6 8 71.79 40.07 30.27 o 14 6 8 159.15 153.76 26.75 o 1 7 8 2075.65 2457.49 131.05 o 3 7 8 198.81 210.39 67.23 o 5 7 8 740.76 813.76 90.57 o 7 7 8 1673.05 1644.65 124.99 o 9 7 8 472.32 395.57 52.58 o 11 7 8 161.56 85.71 34.95 o 13 7 8 13.26 23.74 24.45 o 15 7 8 16.06 16.07 23.94 o 0 8 8 6162.25 6308.97 294.65 o 2 8 8 749.89 708.34 77.26 o 4 8 8 4317.82 4143.34 161.95 o 6 8 8 1898.31 1862.02 144.44 o 8 8 8 365.54 303.55 31.04 o 10 8 8 1180.45 1076.13 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